#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:54 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180910 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/51/2105195.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105195_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; [Ni(MeCN)(H~2~O)~2~(NO~3~)~2~]·(15-crown-5)·MeCN: detailed study of a four-phase sequence that includes an intermediate modulated phase ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 389 _journal_page_last 400 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.410 _cell_angle_gamma 90.000 _cell_length_a 12.1700 _cell_length_b 12.2640 _cell_length_c 16.1960 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file hw5021221K_III_2sup25.hkl _cod_data_source_block 221K_III_2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k06110 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 293.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6158.45 5857.46 89.49 o 2 0 0 25277.74 25971.83 415.50 o 3 0 0 693.36 831.00 14.92 o 4 0 0 1348.29 1103.73 19.18 o 5 0 0 39683.43 43727.45 620.05 o 6 0 0 1678.64 2220.25 40.48 o 7 0 0 8233.78 8514.52 174.72 o 8 0 0 6729.61 6549.95 166.20 o 9 0 0 410.12 443.20 29.83 o 10 0 0 477.76 381.41 34.09 o 11 0 0 961.22 877.87 53.27 o 12 0 0 1265.07 1502.19 91.62 o 13 0 0 914.94 884.27 61.79 o 14 0 0 13.99 36.22 31.96 o 15 0 0 173.75 115.06 51.14 o 1 1 0 45837.95 47111.09 2403.50 o 2 1 0 1187.92 1301.95 16.57 o 3 1 0 9145.01 8582.37 101.63 o 4 1 0 17012.35 17641.67 194.14 o 5 1 0 1247.14 980.78 13.31 o 6 1 0 11701.02 12383.95 178.98 o 7 1 0 2509.10 2592.36 34.81 o 8 1 0 107.65 120.50 10.65 o 9 1 0 763.38 786.02 21.31 o 10 1 0 154.38 156.70 18.79 o 11 1 0 2339.86 2567.34 76.08 o 12 1 0 1047.01 1186.92 55.40 o 13 1 0 138.33 114.46 43.68 o 14 1 0 179.70 125.56 38.35 o 15 1 0 1.80 -13.44 31.21 o 0 2 0 12744.43 12044.95 228.17 o 1 2 0 1050.27 1137.31 15.77 o 2 2 0 3059.40 3339.88 43.62 o 3 2 0 9608.11 9032.45 104.64 o 4 2 0 611.83 804.37 12.05 o 5 2 0 18338.16 19621.84 212.61 o 6 2 0 34.04 24.95 3.55 o 7 2 0 4323.55 4806.31 65.02 o 8 2 0 3352.28 3670.29 51.59 o 9 2 0 865.53 934.38 26.08 o 10 2 0 2402.57 2735.45 64.49 o 11 2 0 4.30 8.52 12.05 o 12 2 0 658.66 748.50 41.55 o 13 2 0 305.69 332.20 33.78 o 14 2 0 9.60 14.67 26.33 o 15 2 0 