#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:54 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180910 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/51/2105196.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105196_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; [Ni(MeCN)(H~2~O)~2~(NO~3~)~2~]·(15-crown-5)·MeCN: detailed study of a four-phase sequence that includes an intermediate modulated phase ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 389 _journal_page_last 400 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.410 _cell_angle_gamma 90.000 _cell_length_a 12.1680 _cell_length_b 12.2700 _cell_length_c 16.2040 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file hw5021224K_III_2sup26.hkl _cod_data_source_block 224K_III_2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k06111 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 293.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6202.64 5897.66 90.83 o 2 0 0 25369.71 26237.76 423.89 o 3 0 0 670.45 847.77 15.14 o 4 0 0 1382.70 1064.04 19.46 o 5 0 0 39023.81 43150.00 605.55 o 6 0 0 1697.92 2428.70 43.25 o 7 0 0 8147.66 8397.73 170.85 o 8 0 0 6800.34 6617.83 170.85 o 9 0 0 377.45 343.87 28.11 o 10 0 0 463.42 400.10 30.28 o 11 0 0 980.85 979.70 51.90 o 12 0 0 1193.34 1425.21 80.02 o 13 0 0 930.44 878.05 60.56 o 14 0 0 12.97 25.95 30.28 o 15 0 0 192.30 114.62 62.72 o 1 1 0 45873.63 47337.68 1639.51 o 2 1 0 1254.35 1351.71 16.82 o 3 1 0 9058.90 8402.21 98.56 o 4 1 0 16962.18 17918.54 197.99 o 5 1 0 1161.05 857.77 11.95 o 6 1 0 11408.42 12176.66 148.14 o 7 1 0 2590.77 2649.64 48.66 o 8 1 0 105.37 139.27 10.80 o 9 1 0 758.73 730.16 40.01 o 10 1 0 133.89 137.11 16.82 o 11 1 0 2210.38 2458.44 77.27 o 12 1 0 1040.64 1126.62 45.80 o 13 1 0 129.96 131.29 41.09 o 14 1 0 176.08 151.39 30.47 o 15 1 0 0.61 38.57 52.99 o 0 2 0 12758.51 12125.14 227.47 o 1 2 0 1038.53 1170.44 16.00 o 2 2 0 3151.71 3369.58 44.27 o 3 2 0 9913.77 9061.09 105.49 o 4 2 0 600.67 815.34 12.23 o 5 2 0 18403.57 19568.61 214.93 o 6 2 0 26.30 19.46 3.60 o 7 2 0 4159.80 4607.42 62.35 o 8 2 0 3365.83 3545.24 49.19 o 9 2 0 815.63 917.59 32.44 o 10 2 0 2357.58 2643.70 62.20 o 11 2 0 7.63 1.53 12.93 o 12 2 0 614.79 634.44 34.38 o 13 2 0 290.10 296.66 30.47 o 14 2 0 6.42 6.92 22.79 o 15 2 0 