#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/46/2104626.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104626_Fobs loop_ _publ_author_name 'Drebushchak, Tatiana N.' 'Chesalov, Yury A.' 'Boldyreva, Elena V.' _publ_section_title ; A conformational polymorphic transition in the high-temperature \e-form of chlorpropamide on cooling: a new \e'-form ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 770 _journal_page_last 781 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 26.6570 _cell_length_b 5.0938 _cell_length_c 8.9941 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.8114 _[local]_cod_data_source_file gp5033acpa105sup5.hkl _[local]_cod_data_source_block acpa105 #BEGIN Tags that were not found in dictionaries: _shelx_title acpa105 _shelx_refln_list_code 4 _shelx_f_calc_maximum 232.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3454.65 3438.60 17.50 o 4 0 0 344.79 360.61 6.35 o 6 0 0 1636.67 1545.89 13.47 o 8 0 0 840.29 848.00 13.88 o 10 0 0 195.48 166.38 7.70 o 12 0 0 3264.55 3223.43 26.40 o 14 0 0 1378.04 1484.02 19.94 o 16 0 0 520.08 543.18 13.64 o 18 0 0 1161.04 1234.15 20.93 o 20 0 0 635.05 734.46 17.59 o 22 0 0 85.34 101.41 8.17 o 24 0 0 982.97 1066.53 44.13 o 26 0 0 19.97 23.77 14.06 o 28 0 0 137.94 156.51 11.33 o 30 0 0 262.69 263.90 18.22 o 32 0 0 382.66 420.91 21.00 o 1 1 0 162.46 151.78 5.67 o 2 1 0 4013.78 3835.62 19.23 o 3 1 0 44.86 44.50 4.27 o 4 1 0 22263.11 21609.54 99.78 o 5 1 0 15699.52 15210.07 46.29 o 6 1 0 229.20 214.66 7.66 o 7 1 0 6053.53 6473.25 31.31 o 8 1 0 167.07 153.15 10.71 o 9 1 0 6306.02 6326.63 77.90 o 10 1 0 665.60 621.75 12.23 o 11 1 0 1085.58 1177.15 16.75 o 12 1 0 49.39 45.52 6.61 o 13 1 0 151.54 124.53 8.42 o 14 1 0 846.74 862.49 16.20 o 15 1 0 636.75 587.99 14.23 o 16 1 0 75.62 63.02 31.82 o 17 1 0 1085.75 1081.31 24.67 o 18 1 0 721.32 731.48 50.29 o 19 1 0 465.99 435.03 77.21 o 20 1 0 259.62 228.78 100.66 o 21 1 0 394.86 357.42 159.50 o 22 1 0 671.71 646.75 119.16 o 23 1 0 11.67 -218.99 942.76 o 24 1 0 1780.85 1790.68 442.83 o 25 1 0 1222.37 1076.35 510.41 o 26 1 0 50.20 -123.29 596.54 o 27 1 0 641.45 590.77 83.45 o 28 1 0 134.82 -9.17 726.29 o 29 1 0 972.74 1063.09 94.00 o 30 1 0 66.76 -14.96 59.22 o 31 1 0 35.23 35.64 9.71 o 32 1 0 