#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/53/2105326.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105326_Fobs loop_ _publ_author_name 'Gholivand, Khodayar' 'Valmoozi, Ali A. Ebrahimi' 'Mahzouni, Hamid R.' _publ_section_title ; Structural and electronic aspects of hydrogen bonding in two polymorphs of butylene-N,N'-bis(O,O'-diarylphosphoramidate) ; _journal_coeditor_code PS5019 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 55 _journal_page_last 61 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.260 _cell_angle_gamma 90.000 _cell_length_a 15.7039 _cell_length_b 5.3299 _cell_length_c 16.9323 _exptl_crystal_F_000 580.00 _reflns_d_resolution_high 0.7330 _[local]_cod_data_source_file ps501972phcu-needlesup2.hkl _[local]_cod_data_source_block 72phcu-needle #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 145.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 24.60 1.77 0.89 o 2 0 0 15155.20 16313.16 115.69 o 3 0 0 7678.21 8592.65 149.00 o 4 0 0 2800.72 2974.80 34.44 o 5 0 0 9086.60 10236.55 72.30 o 6 0 0 4935.57 5881.04 71.60 o 7 0 0 883.45 882.60 25.52 o 8 0 0 2619.84 3019.86 50.06 o 9 0 0 14.38 20.47 8.98 o 10 0 0 1138.19 1211.39 36.56 o 11 0 0 8.90 9.51 8.70 o 12 0 0 453.39 415.04 25.66 o 13 0 0 40.09 26.40 12.44 o 14 0 0 945.75 1044.05 43.38 o 15 0 0 216.13 217.46 30.88 o 16 0 0 87.25 78.34 24.88 o 17 0 0 0.44 12.71 24.46 o 18 0 0 58.15 39.42 27.51 o 19 0 0 1164.09 1198.54 88.82 o 1 1 0 2373.26 2448.87 40.13 o 2 1 0 1053.80 1171.91 15.34 o 3 1 0 2514.53 2803.75 27.64 o 4 1 0 60.60 35.49 4.02 o 5 1 0 91.17 96.78 6.08 o 6 1 0 726.50 773.32 15.83 o 7 1 0 1256.54 1386.76 22.67 o 8 1 0 1440.42 1514.22 24.96 o 9 1 0 11.39 5.93 4.95 o 10 1 0 184.16 179.31 12.31 o 11 1 0 294.78 267.38 14.76 o 12 1 0 591.74 548.52 20.19 o 13 1 0 297.04 268.51 19.90 o 14 1 0 37.26 28.16 12.70 o 15 1 0 34.45 26.23 13.45 o 16 1 0 10.38 -2.72 12.30 o 17 1 0 44.42 19.26 16.29 o 18 1 0 298.30 295.86 33.80 o 19 1 0 120.69 90.79 25.91 o 0 2 0 0.14 -3.00 5.65 o 1 2 0 47.35 21.55 5.03 o 2 2 0 210.02 207.41 10.01 o 3 2 0 521.33 510.74 13.33 o 4 2 0 8.06 1.73 5.03 o 5 2 0 863.28 1007.64 30.40 o 6 2 0 498.07 538.47 19.62 o 7 2 0 29.59 13.99 4.95 o 8 2 0 73.52 49.18 6.81 o 9 2 0 54.77 52.50 7.67 o 10 2 0 0.11 -3.51 6.76 o 11 2 0 65.78 37.40 