288.49 251.17 170.85 o 1 3 0 5094.04 5471.74 66.51 o 2 3 0 5027.94 5606.13 71.10 o 3 3 0 8433.67 9088.11 107.41 o 4 3 0 17574.69 17698.36 195.46 o 5 3 0 1221.81 876.54 15.14 o 6 3 0 972.35 993.68 18.38 o 7 3 0 889.04 959.56 49.74 o 8 3 0 1139.57 1247.88 24.38 o 9 3 0 3039.66 3297.98 54.38 o 10 3 0 504.84 477.95 22.13 o 11 3 0 1672.27 1987.42 63.45 o 12 3 0 58.04 55.91 20.60 o 13 3 0 0.90 6.78 28.11 o 14 3 0 230.32 187.03 49.20 o 0 4 0 44501.69 45147.06 992.32 o 1 4 0 2061.34 2432.73 29.56 o 2 4 0 12674.88 13107.23 151.69 o 3 4 0 8458.11 8293.70 95.50 o 4 4 0 685.48 461.94 9.73 o 5 4 0 9526.92 10181.07 124.07 o 6 4 0 894.56 846.06 19.46 o 7 4 0 3308.45 3362.87 51.08 o 8 4 0 3060.12 3273.14 59.47 o 9 4 0 55.10 47.07 9.45 o 10 4 0 2170.29 2521.58 65.54 o 11 4 0 119.96 141.27 19.60 o 12 4 0 125.84 48.92 21.82 o 13 4 0 117.81 57.33 29.37 o 14 4 0 4.61 22.82 33.70 o 1 5 0 12432.53 12152.62 137.61 o 2 5 0 10644.57 13149.42 168.69 o 3 5 0 8211.56 8457.96 96.31 o 4 5 0 7053.61 7500.01 90.90 o 5 5 0 4.52 8.65 4.59 o 6 5 0 3995.04 4017.22 53.52 o 7 5 0 65.37 83.66 8.65 o 8 5 0 14.58 4.72 8.31 o 9 5 0 1271.27 1318.86 32.72 o 10 5 0 291.27 241.69 19.07 o 11 5 0 955.28 1177.50 69.21 o 12 5 0 40.25 -6.85 25.54 o 13 5 0 27.01 -9.40 57.31 o 14 5 0 351.91 356.75 70.29 o 0 6 0 18998.48 19746.22 313.32 o 1 6 0 116.17 175.23 6.76 o 2 6 0 9674.53 10106.73 122.53 o 3 6 0 506.56 612.04 12.93 o 4 6 0 404.67 409.45 9.85 o 5 6 0 5242.54 5440.65 72.34 o 6 6 0 12.30 6.22 5.56 o 7 6 0 2123.87 1989.64 35.07 o 8 6 0 287.25 232.38 13.99 o 9 6 0 63.38 53.22 11.95 o 10 6 0 1444.40 1659.39 54.07 o 11 6 0 104.25 53.67 38.93 o 12 6 0 241.65 172.94 61.64 o 13 6 0 202.53 176.77 41.20 o 14 6 0 7.38 9.52 42.17 o 1 7 0 2008.33 2018.46 30.47 o 2 7 0 444.01 591.83 14.06 o 3 7 0 1174.12 1170.91 32.44 o 4 7 0 1388.21 1370.09 24.47 o 5 7 0 10.57 6.18 4.02 o 6 7 0 2731.49 2839.09 75.69 o 7 7 0 403.60 507.14 18.38 o 8 7 0 50.48 32.44 9.18 o 9 7 0 403.00 290.25 44.34 o 10 7 0 58.24 39.79 17.99 o 11 7 0 669.30 612.30 50.01 o 12 7 0 137.90 129.61 39.75 o 13 7 0 5.96 -0.08 35.68 o 0 8 0 3002.35 3279.16 68.80 o 1 8 0 466.26 350.59 11.39 o 2 8 0 13.51 29.04 6.49 o 3 8 0 988.65 897.71 22.13 o 4 8 0 70.34 73.53 8.80 o 5 8 0 4242.67 4685.67 86.26 o 6 8 0 537.24 590.83 24.87 o 7 8 0 238.07 197.80 43.25 o 8 8 0 321.36 