1.52 -16.10 16.10 o 0 2 0 1564.25 1571.24 17.26 o 1 2 0 65.06 55.39 5.07 o 2 2 0 1015.79 909.40 14.42 o 3 2 0 2799.04 2778.96 33.31 o 4 2 0 1144.48 1020.78 14.65 o 5 2 0 1158.51 1196.34 19.12 o 6 2 0 64.80 68.66 5.24 o 7 2 0 683.13 741.44 13.76 o 8 2 0 4706.21 4572.23 67.35 o 9 2 0 4058.26 4202.62 31.86 o 10 2 0 1456.77 1528.67 29.21 o 11 2 0 56.43 62.51 5.76 o 12 2 0 292.23 292.86 13.06 o 13 2 0 403.26 413.29 28.69 o 14 2 0 236.06 221.28 10.73 o 15 2 0 159.65 163.80 10.96 o 16 2 0 725.32 707.01 17.11 o 17 2 0 660.11 701.56 27.46 o 18 2 0 147.25 133.97 27.51 o 19 2 0 491.68 474.38 76.92 o 20 2 0 1819.55 1985.44 30.18 o 21 2 0 548.23 488.93 17.33 o 22 2 0 519.90 576.80 22.11 o 23 2 0 12.91 6.86 7.98 o 24 2 0 43.01 42.06 25.08 o 25 2 0 109.04 110.52 22.06 o 26 2 0 130.26 152.37 21.57 o 27 2 0 83.37 55.57 174.88 o 28 2 0 329.51 387.90 187.39 o 29 2 0 324.97 314.08 343.22 o 30 2 0 456.69 500.52 87.22 o 31 2 0 38.71 -181.59 255.54 o 1 3 0 174.59 176.60 10.24 o 2 3 0 27.58 45.71 5.40 o 3 3 0 337.42 308.84 18.73 o 4 3 0 199.81 187.94 24.20 o 5 3 0 260.58 244.46 10.24 o 6 3 0 300.37 298.04 11.20 o 7 3 0 680.01 662.39 15.36 o 8 3 0 0.31 -6.20 6.20 o 9 3 0 60.87 46.73 5.98 o 10 3 0 6.30 6.63 9.83 o 11 3 0 26.64 29.96 10.94 o 12 3 0 147.23 148.28 10.26 o 13 3 0 1288.92 1363.16 23.52 o 14 3 0 137.56 129.95 9.27 o 15 3 0 18.34 -8.31 8.31 o 16 3 0 3119.95 3031.09 36.38 o 17 3 0 1287.99 1339.81 40.44 o 18 3 0 12.99 6.12 23.92 o 19 3 0 500.03 584.06 18.44 o 20 3 0 17.63 -0.99 12.75 o 21 3 0 0.66 -3.26 8.63 o 22 3 0 6.51 -1.79 8.75 o 23 3 0 240.90 299.97 18.68 o 24 3 0 1.29 -52.59 52.59 o 25 3 0 704.66 884.56 24.61 o 26 3 0 0.04 -13.49 13.81 o 27 3 0 0.58 -89.26 104.79 o 28 3 0 963.35 1032.89 28.85 o 0 4 0 307.38 308.09 23.46 o 1 4 0 486.58 472.28 15.09 o 2 4 0 740.31 704.52 36.80 o 3 4 0 16.65 23.20 9.16 o 4 4 0 111.57 109.09 14.09 o 5 4 0 1.19 8.49 7.40 o 6 4 0 1073.02 953.97 29.52 o 7 4 0 516.52 534.01 20.51 o 8 4 0 8.60 -4.01 7.63 o 9 4 0 4.62 9.99 12.08 o 10 4 0 7.38 19.22 8.06 o 11 4 0 858.28 929.62 30.63 o 12 4 0 1401.10 1394.51 26.11 o 13 4 0 9.34 9.16 8.30 o 14 4 0 123.84 129.44 27.35 o 15 4 0 11.18 -3.78 8.67 o 16 4 0 73.11 58.86 17.13 o 17 4 0 55.82 65.68 12.15 o 18 4 0 444.54 472.56 45.52 o 19 4 0 1.05 -2.40 19.66 