312.23 337.20 55.63 o 1 3 0 4992.03 5375.16 65.42 o 2 3 0 5091.36 5561.30 69.31 o 3 3 0 8469.82 9001.62 108.85 o 4 3 0 17643.14 17669.70 194.29 o 5 3 0 1253.50 954.70 13.56 o 6 3 0 1000.71 982.84 18.11 o 7 3 0 863.53 942.61 17.89 o 8 3 0 1189.09 1289.05 23.97 o 9 3 0 3134.86 3355.58 67.12 o 10 3 0 523.12 485.99 24.50 o 11 3 0 1719.06 1980.12 75.64 o 12 3 0 53.18 68.58 20.30 o 13 3 0 1.91 -4.33 23.03 o 14 3 0 252.58 301.50 53.27 o 0 4 0 43897.15 45423.00 998.09 o 1 4 0 2150.70 2426.73 30.64 o 2 4 0 12777.63 13074.48 154.38 o 3 4 0 8489.52 8452.83 98.47 o 4 4 0 723.21 533.40 10.65 o 5 4 0 9584.23 10241.86 122.23 o 6 4 0 886.64 836.81 20.24 o 7 4 0 3355.78 3420.02 51.16 o 8 4 0 3043.59 3302.34 91.62 o 9 4 0 59.83 41.42 11.72 o 10 4 0 2207.10 2542.19 66.43 o 11 4 0 115.11 135.90 20.89 o 12 4 0 126.51 79.03 24.55 o 13 4 0 109.47 -8.57 49.01 o 14 4 0 4.98 -0.61 67.12 o 1 5 0 12268.90 12240.05 140.02 o 2 5 0 10700.42 12829.67 147.56 o 3 5 0 8444.66 8517.94 99.41 o 4 5 0 6970.36 7564.46 90.92 o 5 5 0 9.49 12.78 4.52 o 6 5 0 4002.86 4023.56 54.98 o 7 5 0 56.80 69.07 8.18 o 8 5 0 22.08 24.02 8.18 o 9 5 0 1303.91 1320.77 32.69 o 10 5 0 277.53 225.65 16.57 o 11 5 0 946.67 1198.65 45.12 o 12 5 0 32.02 -3.91 27.70 o 13 5 0 28.12 2.90 33.43 o 14 5 0 373.05 308.38 48.72 o 0 6 0 18636.53 19540.84 307.65 o 1 6 0 105.89 138.53 6.03 o 2 6 0 9848.88 10260.62 122.62 o 3 6 0 440.90 548.92 12.05 o 4 6 0 418.36 409.54 10.23 o 5 6 0 5093.56 5467.67 71.90 o 6 6 0 13.39 11.45 5.48 o 7 6 0 2195.59 2104.16 35.19 o 8 6 0 265.57 248.17 13.31 o 9 6 0 50.31 41.95 13.85 o 10 6 0 1456.61 1635.74 48.63 o 11 6 0 97.21 45.12 29.85 o 12 6 0 247.32 254.84 40.57 o 13 6 0 202.52 199.69 38.63 o 14 6 0 8.46 -12.21 39.21 o 1 7 0 2030.02 1980.70 29.12 o 2 7 0 462.39 581.20 18.11 o 3 7 0 1110.54 1160.46 20.30 o 4 7 0 1353.24 1352.33 23.32 o 5 7 0 7.63 -3.04 3.96 o 6 7 0 2731.18 2803.73 83.10 o 7 7 0 411.05 499.34 13.79 o 8 7 0 47.13 23.11 9.71 o 9 7 0 394.00 323.65 51.14 o 10 7 0 52.45 13.36 18.90 o 11 7 0 669.56 665.09 48.34 o 12 7 0 133.34 104.24 37.17 o 13 7 0 4.12 36.22 42.62 o 0 8 0 2973.30 3273.97 68.96 o 1 8 0 439.48 346.70 11.22 o 2 8 0 16.75 23.74 9.59 o 3 8 0 1024.05 922.86 21.09 o 4 8 0 85.69 74.26 8.67 o 5 8 0 4250.91 4692.67 90.56 o 6 8 0 539.43 591.18 60.73 o 7 8 0 210.05 210.08 16.37 