#------------------------------------------------------------------------------
#$Date: 2018-12-07 05:37:15 +0200 (Fri, 07 Dec 2018) $
#$Revision: 212436 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/83/2108344.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108344
_cell_angle_alpha                90.000
_cell_angle_beta                 102.769
_cell_angle_gamma                90.000
_cell_length_a                   19.5017
_cell_length_b                   5.2408
_cell_length_c                   16.4695
_exptl_crystal_F_000             2407.20
_reflns_d_resolution_high        0.7572
_cod_data_source_file            ps5074CuPb324sup6.hkl
_cod_data_source_block           CuPb324
_shelx_title                     ' mo_r765765_0m in C2/m'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1337.99
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 106.35 273.70 59.05 o
4 0 0 3417.33 2538.16 307.24 o
6 0 0 86241.87 81151.28 1289.04 o
8 0 0 44656.32 43354.05 889.61 o
10 0 0 301.79 1144.69 293.08 o
12 0 0 42046.75 39502.81 840.48 o
14 0 0 1108.38 1002.99 263.56 o
16 0 0 5099.80 5296.28 370.48 o
18 0 0 113261.35 117888.34 2020.66 o
20 0 0 33773.61 33091.75 1158.17 o
22 0 0 37.08 414.86 419.10 o
24 0 0 10181.12 11118.62 1663.08 o
1 1 0 5377.11 5432.70 166.32 o
3 1 0 16402.47 16283.86 228.86 o
5 1 0 596569.69 609295.88 5482.23 o
7 1 0 704.03 940.24 127.80 o
9 1 0 29426.38 33152.05 473.34 o
11 1 0 49954.10 43720.29 597.47 o
13 1 0 99017.87 100720.84 1779.67 o
15 1 0 271784.09 266142.12 3092.51 o
17 1 0 776.56 829.14 199.05 o
19 1 0 5079.54 6484.72 333.53 o
21 1 0 78283.42 74607.91 1435.78 o
23 1 0 4204.00 4993.81 661.17 o
0 2 0 1790214.88 1956420.25 28613.81 o
2 2 0 15.54 104.91 111.70 o
4 2 0 4220.74 6677.09 179.04 o
6 2 0 98043.66 96587.36 1021.86 o
8 2 0 164009.53 167881.70 1817.78 o
10 2 0 41.72 662.37 201.85 o
12 2 0 3185.84 3950.31 320.20 o
14 2 0 452.83 669.66 469.61 o
16 2 0 660.26 714.48 353.61 o
18 2 0 81753.70 84012.39 1807.66 o
20 2 0 26767.56 28066.30 1143.82 o
22 2 0 24.83 -370.80 504.55 o
24 2 0 9497.74 9644.82 787.32 o
1 3 0 987.37 989.40 119.91 o
3 3 0 11000.01 10457.67 268.58 o
5 3 0 268631.94 282143.59 2737.85 o
7 3 0 7944.95 8291.41 312.49 o
9 3 0 4211.74 4181.78 288.97 o
11 3 0 37794.44 41070.62 952.50 o
13 3 0 71477.34 69143.17 1424.02 o
15 3 0 171439.00 168527.58 3435.13 o
17 3 0 554.18 189.46 658.99 o
19 3 0 7024.22 6294.71 685.51 o
21 3 0 43888.14 46661.82 1869.14 o
0 4 0 1135628.00 1158262.62 16771.61 o
2 4 0 11907.65 13788.16 663.10 o
4 4 0 2890.84 4291.70 202.56 o
6 4 0 23077.88 25960.52 805.95 o
8 4 0 31706.19 30544.66 1195.76 o
10 4 0 123.10 291.04 513.27 o
12 4 0 3087.61 4375.60 744.45 o
14 4 0 5917.15 6218.87 902.65 o
16 4 0 160.78 1631.77 1010.41 o
18 4 0 47289.89 41808.30 2341.20 o
20 4 0 17196.06 20128.92 1893.41 o
1 5 0 22.58 -294.42 170.81 o
