#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:01:45 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180905 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/46/2104624.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104624_Fobs loop_ _publ_author_name 'Drebushchak, Tatiana N.' 'Chesalov, Yury A.' 'Boldyreva, Elena V.' _publ_section_title ; A conformational polymorphic transition in the high-temperature \e-form of chlorpropamide on cooling: a new \e'-form ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 770 _journal_page_last 781 _journal_volume 65 _journal_year 2009 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.8050 _cell_length_b 7.3500 _cell_length_c 9.1295 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.7903 _cod_data_source_file gp5033ecpa250sup3.hkl _cod_data_source_block ecpa250 #BEGIN Tags that were not found in dictionaries: _shelx_title ecpa250 _shelx_refln_list_code 4 _shelx_f_calc_maximum 198.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 170.06 161.70 18.92 o 6 0 0 1848.75 1719.15 83.03 o 8 0 0 4071.69 4140.65 72.24 o 10 0 0 706.23 677.94 21.91 o 12 0 0 127.91 139.99 32.43 o 14 0 0 178.58 202.06 26.15 o 16 0 0 164.20 151.42 22.82 o 18 0 0 91.86 107.38 27.87 o 20 0 0 106.27 134.16 34.30 o 22 0 0 93.40 81.90 66.21 o 24 0 0 60.73 100.06 72.69 o 1 1 0 8855.51 8773.04 96.17 o 2 1 0 5702.79 5987.02 111.56 o 3 1 0 325.12 383.22 36.08 o 4 1 0 18662.74 18786.48 346.14 o 5 1 0 4732.80 4605.59 44.28 o 6 1 0 3150.99 2941.09 58.72 o 7 1 0 848.14 889.33 26.66 o 8 1 0 205.46 190.95 10.66 o 9 1 0 1195.99 1060.41 20.11 o 10 1 0 3.42 7.66 10.77 o 11 1 0 37.26 40.12 12.53 o 12 1 0 1386.28 1410.77 21.82 o 13 1 0 292.86 292.81 14.23 o 14 1 0 0.85 2.25 14.88 o 15 1 0 265.12 258.55 16.47 o 16 1 0 33.62 39.08 16.32 o 17 1 0 77.90 73.18 17.15 o 18 1 0 172.95 186.55 18.99 o 19 1 0 0.53 6.68 17.74 o 20 1 0 3.66 24.41 41.20 o 21 1 0 115.28 138.78 33.82 o 22 1 0 43.77 41.53 34.14 o 23 1 0 20.76 39.58 47.01 o 24 1 0 4.25 27.04 72.98 o 0 2 0 62.22 84.98 27.00 o 1 2 0 43.67 43.20 16.27 o 2 2 0 45.87 61.81 20.24 o 3 2 0 4828.73 4654.59 44.00 o 4 2 0 13648.84 13555.93 81.47 o 5 2 0 262.65 249.64 21.79 o 6 2 0 2033.72 2084.83 27.91 o 7 2 0 97.21 93.32 11.42 o 8 2 0 63.92 61.66 10.93 o 9 2 0 200.06 191.70 19.20 o 10 2 0 983.15 1115.37 22.49 o 11 2 0 1554.40 1717.05 37.07 o 12 2 0 294.77 287.59 17.49 o 13 2 0 148.24 161.19 18.78 o 14 2 0 59.08 59.42 21.96 o 15 2 0 57.51 66.85 37.27 o 16 2 0 366.00 435.87 39.93 o 17 2 0 220.86 273.84 37.39 o 18 2 0 0.78 11.82 29.02 o 19 2 0 0.15 8.30 29.84 o 20 2 0 6.79 9.77 38.67 o 21 2 0 20.17 12.88 40.21 o 22 2 0 1.97 16.04 52.70 o 23 2 0 5.10 52.13 74.51 o 24 2 0 0.00 -25.19 79.14 o 1 3 0 96.37 83.78 16.85 o 2 3 0 2863.62 2964.18 24.10 o 3 3 0 88.77 65.45 18.17 o 4 3 0 692.89 720.17 24.28 o 5 3 0 4205.62 4190.87 34.89 o 6 3 0 2475.74 2691.53 32.64 o 7 3 0 50.75 50.56 