o 8 8 0 307.82 264.19 28.77 o 9 8 0 10.55 -14.25 14.25 o 10 8 0 522.51 563.12 30.68 o 11 8 0 40.56 51.14 30.90 o 12 8 0 23.10 0.37 35.08 o 13 8 0 84.05 67.41 45.48 o 1 9 0 885.26 772.41 19.41 o 2 9 0 1304.40 1275.69 40.48 o 3 9 0 60.21 72.93 11.72 o 4 9 0 221.19 157.51 17.05 o 5 9 0 202.02 253.36 17.28 o 6 9 0 518.19 591.52 25.61 o 7 9 0 941.77 956.14 33.11 o 8 9 0 109.69 106.69 37.29 o 9 9 0 154.96 173.49 23.03 o 10 9 0 13.96 -2.35 24.50 o 11 9 0 70.67 157.63 32.23 o 12 9 0 76.21 82.47 67.12 o 0 10 0 6660.78 6884.15 206.95 o 1 10 0 34.05 46.61 9.71 o 2 10 0 110.24 88.54 10.55 o 3 10 0 464.85 652.14 24.83 o 4 10 0 1.82 16.44 9.31 o 5 10 0 234.07 233.42 17.28 o 6 10 0 59.26 69.82 17.05 o 7 10 0 46.53 21.31 15.07 o 8 10 0 208.05 158.29 21.81 o 9 10 0 0.46 -4.69 17.73 o 10 10 0 54.34 34.62 23.55 o 11 10 0 30.74 53.18 46.88 o 1 11 0 510.62 509.30 89.49 o 2 11 0 24.06 30.23 11.77 o 3 11 0 2.38 -1.01 14.25 o 4 11 0 128.69 60.76 21.31 o 5 11 0 26.55 23.44 15.77 o 6 11 0 293.85 293.43 25.48 o 7 11 0 147.11 131.69 21.09 o 8 11 0 3.07 1.69 20.89 o 9 11 0 18.60 7.35 23.32 o 10 11 0 0.09 -5.39 25.48 o 11 11 0 49.43 -9.26 40.48 o 0 12 0 39.45 39.06 22.45 o 1 12 0 7.74 24.61 20.24 o 2 12 0 7.80 11.77 16.13 o 3 12 0 524.86 459.67 27.84 o 4 12 0 11.00 19.62 17.89 o 5 12 0 608.93 718.98 72.45 o 6 12 0 0.72 12.61 24.36 o 7 12 0 1.61 20.73 22.20 o 8 12 0 2.55 12.17 39.42 o 9 12 0 1.51 2.28 32.16 o 10 12 0 51.81 -8.20 38.83 o 1 13 0 2.39 3.03 18.90 o 2 13 0 164.63 109.34 30.86 o 3 13 0 41.22 21.31 19.59 o 4 13 0 258.93 167.26 30.08 o 5 13 0 2.28 12.95 22.37 o 6 13 0 29.38 59.97 26.08 o 7 13 0 8.03 14.14 25.12 o 8 13 0 0.87 -20.74 41.55 o 0 14 0 9.78 10.65 55.40 o 1 14 0 1.44 -19.18 49.01 o 2 14 0 1.14 112.93 49.01 o 3 14 0 2.83 -21.31 31.96 o 4 14 0 23.54 21.31 31.96 o 5 14 0 3.91 49.01 36.22 o 6 14 0 0.05 8.52 36.22 o 7 14 0 6.39 42.62 34.09 o 1 15 0 1.24 -31.96 46.88 o 2 15 0 0.02 29.83 55.40 o 3 15 0 0.40 21.31 44.75 o 4 15 0 5.42 -27.70 51.14 o 5 15 0 0.22 21.31 42.62 o -15 1 1 0.01 2.81 31.29 o -14 1 1 29.88 15.58 26.08 o -13 1 1 0.78 2.40 17.89 o -12 1 1 29.17 -7.20 17.05 o -11 1 1 73.74 46.69 17.28 o -10 1 1 13.01 0.90 23.44 o -9 1 1 789.90 834.66 27.84 o -8 1 1 224.12 182.83 24.50 o -7 1 1 978.57 999.31 19.41 o -6 1 1 4.29 2.56 3.55 o -5 1 1 700.95 702.13 12.05 o -4 