286.06 21.63 o 9 8 0 14.78 23.20 16.61 o 10 8 0 497.48 507.96 31.10 o 11 8 0 38.11 55.15 21.25 o 12 8 0 19.22 -19.13 72.45 o 13 8 0 88.24 55.46 44.08 o 1 9 0 871.41 771.26 19.70 o 2 9 0 1334.63 1250.27 29.79 o 3 9 0 46.78 64.46 9.85 o 4 9 0 230.51 165.64 11.13 o 5 9 0 161.12 182.34 15.14 o 6 9 0 521.98 609.81 26.00 o 7 9 0 876.87 941.61 33.64 o 8 9 0 105.30 69.61 15.57 o 9 9 0 141.97 109.45 21.82 o 10 9 0 10.55 -0.67 24.87 o 11 9 0 65.08 100.35 29.57 o 12 9 0 81.34 106.17 99.48 o 0 10 0 6705.52 7077.71 200.58 o 1 10 0 16.32 41.24 10.70 o 2 10 0 122.50 67.76 10.80 o 3 10 0 418.60 609.88 21.82 o 4 10 0 2.87 15.47 7.91 o 5 10 0 236.20 211.21 33.52 o 6 10 0 63.25 83.03 28.11 o 7 10 0 49.91 18.33 14.47 o 8 10 0 225.99 184.23 34.60 o 9 10 0 0.00 -4.16 19.18 o 10 10 0 50.93 63.95 25.95 o 11 10 0 30.07 15.14 47.58 o 1 11 0 532.78 544.18 26.00 o 2 11 0 20.03 3.11 11.95 o 3 11 0 0.20 15.48 14.47 o 4 11 0 131.47 47.40 30.28 o 5 11 0 19.12 11.89 16.82 o 6 11 0 302.74 240.19 23.67 o 7 11 0 151.13 125.78 22.13 o 8 11 0 4.49 -15.21 40.01 o 9 11 0 26.33 -11.63 22.13 o 10 11 0 0.32 20.70 25.95 o 11 11 0 58.65 -30.73 36.32 o 0 12 0 47.86 47.58 24.47 o 1 12 0 4.70 16.65 15.14 o 2 12 0 9.62 -12.62 23.79 o 3 12 0 525.65 474.73 29.06 o 4 12 0 5.91 39.53 19.07 o 5 12 0 631.87 715.98 45.03 o 6 12 0 0.92 -7.15 24.87 o 7 12 0 4.44 4.39 24.20 o 8 12 0 5.89 31.07 27.17 o 9 12 0 0.60 -22.28 32.64 o 10 12 0 59.36 29.39 78.94 o 1 13 0 0.89 2.03 24.38 o 2 13 0 167.27 99.53 36.77 o 3 13 0 42.13 1.03 23.79 o 4 13 0 282.17 235.02 32.24 o 5 13 0 2.15 -0.97 28.11 o 6 13 0 20.61 51.54 30.00 o 7 13 0 7.90 15.69 26.42 o 8 13 0 0.96 -23.79 29.47 o 0 14 0 21.98 8.65 54.07 o 1 14 0 0.75 82.18 51.90 o 2 14 0 1.98 -28.11 54.07 o 3 14 0 1.11 -2.16 32.44 o 4 14 0 19.65 -10.81 36.77 o 5 14 0 2.59 2.16 38.93 o 6 14 0 0.14 21.63 34.60 o 7 14 0 5.29 2.16 30.28 o 1 15 0 0.01 2.16 49.74 o 2 15 0 0.01 69.21 54.07 o 3 15 0 0.26 60.56 54.07 o 4 15 0 3.93 38.93 62.72 o 5 15 0 0.14 -8.65 43.25 o -15 1 1 0.05 65.54 38.93 o -14 1 1 24.87 43.89 25.95 o -13 1 1 0.61 -20.60 20.60 o -12 1 1 30.80 0.00 15.29 o -11 1 1 67.84 79.31 17.54 o -10 1 1 17.52 21.63 13.76 o -9 1 1 749.03 768.30 51.90 o -8 1 1 180.43 182.79 9.67 o -7 1 1 933.21 957.68 19.70 o -6 1 1 5.66 1.08 3.06 o -5 1 1 640.72 645.58 10.70 o -4 1 1 56.27 