24.23 o 8 3 0 1359.03 1369.26 19.81 o 9 3 0 111.85 105.43 12.91 o 10 3 0 7.05 8.16 11.30 o 11 3 0 0.11 7.39 10.54 o 12 3 0 4.71 13.94 20.19 o 13 3 0 593.60 602.30 23.37 o 14 3 0 165.68 214.31 22.91 o 15 3 0 124.14 128.51 25.80 o 16 3 0 19.73 10.07 25.47 o 17 3 0 51.98 45.25 33.96 o 18 3 0 3.46 24.79 36.00 o 19 3 0 160.91 182.88 37.93 o 20 3 0 80.53 93.46 37.80 o 21 3 0 1.27 -3.17 40.40 o 22 3 0 16.13 28.90 72.06 o 23 3 0 10.57 21.17 73.12 o 0 4 0 595.02 633.43 52.00 o 1 4 0 1602.82 1592.69 20.28 o 2 4 0 133.17 140.56 19.58 o 3 4 0 276.11 259.03 16.73 o 4 4 0 0.24 -0.45 17.37 o 5 4 0 209.99 196.05 25.32 o 6 4 0 0.00 4.85 21.83 o 7 4 0 385.92 384.06 25.77 o 8 4 0 397.65 408.85 26.15 o 9 4 0 82.20 67.97 15.22 o 10 4 0 15.49 13.23 14.31 o 11 4 0 27.89 19.44 13.98 o 12 4 0 216.92 211.81 13.87 o 13 4 0 160.80 135.13 24.17 o 14 4 0 202.82 214.09 19.14 o 15 4 0 121.27 143.69 19.66 o 16 4 0 10.89 11.87 19.69 o 17 4 0 55.65 51.18 33.14 o 18 4 0 21.02 31.54 35.04 o 19 4 0 3.55 -13.15 63.58 o 20 4 0 0.00 16.13 71.03 o 21 4 0 11.76 87.81 67.57 o 22 4 0 15.45 82.68 76.91 o 1 5 0 10.13 29.62 22.74 o 2 5 0 0.39 12.39 20.57 o 3 5 0 134.80 155.71 18.53 o 4 5 0 17.05 18.05 18.83 o 5 5 0 12.57 19.88 20.12 o 6 5 0 10.72 12.24 20.07 o 7 5 0 29.77 22.43 21.03 o 8 5 0 128.32 162.06 47.43 o 9 5 0 368.36 285.40 53.27 o 10 5 0 49.19 53.16 28.08 o 11 5 0 13.13 16.43 10.42 o 12 5 0 0.18 -0.65 8.47 o 13 5 0 72.97 40.60 15.89 o 14 5 0 17.77 41.19 23.77 o 15 5 0 8.58 38.03 25.08 o 16 5 0 240.22 275.28 47.12 o 17 5 0 1.50 11.47 46.17 o 18 5 0 1.90 -4.01 71.17 o 19 5 0 27.62 52.84 71.39 o 20 5 0 1.80 25.50 70.67 o 0 6 0 78.02 174.15 38.35 o 1 6 0 972.11 946.75 32.10 o 2 6 0 24.29 50.59 25.76 o 3 6 0 8.00 32.10 25.28 o 4 6 0 19.66 14.84 21.15 o 5 6 0 229.90 287.19 24.33 o 6 6 0 4.10 1.02 21.71 o 7 6 0 44.99 38.26 19.07 o 8 6 0 5.43 -1.14 15.85 o 9 6 0 58.94 64.15 14.13 o 10 6 0 104.07 148.52 22.09 o 11 6 0 51.43 38.18 41.72 o 12 6 0 0.30 -10.10 42.62 o 13 6 0 9.90 18.73 42.28 o 14 6 0 1.64 23.64 45.11 o 15 6 0 3.75 2.64 46.44 o 16 6 0 10.99 9.22 49.69 o 17 6 0 10.35 -2.52 73.83 o 18 6 0 34.10 47.04 53.87 o 1 7 0 137.03 129.38 24.01 o 2 7 0 54.88 47.62 25.96 o 3 7 0 0.01 9.75 27.71 o 4 7 0 220.86 215.22 33.05 o 5 7 0 238.96 233.55 45.30 o 6 7 0 90.44 112.35 64.43 o 7 7 0 13.37 13.10 62.70 o 8 7 0 45.58 59.53 61.28 o 9 7 0 4.11 -1.07 64.37 o 10 7 0 12.28 33.96 64.28 o 11 7 0 8.93 32.57 63.20 o 12 7 0 158.21 246.52 69.16 o 13 7 0 12.80 46.40 47.48 o 14 7 0 1.17 4.42 49.86 o 15 7 0 0.56 62.94 48.90 o 16 7 0 0.01 0.44 51.35 o 0 8 0 64.33 95.53 71.99 o 1 8 0 0.03 13.79 50.70 o 2 8 0 45.94 49.25 70.82 o 3 8 0 70.55 55.44 70.10 o 5 8 0 3.35 26.65 69.91 o 6 8 0 5.42 42.82 70.77 o 7 8 0 32.37 45.61 69.13 o 8 8 0 0.43 39.67 67.74 o 9 8 0 64.04 99.29 69.91 o 11 8 0 77.30 134.75 76.72 o 12 8 0 19.17 52.15 76.48 o 1 9 0 31.44 59.53 59.22 o 2 9 0 1.48 -16.72 58.98 o 3 9 0 26.22 