1 1 54.98 46.97 3.01 o -3 1 1 10.60 19.68 5.33 o -2 1 1 4.81 4.26 2.13 o -1 1 1 9.61 9.06 2.13 o 0 1 1 18.37 19.41 2.13 o 1 1 1 2.46 3.20 1.51 o 2 1 1 85.83 88.54 3.20 o 3 1 1 168.30 138.53 4.52 o 4 1 1 564.85 581.71 17.05 o 5 1 1 86.98 80.97 4.52 o 6 1 1 1574.47 1611.71 21.81 o 7 1 1 89.75 82.85 6.66 o 8 1 1 365.66 343.14 11.22 o 9 1 1 1.10 -0.27 5.48 o 10 1 1 2.53 -9.31 9.31 o 11 1 1 20.26 11.86 27.70 o 12 1 1 10.37 27.46 20.30 o 13 1 1 29.08 27.38 24.02 o 14 1 1 0.44 -27.12 27.12 o -15 2 1 23.59 46.33 33.89 o -14 2 1 0.42 -0.17 28.15 o -13 2 1 35.05 23.44 21.09 o -12 2 1 12.35 14.18 18.90 o -11 2 1 70.86 54.33 15.07 o -10 2 1 328.00 354.03 17.05 o -9 2 1 26.44 7.55 19.18 o -8 2 1 421.59 461.43 15.07 o -7 2 1 0.79 7.46 4.52 o -6 2 1 1114.32 950.02 15.77 o -5 2 1 51.50 57.61 3.01 o -4 2 1 193.65 191.19 9.59 o -3 2 1 200.44 183.64 8.52 o -2 2 1 14.19 21.31 1.51 o -1 2 1 531.18 433.78 6.66 o 0 2 1 204.66 184.37 3.20 o 1 2 1 786.99 762.96 10.65 o 2 2 1 230.85 260.86 18.11 o 3 2 1 137.74 111.65 3.55 o 4 2 1 293.49 306.08 9.59 o 5 2 1 36.53 23.63 4.52 o 6 2 1 158.81 118.50 6.66 o 7 2 1 578.17 545.00 13.31 o 8 2 1 7.56 -1.52 5.11 o 9 2 1 30.39 21.31 5.48 o 10 2 1 3.64 10.79 11.77 o 11 2 1 3.65 -15.98 15.98 o 12 2 1 133.53 121.35 23.32 o 13 2 1 1.07 29.83 21.09 o 14 2 1 18.99 67.12 52.20 o -15 3 1 12.43 1.02 61.79 o -14 3 1 61.95 48.06 33.21 o -13 3 1 1.07 -12.14 24.83 o -12 3 1 3.11 17.52 19.31 o -11 3 1 9.72 7.81 15.98 o -10 3 1 74.22 39.70 13.85 o -9 3 1 107.41 70.47 20.24 o -8 3 1 74.09 66.72 7.09 o -7 3 1 853.93 837.09 16.37 o -6 3 1 193.96 192.36 10.65 o -5 3 1 726.64 688.83 11.22 o -4 3 1 1118.49 1126.14 30.90 o -3 3 1 7.00 9.18 3.20 o -2 3 1 3805.56 3659.99 46.63 o -1 3 1 168.31 242.22 9.59 o 0 3 1 1536.17 1354.39 18.79 o 1 3 1 2188.34 2079.26 26.33 o 2 3 1 44.10 40.60 3.01 o 3 3 1 808.65 698.89 11.22 o 4 3 1 550.57 542.38 9.04 o 5 3 1 1.62 -1.28 3.55 o 6 3 1 81.83 77.32 12.78 o 7 3 1 34.79 27.70 6.66 o 8 3 1 81.27 65.96 9.59 o 9 3 1 4.09 -2.56 7.09 o 10 3 1 8.31 3.10 7.40 o 11 3 1 61.09 74.44 20.24 o 12 3 1 18.73 1.07 18.11 o 13 3 1 19.28 41.55 27.12 o 14 3 1 4.35 -32.97 44.75 o -14 4 1 11.24 7.10 33.86 o -13 4 1 107.30 66.05 34.30 o -12 4 1 0.07 0.00 22.37 o -11 4 1 36.21 32.27 15.34 o -10 4 1 6.38 5.33 13.85 o -9 4 1 96.60 112.57 14.92 o -8 4 1 