o 20 4 0 101.06 82.12 20.28 o 21 4 0 456.56 429.00 25.57 o 22 4 0 3.21 -9.60 9.60 o 23 4 0 447.76 527.93 69.28 o 24 4 0 228.41 188.03 25.55 o 25 4 0 320.73 376.82 20.41 o 1 5 0 835.66 799.31 21.77 o 2 5 0 49.88 53.60 8.23 o 3 5 0 0.67 8.79 9.26 o 4 5 0 127.99 110.34 8.79 o 5 5 0 50.15 66.93 24.31 o 6 5 0 19.34 21.07 7.86 o 7 5 0 7.47 -16.15 16.15 o 8 5 0 146.11 150.82 15.92 o 9 5 0 71.76 75.02 8.37 o 10 5 0 22.06 30.69 14.06 o 11 5 0 710.60 729.44 37.65 o 12 5 0 151.87 169.75 12.23 o 13 5 0 92.06 87.70 15.74 o 14 5 0 260.67 288.48 39.45 o 15 5 0 363.19 350.99 20.01 o 16 5 0 7.34 4.03 33.00 o 17 5 0 422.05 439.31 21.68 o 18 5 0 67.79 54.34 10.77 o 19 5 0 26.75 15.24 13.47 o 0 6 0 747.45 673.98 23.08 o 1 6 0 112.82 106.30 16.64 o 2 6 0 217.33 212.14 18.66 o 3 6 0 714.70 713.24 30.04 o 4 6 0 9.41 11.66 9.98 o 5 6 0 55.91 50.76 9.28 o 6 6 0 539.19 565.89 21.31 o 7 6 0 7.81 15.76 10.26 o 8 6 0 21.60 27.08 9.61 o 9 6 0 520.23 535.72 22.19 o 1 0 1 9.66 10.19 3.10 o 2 0 1 8443.38 8512.09 23.14 o 3 0 1 5.28 1.80 3.71 o 4 0 1 784.51 772.10 9.01 o 5 0 1 144.79 159.77 6.28 o 6 0 1 805.16 852.50 11.13 o 7 0 1 110.77 149.91 14.35 o 8 0 1 645.94 723.33 33.06 o 9 0 1 1161.26 1145.90 821.22 o 10 0 1 5935.99 5843.94 45.54 o 11 0 1 4.02 -136.53 984.69 o 12 0 1 524.76 468.03 24.75 o 13 0 1 38.44 5.74 278.17 o 14 0 1 16.24 -24.17 91.99 o 15 0 1 497.34 446.46 489.74 o 16 0 1 7661.80 7918.68 364.17 o 17 0 1 485.12 125.93 2757.05 o 18 0 1 12.62 -157.93 177.20 o 19 0 1 722.99 735.77 17.59 o 20 0 1 342.01 239.72 100.38 o 21 0 1 174.18 56.33 176.01 o 22 0 1 5025.70 5293.89 47.84 o 23 0 1 269.47 18.74 465.38 o 24 0 1 474.11 521.78 32.38 o 25 0 1 7.29 -23.09 31.15 o 26 0 1 125.05 97.53 16.36 o 27 0 1 84.18 74.09 22.19 o 28 0 1 410.76 443.53 18.78 o 29 0 1 0.12 -20.15 20.15 o 30 0 1 88.97 111.06 16.67 o 31 0 1 10.04 -10.99 10.99 o 32 0 1 862.40 1054.77 33.26 o -32 1 1 44.80 16.67 16.51 o -31 1 1 15.33 -13.78 13.78 o -30 1 1 63.43 54.14 13.52 o -29 1 1 12.18 -12.90 12.90 o -28 1 1 57.38 46.50 11.87 o -27 1 1 42.03 37.16 15.17 o -26 1 1 688.48 744.50 30.66 o -25 1 1 224.68 259.23 24.15 o -24 1 1 229.97 229.92 22.76 o -23 1 1 391.94 432.63 22.40 o -22 1 1 104.21 114.00 12.02 o -21 1 1 50.46 51.25 10.84 o -20 1 1 1072.55 1135.75 31.48 o -19 1 1 178.89 177.84 15.95 o -18 1 1 1487.72 1589.49 34.73 o -17 1 1 113.25 106.06 10.63 o -16 1 1 160.35 203.08 13.93 o -15 1 1 125.38 123.40 11.04 o -14 1 1 1376.24 1405.04 28.69 o -13 1 1 1899.20 2050.76 32.98 o -12 1 1 1788.97 1945.59 31.33 o -11 1 1 3859.52 4021.64 42.32 o -10 1 1 1334.09 1434.92 25.29 o -9 1 1 1158.70 1298.88 23.12 o -8 1 1 2735.55 2727.61 31.33 o -7 1 1 5527.66 5636.36 42.58 o -6 1 1 5069.31 4889.07 38.29 o -5 1 1 8032.88 7993.99 46.50 o -4 1 1 3659.22 3630.55 30.24 o -3 1 1 5042.74 4709.94 33.13 o -2 1 1 1708.84 1670.20 19.82 o -1 1 1 239.57 219.80 9.50 o 0 1 1 247.54 288.48 10.12 o 1 1 1 201.64 194.82 9.08 o 2 1 1 1711.13 1680.37 19.92 o 3 1 1 5005.35 4677.79 32.87 o 4 1 1 3675.87 3582.61 29.98 o 5 1 1 8001.53 7834.11 45.88 o 6 1 1 5009.02 4813.16 37.93 o 7 1 1 5586.69 5602.87 42.58 o 8 1 1 2718.24 2743.04 31.38 o 9 1 1 1171.79 1352.61 23.48 o 10 1 1 1320.65 1445.29 25.29 o 11 1 1 3886.90 3995.32 42.42 o 12 1 1 1767.67 1770.74 30.66 o 13 1 1 1899.33 1814.14 32.10 o 14 1 1 1360.46 1377.02 28.28 o 15 1 1 117.89 96.97 10.32 o 16 1 1 162.63 169.64 14.40 o 17 1 1 107.57 -28.49 28.49 o 18 1 1 1482.28 1440.65 35.09 o 19 1 1 179.83 -65.39 65.39 o 20 1 1 1056.49 969.62 32.56 o 21 1 1 51.68 -42.58 42.58 o 22 1 1 107.88 -21.06 21.06 o 23 1 1 396.25 56.51 20.28 o 24 1 1 215.18 -23.59 23.59 o 25 1 1 222.82 -34.42 34.42 o 26 1 1 686.52 506.43 30.40 o 27 1 1 42.31 -17.24 17.24 o 28 1 1 53.20 10.84 15.48 o 29 1 1 12.64 -13.37 13.37 o 30 1 1 64.33 33.49 15.90 o 31 1 1 17.46 -12.95 12.95 o 32 1 1 42.80 -17.91 17.91 o -31 2 1 120.49 111.27 16.51 o -30 2 1 1047.94 1298.42 43.87 o -29 2 1 137.89 138.93 15.84 o -28 2 1 20.31 8.98 13.78 o -27 2 1 72.04 96.87 14.09 o -26 2 1 156.50 154.52 17.29 o -25 2 1 111.42 165.20 15.69 o -24 2 1 807.79 864.96 31.95 o -23 2 1 10.63 33.70 12.85 o -22 2 1 16.72 23.43 12.13 o -21 2 1 262.42 227.64 21.52 o -20 2 1 567.33 559.69 24.98 o -19 2 1 216.76 238.64 20.33 o -18 2 1 618.53 682.26 25.03 o -17 2 1 153.44 192.09 15.64 o -16 2 1 187.60 191.83 17.55 o -15 2 1 1036.42 1112.94 28.85 o -14 2 1 546.59 536.26 20.39 o -13 2 1 3482.01 3735.52 48.05 o -12 2 1 2768.27 2714.50 40.15 o -11 2 1 374.48 398.98 16.77 o -10 2 1 1360.72 1462.12 28.64 o -9 2 1 384.33 334.94 15.69 o -8 2 