#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:54 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180910 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/51/2105197.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105197_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; [Ni(MeCN)(H~2~O)~2~(NO~3~)~2~]·(15-crown-5)·MeCN: detailed study of a four-phase sequence that includes an intermediate modulated phase ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 389 _journal_page_last 400 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.420 _cell_angle_gamma 90.000 _cell_length_a 12.1640 _cell_length_b 12.2780 _cell_length_c 16.2120 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.7698 _cod_data_source_file hw5021227K_III_2sup27.hkl _cod_data_source_block 227K_III_2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k06112 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 338.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6334.18 5979.70 89.98 o 2 0 0 25568.66 26551.93 428.50 o 3 0 0 874.60 869.85 15.00 o 4 0 0 1208.23 1004.83 19.28 o 5 0 0 38815.92 43115.55 606.33 o 6 0 0 2049.50 2821.66 55.70 o 7 0 0 7762.57 8075.06 167.11 o 8 0 0 6756.72 6609.59 177.83 o 9 0 0 335.15 342.80 27.85 o 10 0 0 457.14 424.21 29.99 o 11 0 0 959.85 1004.83 55.70 o 12 0 0 1036.64 1210.51 79.27 o 13 0 0 898.92 859.14 62.13 o 14 0 0 16.92 42.85 36.42 o 15 0 0 160.69 64.27 47.13 o 1 1 0 45992.81 47971.20 1646.55 o 2 1 0 1305.55 1397.70 17.37 o 3 1 0 8844.82 8245.54 97.50 o 4 1 0 17102.83 17965.42 200.96 o 5 1 0 897.54 673.04 27.85 o 6 1 0 11096.06 11851.84 124.97 o 7 1 0 2597.64 2742.43 38.08 o 8 1 0 126.76 125.81 9.08 o 9 1 0 788.16 686.48 19.42 o 10 1 0 92.07 121.50 16.46 o 11 1 0 2078.12 2341.65 68.82 o 12 1 0 973.52 1184.54 44.52 o 13 1 0 95.77 107.41 37.49 o 14 1 0 171.53 150.70 30.19 o 15 1 0 0.65 -9.76 33.46 o 0 2 0 12969.41 12370.36 241.55 o 1 2 0 1065.86 1178.06 15.85 o 2 2 0 3163.95 3406.63 45.45 o 3 2 0 9910.02 9275.88 109.83 o 4 2 0 594.70 813.11 12.12 o 5 2 0 18746.59 19787.11 213.83 o 6 2 0 34.67 17.30 3.57 o 7 2 0 3973.77 4521.72 60.74 o 8 2 0 3228.07 3599.54 48.73 o 9 2 0 751.15 813.91 24.69 o 10 2 0 2278.00 2492.33 62.20 o 11 2 0 7.56 30.23 26.78 o 12 2 0 564.65 530.84 31.03 o 13 2 0 263.85 299.24 35.35 o 14 2 0 5.72 -0.74 