9.67 o 12 2 0 172.14 151.72 19.47 o 13 2 0 63.32 45.21 14.35 o 14 2 0 143.32 105.29 18.73 o 15 2 0 7.77 -2.57 13.66 o 16 2 0 62.82 38.37 17.05 o 17 2 0 11.67 3.75 15.99 o 18 2 0 1.66 -21.08 20.22 o 19 2 0 63.02 57.85 26.31 o 1 3 0 4.74 2.05 5.79 o 2 3 0 75.00 35.91 7.63 o 3 3 0 443.95 510.31 17.89 o 4 3 0 652.41 628.16 18.02 o 5 3 0 2.53 0.25 7.05 o 6 3 0 57.94 41.82 9.85 o 7 3 0 71.65 54.90 10.60 o 8 3 0 71.65 51.69 10.86 o 9 3 0 2.66 1.54 8.35 o 10 3 0 0.84 -2.33 10.70 o 11 3 0 130.30 103.92 19.25 o 12 3 0 65.09 48.94 16.32 o 13 3 0 0.07 -1.37 13.22 o 14 3 0 374.89 310.25 30.80 o 15 3 0 148.71 129.38 24.37 o 16 3 0 3.35 -1.14 17.20 o 17 3 0 50.23 53.61 22.82 o 18 3 0 15.67 -2.95 26.21 o 0 4 0 630.14 586.02 32.09 o 1 4 0 1482.32 1537.73 35.20 o 2 4 0 530.64 526.30 21.73 o 3 4 0 1230.14 1277.24 31.57 o 4 4 0 130.99 113.89 15.65 o 5 4 0 2341.92 2614.80 54.34 o 6 4 0 0.08 0.12 9.54 o 7 4 0 639.18 663.01 28.44 o 8 4 0 238.70 198.49 24.34 o 9 4 0 190.28 169.22 23.54 o 10 4 0 307.24 343.09 32.45 o 11 4 0 79.84 66.19 19.34 o 12 4 0 197.02 246.62 29.99 o 13 4 0 32.88 18.75 17.87 o 14 4 0 315.99 298.62 33.81 o 15 4 0 197.92 189.99 35.17 o 16 4 0 28.21 8.52 26.57 o 1 5 0 1245.00 1437.52 44.17 o 2 5 0 2532.89 2801.72 61.83 o 3 5 0 1411.62 1619.02 47.78 o 4 5 0 599.43 595.82 30.53 o 5 5 0 19.30 25.58 13.69 o 6 5 0 609.41 629.06 40.07 o 7 5 0 44.23 26.71 17.58 o 8 5 0 17.89 13.10 18.14 o 9 5 0 245.72 240.81 30.44 o 10 5 0 1.14 -10.61 18.49 o 11 5 0 23.77 44.66 25.91 o 12 5 0 0.00 6.23 23.39 o 13 5 0 334.64 404.43 48.45 o 14 5 0 19.40 13.41 27.89 o 0 6 0 581.10 507.51 56.34 o 1 6 0 322.27 288.48 32.01 o 2 6 0 60.04 45.51 20.84 o 3 6 0 40.92 56.94 22.44 o 4 6 0 2.86 -10.98 16.87 o 5 6 0 42.38 38.02 22.01 o 6 6 0 15.64 29.81 22.63 o 7 6 0 30.93 46.40 26.47 o 8 6 0 19.29 21.31 25.22 o 9 6 0 23.71 26.17 28.02 o 10 6 0 0.22 9.55 28.12 o 11 6 0 51.55 91.05 36.54 o 1 7 0 5.45 0.00 30.33 o 2 7 0 0.02 -14.55 30.18 o 3 7 0 2.29 10.60 36.84 o 4 7 0 1.58 -10.95 36.69 o 5 7 0 80.73 44.01 43.09 o -20 1 1 9.85 1.43 23.41 o -19 1 1 169.35 146.77 28.82 o -18 1 1 226.11 225.78 29.98 o -17 1 1 8.94 13.33 16.34 o -16 1 1 6.62 0.38 12.50 o -15 1 1 149.20 130.57 18.47 o -14 1 1 19.87 14.17 9.92 o -13 1 1 498.65 504.89 22.85 o -12 1 1 121.93 111.74 11.96 o -11 1 1 475.45 436.40 17.32 