1 2474.89 2427.97 34.22 o -7 2 1 546.27 537.19 17.29 o -6 2 1 2186.59 2260.09 31.69 o -5 2 1 241.84 258.30 12.90 o -4 2 1 55.80 69.36 8.00 o -3 2 1 350.57 358.63 13.73 o -2 2 1 1332.17 1262.45 22.76 o -1 2 1 1651.87 1670.77 25.60 o 0 2 1 1045.51 1034.88 14.60 o 1 2 1 1621.97 1633.10 25.39 o 2 2 1 1285.31 1296.04 23.02 o 3 2 1 352.39 373.03 13.93 o 4 2 1 61.04 62.19 7.38 o 5 2 1 232.25 280.60 12.64 o 6 2 1 2177.58 2245.59 31.48 o 7 2 1 561.79 548.03 17.24 o 8 2 1 2497.44 2483.60 34.63 o 9 2 1 384.93 363.68 15.43 o 10 2 1 1354.95 1434.30 28.13 o 11 2 1 382.39 397.64 16.67 o 12 2 1 2779.53 2681.42 39.84 o 13 2 1 3447.69 3668.74 47.43 o 14 2 1 528.73 446.36 19.40 o 15 2 1 1036.31 1080.78 28.07 o 16 2 1 189.43 193.58 17.44 o 17 2 1 157.49 139.91 12.33 o 18 2 1 602.96 607.07 24.31 o 19 2 1 212.73 174.64 17.96 o 20 2 1 557.42 597.06 25.08 o 21 2 1 264.29 257.89 21.62 o 22 2 1 16.94 3.66 11.20 o 23 2 1 9.66 -12.44 12.44 o 24 2 1 801.42 870.12 32.82 o 25 2 1 108.39 -20.44 20.44 o 26 2 1 156.17 105.18 16.31 o 27 2 1 71.60 11.41 17.50 o 28 2 1 21.18 -15.53 15.53 o 29 2 1 137.54 -48.67 48.67 o 30 2 1 1034.24 1020.14 43.51 o 31 2 1 119.74 -34.11 34.11 o -28 3 1 33.23 56.00 13.16 o -27 3 1 8.14 -0.98 13.99 o -26 3 1 632.18 594.58 31.33 o -25 3 1 3.28 6.97 13.06 o -24 3 1 84.39 94.29 13.42 o -23 3 1 119.87 133.77 14.40 o -22 3 1 108.93 133.46 14.45 o -21 3 1 173.88 219.70 21.06 o -20 3 1 46.44 53.88 11.35 o -19 3 1 234.12 237.81 21.42 o -18 3 1 10.05 5.21 11.56 o -17 3 1 170.61 207.16 19.97 o -16 3 1 640.48 676.53 26.17 o -15 3 1 833.63 825.84 27.77 o -14 3 1 737.46 703.37 26.06 o -13 3 1 457.30 430.62 21.06 o -12 3 1 1292.18 1261.67 31.69 o -11 3 1 87.50 106.52 10.63 o -10 3 1 335.62 351.40 17.80 o -9 3 1 1427.21 1370.56 31.33 o -8 3 1 267.21 245.24 15.84 o -7 3 1 2115.29 2214.93 37.52 o -6 3 1 1088.86 1151.13 27.46 o -5 3 1 113.83 94.08 9.96 o -4 3 1 564.27 545.04 19.51 o -3 3 1 2112.36 2073.78 34.99 o -2 3 1 394.03 366.21 16.98 o -1 3 1 662.28 667.86 20.54 o 0 3 1 151.46 151.11 13.62 o 1 3 1 637.66 644.69 20.54 o 2 3 1 394.64 443.16 17.24 o 3 3 1 2154.51 2044.62 34.78 o 4 3 1 570.44 597.94 20.75 o 5 3 1 109.12 74.01 8.83 o 6 3 1 1082.51 1082.85 26.73 o 7 3 1 2139.99 2206.62 37.42 o 8 3 1 270.70 232.81 15.53 o 9 3 1 