40.71 o 15 2 0 264.22 206.55 52.59 o 1 3 0 5059.16 5558.84 68.12 o 2 3 0 5096.69 5710.99 73.37 o 3 3 0 8222.20 9079.63 107.93 o 4 3 0 17542.93 17447.63 197.18 o 5 3 0 1076.54 762.76 28.92 o 6 3 0 937.06 1035.85 16.46 o 7 3 0 838.49 1032.08 19.52 o 8 3 0 1056.43 1193.37 24.10 o 9 3 0 2893.30 3179.17 50.95 o 10 3 0 431.40 405.02 21.05 o 11 3 0 1613.73 1747.64 81.41 o 12 3 0 52.83 47.44 27.85 o 13 3 0 0.71 -15.00 58.92 o 14 3 0 224.05 193.77 54.63 o 0 4 0 44312.62 45650.29 1000.95 o 1 4 0 1993.95 2537.06 31.38 o 2 4 0 12582.74 13012.45 153.09 o 3 4 0 8237.01 8357.89 95.44 o 4 4 0 543.56 367.25 8.23 o 5 4 0 9337.32 10088.08 122.60 o 6 4 0 951.85 872.04 15.15 o 7 4 0 3013.65 3148.64 50.73 o 8 4 0 2929.39 3183.29 51.44 o 9 4 0 43.80 50.72 8.72 o 10 4 0 2007.61 2524.02 64.27 o 11 4 0 115.85 112.01 20.57 o 12 4 0 129.65 72.93 51.42 o 13 4 0 120.70 62.13 32.93 o 14 4 0 1.84 -38.56 38.56 o 1 5 0 12454.28 12146.89 134.81 o 2 5 0 10838.84 13740.83 171.40 o 3 5 0 8104.56 8218.02 93.93 o 4 5 0 6964.83 7590.00 94.60 o 5 5 0 6.38 18.68 6.43 o 6 5 0 3869.20 3892.14 53.77 o 7 5 0 106.75 134.12 8.23 o 8 5 0 10.34 -1.17 12.85 o 9 5 0 1164.67 1253.51 31.71 o 10 5 0 282.05 217.25 17.37 o 11 5 0 927.19 1121.02 72.84 o 12 5 0 50.24 12.80 31.07 o 13 5 0 21.82 10.67 33.25 o 14 5 0 297.69 348.18 63.20 o 0 6 0 19392.06 19789.12 325.72 o 1 6 0 157.15 251.98 16.07 o 2 6 0 9675.87 10055.44 120.49 o 3 6 0 618.44 747.67 13.38 o 4 6 0 407.42 398.27 18.21 o 5 6 0 5125.12 5399.93 73.61 o 6 6 0 3.97 6.70 5.51 o 7 6 0 2036.90 1839.95 68.56 o 8 6 0 315.93 283.63 14.33 o 9 6 0 62.30 61.36 11.84 o 10 6 0 1344.38 1610.58 47.27 o 11 6 0 123.09 138.72 28.93 o 12 6 0 231.46 135.16 37.70 o 13 6 0 195.30 148.26 35.65 o 14 6 0 4.83 -29.19 52.49 o 1 7 0 2090.21 2072.55 30.19 o 2 7 0 506.03 672.64 14.33 o 3 7 0 1163.05 1199.83 21.21 o 4 7 0 1443.17 1484.77 26.48 o 5 7 0 13.68 10.00 4.28 o 6 7 0 2704.23 2835.47 45.30 o 7 7 0 404.68 524.00 15.43 o 8 7 0 59.40 34.95 9.76 o 9 7 0 416.96 288.90 21.93 o 10 7 0 39.95 7.45 16.22 o 11 7 0 594.98 606.56 95.34 o 12 7 0 125.73 73.88 35.78 o 13 7 0 3.86 40.46 32.93 o 0 8 0 2900.21 3343.77 88.91 o 1 8 0 434.38 338.09 20.35 o 2 8 0 6.76 3.81 6.69 o 3 8 0 1019.35 921.26 28.92 o 4 8 0 75.66 72.53 8.72 o 5 8 0 4158.92 4710.15 111.41 o 6 8 0 474.16 560.23 21.62 o 7 8 0 272.49 