o -10 1 1 1545.49 1639.89 33.54 o -9 1 1 43.50 26.41 6.04 o -8 1 1 4381.83 4903.09 43.61 o -7 1 1 1287.71 1459.51 22.22 o -6 1 1 73.86 56.46 5.89 o -5 1 1 16419.49 18071.43 103.07 o -4 1 1 4644.28 5164.53 49.20 o -3 1 1 12347.50 13505.78 56.97 o -2 1 1 4855.91 5358.70 82.82 o -1 1 1 378.09 377.21 8.94 o 0 1 1 578.29 605.59 13.49 o 1 1 1 226.63 213.22 6.04 o 2 1 1 3770.25 4072.02 57.18 o 3 1 1 326.26 333.75 7.75 o 4 1 1 97.25 74.42 5.72 o 5 1 1 250.68 228.14 8.69 o 6 1 1 13.24 4.30 3.75 o 7 1 1 1561.87 1707.69 45.78 o 8 1 1 20.06 8.22 4.84 o 9 1 1 1090.86 1124.09 23.87 o 10 1 1 226.75 206.76 13.22 o 11 1 1 516.57 504.78 18.76 o 12 1 1 451.39 439.46 19.03 o 13 1 1 78.85 49.62 11.95 o 14 1 1 85.98 63.70 14.60 o 15 1 1 62.77 43.31 14.92 o 16 1 1 91.16 82.85 17.37 o 17 1 1 612.01 596.67 39.94 o 18 1 1 12.01 -3.41 17.62 o 19 1 1 6.05 0.53 25.14 o -19 2 1 87.72 66.60 24.32 o -18 2 1 10.11 14.06 21.29 o -17 2 1 202.58 193.21 26.47 o -16 2 1 125.41 118.21 21.37 o -15 2 1 47.10 23.33 13.85 o -14 2 1 70.68 74.83 16.79 o -13 2 1 67.31 66.88 15.38 o -12 2 1 499.30 476.18 28.04 o -11 2 1 836.18 856.35 33.83 o -10 2 1 23.77 13.97 6.57 o -9 2 1 1625.58 1658.04 27.24 o -8 2 1 67.96 39.49 6.72 o -7 2 1 7.76 2.24 4.39 o -6 2 1 560.39 535.38 20.50 o -5 2 1 111.11 126.73 8.07 o -4 2 1 982.28 917.27 18.35 o -3 2 1 270.47 275.94 10.73 o -2 2 1 57.11 73.14 7.04 o -1 2 1 1987.24 2023.98 41.30 o 0 2 1 125.09 154.35 9.53 o 1 2 1 285.91 223.71 10.17 o 2 2 1 174.36 150.77 8.52 o 3 2 1 2376.82 2560.11 55.91 o 4 2 1 40.54 44.60 7.57 o 5 2 1 267.18 272.32 14.19 o 6 2 1 550.92 575.19 20.96 o 7 2 1 246.63 245.95 14.45 o 8 2 1 452.84 465.79 13.90 o 9 2 1 42.90 40.66 7.28 o 10 2 1 916.93 1026.64 35.47 o 11 2 1 308.03 290.58 18.52 o 12 2 1 7.81 -2.41 9.97 o 13 2 1 23.25 23.13 12.83 o 14 2 1 30.17 18.49 13.59 o 15 2 1 48.98 49.36 16.54 o 16 2 1 10.82 10.14 16.10 o 17 2 1 115.17 89.50 22.51 o 18 2 1 80.44 56.31 25.96 o -18 3 1 56.70 31.44 21.08 o -17 3 1 96.04 73.60 23.47 o -16 3 1 98.75 84.66 22.16 o -15 3 1 110.56 118.15 22.13 o -14 3 1 0.23 -3.67 14.35 o -13 3 1 393.86 402.50 32.82 o -12 3 1 99.27 81.83 17.80 o -11 3 1 590.62 577.76 33.33 o -10 3 1 950.59 913.23 37.82 o -9 3 1 0.15 -10.88 9.56 o -8 3 1 1195.77 1297.11 31.38 o -7 3 1 435.71 451.62 20.89 o -6 3 1 735.45 757.45 