#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:54 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180910 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/51/2105198.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105198_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; [Ni(MeCN)(H~2~O)~2~(NO~3~)~2~]·(15-crown-5)·MeCN: detailed study of a four-phase sequence that includes an intermediate modulated phase ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 389 _journal_page_last 400 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.430 _cell_angle_gamma 90.000 _cell_length_a 12.1590 _cell_length_b 12.2880 _cell_length_c 16.2260 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.7699 _cod_data_source_file hw5021230K_III_2sup28.hkl _cod_data_source_block 230K_III_2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k06113 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 293.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6300.25 6078.08 92.29 o 2 0 0 25452.00 27217.33 432.89 o 3 0 0 955.64 889.96 17.58 o 4 0 0 1200.53 927.31 17.58 o 5 0 0 37952.17 42153.24 637.25 o 6 0 0 2326.23 3348.88 61.53 o 7 0 0 7316.15 7684.40 156.02 o 8 0 0 6967.99 6546.13 177.99 o 9 0 0 288.58 276.88 26.37 o 10 0 0 556.82 430.70 32.96 o 11 0 0 971.04 927.31 50.54 o 12 0 0 915.26 1083.33 70.32 o 13 0 0 843.33 843.81 57.13 o 14 0 0 12.50 28.57 32.96 o 15 0 0 160.99 92.29 57.13 o 1 1 0 46409.50 48496.75 1671.63 o 2 1 0 1484.96 1438.46 18.68 o 3 1 0 8432.10 7995.08 92.61 o 4 1 0 16862.26 18404.00 205.72 o 5 1 0 681.72 468.09 10.99 o 6 1 0 10264.63 11310.65 119.32 o 7 1 0 2797.55 2910.19 40.59 o 8 1 0 138.63 143.52 10.97 o 9 1 0 819.22 719.34 21.54 o 10 1 0 51.66 51.03 24.17 o 11 1 0 1739.57 2114.76 69.13 o 12 1 0 917.07 1129.99 45.06 o 13 1 0 77.97 70.61 23.15 o 14 1 0 178.53 132.11 27.16 o 15 1 0 0.18 -3.90 37.58 o 0 2 0 13513.64 12729.82 246.28 o 1 2 0 1054.09 1235.43 24.17 o 2 2 0 3207.86 3495.17 54.94 o 3 2 0 10299.16 9495.37 113.40 o 4 2 0 588.65 824.04 12.43 o 5 2 0 19193.85 19900.93 220.68 o 6 2 0 16.69 4.83 3.66 o 7 2 0 3604.27 4361.02 67.02 o 8 2 0 2957.64 3486.64 48.37 o 9 2 0 692.00 744.71 24.28 o 10 2 0 2161.13 2439.13 58.13 o 11 2 0 19.84 37.82 14.70 o 12 2 0 482.68 520.14 43.95 o 13 2 0 256.76 250.84 30.27 o 14 2 0 1.26 13.57 26.28 