37.79 59.85 o 4 9 0 8.09 30.66 80.76 o 5 9 0 66.64 99.63 83.43 o 2 0 1 7085.52 7178.94 133.69 o 4 0 1 4169.10 4007.79 33.04 o 6 0 1 3845.26 3391.86 36.94 o 8 0 1 498.81 519.06 13.62 o 10 0 1 806.85 785.74 16.65 o 12 0 1 1011.19 1020.41 19.58 o 14 0 1 31.14 41.21 18.51 o 16 0 1 2.67 17.84 20.42 o 18 0 1 459.14 500.75 22.96 o 20 0 1 21.01 22.63 21.73 o 22 0 1 10.22 -17.64 39.00 o 24 0 1 21.06 11.82 49.53 o 0 1 1 118.43 122.55 16.93 o 1 1 1 234.31 234.81 22.78 o 2 1 1 1134.20 1200.95 33.76 o 3 1 1 10951.90 10464.04 190.21 o 4 1 1 2822.95 2715.10 35.91 o 5 1 1 4426.68 4379.97 22.65 o 6 1 1 2551.62 2476.71 15.45 o 7 1 1 778.89 737.57 10.18 o 8 1 1 1872.33 1734.65 19.20 o 9 1 1 789.43 773.60 11.85 o 10 1 1 524.94 508.68 12.53 o 11 1 1 112.56 102.18 12.50 o 12 1 1 216.95 238.52 12.59 o 13 1 1 53.33 54.55 7.23 o 14 1 1 590.37 654.43 15.42 o 15 1 1 36.28 33.72 8.01 o 16 1 1 50.79 37.54 7.91 o 17 1 1 57.34 68.11 17.23 o 18 1 1 7.73 0.35 16.73 o 19 1 1 84.67 72.62 17.82 o 20 1 1 41.53 44.75 18.86 o 21 1 1 4.86 26.59 25.04 o 22 1 1 7.09 9.72 27.44 o 23 1 1 7.59 -1.44 37.25 o 24 1 1 9.84 0.89 35.20 o 1 2 1 329.71 300.06 8.96 o 2 2 1 3095.52 2812.22 31.90 o 3 2 1 116.42 149.36 30.81 o 4 2 1 275.09 281.34 16.39 o 5 2 1 78.55 78.01 13.02 o 6 2 1 718.16 751.59 14.54 o 7 2 1 1302.67 1269.54 16.85 o 8 2 1 2155.28 2174.25 19.60 o 9 2 1 813.90 764.26 12.20 o 10 2 1 869.75 862.52 13.98 o 11 2 1 444.41 428.55 15.39 o 12 2 1 18.48 10.51 13.98 o 13 2 1 95.12 98.40 15.17 o 14 2 1 473.95 513.08 21.86 o 15 2 1 528.61 556.51 25.12 o 16 2 1 84.47 107.04 22.16 o 17 2 1 8.84 4.92 21.32 o 18 2 1 40.59 28.34 20.41 o 19 2 1 0.77 7.40 24.57 o 20 2 1 8.72 8.73 28.37 o 21 2 1 1.74 3.63 24.68 o 22 2 1 29.85 38.11 24.91 o 23 2 1 16.97 11.33 29.54 o 24 2 1 11.32 25.06 42.05 o 0 3 1 237.93 208.61 14.75 o 1 3 1 381.70 345.70 10.80 o 2 3 1 2085.72 2085.48 21.73 o 3 3 1 547.66 488.95 10.65 o 4 3 1 332.37 314.49 10.97 o 5 3 1 651.68 744.90 15.67 o 6 3 1 891.62 892.17 18.93 o 7 3 1 2165.69 2186.69 19.69 o 8 3 1 298.70 275.12 9.77 o 9 3 1 148.49 135.23 10.72 o 10 3 1 393.90 406.68 11.88 o 11 3 1 308.58 298.53 11.85 o 12 3 1 75.00 81.97 13.03 o 13 3 1 644.89 640.47 16.40 o 14 3 1 179.65 173.24 20.15 o 15 3 1 25.38 21.19 21.75 o 16 3 1 68.70 55.74 21.22 o 17 3 1 56.48 72.61 22.25 o 18 3 1 8.55 7.18 20.80 o 19 3 1 7.03 25.14 22.89 o 20 3 1 23.75 15.29 23.73 o 21 3 1 45.04 51.00 30.65 o 22 3 1 7.00 0.31 44.95 o 23 3 1 14.16 10.71 53.04 o 1 4 1 642.49 610.79 16.23 o 2 4 1 21.90 11.05 12.79 o 3 4 1 154.71 159.51 13.19 o 4 4 1 17.88 12.91 10.93 o 5 4 1 169.12 148.47 17.19 o 6 4 1 151.51 156.00 10.70 o 7 4 1 467.56 426.20 10.59 o 8 4 1 164.94 136.56 8.57 o 9 4 1 264.01 215.57 13.74 o 10 4 1 224.98 202.04 18.02 o 11 4 1 1024.78 1057.85 34.14 o 12 4 1 259.80 214.34 12.58 o 13 4 1 112.00 106.50 12.43 o 14 4 1 172.66 172.78 12.90 o 15 4 1 52.81 68.50 16.60 o 16 4 1 22.41 27.69 16.03 o 17 