1397.39 1278.44 30.60 o 10 3 1 330.40 334.84 17.39 o 11 3 1 88.87 114.26 11.35 o 12 3 1 1293.08 1255.43 31.33 o 13 3 1 455.43 415.76 20.02 o 14 3 1 735.93 742.03 26.06 o 15 3 1 816.34 803.70 27.66 o 16 3 1 649.81 716.32 26.78 o 17 3 1 170.03 175.52 19.30 o 18 3 1 10.34 20.33 11.72 o 19 3 1 228.02 231.88 21.52 o 20 3 1 51.72 20.95 13.31 o 21 3 1 171.56 173.46 15.02 o 22 3 1 105.61 124.48 14.19 o 23 3 1 116.16 100.07 13.68 o 24 3 1 84.48 106.26 13.88 o 25 3 1 2.85 -13.06 13.06 o 26 3 1 630.53 695.78 32.10 o 27 3 1 7.37 -14.97 14.97 o 28 3 1 32.48 14.71 15.07 o -25 4 1 9.22 24.57 15.17 o -24 4 1 132.00 117.93 14.97 o -23 4 1 96.22 111.94 14.97 o -22 4 1 516.97 565.06 29.37 o -21 4 1 901.86 912.85 36.07 o -20 4 1 115.38 125.46 14.66 o -19 4 1 327.72 357.13 24.36 o -18 4 1 195.94 213.97 19.46 o -17 4 1 317.16 295.77 25.34 o -16 4 1 226.16 237.45 22.35 o -15 4 1 68.04 74.94 12.18 o -14 4 1 31.41 38.65 10.58 o -13 4 1 44.84 54.96 10.63 o -12 4 1 56.72 51.92 10.58 o -11 4 1 138.58 148.22 14.71 o -10 4 1 1161.33 1184.21 33.75 o -9 4 1 1415.02 1463.51 36.80 o -8 4 1 356.89 338.29 19.82 o -7 4 1 574.49 581.83 24.41 o -6 4 1 493.94 511.49 22.19 o -5 4 1 674.43 652.38 25.29 o -4 4 1 34.73 13.47 11.35 o -3 4 1 438.08 421.07 20.69 o -2 4 1 261.30 251.02 20.13 o -1 4 1 114.05 102.60 11.04 o 0 4 1 248.56 256.54 25.62 o 1 4 1 112.26 119.73 13.68 o 2 4 1 264.11 295.87 17.39 o 3 4 1 441.37 424.94 20.49 o 4 4 1 38.02 55.84 9.13 o 5 4 1 668.92 663.22 25.03 o 6 4 1 487.75 501.53 23.07 o 7 4 1 584.72 594.01 24.31 o 8 4 1 351.95 369.26 20.54 o 9 4 1 1412.88 1299.14 35.30 o 10 4 1 1175.30 1174.50 33.55 o 11 4 1 124.53 137.18 13.47 o 12 4 1 56.64 62.70 10.68 o 13 4 1 42.21 34.73 10.27 o 14 4 1 30.58 35.04 10.12 o 15 4 1 74.37 91.60 11.92 o 16 4 1 231.96 232.29 22.97 o 17 4 1 308.91 355.43 22.81 o 18 4 1 193.57 193.38 17.39 o 19 4 1 328.36 350.06 23.95 o 20 4 1 113.10 66.83 14.97 o 21 4 1 895.73 829.50 35.92 o 22 4 1 518.33 566.66 30.14 o 23 4 1 102.44 96.97 14.61 o 24 4 1 131.41 112.04 15.33 o 25 4 1 9.76 17.60 13.93 o -19 5 1 68.21 88.04 14.04 o -18 5 1 123.38 134.23 15.48 o -17 5 1 604.46 689.69 32.56 o -16 5 1 91.49 39.43 17.03 o -15 5 1 281.36 318.27 28.13 o -14 5 1 23.70 36.02 11.25 o -13 5 1 105.18 101.67 13.52 o -12 5 1 2.93 -2.99 