o 15 2 0 230.15 219.97 75.81 o 1 3 0 5106.47 5644.91 66.76 o 2 3 0 5011.52 5790.13 73.79 o 3 3 0 7840.60 8954.36 107.78 o 4 3 0 17373.52 17333.63 193.93 o 5 3 0 934.39 611.86 10.01 o 6 3 0 929.72 1029.41 18.68 o 7 3 0 847.29 1091.61 19.01 o 8 3 0 1004.92 1071.47 21.59 o 9 3 0 2696.05 3047.56 58.23 o 10 3 0 366.61 340.95 20.02 o 11 3 0 1429.23 1629.94 51.90 o 12 3 0 56.19 48.83 20.59 o 13 3 0 0.69 35.30 42.85 o 14 3 0 193.02 156.17 47.15 o 0 4 0 44186.96 46021.14 1038.42 o 1 4 0 1906.11 2619.57 34.08 o 2 4 0 12044.50 13111.41 168.10 o 3 4 0 8013.77 8393.78 95.55 o 4 4 0 397.83 232.58 7.69 o 5 4 0 9466.91 10083.55 118.68 o 6 4 0 965.97 861.44 15.54 o 7 4 0 2771.20 3000.00 49.65 o 8 4 0 2796.89 3234.72 52.76 o 9 4 0 34.49 6.23 24.17 o 10 4 0 1958.77 2406.18 69.46 o 11 4 0 127.92 166.28 26.37 o 12 4 0 136.53 82.60 34.06 o 13 4 0 133.52 131.43 110.97 o 14 4 0 0.18 30.35 38.33 o 1 5 0 12247.68 11909.44 153.82 o 2 5 0 11286.88 14820.78 174.03 o 3 5 0 7687.60 8025.71 93.19 o 4 5 0 6963.56 7609.14 92.88 o 5 5 0 6.60 17.89 5.27 o 6 5 0 3644.97 3729.51 50.34 o 7 5 0 165.79 217.05 11.58 o 8 5 0 2.61 18.38 8.44 o 9 5 0 1104.11 1164.02 32.73 o 10 5 0 289.01 263.81 24.17 o 11 5 0 797.89 983.39 51.64 o 12 5 0 61.93 18.30 32.23 o 13 5 0 21.93 39.60 32.75 o 14 5 0 275.18 312.08 59.33 o 0 6 0 20396.05 20308.74 336.85 o 1 6 0 280.06 418.80 10.01 o 2 6 0 9473.92 9735.87 114.70 o 3 6 0 795.34 965.39 19.78 o 4 6 0 392.51 372.91 10.01 o 5 6 0 5194.79 5510.12 87.90 o 6 6 0 1.96 8.79 7.69 o 7 6 0 1823.86 1644.82 46.15 o 8 6 0 374.67 313.35 15.31 o 9 6 0 71.17 73.02 13.73 o 10 6 0 1332.59 1624.22 82.40 o 11 6 0 129.44 100.57 31.24 o 12 6 0 223.99 123.14 37.88 o 13 6 0 195.57 176.79 49.44 o 14 6 0 4.98 59.04 68.12 o 1 7 0 2118.62 2142.42 30.96 o 2 7 0 516.57 768.01 15.54 o 3 7 0 1307.69 1220.14 26.37 o 4 7 0 1604.96 1549.63 64.82 o 5 7 0 24.84 22.76 3.93 o 6 7 0 2650.29 2811.84 44.26 o 7 7 0 402.07 531.36 15.38 o 8 7 0 71.93 33.69 11.58 o 9 7 0 451.65 261.18 20.93 o 10 7 0 31.62 37.36 16.64 o 11 7 0 551.28 576.08 76.91 o 12 7 0 125.70 147.22 42.82 o 13 7 0 3.13 -24.21 32.27 o 0 8 0 3027.91 3458.78 73.57 o 1 8 0 471.89 326.09 25.27 o 2 8 0 5.52 0.00 6.59 o 3 8 0 931.16 854.55 56.03 o 4 8 0 66.97 67.09 7.63 o 5 8 0 4145.37 4609.04 87.55 o 6 8 0 433.40 582.05 22.17 o 7 8 0 366.36 312.61 