4 1 4.13 13.30 18.85 o 18 4 1 23.63 47.99 32.06 o 19 4 1 123.32 140.98 40.58 o 20 4 1 10.28 25.05 48.93 o 21 4 1 10.82 -11.33 49.09 o 22 4 1 3.72 18.60 51.73 o 0 5 1 5.01 3.08 24.02 o 1 5 1 9.04 28.79 18.22 o 2 5 1 1189.81 1165.56 18.38 o 3 5 1 141.71 131.23 14.72 o 4 5 1 400.26 400.80 13.73 o 5 5 1 30.14 32.92 12.48 o 6 5 1 644.54 643.50 16.79 o 7 5 1 111.62 120.84 14.84 o 8 5 1 21.10 18.53 12.50 o 9 5 1 46.21 46.99 12.63 o 10 5 1 487.70 505.06 25.17 o 11 5 1 47.20 48.95 17.63 o 12 5 1 61.91 62.39 12.69 o 13 5 1 7.58 8.74 8.29 o 14 5 1 35.02 55.75 21.76 o 15 5 1 1.34 8.07 22.51 o 16 5 1 20.00 21.76 31.86 o 17 5 1 42.73 80.58 38.69 o 18 5 1 19.69 36.02 40.17 o 19 5 1 21.55 18.87 40.17 o 20 5 1 44.54 1.83 52.09 o 1 6 1 57.67 75.51 18.22 o 2 6 1 509.32 506.15 19.16 o 3 6 1 1.74 3.70 17.33 o 4 6 1 0.53 -5.48 17.48 o 5 6 1 47.13 47.54 16.56 o 6 6 1 134.89 129.03 15.65 o 7 6 1 340.10 307.38 20.59 o 8 6 1 267.52 270.85 16.98 o 9 6 1 12.05 4.92 11.38 o 10 6 1 26.21 6.86 33.59 o 11 6 1 74.05 75.95 27.93 o 12 6 1 46.20 79.79 19.69 o 13 6 1 0.84 18.69 43.37 o 14 6 1 8.76 2.92 31.87 o 15 6 1 34.86 29.77 33.78 o 16 6 1 48.64 66.16 35.08 o 17 6 1 10.07 20.78 35.22 o 18 6 1 26.48 32.35 41.91 o 19 6 1 10.39 43.69 79.90 o 0 7 1 15.35 29.88 26.79 o 1 7 1 7.67 5.31 19.80 o 2 7 1 77.31 62.13 19.79 o 3 7 1 4.47 13.30 23.20 o 4 7 1 11.75 35.33 19.30 o 5 7 1 36.67 24.13 25.94 o 6 7 1 495.91 572.32 35.83 o 7 7 1 103.18 144.51 44.80 o 8 7 1 30.27 60.82 35.79 o 9 7 1 3.77 -10.25 35.58 o 10 7 1 71.86 111.19 36.16 o 11 7 1 7.52 20.08 37.12 o 12 7 1 0.67 0.64 37.59 o 13 7 1 7.90 17.03 39.07 o 14 7 1 75.46 92.55 40.95 o 15 7 1 6.60 39.55 41.44 o 16 7 1 7.42 11.30 44.53 o 1 8 1 5.91 26.52 41.55 o 2 8 1 39.77 51.53 41.71 o 3 8 1 54.61 92.28 41.46 o 4 8 1 5.55 11.74 49.21 o 5 8 1 56.94 54.43 48.26 o 6 8 1 2.41 36.07 48.27 o 7 8 1 120.33 150.83 50.38 o 8 8 1 6.30 1.17 50.05 o 9 8 1 68.76 64.20 49.68 o 10 8 1 7.80 3.00 48.73 o 11 8 1 8.33 24.41 49.91 o 12 8 1 33.53 20.12 52.87 o 0 9 1 20.14 38.00 60.58 o 1 9 1 5.66 17.19 42.34 o 2 9 1 26.18 46.74 49.34 o 3 9 1 106.75 207.44 49.67 o 4 9 1 3.55 19.77 59.89 o 5 9 1 14.24 97.95 48.97 o 0 0 2 39287.83 47047.93 422.75 o 2 0 2 8552.58 9433.42 56.51 o 4 0 2 9224.30 10328.05 180.18 o 6 0 2 2927.56 2673.15 31.61 o 8 0 2 1294.94 1280.69 17.18 o 10 0 2 1554.25 1537.09 24.22 o 12 0 2 1152.79 1261.81 38.72 o 14 0 2 200.11 166.06 21.34 o 16 0 2 221.57 212.43 23.17 o 18 0 2 117.85 168.28 25.23 o 20 0 2 128.47 141.42 30.38 o 22 0 2 16.53 15.65 39.58 o 24 0 2 55.16 50.17 44.42 o 1 1 2 724.64 747.51 18.01 o 2 1 2 2209.57 2377.12 22.59 o 3 1 2 499.44 541.51 35.00 o 4 1 2 3251.78 2982.81 18.93 o 5 1 2 2293.70 2390.66 17.06 o 6 1 2 629.07 598.77 10.03 o 7 1 2 446.55 425.80 8.55 o 8 1 2 991.56 980.94 10.45 o 9 1 2 847.56 867.43 10.29 o 10 1 2 1208.50 1192.18 13.80 o 11 1 2 83.30 99.52 10.76 o 12 1 2 786.34 804.50 16.97 o 13 1 2 494.70 