231.66 16.46 o 8 8 0 303.05 289.19 28.92 o 9 8 0 15.19 -1.92 14.33 o 10 8 0 489.54 496.54 55.70 o 11 8 0 36.55 42.63 21.62 o 12 8 0 17.61 9.38 40.22 o 13 8 0 80.24 55.96 46.53 o 1 9 0 834.72 768.13 23.57 o 2 9 0 1280.92 1201.47 28.00 o 3 9 0 17.67 49.39 19.28 o 4 9 0 288.05 188.17 21.42 o 5 9 0 137.36 197.83 15.85 o 6 9 0 497.37 622.59 26.48 o 7 9 0 764.39 890.95 33.23 o 8 9 0 91.36 44.14 20.35 o 9 9 0 150.97 170.85 23.68 o 10 9 0 10.59 24.38 21.62 o 11 9 0 72.58 78.78 35.35 o 12 9 0 69.90 136.85 80.34 o 0 10 0 6674.60 7152.36 190.93 o 1 10 0 8.42 27.85 9.76 o 2 10 0 180.18 96.98 36.42 o 3 10 0 335.32 533.69 51.42 o 4 10 0 4.23 8.24 7.83 o 5 10 0 245.16 186.30 17.37 o 6 10 0 72.07 69.95 18.18 o 7 10 0 55.36 -1.71 14.26 o 8 10 0 231.24 164.73 22.57 o 9 10 0 0.39 23.41 19.42 o 10 10 0 65.61 112.60 28.52 o 11 10 0 30.17 15.33 28.14 o 1 11 0 548.41 562.09 40.71 o 2 11 0 7.31 -4.59 10.28 o 3 11 0 3.02 18.16 15.85 o 4 11 0 148.00 48.50 16.46 o 5 11 0 9.28 -15.85 15.85 o 6 11 0 298.89 280.76 25.62 o 7 11 0 175.23 131.41 22.57 o 8 11 0 9.56 -10.44 51.42 o 9 11 0 32.72 -10.65 26.22 o 10 11 0 1.28 -6.12 25.71 o 11 11 0 54.10 0.62 41.48 o 0 12 0 57.30 73.27 21.39 o 1 12 0 0.48 8.91 14.33 o 2 12 0 8.46 -2.41 39.64 o 3 12 0 504.88 508.94 31.71 o 4 12 0 3.98 26.20 21.42 o 5 12 0 609.51 754.11 43.88 o 6 12 0 1.82 -8.57 38.56 o 7 12 0 11.56 -5.23 23.68 o 8 12 0 10.04 -28.92 28.92 o 9 12 0 0.17 12.32 33.23 o 10 12 0 55.48 2.26 51.42 o 1 13 0 0.27 -2.75 25.71 o 2 13 0 169.06 165.44 33.21 o 3 13 0 53.03 16.90 20.08 o 4 13 0 273.93 187.86 31.07 o 5 13 0 0.63 8.31 25.42 o 6 13 0 11.23 -8.88 25.71 o 7 13 0 12.16 -6.66 25.62 o 8 13 0 0.92 -8.80 26.55 o 0 14 0 49.58 6.43 64.27 o 1 14 0 0.16 -19.28 55.70 o 2 14 0 7.12 27.85 38.56 o 3 14 0 0.22 -17.14 32.14 o 4 14 0 11.79 36.42 29.99 o 5 14 0 0.30 42.85 38.56 o 6 14 0 0.43 4.28 32.14 o 7 14 0 7.56 -9.13 36.42 o 1 15 0 1.29 -10.71 49.28 o 2 15 0 0.68 17.14 49.28 o 3 15 0 0.28 -25.71 53.56 o 4 15 0 1.00 34.28 49.28 o 5 15 0 0.03 38.56 44.99 o -15 1 1 0.52 4.28 33.07 o -14 1 1 18.15 38.90 28.31 o -13 1 1 1.03 -1.71 18.89 o -12 1 1 22.46 9.59 17.37 o -11 1 1 67.75 40.71 16.66 o -10 1 1 10.60 -2.71 14.33 o -9 1 1 664.69 643.53 58.92 o -8 1 1 150.95 142.86 7.83 o -7 1 1 834.37 881.97 18.53 o -6 1 1 5.18 6.43 4.28 o -5 1 1 533.18 564.39 