17.42 o 8 8 0 298.56 277.96 49.44 o 9 8 0 16.55 28.04 16.26 o 10 8 0 467.74 488.72 57.13 o 11 8 0 46.40 31.82 20.93 o 12 8 0 11.60 -12.09 33.92 o 13 8 0 83.49 -29.98 106.58 o 1 9 0 809.28 774.97 19.38 o 2 9 0 1194.63 1098.64 28.46 o 3 9 0 3.95 36.17 10.01 o 4 9 0 349.16 215.24 11.31 o 5 9 0 74.04 149.72 15.54 o 6 9 0 464.43 585.86 26.41 o 7 9 0 681.84 851.41 31.60 o 8 9 0 71.89 24.72 16.48 o 9 9 0 132.85 107.12 20.20 o 10 9 0 7.36 32.65 21.10 o 11 9 0 55.81 55.24 35.16 o 12 9 0 68.81 79.51 67.02 o 0 10 0 7250.84 7256.47 180.57 o 1 10 0 0.33 8.39 8.44 o 2 10 0 214.69 121.02 15.38 o 3 10 0 274.29 526.53 20.59 o 4 10 0 4.50 4.39 8.03 o 5 10 0 248.71 157.78 17.82 o 6 10 0 85.45 87.48 17.42 o 7 10 0 63.59 30.14 16.26 o 8 10 0 264.60 149.03 23.75 o 9 10 0 0.01 11.83 19.49 o 10 10 0 66.31 35.16 53.84 o 11 10 0 27.27 50.39 33.16 o 1 11 0 595.97 565.86 40.65 o 2 11 0 4.56 11.43 14.28 o 3 11 0 20.69 -4.28 14.70 o 4 11 0 191.76 47.06 25.27 o 5 11 0 4.28 -16.22 16.26 o 6 11 0 278.38 252.78 24.86 o 7 11 0 188.16 132.08 25.27 o 8 11 0 10.75 18.46 23.07 o 9 11 0 42.08 12.15 26.28 o 10 11 0 3.57 -16.62 23.58 o 11 11 0 68.39 23.32 47.24 o 0 12 0 81.12 120.75 26.28 o 1 12 0 0.79 -4.39 12.43 o 2 12 0 9.21 19.21 21.18 o 3 12 0 496.49 512.23 31.82 o 4 12 0 0.05 23.73 19.38 o 5 12 0 609.98 800.03 45.79 o 6 12 0 1.42 26.93 21.97 o 7 12 0 21.70 -22.89 22.89 o 8 12 0 24.67 -23.16 23.16 o 9 12 0 0.11 -22.29 36.92 o 10 12 0 71.15 24.46 40.59 o 1 13 0 0.31 17.98 25.32 o 2 13 0 174.76 130.98 28.46 o 3 13 0 64.71 26.09 21.18 o 4 13 0 321.75 212.51 29.05 o 5 13 0 0.34 -17.58 27.09 o 6 13 0 3.97 35.40 27.45 o 7 13 0 18.88 18.31 26.37 o 8 13 0 0.40 41.17 31.93 o 0 14 0 89.08 -13.18 63.73 o 1 14 0 1.20 -17.58 50.54 o 2 14 0 9.29 -41.75 41.75 o 3 14 0 2.61 -13.18 32.96 o 4 14 0 10.72 -30.76 30.76 o 5 14 0 1.59 -32.96 32.96 o 6 14 0 1.82 -30.76 30.76 o 7 14 0 13.17 8.79 37.36 o 1 15 0 5.68 -6.59 43.95 o 2 15 0 2.45 48.34 48.34 o 3 15 0 0.52 -4.39 70.32 o 4 15 0 0.08 54.94 43.95 o 5 15 0 0.02 4.39 46.15 o -15 1 1 1.16 -3.43 35.60 o -14 1 1 10.88 16.42 28.43 o -13 1 1 0.05 14.18 16.88 o -12 1 1 22.61 17.58 17.09 o -11 1 1 47.89 41.66 18.45 o -10 1 1 9.82 11.80 14.70 o -9 1 1 497.67 506.79 28.57 o -8 1 1 114.60 101.34 17.58 o -7 1 1 687.72 661.46 15.31 o -6 1 1 4.05 3.52 4.39 o -5 1 1 460.80 443.98 