503.16 13.82 o 14 1 2 78.42 92.21 13.68 o 15 1 2 92.95 92.28 15.26 o 16 1 2 120.63 135.28 17.32 o 17 1 2 240.47 249.15 16.49 o 18 1 2 120.42 118.93 17.30 o 19 1 2 80.70 84.66 17.61 o 20 1 2 8.93 36.94 20.03 o 21 1 2 51.18 22.08 23.90 o 22 1 2 26.97 24.62 24.62 o 23 1 2 16.21 7.50 30.79 o 24 1 2 6.46 20.64 35.41 o 0 2 2 4550.75 4780.75 60.36 o 1 2 2 2085.41 2088.33 23.70 o 2 2 2 951.49 996.04 16.13 o 3 2 2 1010.45 853.88 19.74 o 4 2 2 1703.06 1510.82 37.19 o 5 2 2 1697.36 1755.04 28.90 o 6 2 2 1011.64 1069.87 14.52 o 7 2 2 524.88 408.71 27.06 o 8 2 2 1470.10 1402.11 34.32 o 9 2 2 171.78 179.87 13.11 o 10 2 2 758.19 699.34 14.28 o 11 2 2 801.54 744.99 13.01 o 12 2 2 105.78 103.73 12.20 o 13 2 2 381.42 378.93 16.23 o 14 2 2 371.58 368.94 17.73 o 15 2 2 170.16 173.51 19.12 o 16 2 2 215.50 196.22 20.97 o 17 2 2 123.15 125.87 18.18 o 18 2 2 3.04 3.52 18.31 o 19 2 2 9.63 -2.74 22.76 o 20 2 2 20.70 33.98 22.36 o 21 2 2 12.86 19.07 24.76 o 22 2 2 9.13 4.54 31.44 o 23 2 2 10.30 -4.70 34.09 o 24 2 2 3.06 -0.37 35.59 o 1 3 2 1968.50 2130.01 29.44 o 2 3 2 556.84 584.32 12.41 o 3 3 2 23.37 28.10 9.44 o 4 3 2 546.80 554.29 19.80 o 5 3 2 2207.41 2034.40 29.14 o 6 3 2 1056.01 1118.04 19.69 o 7 3 2 52.75 38.29 17.13 o 8 3 2 593.98 548.83 13.20 o 9 3 2 142.17 129.25 12.77 o 10 3 2 11.33 19.24 15.44 o 11 3 2 158.24 156.78 15.47 o 12 3 2 23.50 18.24 20.64 o 13 3 2 435.36 408.44 23.07 o 14 3 2 192.85 205.81 15.62 o 15 3 2 188.09 183.52 17.56 o 16 3 2 116.33 103.49 18.13 o 17 3 2 8.20 16.24 21.06 o 18 3 2 22.20 35.68 20.21 o 19 3 2 53.86 73.89 22.20 o 20 3 2 23.72 26.56 31.01 o 21 3 2 27.81 7.25 30.75 o 22 3 2 7.34 -0.37 32.06 o 23 3 2 16.16 37.54 36.91 o 0 4 2 1407.73 1472.92 21.81 o 1 4 2 1462.62 1429.98 20.27 o 2 4 2 97.99 102.06 12.77 o 3 4 2 561.47 585.97 23.19 o 4 4 2 398.89 394.17 20.82 o 5 4 2 105.31 103.43 21.18 o 6 4 2 91.99 98.24 18.24 o 7 4 2 318.36 287.82 18.34 o 8 4 2 9.20 4.55 17.06 o 9 4 2 535.07 546.12 21.73 o 10 4 2 11.89 13.15 14.14 o 11 4 2 89.30 55.86 17.91 o 12 4 2 98.34 109.70 21.60 o 13 4 2 10.05 17.71 22.10 o 14 4 2 151.34 136.60 22.36 o 15 4 2 10.54 9.93 23.03 o 16 4 2 13.22 14.28 26.23 o 17 4 2 142.95 123.98 27.69 o 18 4 2 9.79 11.93 35.03 o 19 4 2 0.82 3.95 29.95 o 20 4 2 5.71 13.54 36.60 o 21 4 2 11.48 5.29 52.42 o 22 4 2 3.16 21.48 52.90 o 1 5 2 233.28 238.98 14.38 o 2 5 2 198.98 202.45 17.95 o 3 5 2 63.30 51.45 18.17 o 4 5 2 440.65 423.48 24.33 o 5 5 2 294.55 280.96 23.19 o 6 5 2 230.63 214.89 27.74 o 7 5 2 72.18 56.56 25.78 o 8 5 2 94.23 85.45 29.03 o 9 5 2 106.88 121.54 25.00 o 10 5 2 86.40 69.02 29.72 o 11 5 2 108.44 96.50 29.23 o 12 5 2 107.91 95.57 25.45 o 13 5 2 6.09 4.02 33.14 o 14 5 2 5.87 19.34 35.08 o 15 5 2 5.08 17.07 45.35 o 16 5 2 55.29 93.18 46.46 o 17 5 2 5.95 -6.05 48.22 o 18 5 2 81.14 103.41 49.46 o 19 5 2 20.36 20.49 52.83 o 20 5 2 22.13 90.79 55.22 o 0 6 2 367.84 379.21 30.80 o 1 6 2 325.85 342.54 20.68 