46.78 2.16 o -3 1 1 13.45 17.57 2.16 o -2 1 1 5.95 5.41 1.53 o -1 1 1 7.78 6.49 1.53 o 0 1 1 19.27 22.76 1.53 o 1 1 1 2.76 4.33 1.53 o 2 1 1 83.42 82.24 3.06 o 3 1 1 149.20 133.08 4.59 o 4 1 1 537.12 552.74 9.73 o 5 1 1 80.59 81.18 5.19 o 6 1 1 1493.75 1498.13 21.25 o 7 1 1 80.60 68.65 5.56 o 8 1 1 345.16 332.46 10.38 o 9 1 1 0.44 2.43 5.56 o 10 1 1 2.42 4.33 9.45 o 11 1 1 19.41 33.23 16.61 o 12 1 1 11.22 -4.99 19.18 o 13 1 1 28.53 13.18 24.33 o 14 1 1 0.40 -6.60 27.52 o -15 2 1 21.22 53.04 60.56 o -14 2 1 1.15 11.58 25.86 o -13 2 1 35.66 41.09 22.79 o -12 2 1 11.64 11.16 18.71 o -11 2 1 70.61 29.37 14.47 o -10 2 1 287.86 315.36 37.85 o -9 2 1 18.82 6.49 7.65 o -8 2 1 398.61 428.22 13.76 o -7 2 1 1.56 14.13 15.14 o -6 2 1 1050.49 864.07 14.47 o -5 2 1 43.45 48.88 3.24 o -4 2 1 191.77 183.93 4.59 o -3 2 1 176.55 170.19 3.60 o -2 2 1 13.45 19.70 2.16 o -1 2 1 490.69 396.93 6.12 o 0 2 1 192.68 172.00 3.24 o 1 2 1 760.17 704.71 9.85 o 2 2 1 225.04 242.76 5.41 o 3 2 1 129.44 100.58 4.59 o 4 2 1 283.24 289.41 7.57 o 5 2 1 48.35 31.14 6.49 o 6 2 1 155.13 126.53 6.12 o 7 2 1 525.17 531.54 13.51 o 8 2 1 6.33 2.78 5.19 o 9 2 1 29.67 19.35 5.56 o 10 2 1 2.20 -6.06 10.80 o 11 2 1 1.49 5.54 23.79 o 12 2 1 119.86 71.65 23.67 o 13 2 1 1.18 -22.71 22.71 o 14 2 1 20.04 14.06 33.64 o -15 3 1 12.66 -20.63 41.44 o -14 3 1 57.38 85.89 36.55 o -13 3 1 1.43 9.73 24.47 o -12 3 1 3.37 -17.99 17.99 o -11 3 1 9.29 8.14 12.40 o -10 3 1 67.96 38.35 11.39 o -9 3 1 99.85 87.51 18.38 o -8 3 1 70.28 54.08 6.76 o -7 3 1 795.41 724.53 19.46 o -6 3 1 185.35 165.51 6.12 o -5 3 1 688.15 620.72 10.70 o -4 3 1 1018.09 1062.01 23.79 o -3 3 1 3.06 5.05 2.16 o -2 3 1 3507.96 3433.20 44.27 o -1 3 1 162.59 231.59 6.49 o 0 3 1 1504.80 1245.80 21.63 o 1 3 1 2095.42 1988.43 27.03 o 2 3 1 35.78 30.90 4.33 o 3 3 1 753.50 686.66 10.70 o 4 3 1 541.09 511.53 9.18 o 5 3 1 2.01 1.73 3.60 o 6 3 1 83.11 90.00 6.76 o 7 3 1 34.37 39.52 6.76 o 8 3 1 77.40 58.98 8.31 o 9 3 1 3.33 -2.60 7.20 o 10 3 1 9.54 -1.16 9.17 o 11 3 1 56.97 36.77 16.00 o 12 3 1 16.68 18.38 24.87 o 13 3 1 18.27 44.53 25.86 o 14 3 1 4.46 3.60 36.75 o -14 4 1 9.64 15.73 36.35 o -13 4 1 90.72 43.83 37.97 o -12 4 1 0.43 14.88 25.86 o -11 4 1 28.43 -4.76 17.30 o -10 4 1 6.05 -11.39 11.39 o -9 4 1 90.78 95.01 10.38 o -8 4 1 14.41 4.57 6.76 o -7 4 1 