14.87 -1.18 8.52 o -7 4 1 648.01 642.75 29.83 o -6 4 1 1698.17 1560.85 23.32 o -5 4 1 1090.01 1130.39 16.57 o -4 4 1 1049.08 1122.66 17.05 o -3 4 1 134.12 128.48 5.33 o -2 4 1 115.52 104.67 9.59 o -1 4 1 1476.73 1229.98 17.28 o 0 4 1 1022.43 923.74 13.56 o 1 4 1 511.50 472.13 8.18 o 2 4 1 54.52 67.54 5.33 o 3 4 1 49.03 48.16 4.52 o 4 4 1 490.23 452.21 14.92 o 5 4 1 954.61 892.57 14.25 o 6 4 1 193.65 149.38 7.09 o 7 4 1 557.45 588.60 24.50 o 8 4 1 105.26 112.28 10.23 o 9 4 1 59.56 34.76 9.71 o 10 4 1 18.37 32.87 10.23 o 11 4 1 33.17 32.30 18.43 o 12 4 1 155.22 171.04 37.29 o 13 4 1 0.50 11.12 28.71 o 14 4 1 32.01 74.65 38.35 o -14 5 1 145.03 141.56 45.12 o -13 5 1 6.68 27.70 34.30 o -12 5 1 165.13 181.33 40.48 o -11 5 1 47.82 52.20 19.59 o -10 5 1 531.74 559.91 23.32 o -9 5 1 479.05 418.00 15.77 o -8 5 1 38.20 36.30 7.09 o -7 5 1 612.41 572.46 14.25 o -6 5 1 905.53 873.30 22.37 o -5 5 1 186.25 187.88 10.65 o -4 5 1 760.40 771.34 13.56 o -3 5 1 20.04 14.92 4.52 o -2 5 1 3486.98 3341.22 38.40 o -1 5 1 2111.88 2060.63 24.83 o 0 5 1 864.55 947.74 18.11 o 1 5 1 2840.78 2636.20 32.16 o 2 5 1 99.14 95.41 7.46 o 3 5 1 2022.25 1927.60 26.33 o 4 5 1 1065.18 1002.01 23.44 o 5 5 1 703.10 653.05 14.25 o 6 5 1 1447.22 1465.97 24.11 o 7 5 1 144.53 108.79 10.65 o 8 5 1 555.01 557.42 18.79 o 9 5 1 105.95 120.52 24.50 o 10 5 1 98.37 104.67 15.07 o 11 5 1 257.97 234.72 23.32 o 12 5 1 1.03 -10.26 26.77 o 13 5 1 37.70 32.08 33.06 o 14 5 1 0.10 -30.94 50.07 o -14 6 1 18.73 56.47 37.80 o -13 6 1 200.16 150.73 90.56 o -12 6 1 99.87 99.08 27.41 o -11 6 1 411.08 335.88 33.50 o -10 6 1 1146.99 1027.28 43.21 o -9 6 1 400.94 385.47 27.70 o -8 6 1 496.50 447.82 15.07 o -7 6 1 93.53 66.50 8.18 o -6 6 1 302.36 273.60 7.62 o -5 6 1 1365.48 1314.30 23.97 o -4 6 1 57.68 53.27 6.03 o -3 6 1 2466.41 2503.73 30.13 o -2 6 1 628.15 621.64 11.22 o -1 6 1 1737.29 1762.53 23.32 o 0 6 1 2392.48 2241.22 27.60 o 1 6 1 430.20 469.08 9.71 o 2 6 1 5388.25 5588.44 64.02 o 3 6 1 59.65 50.28 5.11 o 4 6 1 3758.35 3868.17 121.45 o 5 6 1 131.47 108.67 8.18 o 6 6 1 157.42 156.16 9.59 o 7 6 1 1420.24 1438.81 31.21 o 8 6 1 263.06 239.58 18.11 o 9 6 1 655.72 694.65 25.61 o 10 6 1 255.15 228.11 20.24 o 11 6 1 239.04 288.62 44.75 o 12 6 1 188.61 129.30 37.17 o 13 6 1 4.29 49.14 35.32 o -13 7 1 0.79 18.23 33.28 o -12 