o 2 6 2 4.80 9.62 18.32 o 3 6 2 363.57 394.16 22.77 o 4 6 2 177.22 153.61 24.76 o 5 6 2 42.17 35.12 25.55 o 6 6 2 17.24 5.90 32.77 o 7 6 2 106.08 137.55 32.39 o 8 6 2 27.31 3.29 31.81 o 9 6 2 13.45 16.37 33.34 o 10 6 2 118.34 124.12 29.39 o 11 6 2 42.51 25.85 28.73 o 12 6 2 53.85 59.97 35.50 o 13 6 2 43.30 18.17 36.75 o 14 6 2 36.43 63.44 38.10 o 15 6 2 1.44 -0.55 38.24 o 16 6 2 5.17 16.84 72.42 o 17 6 2 6.47 17.81 50.82 o 18 6 2 10.54 0.04 53.67 o 1 7 2 79.38 76.78 25.10 o 2 7 2 18.68 32.80 24.18 o 3 7 2 15.38 31.51 45.52 o 4 7 2 118.56 114.17 37.46 o 5 7 2 62.24 67.87 35.10 o 6 7 2 55.56 69.74 35.50 o 7 7 2 0.85 -7.62 35.56 o 8 7 2 232.89 335.42 37.76 o 9 7 2 12.34 -1.38 36.56 o 10 7 2 1.18 49.51 45.18 o 11 7 2 21.17 27.99 38.62 o 12 7 2 82.94 122.79 38.34 o 13 7 2 4.22 41.34 39.50 o 14 7 2 23.74 29.72 41.57 o 15 7 2 0.15 16.46 51.33 o 0 8 2 55.77 37.54 74.37 o 1 8 2 22.05 41.07 53.07 o 2 8 2 4.12 -17.88 74.19 o 3 8 2 31.54 7.85 41.48 o 4 8 2 41.22 63.84 41.29 o 5 8 2 0.85 -8.61 40.83 o 6 8 2 9.33 15.48 39.95 o 7 8 2 41.05 49.51 49.94 o 8 8 2 6.94 41.43 50.81 o 9 8 2 28.75 31.99 41.04 o 10 8 2 22.22 36.91 41.36 o 11 8 2 28.08 22.01 42.96 o 12 8 2 2.79 -9.88 51.69 o 1 9 2 15.22 87.12 62.07 o 2 9 2 4.22 3.43 49.53 o 3 9 2 10.16 7.01 49.21 o 4 9 2 12.05 11.77 49.49 o 2 0 3 954.72 926.36 36.16 o 4 0 3 1123.76 1128.50 27.64 o 6 0 3 332.04 303.01 13.68 o 8 0 3 103.73 101.88 15.51 o 10 0 3 870.27 838.15 24.05 o 12 0 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o 7 1 4 132.32 155.33 13.75 o 8 1 4 813.32 846.85 16.68 o 9 1 4 28.52 41.72 15.15 o 10 1 4 55.13 58.54 15.06 o 11 1 4 137.78 140.35 14.06 o 12 1 4 207.91 197.88 15.02 o 13 1 4 182.29 186.20 15.12 o 14 1 4 134.97 143.80 15.58 o 15 1 4 11.60 -1.26 13.30 o 16 1 4 167.91 124.62 14.71 o 17 1 4 101.19 93.94 19.66 o 18 1 4 46.07 71.58 29.67 o 19 1 4 86.00 67.14 28.05 o 20 1 4 19.44 30.59 28.58 o 21 1 4 5.56 -1.40 31.80 o 22 1 4 36.40 45.15 35.80 o 23 1 4 3.20 8.75 41.08 o 0 2 4 427.51 449.23 53.33 o 1 2 4 914.64 958.60 17.72 o 2 2 4 502.01 472.39 23.07 o 3 2 4 336.40 334.23 20.47 o 4 2 4 1024.47 1062.33 22.46 o 5 2 4 389.32 436.45 20.89 o 6 2 4 411.87 361.63 18.29 o 7 2 4 1404.78 1422.12 19.37 o 8 2 4 47.96 49.66 13.27 o 9 2 4 66.29 74.66 15.87 o 10 2 4 199.85 203.03 15.64 o 11 2 4 139.94 128.45 15.04 o 12 2 4 121.45 116.89 11.07 o 13 2 4 383.06 345.50 13.51 o 14 2 4 311.10 296.69 16.31 o 15 2 4 102.49 95.31 16.43 o 16 2 4 73.19 50.65 17.15 o 17 2 4 18.53 47.41 27.98 o 18 2 4 16.77 7.83 29.45 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166.21 18.75 o 11 4 4 88.89 68.28 14.67 o 12 4 4 33.87 56.03 29.98 o 13 4 4 89.48 73.70 29.58 o 14 4 4 51.19 52.84 25.40 o 15 4 4 105.21 87.49 31.08 o 16 4 4 1.92 17.24 31.73 o 17 4 4 110.91 125.67 30.84 o 18 4 4 2.71 6.10 30.88 o 19 4 4 6.92 24.98 32.21 o 20 4 4 0.84 -24.34 53.89 o 1 5 4 325.50 350.63 18.98 o 2 5 4 362.26 363.46 21.80 