589.69 599.10 13.76 o -6 4 1 1623.66 1469.99 44.34 o -5 4 1 980.01 1044.66 25.95 o -4 4 1 999.01 1059.41 16.00 o -3 4 1 121.72 115.79 4.59 o -2 4 1 111.14 100.67 3.24 o -1 4 1 1369.32 1150.02 16.00 o 0 4 1 961.34 840.87 12.93 o 1 4 1 475.66 462.44 8.31 o 2 4 1 49.27 55.52 5.41 o 3 4 1 52.30 53.54 5.19 o 4 4 1 448.24 424.06 9.18 o 5 4 1 905.49 834.11 12.93 o 6 4 1 171.36 141.48 8.31 o 7 4 1 500.62 523.57 14.06 o 8 4 1 92.62 104.08 10.38 o 9 4 1 69.60 59.00 28.11 o 10 4 1 15.70 13.84 10.80 o 11 4 1 35.69 23.00 16.61 o 12 4 1 136.70 121.39 23.37 o 13 4 1 0.10 26.70 30.53 o 14 4 1 27.72 9.79 38.88 o -14 5 1 124.45 108.83 49.67 o -13 5 1 5.06 -44.49 45.42 o -12 5 1 148.05 69.56 26.80 o -11 5 1 39.15 48.46 20.60 o -10 5 1 490.18 443.05 22.13 o -9 5 1 441.85 380.38 15.14 o -8 5 1 39.92 32.17 6.76 o -7 5 1 576.36 521.33 12.93 o -6 5 1 808.76 789.44 20.55 o -5 5 1 180.57 184.70 7.57 o -4 5 1 682.37 711.69 13.76 o -3 5 1 15.32 10.81 4.59 o -2 5 1 3253.04 3112.85 40.01 o -1 5 1 1932.23 1879.77 23.67 o 0 5 1 803.20 896.56 12.93 o 1 5 1 2624.16 2433.92 30.13 o 2 5 1 94.83 84.40 4.59 o 3 5 1 1882.16 1795.51 23.67 o 4 5 1 972.43 916.99 15.29 o 5 5 1 654.73 640.62 17.30 o 6 5 1 1344.48 1362.21 22.13 o 7 5 1 119.90 93.74 8.80 o 8 5 1 519.48 511.95 18.71 o 9 5 1 92.99 84.34 16.22 o 10 5 1 90.62 101.65 15.06 o 11 5 1 233.70 267.16 24.92 o 12 5 1 0.80 -25.54 25.54 o 13 5 1 37.53 11.20 35.18 o 14 5 1 0.18 -26.30 42.17 o -14 6 1 19.31 87.78 40.60 o -13 6 1 178.91 128.18 70.29 o -12 6 1 81.79 65.31 46.50 o -11 6 1 385.16 401.85 35.20 o -10 6 1 1026.38 973.20 47.96 o -9 6 1 364.00 348.20 19.46 o -8 6 1 451.66 415.00 12.98 o -7 6 1 86.21 70.15 11.89 o -6 6 1 296.49 259.81 10.81 o -5 6 1 1228.29 1211.29 23.67 o -4 6 1 50.21 52.69 9.73 o -3 6 1 2306.54 2343.33 29.79 o -2 6 1 562.89 584.21 12.98 o -1 6 1 1629.80 1655.04 22.79 o 0 6 1 2216.51 2087.46 25.86 o 1 6 1 408.28 450.99 10.70 o 2 6 1 5015.41 5228.38 59.64 o 3 6 1 53.88 47.68 6.12 o 4 6 1 3565.51 3667.58 51.93 o 5 6 1 123.35 103.30 12.98 o 6 6 1 149.98 163.64 8.80 o 7 6 1 1309.92 1346.24 28.58 o 8 6 1 244.09 252.64 15.06 o 9 6 1 587.19 631.96 23.67 o 10 6 1 229.76 189.83 18.71 o 11 6 1 192.30 210.50 31.10 o 12 6 1 176.29 91.34 63.80 o 13 6 1 2.78 15.89 37.60 o -13 7 1 1.61 39.02 32.75 o -12 7 1 114.87 80.88 32.39 o -11 7 1 