9.76 o -4 1 1 48.78 41.16 5.36 o -3 1 1 11.90 14.01 1.51 o -2 1 1 5.61 5.36 1.51 o -1 1 1 7.69 6.70 5.36 o 0 1 1 15.40 18.27 1.51 o 1 1 1 2.80 5.36 1.51 o 2 1 1 69.86 70.70 3.03 o 3 1 1 139.09 116.05 6.43 o 4 1 1 470.57 496.24 11.78 o 5 1 1 64.74 57.93 4.54 o 6 1 1 1300.00 1335.97 20.41 o 7 1 1 73.31 62.00 9.64 o 8 1 1 326.31 282.14 17.14 o 9 1 1 0.26 6.96 6.43 o 10 1 1 0.31 21.58 9.36 o 11 1 1 12.85 11.69 17.99 o 12 1 1 6.58 7.75 19.00 o 13 1 1 20.71 2.95 24.10 o 14 1 1 0.01 6.20 35.35 o -15 2 1 16.64 109.36 48.21 o -14 2 1 1.70 -15.00 24.69 o -13 2 1 32.51 13.33 20.08 o -12 2 1 8.72 23.22 18.53 o -11 2 1 59.06 31.07 15.15 o -10 2 1 237.17 271.72 32.14 o -9 2 1 18.95 6.04 8.23 o -8 2 1 352.71 364.27 13.63 o -7 2 1 1.44 6.43 4.54 o -6 2 1 885.07 737.50 12.81 o -5 2 1 33.89 38.56 3.03 o -4 2 1 171.76 172.48 4.54 o -3 2 1 162.79 150.01 3.03 o -2 2 1 13.18 25.06 3.21 o -1 2 1 424.43 346.94 5.14 o 0 2 1 165.32 153.20 3.03 o 1 2 1 687.90 625.79 10.71 o 2 2 1 199.90 218.62 4.54 o 3 2 1 122.71 85.93 7.50 o 4 2 1 250.32 262.94 6.69 o 5 2 1 41.36 30.61 4.54 o 6 2 1 131.92 97.55 6.69 o 7 2 1 450.10 459.99 11.84 o 8 2 1 3.66 2.14 7.50 o 9 2 1 30.97 28.95 5.75 o 10 2 1 2.75 6.86 10.70 o 11 2 1 0.77 -3.26 17.37 o 12 2 1 94.04 69.25 23.45 o 13 2 1 1.07 44.00 28.92 o 14 2 1 18.33 -41.78 41.78 o -15 3 1 11.83 16.69 91.06 o -14 3 1 50.34 63.66 37.46 o -13 3 1 0.99 -23.15 23.15 o -12 3 1 4.82 -15.24 19.42 o -11 3 1 14.02 -10.24 17.14 o -10 3 1 56.49 44.99 12.12 o -9 3 1 74.41 62.43 9.09 o -8 3 1 56.40 45.44 5.51 o -7 3 1 734.58 686.05 14.92 o -6 3 1 155.17 159.62 6.06 o -5 3 1 587.05 548.16 9.76 o -4 3 1 905.73 960.38 14.33 o -3 3 1 2.90 3.57 2.14 o -2 3 1 3173.40 3060.30 39.30 o -1 3 1 151.75 226.28 7.50 o 0 3 1 1360.22 1101.89 19.28 o 1 3 1 1892.81 1778.27 22.72 o 2 3 1 41.29 35.38 3.03 o 3 3 1 679.96 587.34 9.76 o 4 3 1 460.04 443.01 16.07 o 5 3 1 1.34 3.21 9.64 o 6 3 1 68.05 77.98 6.69 o 7 3 1 36.72 37.81 12.85 o 8 3 1 68.58 55.40 8.23 o 9 3 1 2.91 -2.14 7.13 o 10 3 1 4.88 0.18 8.72 o 11 3 1 38.24 46.16 16.46 o 12 3 1 18.54 19.28 24.64 o 13 3 1 18.61 8.38 24.96 o 14 3 1 2.99 -10.29 33.39 o -14 4 1 7.50 -6.83 38.13 o -13 4 1 78.14 106.05 38.58 o -12 4 1 0.05 8.88 20.57 o -11 4 1 30.08 12.00 34.28 o -10 4 1 6.56 18.21 12.12 o -9 4 1 73.70 74.46 8.72 o -8 4 1 16.83 12.38 