o 3 5 4 24.17 22.31 16.61 o 4 5 4 70.06 90.08 24.52 o 5 5 4 187.40 176.23 24.98 o 6 5 4 616.11 684.28 23.86 o 7 5 4 8.13 8.56 20.45 o 8 5 4 32.27 32.08 18.69 o 9 5 4 93.13 81.14 19.37 o 10 5 4 13.20 17.51 21.19 o 11 5 4 17.35 18.45 18.72 o 12 5 4 70.92 45.54 13.76 o 13 5 4 44.26 47.64 38.39 o 14 5 4 18.29 26.36 40.24 o 15 5 4 4.55 8.11 31.25 o 16 5 4 5.46 0.42 32.27 o 17 5 4 2.89 20.63 45.36 o 18 5 4 79.11 45.46 46.82 o 19 5 4 15.38 6.06 55.75 o 0 6 4 465.24 492.66 47.00 o 1 6 4 97.48 112.96 22.24 o 2 6 4 30.69 17.22 19.72 o 3 6 4 65.71 38.68 25.49 o 4 6 4 235.03 232.36 26.96 o 5 6 4 84.59 77.37 26.68 o 6 6 4 45.59 36.16 26.34 o 7 6 4 71.30 72.76 24.37 o 8 6 4 73.58 82.74 21.50 o 9 6 4 5.86 12.78 20.77 o 10 6 4 80.34 76.06 20.11 o 11 6 4 1.76 24.23 27.12 o 12 6 4 7.31 13.03 39.38 o 13 6 4 19.92 28.32 40.59 o 14 6 4 44.56 17.83 42.39 o 15 6 4 9.05 45.36 55.98 o 16 6 4 7.81 33.47 45.09 o 17 6 4 1.54 -22.31 52.99 o 1 7 4 12.04 1.25 30.12 o 2 7 4 204.94 244.44 36.73 o 3 7 4 0.76 27.66 32.24 o 4 7 4 31.98 7.08 31.93 o 5 7 4 1.82 4.92 37.39 o 6 7 4 13.29 5.22 33.46 o 7 7 4 2.37 18.44 32.84 o 8 7 4 113.99 135.51 29.94 o 9 7 4 15.91 20.42 39.46 o 10 7 4 29.94 47.19 39.90 o 11 7 4 4.68 8.20 39.88 o 12 7 4 29.59 39.87 49.13 o 13 7 4 3.38 15.31 49.41 o 14 7 4 10.37 22.53 52.55 o 0 8 4 20.90 34.48 65.41 o 1 8 4 28.03 5.91 46.81 o 2 8 4 21.41 4.86 45.99 o 3 8 4 0.31 9.90 45.76 o 4 8 4 57.62 56.62 36.73 o 5 8 4 12.90 13.34 32.87 o 6 8 4 15.50 10.61 41.29 o 7 8 4 20.47 43.22 43.55 o 8 8 4 1.10 15.01 53.66 o 9 8 4 6.10 -6.31 44.60 o 2 0 5 289.41 309.55 25.06 o 4 0 5 33.05 55.81 26.37 o 6 0 5 52.23 43.73 24.35 o 8 0 5 798.14 809.12 17.91 o 10 0 5 102.97 86.48 22.78 o 12 0 5 497.09 529.45 26.16 o 14 0 5 51.46 54.27 23.59 o 16 0 5 424.41 446.01 31.05 o 18 0 5 27.97 42.14 40.68 o 20 0 5 4.41 8.30 43.10 o 22 0 5 39.70 23.98 46.79 o 0 1 5 244.56 289.61 30.69 o 1 1 5 1526.48 1627.72 26.25 o 2 1 5 85.85 117.13 20.94 o 3 1 5 8.89 7.79 17.83 o 4 1 5 220.27 220.12 18.76 o 5 1 5 121.36 127.76 16.65 o 6 1 5 385.07 406.08 17.62 o 7 1 5 537.86 550.53 17.58 o 8 1 5 8.51 17.87 14.15 o 9 1 5 96.55 94.36 14.95 o 10 1 5 146.02 135.03 15.51 o 11 1 5 80.85 93.19 15.36 o 12 1 5 33.60 39.64 15.69 o 13 1 5 1.03 6.23 15.43 o 14 1 5 155.40 152.65 17.74 o 15 1 5 30.41 25.97 17.37 o 16 1 5 71.22 75.44 20.62 o 17 1 5 91.68 122.15 30.29 o 18 1 5 66.26 53.74 31.92 o 19 1 5 4.56 -0.46 31.53 o 20 1 5 44.45 66.49 33.24 o 21 1 5 19.42 26.72 36.46 o 22 1 5 11.97 12.46 38.80 o 1 2 5 609.01 610.38 27.69 o 2 2 5 136.64 156.14 15.82 o 3 2 5 39.59 26.97 11.37 o 4 2 5 208.24 209.97 18.75 o 5 2 5 1609.91 1660.37 23.31 o 6 2 5 20.76 18.66 18.11 o 7 2 5 0.87 6.34 18.32 o 8 2 5 46.42 35.77 14.39 o 9 2 5 13.34 9.71 16.89 o 10 2 5 27.08 26.25 19.62 o 11 2 5 269.07 275.26 21.37 o 12 2 5 230.45 219.63 18.76 o 13 2 5 161.74 152.52 18.17 o 14 2 5 130.60 91.80 18.57 o 15 2 5 50.17 57.02 19.15 o 