222.01 200.35 41.09 o -10 7 1 327.96 294.18 31.62 o -9 7 1 1349.09 1377.23 50.75 o -8 7 1 266.67 252.31 16.00 o -7 7 1 1326.65 1456.24 36.33 o -6 7 1 100.20 97.51 10.70 o -5 7 1 331.90 358.63 18.38 o -4 7 1 2714.45 2762.85 44.63 o -3 7 1 0.75 7.93 3.87 o -2 7 1 4410.77 4517.31 59.47 o -1 7 1 246.26 334.59 16.22 o 0 7 1 1075.41 1183.67 19.70 o 1 7 1 3663.81 3731.21 52.99 o 2 7 1 0.66 -3.24 7.57 o 3 7 1 3311.67 3409.82 50.40 o 4 7 1 598.83 533.88 20.55 o 5 7 1 192.51 206.91 17.30 o 6 7 1 551.19 569.53 21.63 o 7 7 1 14.62 19.86 8.31 o 8 7 1 871.54 860.54 28.58 o 9 7 1 367.80 321.07 22.79 o 10 7 1 135.27 120.91 23.90 o 11 7 1 141.18 159.16 44.34 o 12 7 1 6.12 -4.04 30.17 o 13 7 1 35.65 2.39 52.99 o -13 8 1 134.43 221.95 41.20 o -12 8 1 9.09 8.03 34.60 o -11 8 1 37.99 22.62 50.82 o -10 8 1 199.23 220.87 29.20 o -9 8 1 2.81 -6.60 15.06 o -8 8 1 342.07 432.24 22.79 o -7 8 1 2.66 4.87 12.98 o -6 8 1 873.30 961.90 27.02 o -5 8 1 1567.33 1598.72 35.07 o -4 8 1 443.11 455.91 15.06 o -3 8 1 1957.41 2056.83 38.23 o -2 8 1 2.59 15.14 6.12 o -1 8 1 1185.91 1232.86 22.79 o 0 8 1 352.12 373.62 11.39 o 1 8 1 420.62 436.90 40.01 o 2 8 1 1656.56 1754.07 40.01 o 3 8 1 89.03 63.34 12.98 o 4 8 1 772.95 794.63 47.58 o 5 8 1 118.95 133.58 9.85 o 6 8 1 42.23 29.56 11.89 o 7 8 1 176.81 170.32 13.51 o 8 8 1 1.75 1.08 12.23 o 9 8 1 224.92 206.84 36.77 o 10 8 1 95.82 103.13 26.00 o 11 8 1 31.34 -5.72 24.87 o 12 8 1 67.98 93.38 35.03 o -12 9 1 85.48 107.97 40.50 o -11 9 1 26.02 -9.89 29.57 o -10 9 1 78.04 75.06 25.86 o -9 9 1 288.82 356.17 25.86 o -8 9 1 23.77 28.66 15.06 o -7 9 1 485.05 590.79 28.11 o -6 9 1 489.30 524.17 37.85 o -5 9 1 58.33 56.30 12.93 o -4 9 1 990.60 1137.04 29.06 o -3 9 1 55.55 47.46 8.80 o -2 9 1 1980.66 2163.14 42.61 o -1 9 1 191.92 203.70 20.55 o 0 9 1 314.86 299.73 12.93 o 1 9 1 641.14 661.70 18.16 o 2 9 1 16.80 27.03 8.80 o 3 9 1 594.72 606.29 56.23 o 4 9 1 142.01 141.85 11.95 o 5 9 1 252.93 269.62 13.99 o 6 9 1 204.09 208.57 18.38 o 7 9 1 1.30 -4.45 12.93 o 8 9 1 77.26 66.68 16.61 o 9 9 1 136.43 150.57 36.77 o 10 9 1 77.78 81.16 25.86 o 11 9 1 117.31 83.71 36.32 o 12 9 1 0.03 30.31 56.23 o -12 10 1 28.48 -24.65 37.87 o -11 10 1 109.83 81.72 34.00 o -10 10 1 145.80 81.10 24.47 o -9 10 1 5.07 7.72 20.76 o -8 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