6.69 o -7 4 1 481.68 483.19 12.12 o -6 4 1 1460.19 1285.50 19.69 o -5 4 1 830.26 875.56 22.50 o -4 4 1 878.62 937.35 13.63 o -3 4 1 111.70 101.81 5.14 o -2 4 1 95.81 96.41 3.03 o -1 4 1 1213.83 1025.82 14.33 o 0 4 1 824.27 726.64 11.29 o 1 4 1 435.48 448.04 10.71 o 2 4 1 44.77 49.37 4.54 o 3 4 1 34.81 41.72 6.43 o 4 4 1 409.51 351.38 9.09 o 5 4 1 776.52 709.35 12.81 o 6 4 1 147.31 137.22 8.23 o 7 4 1 412.09 439.79 21.42 o 8 4 1 85.01 78.56 8.72 o 9 4 1 58.53 42.85 10.28 o 10 4 1 14.13 13.71 20.35 o 11 4 1 23.83 16.03 18.53 o 12 4 1 119.39 109.07 21.62 o 13 4 1 0.73 -20.78 71.77 o 14 4 1 22.72 -13.02 37.50 o -14 5 1 106.43 117.57 49.60 o -13 5 1 5.16 7.86 30.66 o -12 5 1 125.98 91.41 25.91 o -11 5 1 30.82 33.79 19.52 o -10 5 1 424.28 400.36 22.57 o -9 5 1 357.71 323.96 25.71 o -8 5 1 26.68 23.76 8.57 o -7 5 1 536.63 458.03 12.81 o -6 5 1 720.22 705.66 15.85 o -5 5 1 165.40 162.39 6.69 o -4 5 1 584.63 652.48 13.63 o -3 5 1 12.46 6.43 4.54 o -2 5 1 2839.26 2739.27 32.55 o -1 5 1 1752.18 1614.55 20.41 o 0 5 1 711.99 805.14 12.85 o 1 5 1 2350.70 2187.06 44.99 o 2 5 1 92.45 87.42 7.50 o 3 5 1 1641.93 1536.20 21.21 o 4 5 1 873.57 788.44 13.63 o 5 5 1 564.12 549.80 13.63 o 6 5 1 1146.64 1217.13 21.05 o 7 5 1 116.13 94.27 9.76 o 8 5 1 445.53 470.37 17.99 o 9 5 1 89.62 94.85 29.99 o 10 5 1 65.45 94.11 15.85 o 11 5 1 203.50 215.62 24.24 o 12 5 1 0.18 -15.95 31.13 o 13 5 1 34.11 43.54 36.65 o 14 5 1 0.20 -13.81 40.15 o -14 6 1 18.28 17.74 37.06 o -13 6 1 145.62 104.41 67.49 o -12 6 1 65.56 41.58 31.71 o -11 6 1 338.96 275.06 31.13 o -10 6 1 904.59 851.88 43.41 o -9 6 1 315.99 344.50 24.64 o -8 6 1 371.59 378.39 13.38 o -7 6 1 69.23 51.00 8.23 o -6 6 1 270.20 226.64 21.42 o -5 6 1 1099.47 1072.41 21.93 o -4 6 1 56.39 55.16 6.06 o -3 6 1 2026.40 2097.94 55.70 o -2 6 1 487.00 494.70 9.76 o -1 6 1 1418.26 1493.63 21.93 o 0 6 1 2012.95 1820.13 23.15 o 1 6 1 352.98 412.77 11.78 o 2 6 1 4491.44 4582.37 53.64 o 3 6 1 43.06 32.60 5.14 o 4 6 1 3096.36 3225.63 46.19 o 5 6 1 122.01 105.03 9.09 o 6 6 1 126.28 123.31 8.72 o 7 6 1 1148.29 1156.48 36.42 o 8 6 1 215.98 197.88 22.50 o 9 6 1 479.77 524.71 36.42 o 10 6 1 196.92 174.55 17.99 o 11 6 1 156.20 227.96 32.87 o 12 6 1 164.58 66.92 34.68 o 13 6 1 1.64 -34.56 39.84 o -13 7 1 0.78 -8.75 34.87 o -12 7 1 81.96 103.32 33.46 o -11 7 