21.17 o -5 3 1 168.03 159.31 13.45 o -4 3 1 49.80 29.70 7.22 o -3 3 1 1849.22 1982.48 34.37 o -2 3 1 1195.32 1270.37 27.92 o -1 3 1 213.62 168.72 12.53 o 0 3 1 549.98 533.99 17.27 o 1 3 1 692.06 681.56 20.87 o 2 3 1 1390.62 1355.78 27.54 o 3 3 1 0.97 -0.34 5.65 o 4 3 1 898.04 876.67 27.69 o 5 3 1 643.84 607.83 23.25 o 6 3 1 493.94 520.52 21.93 o 7 3 1 612.36 578.26 23.14 o 8 3 1 23.28 14.71 8.92 o 9 3 1 726.72 789.98 27.48 o 10 3 1 256.79 199.84 22.94 o 11 3 1 217.68 241.53 25.64 o 12 3 1 337.77 326.52 29.87 o 13 3 1 2.77 -5.63 13.98 o 14 3 1 19.80 27.81 17.39 o 15 3 1 0.02 -6.42 17.03 o 16 3 1 112.01 134.78 42.20 o 17 3 1 25.43 -3.94 22.10 o -16 4 1 98.98 101.20 28.01 o -15 4 1 0.11 -9.67 18.64 o -14 4 1 5.63 -1.68 17.96 o -13 4 1 1.08 -8.46 17.23 o -12 4 1 54.26 27.25 17.79 o -11 4 1 50.75 34.09 17.11 o -10 4 1 5.10 1.69 14.57 o -9 4 1 239.84 224.78 32.95 o -8 4 1 430.81 450.41 33.34 o -7 4 1 822.41 862.44 31.31 o -6 4 1 176.03 166.45 16.88 o -5 4 1 307.54 304.94 22.57 o -4 4 1 362.33 364.21 18.90 o -3 4 1 348.66 354.48 19.62 o -2 4 1 1198.81 1272.09 32.47 o -1 4 1 118.55 92.73 12.64 o 0 4 1 185.24 181.56 16.02 o 1 4 1 53.85 37.55 10.09 o 2 4 1 48.21 30.65 9.52 o 3 4 1 4.97 -4.90 9.69 o 4 4 1 548.76 541.51 25.81 o 5 4 1 12.92 6.44 10.30 o 6 4 1 150.09 119.52 16.70 o 7 4 1 1.34 -0.82 10.29 o 8 4 1 158.53 153.69 18.16 o 9 4 1 1.94 2.08 12.98 o 10 4 1 89.57 60.96 18.06 o 11 4 1 210.23 145.47 23.23 o 12 4 1 40.22 27.31 17.82 o 13 4 1 21.14 11.69 20.36 o 14 4 1 3.45 5.63 22.10 o 15 4 1 30.63 33.41 25.37 o 16 4 1 29.28 24.22 26.06 o -14 5 1 10.79 1.43 26.15 o -13 5 1 89.23 106.98 31.55 o -12 5 1 12.75 5.74 20.15 o -11 5 1 35.15 58.16 22.62 o -10 5 1 93.90 70.46 22.08 o -9 5 1 11.03 10.50 18.02 o -8 5 1 211.98 210.19 28.04 o -7 5 1 151.69 135.44 24.55 o -6 5 1 49.46 45.68 18.45 o -5 5 1 555.01 504.64 34.62 o -4 5 1 112.30 96.12 17.78 o -3 5 1 686.87 716.46 32.36 o -2 5 1 43.98 37.28 14.17 o -1 5 1 24.80 20.24 11.40 o 0 5 1 30.42 11.86 13.13 o 1 5 1 20.93 18.32 13.13 o 2 5 1 289.84 286.21 24.80 o 3 5 1 1.10 -0.76 12.66 o 4 5 1 80.17 72.70 16.11 o 5 5 1 45.49 39.46 14.58 o 6 5 1 63.91 60.42 16.86 o 7 5 1 271.51 281.64 31.72 o 8 5 1 15.39 5.93 17.64 o 9 5 1 123.80 119.46 26.33 o 10 5 1 37.47 35.22 24.34 o 11 5 1 36.80 39.06 24.20 o 12 5 1 65.79 64.98 