3 5 0 8460.42 8409.82 875.09 o
5 5 0 96066.95 93514.03 2044.83 o
7 5 0 11136.38 13998.12 912.46 o
9 5 0 146.97 984.98 575.66 o
11 5 0 19758.94 26836.99 1434.46 o
13 5 0 43777.58 37441.91 1730.69 o
15 5 0 83474.96 79759.20 3214.68 o
17 5 0 768.91 602.17 1131.23 o
0 6 0 255194.08 230813.27 5418.31 o
2 6 0 7665.23 12645.52 517.78 o
4 6 0 155.01 1371.52 367.49 o
6 6 0 12597.24 16549.26 781.08 o
8 6 0 40168.81 37567.59 2552.91 o
10 6 0 217.66 -93.45 920.22 o
12 6 0 1309.62 2844.66 864.90 o
-24 0 1 736.51 1270.27 393.41 o
-22 0 1 14211.22 13145.57 658.53 o
-20 0 1 250.50 533.76 337.38 o
-18 0 1 29336.10 30948.49 847.05 o
-16 0 1 86637.74 81358.54 1525.89 o
-14 0 1 3059.83 2138.40 284.26 o
-12 0 1 2130.17 2761.07 272.72 o
-10 0 1 1851.27 2005.19 246.18 o
-8 0 1 55111.21 49614.43 996.10 o
-6 0 1 155444.83 149313.31 2418.78 o
-4 0 1 2671.50 4520.73 399.25 o
-2 0 1 189981.95 177243.83 4342.19 o
2 0 1 37212.54 33857.56 462.83 o
4 0 1 112577.53 107308.14 1717.48 o
6 0 1 306722.81 314767.12 4437.43 o
8 0 1 2883.36 2966.74 246.61 o
10 0 1 209367.59 201052.58 2664.83 o
12 0 1 64111.61 61263.34 1500.97 o
14 0 1 1010.69 851.71 228.79 o
16 0 1 15532.34 15409.55 529.47 o
18 0 1 14810.97 14717.61 843.56 o
20 0 1 9312.38 10356.30 462.48 o
22 0 1 3028.62 5231.10 1510.01 o
24 0 1 2288.02 3613.16 1509.98 o
-25 1 1 6839.64 6936.89 1869.68 o
-23 1 1 16137.08 16192.27 916.34 o
-21 1 1 13950.29 15929.70 627.24 o
-19 1 1 11927.09 10710.10 404.72 o
-17 1 1 684.91 933.98 213.51 o
-15 1 1 3924.14 4594.59 250.88 o
-13 1 1 275.54 -61.77 155.20 o
-11 1 1 358166.50 349644.62 3446.13 o
-9 1 1 111511.55 105992.27 1083.63 o
-7 1 1 135663.84 125798.62 1261.73 o
-5 1 1 14063.50 14516.09 262.85 o
-3 1 1 11052.47 10285.46 307.07 o
-1 1 1 4058.63 5412.90 161.35 o
1 1 1 5668.98 5502.28 190.36 o
3 1 1 169253.22 167784.33 1887.01 o
5 1 1 55422.90 61383.31 850.40 o
7 1 1 39777.03 38680.87 697.21 o
9 1 1 7594.71 5060.40 223.58 o
11 1 1 11180.10 11357.62 287.22 o
13 1 1 29938.80 29324.63 537.87 o
15 1 1 61870.89 57827.80 1120.33 o
17 1 1 56323.65 54404.42 1645.70 o
19 1 1 9328.23 8254.76 542.77 o
21 1 1 46807.76 45062.13 1019.00 o
23 1 1 12394.58 12332.41 656.48 o
-24 2 1 2539.77 2943.95 797.52 o
-22 2 1 11832.23 15016.25 896.92 o
-20 2 1 118.89 1132.32 505.34 o
-18 2 1 15427.24 16863.08 812.34 o
-16 2 1 30057.01 30196.84 599.95 o
-14 2 1 848.21 1316.49 185.83 o
-12 2 1 5585.10 5357.48 209.25 o
-10 2 1 641.59 1235.61 141.13 o
-8 2 1 3781.20 3151.75 165.03 o
-6 2 1 119411.60 121012.48 1205.29 o
-4 2 1 1795.93 1155.56 113.61 o
-2 2 1 61150.61 62027.48 764.71 o
0 2 1 5752.94 4564.88 151.90 o
2 2 1 12354.45 12671.14 274.96 o
4 2 1 97009.70 93858.54 1081.89 o
6 2 1 145141.69 144507.23 1893.19 o
8 2 1 34948.04 32272.44 636.31 o
10 2 1 165792.27 165810.03 2093.98 o
12 2 1 103878.01 100430.24 1684.40 o
14 2 1 15244.40 15124.66 703.52 o
16 2 1 17610.27 16314.39 934.49 o