1 197.07 159.63 29.99 o -10 7 1 304.84 266.89 31.02 o -9 7 1 1175.03 1142.23 42.69 o -8 7 1 232.55 199.07 13.93 o -7 7 1 1124.79 1225.73 32.41 o -6 7 1 97.35 96.79 9.76 o -5 7 1 331.50 319.21 13.38 o -4 7 1 2405.24 2472.14 41.15 o -3 7 1 2.67 0.00 3.83 o -2 7 1 3884.74 3967.37 52.50 o -1 7 1 230.17 293.87 20.35 o 0 7 1 938.14 1030.00 26.78 o 1 7 1 3330.93 3370.54 54.63 o 2 7 1 1.26 1.22 6.43 o 3 7 1 2905.72 3075.87 47.70 o 4 7 1 546.43 467.86 14.33 o 5 7 1 159.99 204.51 20.35 o 6 7 1 512.64 519.29 21.42 o 7 7 1 9.49 18.75 8.72 o 8 7 1 781.78 762.80 57.85 o 9 7 1 326.63 301.58 22.57 o 10 7 1 115.03 134.01 23.15 o 11 7 1 114.17 159.99 31.30 o 12 7 1 9.32 17.80 32.76 o 13 7 1 26.53 4.28 35.81 o -13 8 1 99.17 106.59 35.51 o -12 8 1 4.91 7.47 24.96 o -11 8 1 37.77 16.82 23.68 o -10 8 1 187.06 213.25 24.96 o -9 8 1 5.46 15.92 15.43 o -8 8 1 276.78 392.46 21.05 o -7 8 1 1.37 4.82 11.84 o -6 8 1 751.18 827.44 35.35 o -5 8 1 1333.64 1344.88 33.23 o -4 8 1 404.17 409.43 15.85 o -3 8 1 1728.03 1829.42 34.75 o -2 8 1 2.04 9.64 11.78 o -1 8 1 1040.69 1088.37 21.42 o 0 8 1 297.01 340.72 11.29 o 1 8 1 356.70 364.11 26.78 o 2 8 1 1474.29 1588.65 29.51 o 3 8 1 73.49 56.38 12.85 o 4 8 1 685.94 697.34 25.71 o 5 8 1 100.47 121.29 10.60 o 6 8 1 38.18 29.22 10.71 o 7 8 1 166.94 128.50 27.85 o 8 8 1 2.49 7.14 13.38 o 9 8 1 184.74 179.47 21.42 o 10 8 1 71.13 67.49 28.92 o 11 8 1 34.97 46.68 28.31 o 12 8 1 62.48 58.65 33.07 o -12 9 1 66.40 110.74 38.61 o -11 9 1 17.13 0.86 34.28 o -10 9 1 70.82 24.72 21.05 o -9 9 1 236.06 279.01 23.15 o -8 9 1 14.84 19.28 20.35 o -7 9 1 407.94 478.37 23.45 o -6 9 1 405.85 396.29 21.05 o -5 9 1 47.20 48.13 11.84 o -4 9 1 825.38 1007.72 27.14 o -3 9 1 41.58 51.81 17.14 o -2 9 1 1723.91 1910.52 39.11 o -1 9 1 167.46 149.10 12.85 o 0 9 1 269.94 293.33 16.07 o 1 9 1 544.66 561.17 19.28 o 2 9 1 15.72 11.10 8.23 o 3 9 1 534.44 543.08 19.52 o 4 9 1 119.91 129.37 11.84 o 5 9 1 214.79 232.08 13.86 o 6 9 1 165.35 190.66 34.28 o 7 9 1 2.60 -2.82 14.33 o 8 9 1 69.61 74.09 16.46 o 9 9 1 112.32 119.44 29.99 o 10 9 1 58.55 58.95 32.14 o 11 9 1 97.79 54.92 36.91 o 12 9 1 0.01 35.11 40.05 o -12 10 1 21.02 -19.28 45.09 o -11 10 1 84.69 54.59 35.28 o -10 10 1 125.84 128.00 32.14 o -9 10 1 3.82 -6.35 21.62 o -8 10 1 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