11.61 o -11 5 1 211.71 204.01 20.54 o -10 5 1 71.58 73.75 11.87 o -9 5 1 41.71 48.98 10.73 o -8 5 1 43.64 28.75 14.14 o -7 5 1 78.79 85.57 12.28 o -6 5 1 195.65 197.97 19.56 o -5 5 1 594.31 577.65 27.71 o -4 5 1 1429.72 1316.17 39.12 o -3 5 1 276.90 252.98 22.76 o -2 5 1 108.47 104.66 12.90 o -1 5 1 1509.68 1507.84 40.62 o 0 5 1 62.00 79.38 8.49 o 1 5 1 1498.07 1499.12 41.03 o 2 5 1 100.01 99.35 12.54 o 3 5 1 279.84 310.22 21.11 o 4 5 1 1433.24 1430.07 39.89 o 5 5 1 598.42 607.38 27.46 o 6 5 1 193.45 175.83 17.19 o 7 5 1 74.64 8.98 13.73 o 8 5 1 39.54 56.67 11.10 o 9 5 1 40.03 65.85 11.66 o 10 5 1 74.55 64.61 12.44 o 11 5 1 227.11 222.33 23.22 o 12 5 1 3.08 23.69 12.33 o 13 5 1 100.30 94.91 12.75 o 14 5 1 20.93 0.77 13.21 o 15 5 1 283.67 286.01 26.89 o 16 5 1 90.94 91.60 13.57 o 17 5 1 598.18 544.00 30.14 o 18 5 1 120.11 136.04 16.46 o 19 5 1 68.41 54.03 13.68 o -9 6 1 49.33 25.24 15.12 o -8 6 1 37.68 15.28 16.10 o -7 6 1 153.87 137.18 15.79 o -6 6 1 83.97 104.35 14.14 o -5 6 1 109.96 95.48 14.55 o -4 6 1 49.05 60.90 12.95 o -3 6 1 95.68 103.11 14.55 o -2 6 1 283.13 265.47 26.53 o -1 6 1 322.65 344.74 29.26 o 0 6 1 188.35 217.03 19.51 o 1 6 1 319.81 356.15 24.72 o 2 6 1 285.34 265.47 24.10 o 3 6 1 96.69 110.96 14.55 o 4 6 1 49.34 32.51 15.12 o 5 6 1 110.56 94.65 14.04 o 6 6 1 82.04 74.57 13.62 o 7 6 1 155.23 153.17 16.46 o 8 6 1 38.13 26.32 15.95 o 9 6 1 48.99 55.27 13.06 o 0 0 2 54257.57 51525.51 87.55 o 1 0 2 1540.66 1421.24 20.64 o 2 0 2 2.00 4.72 5.05 o 3 0 2 193.51 139.77 6.98 o 4 0 2 402.73 368.03 16.59 o 5 0 2 0.10 15.34 8.85 o 6 0 2 4271.08 4097.89 24.76 o 7 0 2 3120.11 3229.72 23.12 o 8 0 2 1349.15 1432.09 16.59 o 9 0 2 70.71 83.38 5.96 o 10 0 2 604.14 602.78 12.30 o 11 0 2 28.49 34.56 13.78 o 12 0 2 419.45 335.03 10.74 o 13 0 2 64.35 51.02 67.68 o 14 0 2 860.85 884.60 338.14 o 15 0 2 3123.48 3068.43 537.63 o 16 0 2 855.25 831.53 2443.09 o 17 0 2 1826.89 1907.55 36.69 o 18 0 2 621.80 481.68 1082.13 o 19 0 2 460.53 445.22 263.69 o 20 0 2 85.00 45.49 156.04 o 21 0 2 79.72 52.91 43.20 o 22 0 2 62.47 62.98 15.95 o 23 0 2 70.89 55.46 23.43 o 24 0 2 287.08 244.76 64.28 o 25 0 2 745.73 796.54 43.82 o 26 0 2 267.02 247.58 56.54 o 27 0 2 154.94 147.10 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