18 2 1 11043.73 11058.84 1253.50 o
20 2 1 513.64 1697.16 461.60 o
22 2 1 6203.16 6857.03 671.29 o
-21 3 1 15536.38 14657.40 941.62 o
-19 3 1 10637.58 12127.26 830.81 o
-17 3 1 353.26 800.30 483.05 o
-15 3 1 2590.43 2480.43 454.21 o
-13 3 1 2432.82 2819.12 374.28 o
-11 3 1 184943.91 181269.53 2447.85 o
-9 3 1 39827.48 42503.50 724.25 o
-7 3 1 58861.56 59499.88 729.27 o
-5 3 1 8732.96 8954.67 367.34 o
-3 3 1 4489.87 5348.18 312.83 o
-1 3 1 3300.86 4357.90 174.57 o
1 3 1 6577.84 7355.14 220.04 o
3 3 1 57707.96 60922.44 811.28 o
5 3 1 7093.97 9609.42 334.49 o
7 3 1 11366.86 10635.93 363.61 o
9 3 1 9180.52 10002.83 426.82 o
11 3 1 10579.39 9722.43 486.98 o
13 3 1 21809.15 20485.20 820.39 o
15 3 1 35410.71 37602.90 1094.88 o
17 3 1 25593.69 27654.05 1148.82 o
19 3 1 2052.14 1128.61 1081.33 o
21 3 1 26227.78 25007.12 1213.76 o
-20 4 1 1290.83 2819.41 1251.56 o
-18 4 1 3880.49 2945.28 1188.46 o
-16 4 1 20682.76 24131.03 1805.26 o
-14 4 1 146.23 535.33 688.19 o
-12 4 1 906.94 986.05 574.06 o
-10 4 1 478.21 777.08 507.52 o
-8 4 1 11719.54 13019.65 426.90 o
-6 4 1 57970.10 53889.68 832.69 o
-4 4 1 6453.64 7952.53 374.90 o
-2 4 1 18291.17 17553.72 886.80 o
0 4 1 15700.15 16724.97 689.87 o
2 4 1 10486.10 10436.24 553.84 o
4 4 1 25641.99 24890.05 683.34 o
6 4 1 88899.26 83019.73 1574.74 o
8 4 1 8784.96 7378.05 702.05 o
10 4 1 46890.92 48600.89 1581.91 o
12 4 1 9496.18 9504.83 1240.18 o
14 4 1 6827.63 9323.21 1191.73 o
16 4 1 7753.56 5082.63 1162.74 o
18 4 1 5443.94 8008.07 1357.32 o
20 4 1 7818.49 8124.07 1464.95 o
-17 5 1 181.88 1385.07 1154.75 o
-15 5 1 1595.00 720.79 826.49 o
-13 5 1 4976.72 9762.46 1028.15 o
-11 5 1 72419.65 64111.66 2042.22 o
-9 5 1 6893.52 8584.08 800.71 o
-7 5 1 17639.26 19483.14 1240.19 o
-5 5 1 2911.45 3682.60 393.54 o
-3 5 1 358.53 545.15 187.48 o
-1 5 1 2215.17 2272.99 222.83 o
1 5 1 10097.52 11811.88 501.77 o
3 5 1 10839.75 10022.45 476.41 o
5 5 1 680.96 2876.82 583.85 o
7 5 1 1239.05 337.91 543.92 o
9 5 1 4925.51 7045.65 853.46 o
11 5 1 6916.03 5838.51 1420.59 o
13 5 1 10718.80 11872.52 1116.08 o
15 5 1 18942.51 25249.32 1968.98 o
17 5 1 6423.66 8539.16 1512.57 o
-12 6 1 555.07 640.76 751.29 o
-10 6 1 2543.96 4486.37 790.04 o
-8 6 1 388.81 1384.15 417.96 o
-6 6 1 22779.56 17737.14 1096.67 o
-4 6 1 12124.44 16185.46 1339.22 o
-2 6 1 1425.57 1308.03 636.28 o
0 6 1 10027.60 15291.32 753.37 o
2 6 1 4678.17 3764.67 448.88 o
4 6 1 7656.82 9451.48 576.49 o
6 6 1 24359.20 23305.34 1175.45 o
8 6 1 15726.25 15634.58 1155.18 o
10 6 1 17284.72 16496.91 1226.24 o
12 6 1 7718.18 5721.46 1001.38 o
-24 0 2 6582.17 6797.34 1406.40 o
-22 0 2 2954.30 2152.22 555.26 o
-20 0 2 101896.66 100769.02 1872.63 o
-18 0 2 19043.16 17898.11 763.20 o
-16 0 2 65698.79 61503.56 2314.09 o
-14 0 2 12372.45 13577.07 902.04 o
-12 0 2 1530.06 2903.34 479.08 o
-10 0 2 170544.44 159426.56 2690.35 o