9.32 o -4 1 1 34.71 33.77 4.39 o -3 1 1 7.93 12.19 1.55 o -2 1 1 5.04 3.30 1.55 o -1 1 1 4.58 4.39 1.55 o 0 1 1 13.75 12.19 1.55 o 1 1 1 4.16 7.85 1.55 o 2 1 1 45.73 50.64 3.11 o 3 1 1 124.91 97.80 4.66 o 4 1 1 362.96 402.24 7.77 o 5 1 1 47.91 45.39 3.66 o 6 1 1 1046.92 1060.73 18.28 o 7 1 1 48.90 50.91 5.27 o 8 1 1 252.30 224.25 8.94 o 9 1 1 0.13 2.20 5.65 o 10 1 1 0.37 -11.77 14.28 o 11 1 1 9.65 -15.82 15.82 o 12 1 1 3.98 -8.03 17.82 o 13 1 1 19.94 -20.84 25.60 o 14 1 1 0.26 15.73 34.08 o -15 2 1 10.45 40.88 47.24 o -14 2 1 0.86 23.04 36.26 o -13 2 1 19.98 -6.59 20.93 o -12 2 1 5.25 1.10 17.88 o -11 2 1 57.24 25.74 27.47 o -10 2 1 179.12 181.01 17.58 o -9 2 1 13.62 9.67 9.89 o -8 2 1 286.41 306.86 11.58 o -7 2 1 0.71 6.59 6.22 o -6 2 1 692.95 569.31 11.58 o -5 2 1 25.80 31.90 3.11 o -4 2 1 144.49 130.76 4.66 o -3 2 1 127.75 123.06 3.11 o -2 2 1 17.63 22.19 2.20 o -1 2 1 341.42 283.74 8.79 o 0 2 1 122.95 118.66 3.11 o 1 2 1 525.80 492.26 7.77 o 2 2 1 162.94 181.35 4.66 o 3 2 1 80.22 57.13 3.11 o 4 2 1 210.19 188.04 15.38 o 5 2 1 32.76 22.70 3.66 o 6 2 1 84.92 69.34 5.27 o 7 2 1 338.08 348.02 15.38 o 8 2 1 5.68 1.10 5.65 o 9 2 1 30.31 23.73 7.31 o 10 2 1 0.31 -1.10 13.18 o 11 2 1 0.95 4.39 18.45 o 12 2 1 68.76 56.98 36.26 o 13 2 1 0.49 -16.56 21.59 o 14 2 1 13.61 23.20 46.15 o -15 3 1 9.25 -20.94 49.44 o -14 3 1 33.26 -9.91 31.98 o -13 3 1 0.73 2.20 26.41 o -12 3 1 6.17 3.72 24.17 o -11 3 1 6.14 -2.69 15.38 o -10 3 1 35.26 28.27 11.58 o -9 3 1 50.10 45.15 10.01 o -8 3 1 42.00 27.36 5.90 o -7 3 1 606.47 530.81 13.14 o -6 3 1 123.81 116.21 9.89 o -5 3 1 453.83 430.71 9.32 o -4 3 1 691.75 743.41 11.58 o -3 3 1 3.95 3.66 2.20 o -2 3 1 2551.69 2478.39 31.82 o -1 3 1 115.72 179.42 7.69 o 0 3 1 1099.50 855.90 12.43 o 1 3 1 1522.53 1469.25 19.38 o 2 3 1 29.07 22.19 3.11 o 3 3 1 527.58 490.38 13.18 o 4 3 1 373.61 339.79 9.89 o 5 3 1 2.60 0.00 8.79 o 6 3 1 62.66 63.51 6.86 o 7 3 1 28.42 34.97 6.86 o 8 3 1 57.76 37.36 6.86 o 9 3 1 0.47 3.96 7.31 o 10 3 1 3.67 7.32 8.94 o 11 3 1 21.21 29.19 16.26 o 12 3 1 11.37 1.62 17.82 o 13 3 1 14.32 12.06 28.71 o 14 3 1 1.23 45.15 65.92 o -14 4 1 5.01 6.76 47.24 o -13 4 1 50.64 52.40 31.93 o -12 4 1 0.05 -37.36 37.36 o -11 4 1 19.80 -5.16 15.31 o -10 4 1 4.22 -2.20 10.88 o -9 4 1 64.95 51.01 17.58 o -8 4 1 18.26 13.43 12.09 o -7 4 