16 2 5 0.46 5.50 26.72 o 17 2 5 13.03 20.85 30.36 o 18 2 5 9.92 -5.80 31.20 o 19 2 5 87.90 95.89 33.15 o 20 2 5 51.08 72.76 40.19 o 21 2 5 23.57 57.28 47.05 o 0 3 5 1.41 22.14 21.45 o 1 3 5 194.28 216.34 18.47 o 2 3 5 134.96 125.11 17.39 o 3 3 5 864.80 838.95 32.55 o 4 3 5 305.65 347.06 23.25 o 5 3 5 12.13 5.24 21.96 o 6 3 5 15.95 37.69 21.12 o 7 3 5 577.25 560.50 21.91 o 8 3 5 93.36 71.40 12.87 o 9 3 5 443.36 331.12 26.97 o 10 3 5 279.18 300.88 20.36 o 11 3 5 464.88 344.34 22.43 o 12 3 5 62.81 36.37 19.90 o 13 3 5 94.58 97.66 21.20 o 14 3 5 16.33 -6.64 27.40 o 15 3 5 44.41 54.76 28.61 o 16 3 5 9.39 18.81 29.87 o 17 3 5 84.61 90.95 30.81 o 18 3 5 23.80 23.52 32.18 o 19 3 5 1.28 20.91 45.23 o 20 3 5 5.53 39.23 40.62 o 21 3 5 21.12 -0.81 56.46 o 1 4 5 581.07 525.79 21.82 o 2 4 5 312.20 334.28 19.29 o 3 4 5 130.36 146.27 18.56 o 4 4 5 305.38 305.77 17.95 o 5 4 5 312.55 260.49 16.00 o 6 4 5 179.79 226.61 19.39 o 7 4 5 11.38 8.22 17.26 o 8 4 5 97.91 91.98 13.34 o 9 4 5 213.40 224.56 22.85 o 10 4 5 80.90 67.31 20.73 o 11 4 5 210.92 181.36 19.61 o 12 4 5 140.14 129.82 34.32 o 13 4 5 34.54 37.96 33.52 o 14 4 5 5.47 50.85 35.45 o 15 4 5 191.10 185.78 31.08 o 16 4 5 14.84 17.85 30.83 o 17 4 5 21.99 42.02 34.13 o 18 4 5 7.36 13.29 36.00 o 19 4 5 1.23 27.95 34.85 o 0 5 5 1875.06 1785.33 32.01 o 1 5 5 141.64 163.05 18.40 o 2 5 5 14.46 17.90 17.14 o 3 5 5 117.60 98.03 16.44 o 4 5 5 80.93 84.55 15.00 o 5 5 5 3.64 20.73 17.25 o 6 5 5 249.10 252.56 20.91 o 7 5 5 177.90 177.94 18.74 o 8 5 5 113.42 106.28 15.65 o 9 5 5 34.54 33.82 12.99 o 10 5 5 105.71 118.66 24.35 o 11 5 5 51.10 49.92 21.57 o 12 5 5 9.62 12.71 40.26 o 13 5 5 37.80 38.49 40.12 o 14 5 5 27.12 31.26 36.00 o 15 5 5 12.19 13.06 52.69 o 16 5 5 40.92 60.20 32.11 o 17 5 5 35.05 43.76 33.22 o 18 5 5 26.95 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6 38.53 41.41 29.85 o 9 6 6 14.76 30.60 35.44 o 10 6 6 45.80 51.74 35.49 o 11 6 6 8.43 15.41 36.72 o 12 6 6 6.03 34.10 46.86 o 13 6 6 9.21 -6.70 43.61 o 14 6 6 44.85 38.19 48.82 o 1 7 6 11.50 20.19 34.00 o 2 7 6 67.64 83.62 32.92 o 3 7 6 1.29 -1.07 32.77 o 4 7 6 25.52 17.24 33.56 o 5 7 6 15.17 16.23 34.01 o 6 7 6 23.98 42.38 33.40 o 7 7 6 9.03 -7.64 29.99 o 8 7 6 10.89 -10.44 38.04 o 9 7 6 26.25 64.09 46.34 o 10 7 6 20.48 42.40 47.92 o 2 0 7 844.21 905.12 42.79 o 4 0 7 320.68 363.75 38.19 o 6 0 7 659.08 695.97 40.72 o 8 0 7 611.08 614.85 22.79 o 10 0 7 28.75 15.61 16.20 o 12 0 7 334.65 341.60 35.20 o 14 0 7 43.75 20.17 45.44 o 16 0 7 142.00 176.82 50.68 o 18 0 7 63.46 38.88 53.32 o 0 1 7 1338.65 1317.45 62.58 o 1 1 7 294.45 386.32 39.86 o 2 1 7 7.22 18.51 26.24 o 3 1 7 208.87 181.69 27.48 o 4 1 7 873.19 979.63 29.92 o 5 1 7 9.13 -0.57 26.23 o 6 1 7 320.54 341.43 32.73 o 7 1 7 49.37 109.95 32.05 o 8 1 7 57.53 56.41 22.65 o 9 1 7 228.10 212.93 23.84 o 10 1 7 77.17 67.73 20.64 o 11 1 7 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