7 1 120.22 115.60 36.22 o -11 7 1 240.29 220.98 34.52 o -10 7 1 338.89 322.05 30.29 o -9 7 1 1443.12 1431.87 50.00 o -8 7 1 283.08 242.59 15.34 o -7 7 1 1447.98 1573.96 38.40 o -6 7 1 127.09 134.57 11.22 o -5 7 1 370.46 393.78 14.84 o -4 7 1 2892.36 3017.35 46.42 o -3 7 1 0.32 3.04 6.39 o -2 7 1 4660.61 4811.64 62.44 o -1 7 1 280.09 359.20 9.71 o 0 7 1 1194.53 1313.69 20.46 o 1 7 1 3922.81 3940.92 54.24 o 2 7 1 1.19 7.46 6.03 o 3 7 1 3515.46 3630.81 51.96 o 4 7 1 634.60 562.69 14.84 o 5 7 1 199.90 236.96 24.50 o 6 7 1 585.32 609.48 16.37 o 7 7 1 20.01 31.47 9.71 o 8 7 1 944.26 958.21 29.12 o 9 7 1 396.93 334.21 21.81 o 10 7 1 159.60 178.87 25.57 o 11 7 1 152.65 201.41 32.69 o 12 7 1 6.71 23.91 44.75 o 13 7 1 37.96 15.26 37.29 o -13 8 1 152.94 128.79 36.07 o -12 8 1 10.76 45.15 27.12 o -11 8 1 45.80 45.52 24.55 o -10 8 1 218.49 242.02 26.99 o -9 8 1 1.78 9.38 14.84 o -8 8 1 375.13 506.94 50.07 o -7 8 1 7.23 -6.39 11.77 o -6 8 1 947.60 1021.98 26.62 o -5 8 1 1711.33 1739.37 44.75 o -4 8 1 502.50 527.10 16.37 o -3 8 1 2100.22 2257.82 41.41 o -2 8 1 5.09 -2.13 6.03 o -1 8 1 1298.94 1306.84 23.03 o 0 8 1 370.54 395.51 20.24 o 1 8 1 466.66 482.57 14.92 o 2 8 1 1773.36 1834.02 33.04 o 3 8 1 84.82 83.72 14.92 o 4 8 1 840.48 846.88 31.96 o 5 8 1 131.73 141.90 10.55 o 6 8 1 42.73 42.90 7.46 o 7 8 1 191.43 170.15 13.31 o 8 8 1 2.13 -12.28 12.74 o 9 8 1 233.40 195.97 25.57 o 10 8 1 103.50 85.00 24.50 o 11 8 1 33.28 34.09 28.63 o 12 8 1 80.63 65.01 34.11 o -12 9 1 94.42 144.20 38.40 o -11 9 1 34.81 47.46 32.74 o -10 9 1 86.61 57.74 22.37 o -9 9 1 327.74 396.32 26.08 o -8 9 1 24.28 12.67 18.11 o -7 9 1 538.11 590.22 26.99 o -6 9 1 550.60 575.92 26.33 o -5 9 1 55.89 46.46 10.55 o -4 9 1 1078.17 1299.19 42.62 o -3 9 1 52.54 44.38 8.18 o -2 9 1 2187.74 2365.32 45.55 o -1 9 1 213.67 214.87 33.03 o 0 9 1 369.24 359.98 34.09 o 1 9 1 694.96 714.97 17.89 o 2 9 1 16.90 17.05 9.04 o 3 9 1 638.03 663.60 35.16 o 4 9 1 141.89 152.84 11.22 o 5 9 1 269.07 301.15 19.18 o 6 9 1 220.05 240.24 24.50 o 7 9 1 0.46 -5.33 12.05 o 8 9 1 86.03 98.20 16.57 o 9 9 1 159.49 143.60 22.45 o 10 9 1 79.33 99.97 25.48 o 11 9 1 129.44 150.34 37.87 o 12 9 1 0.04 65.33 39.40 o -12 10 1 28.91 -5.00 36.89 o -11 10 1 121.88 47.90 42.62 o -10 10 1 171.00 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