1 360.33 360.04 16.48 o -6 4 1 1175.67 1013.85 17.82 o -5 4 1 629.35 663.62 21.97 o -4 4 1 761.26 777.91 12.43 o -3 4 1 89.83 76.97 4.66 o -2 4 1 70.34 64.03 4.39 o -1 4 1 981.40 828.43 12.43 o 0 4 1 656.89 530.68 9.32 o 1 4 1 365.01 373.97 6.86 o 2 4 1 34.91 42.45 3.66 o 3 4 1 32.59 35.30 4.66 o 4 4 1 348.28 280.38 7.77 o 5 4 1 638.83 582.93 11.58 o 6 4 1 109.28 114.49 9.89 o 7 4 1 311.86 318.62 18.68 o 8 4 1 91.52 80.30 9.32 o 9 4 1 59.43 25.43 10.55 o 10 4 1 13.88 -0.90 15.38 o 11 4 1 13.18 -3.52 19.01 o 12 4 1 80.83 91.64 21.75 o 13 4 1 1.42 -39.55 39.55 o 14 4 1 18.56 32.86 42.85 o -14 5 1 85.67 87.36 44.26 o -13 5 1 3.41 -16.46 36.92 o -12 5 1 98.22 134.39 28.43 o -11 5 1 25.91 8.87 20.93 o -10 5 1 323.08 283.46 20.59 o -9 5 1 275.15 234.28 13.14 o -8 5 1 16.13 16.48 7.77 o -7 5 1 469.74 375.80 11.58 o -6 5 1 590.31 533.89 13.14 o -5 5 1 144.04 146.12 6.86 o -4 5 1 486.66 505.01 14.28 o -3 5 1 7.40 8.79 4.66 o -2 5 1 2352.40 2140.68 28.57 o -1 5 1 1436.85 1305.27 17.82 o 0 5 1 598.14 679.96 11.58 o 1 5 1 1936.47 1710.51 22.17 o 2 5 1 86.80 71.84 5.49 o 3 5 1 1238.65 1222.91 21.97 o 4 5 1 724.85 615.29 12.43 o 5 5 1 435.85 424.10 12.43 o 6 5 1 919.21 960.50 18.45 o 7 5 1 104.01 82.32 8.44 o 8 5 1 367.61 357.15 18.68 o 9 5 1 70.01 51.82 18.68 o 10 5 1 43.66 36.20 21.97 o 11 5 1 150.00 86.76 20.88 o 12 5 1 0.03 -2.56 29.05 o 13 5 1 32.32 8.74 31.61 o 14 5 1 0.30 -4.47 42.71 o -14 6 1 13.36 19.94 40.59 o -13 6 1 104.30 120.90 37.14 o -12 6 1 44.70 39.16 29.56 o -11 6 1 281.74 202.69 31.61 o -10 6 1 685.55 633.67 51.64 o -9 6 1 243.13 255.01 24.17 o -8 6 1 288.36 285.97 11.58 o -7 6 1 50.10 53.22 8.44 o -6 6 1 206.75 180.19 6.06 o -5 6 1 909.19 802.45 18.65 o -4 6 1 38.09 41.39 6.22 o -3 6 1 1665.93 1624.14 22.49 o -2 6 1 396.41 391.45 10.99 o -1 6 1 1103.63 1178.41 24.17 o 0 6 1 1671.49 1436.14 20.02 o 1 6 1 286.67 348.10 8.44 o 2 6 1 3626.00 3673.39 44.98 o 3 6 1 40.40 30.92 5.27 o 4 6 1 2486.02 2567.89 45.05 o 5 6 1 97.26 69.74 8.44 o 6 6 1 78.85 79.55 8.44 o 7 6 1 861.72 813.09 23.15 o 8 6 1 173.68 165.88 13.73 o 9 6 1 363.05 379.78 20.02 o 10 6 1 155.58 185.01 19.49 o 11 6 1 114.78 139.63 30.61 o 12 6 1 147.45 78.78 36.69 o 13 6 1 0.73 50.16 39.85 o -13 7 1 0.39 19.52 37.80 o -12 7 1 58.47 60.80 34.32 o -11 7 1 126.75 128.29 28.81 o -10 7 1 257.20 228.75 