29.20 o 13 5 1 25.27 28.53 27.65 o 14 5 1 12.06 11.79 27.41 o -11 6 1 165.29 262.63 42.11 o -10 6 1 22.12 10.54 25.77 o -9 6 1 229.32 290.74 42.10 o -8 6 1 225.98 280.50 36.44 o -7 6 1 345.47 415.47 40.87 o -6 6 1 434.15 573.19 45.31 o -5 6 1 0.91 -1.79 19.88 o -4 6 1 517.77 571.07 40.61 o -3 6 1 223.90 208.45 28.78 o -2 6 1 347.38 356.50 35.31 o -1 6 1 100.61 85.17 23.26 o 0 6 1 65.31 53.23 19.75 o 1 6 1 194.50 185.10 28.07 o 2 6 1 0.11 1.37 18.11 o 3 6 1 30.52 21.96 18.64 o 4 6 1 129.63 131.79 23.03 o 5 6 1 100.14 104.09 29.33 o 6 6 1 25.34 12.83 25.79 o 7 6 1 19.83 9.25 24.13 o 8 6 1 87.70 66.79 29.48 o 9 6 1 7.02 3.61 26.05 o 10 6 1 60.59 63.07 34.43 o -5 7 1 0.26 -8.00 37.19 o -4 7 1 5.15 8.75 38.96 o -3 7 1 200.58 190.62 38.37 o -2 7 1 75.07 65.18 32.53 o -1 7 1 3.19 -0.83 29.20 o 0 7 1 10.62 20.67 30.46 o 1 7 1 54.58 43.43 32.86 o 2 7 1 155.61 209.36 42.34 o 3 7 1 15.23 41.00 36.65 o 4 7 1 267.58 334.81 86.40 o -20 0 2 300.11 334.83 61.95 o -19 0 2 90.58 51.97 30.09 o -18 0 2 154.04 142.40 39.42 o -17 0 2 41.38 46.36 23.37 o -16 0 2 413.31 423.94 40.12 o -15 0 2 410.85 378.40 35.82 o -14 0 2 16.30 14.77 13.84 o -13 0 2 1999.70 2137.74 56.19 o -12 0 2 183.43 161.75 18.86 o -11 0 2 1196.98 1205.07 36.88 o -10 0 2 4726.24 5323.45 72.72 o -9 0 2 3122.75 3429.47 70.41 o -8 0 2 868.46 812.58 26.13 o -7 0 2 3284.98 3821.35 57.95 o -6 0 2 4726.79 5159.28 61.29 o -5 0 2 152.62 162.23 9.73 o -4 0 2 14705.25 16275.33 214.72 o -3 0 2 3799.20 4200.40 36.50 o -2 0 2 765.04 764.86 17.69 o -1 0 2 14450.33 14200.52 208.61 o 0 0 2 1012.16 926.66 17.10 o 1 0 2 1365.18 1306.54 26.59 o 2 0 2 9547.43 9685.47 318.53 o 3 0 2 689.26 720.49 17.26 o 4 0 2 3843.07 4140.95 112.31 o 5 0 2 579.16 587.38 18.85 o 6 0 2 2403.47 2389.45 40.01 o 7 0 2 820.12 878.52 27.12 o 8 0 2 145.33 115.43 13.59 o 9 0 2 1400.49 1402.75 38.44 o 10 0 2 12.71 6.90 8.60 o 11 0 2 98.85 83.63 15.46 o 12 0 2 58.71 66.23 14.76 o 13 0 2 1726.24 1953.82 57.19 o 14 0 2 31.55 18.23 14.33 o 15 0 2 956.78 931.64 44.63 o 16 0 2 844.09 944.64 73.69 o 17 0 2 16.86 12.55 29.12 o 18 0 2 1183.15 1327.26 94.13 o 19 0 2 39.76 12.07 32.82 o -20 1 2 193.71 179.60 33.07 o -19 1 2 325.82 381.40 37.81 o -18 1 2 33.59 19.20 17.41 o -17 1 2 118.70 134.40 24.28 o -16 1 2 4.20 -7.45 11.39 o -15 1 2 39.75 30.31 11.97 o -14 1 2 436.88 374.29 23.52 o -13 1 2 8.49 1.85 8.24 o -12 1 2 28.55 11.78 7.75 o -11 1 2 620.71 597.69 19.25 o -10 1 2 0.24 -0.65 5.44 o -9 1 2 526.16 482.28 18.50 o -8 1 2 476.97 487.69 14.00 o -7 1 2 1068.81 1030.48 18.15 o -6 1 2 12.61 11.55 3.50 o -5 1 2 780.30 781.22 16.16 o -4 1 2 2785.09 2977.10 44.49 o -3 1 2 45.45 48.90 4.46 o -2 1 2 21254.27 23151.25 161.98 o -1 1 2 7144.17 7666.52 69.56 o 0 1 2 8559.13 8940.46 45.37 o 1 1 2 2059.61 2046.44 19.40 o 2 1 2 152.22 117.61 5.41 o 3 1 2 3.53 -0.43 2.61 o 4 1 2 2543.28 2923.68 34.69 o 5 1 2 169.19 138.12 7.93 o 6 1 2 927.13 1003.72 20.80 o 7 1 2 255.16 272.78 16.79 o 8 1 2 1134.60 1241.67 24.38 o 9 1 2 177.86 180.79 12.48 o 10 1 2 18.17 14.46 6.68 o 11 1 2 270.73 225.21 14.81 o 12 1 2 282.79 272.45 17.59 o 13 1 2 419.79 396.13 22.03 o 14 1 2 62.27 38.02 14.08 o 15 1 2 230.03 205.64 24.00 o 16 1 2 5.56 -13.94 13.42 o 17 1 2 209.13 211.95 29.87 o 18 1 2 176.82 144.90 31.35 o 19 1 2 135.02 124.57 33.30 o -19 2 2 4.95 -8.67 20.60 o -18 2 2 74.59 73.11 22.83 o -17 2 2 5.46 3.31 16.37 o -16 2 2 41.88 28.12 16.07 o -15 2 2 129.64 82.57 17.39 o -14 2 2 12.26 7.02 12.46 o -13 2 2 238.51 243.98 23.51 o -12 2 2 74.87 50.56 14.17 o -11 2 2 1.33 -3.85 7.48 o -10 2 2 99.94 63.74 10.37 o -9 2 2 64.65 58.07 7.93 o -8 2 2 23.50 10.35 5.19 o -7 2 2 71.59 67.11 6.89 o -6 2 2 320.09 341.02 11.47 o -5 2 2 82.73 67.42 6.87 o -4 2 2 1622.12 1796.88 26.24 o -3 2 2 151.50 137.14 9.31 o -2 2 2 42.19 31.61 5.93 o -1 2 2 979.86 1016.04 20.38 o 0 2 2 93.64 74.37 7.16 o 1 2 2 4946.21 5694.11 59.81 o 2 2 2 1607.75 1723.20 35.37 o 3 2 2 2.68 1.82 4.97 o 4 2 2 16.79 7.80 5.52 o 5 2 2 69.35 57.99 8.46 o 6 2 2 223.36 236.06 13.80 o 7 2 2 102.71 93.89 10.53 o 8 2 2 10.83 9.76 5.62 o 9 2 2 66.58 51.49 10.18 o 10 2 2 408.22 416.77 21.02 o 11 2 2 3.11 2.86 8.76 o 12 2 2 463.31 393.36 27.26 o 13 2 2 43.16 34.87 13.06 o 14 2 2 3.63 -5.53 12.87 o 15 2 2 0.72 5.51 14.53 o 16 2 2 0.71 -0.60 16.76 o 17 2 2 4.54 -5.16 19.08 o 18 2 2 71.27 74.75 35.68 o -18 3 2 194.19 173.47 30.46 o -17 3 2 57.19 41.48 21.41 o -16 3 2 483.58 499.68 49.23 o -15 3 2 208.21 208.09 26.54 o -14 3 2 222.65 236.02 26.80 o -13 3 2 195.33 180.91 24.00 o -12 3 2 199.21 172.84 22.07 o -11 3 2 26.97 16.54 12.14 o 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