29.48 o -9 7 1 895.27 902.63 47.24 o -8 7 1 165.67 127.45 12.60 o -7 7 1 863.56 965.46 27.45 o -6 7 1 75.29 87.49 23.07 o -5 7 1 231.34 250.87 12.14 o -4 7 1 1809.04 2025.00 35.33 o -3 7 1 1.19 5.13 10.99 o -2 7 1 3085.32 3248.82 42.20 o -1 7 1 196.02 239.70 9.32 o 0 7 1 707.95 789.76 15.38 o 1 7 1 2661.76 2738.92 40.59 o 2 7 1 0.79 5.65 5.27 o 3 7 1 2278.24 2470.17 64.82 o 4 7 1 461.90 362.54 13.14 o 5 7 1 117.94 162.96 20.88 o 6 7 1 400.74 395.86 12.98 o 7 7 1 2.60 12.39 8.79 o 8 7 1 603.42 572.34 23.75 o 9 7 1 283.14 272.22 21.59 o 10 7 1 78.68 73.10 22.69 o 11 7 1 90.62 95.99 41.75 o 12 7 1 5.40 18.51 32.50 o 13 7 1 17.77 13.33 37.88 o -13 8 1 63.36 83.17 35.33 o -12 8 1 2.38 -5.86 61.53 o -11 8 1 30.38 9.89 24.29 o -10 8 1 139.01 115.54 22.49 o -9 8 1 3.14 -3.91 14.28 o -8 8 1 187.21 249.13 26.37 o -7 8 1 0.13 7.69 13.98 o -6 8 1 585.76 688.27 22.49 o -5 8 1 964.86 1043.68 29.03 o -4 8 1 294.87 320.93 15.31 o -3 8 1 1312.04 1415.19 30.76 o -2 8 1 1.52 8.79 6.22 o -1 8 1 805.75 888.55 26.37 o 0 8 1 233.85 268.72 17.58 o 1 8 1 258.25 298.66 16.48 o 2 8 1 1177.82 1234.14 58.23 o 3 8 1 64.20 68.85 15.38 o 4 8 1 561.74 561.28 24.17 o 5 8 1 79.50 73.11 9.32 o 6 8 1 23.08 9.99 7.63 o 7 8 1 134.93 129.83 11.58 o 8 8 1 5.05 7.69 14.28 o 9 8 1 143.34 153.42 21.94 o 10 8 1 43.56 50.54 23.31 o 11 8 1 33.24 4.28 28.57 o 12 8 1 48.24 2.90 31.61 o -12 9 1 44.24 63.53 32.52 o -11 9 1 11.75 22.51 48.34 o -10 9 1 64.96 65.29 21.59 o -9 9 1 178.72 237.65 24.28 o -8 9 1 8.95 22.78 14.22 o -7 9 1 298.08 392.99 24.05 o -6 9 1 290.94 313.14 39.55 o -5 9 1 38.22 51.52 11.58 o -4 9 1 646.53 771.37 30.76 o -3 9 1 28.81 23.57 8.44 o -2 9 1 1416.47 1486.00 30.61 o -1 9 1 138.68 141.10 10.01 o 0 9 1 209.24 246.61 27.47 o 1 9 1 430.98 470.25 15.31 o 2 9 1 8.89 1.80 8.44 o 3 9 1 432.20 450.53 16.26 o 4 9 1 106.90 86.61 11.58 o 5 9 1 168.50 207.94 15.38 o 6 9 1 110.15 148.41 15.54 o 7 9 1 3.77 -3.30 13.98 o 8 9 1 62.51 62.98 16.26 o 9 9 1 91.13 96.42 21.59 o 10 9 1 43.56 16.66 24.05 o 11 9 1 71.47 103.28 35.74 o 12 9 1 0.06 36.22 61.53 o -12 10 1 16.91 -28.39 38.47 o -11 10 1 69.32 92.66 32.75 o -10 10 1 111.77 54.72 27.47 o -9 10 1 2.32 -15.21 19.49 o -8 10 1 221.28 265.45 23.75 o -7 10 1 82.94 79.11 18.65 o -6 10 1 212.35 191.28 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