-8 0 2 467711.97 481619.06 7393.07 o
-6 0 2 76344.18 68316.07 1234.44 o
-4 0 2 1949.15 2128.63 146.34 o
-2 0 2 9.01 -47.65 117.47 o
0 0 2 21893.71 16248.21 668.12 o
2 0 2 23461.11 20176.01 821.97 o
4 0 2 25762.33 26166.12 728.37 o
6 0 2 168234.70 156911.09 2171.97 o
8 0 2 182.40 562.82 146.84 o
10 0 2 517656.28 507597.91 11788.51 o
12 0 2 9643.00 9823.88 354.45 o
14 0 2 22078.66 22771.03 565.50 o
16 0 2 103822.59 101019.85 1670.81 o
18 0 2 11354.70 9884.91 539.30 o
20 0 2 6638.43 7011.45 1492.18 o
22 0 2 17138.58 16723.64 2014.03 o
24 0 2 400.41 898.76 1330.16 o
-25 1 2 37979.96 37987.58 1778.59 o
-23 1 2 8916.23 9198.32 431.24 o
-21 1 2 2461.41 2527.21 305.38 o
-19 1 2 4436.25 4123.54 301.18 o
-17 1 2 1151.40 1543.87 286.08 o
-15 1 2 21584.09 22293.79 642.59 o
-13 1 2 102683.16 103935.09 1227.23 o
-11 1 2 1308.29 1738.40 177.47 o
-9 1 2 78090.21 78307.02 918.56 o
-7 1 2 16763.68 15285.28 456.40 o
-5 1 2 402454.44 396443.72 3707.15 o
-3 1 2 20595.98 21659.69 303.70 o
-1 1 2 7594.51 8826.72 397.27 o
1 1 2 125323.05 130843.30 1457.12 o
3 1 2 1374.15 1630.19 175.43 o
5 1 2 312082.09 319105.38 3778.05 o
7 1 2 29901.56 29882.91 570.54 o
9 1 2 15181.60 14738.52 485.04 o
11 1 2 4072.63 5137.39 271.58 o
13 1 2 16686.16 15128.39 513.10 o
15 1 2 113411.79 110971.84 1791.86 o
17 1 2 228.87 682.40 288.12 o
19 1 2 4048.35 4076.74 462.41 o
21 1 2 34424.86 34847.15 985.87 o
23 1 2 1437.24 1177.21 404.05 o
-24 2 2 4795.94 3621.86 670.77 o
-22 2 2 337.06 931.07 557.54 o
-20 2 2 105209.48 104738.51 1621.79 o
-18 2 2 4025.23 4770.97 312.18 o
-16 2 2 41723.08 41526.21 782.08 o
-14 2 2 3035.69 3280.73 268.00 o
-12 2 2 712.33 866.05 152.96 o
-10 2 2 164801.98 162303.25 1815.85 o
-8 2 2 286343.75 289687.78 2813.69 o
-6 2 2 51734.55 50946.19 669.29 o
-4 2 2 5609.91 8481.49 239.15 o
-2 2 2 5828.04 7383.90 210.07 o
0 2 2 1884.99 1452.26 126.51 o
2 2 2 2001.83 3734.89 185.73 o
4 2 2 217.46 695.14 168.15 o
6 2 2 115980.48 118252.38 1494.74 o
8 2 2 3147.65 2663.06 230.22 o
10 2 2 497191.72 491234.03 6803.15 o
12 2 2 11604.71 11668.10 511.52 o
14 2 2 13500.49 13320.43 629.74 o
16 2 2 86017.62 85033.80 2015.71 o
18 2 2 4125.90 4481.13 673.45 o
20 2 2 6074.43 7063.24 796.62 o
22 2 2 9448.71 9289.00 843.39 o
-23 3 2 7387.53 6066.37 1689.93 o
-21 3 2 2552.48 2188.11 1147.77 o
-19 3 2 2012.22 2099.67 1072.66 o
-17 3 2 153.05 -108.11 863.18 o
-15 3 2 8936.06 9259.16 448.99 o
-13 3 2 43159.64 45340.98 1204.57 o
-11 3 2 441.92 803.83 181.44 o
-9 3 2 51622.27 47308.30 668.68 o
-7 3 2 12541.36 13503.17 355.66 o
-5 3 2 232438.67 228955.16 2417.27 o
-3 3 2 12004.89 13065.17 306.29 o
-1 3 2 9461.02 9281.70 322.73 o
1 3 2 43307.70 47176.90 676.91 o
3 3 2 5866.57 6735.65 252.72 o
5 3 2 171678.31 175143.22 1945.27 o
7 3 2 14318.95 15399.03 501.60 o
9 3 2 5061.10 4520.15 485.90 o
11 3 2 2061.37 1467.57 306.98 o
13 3 2 4366.15 5831.41 473.18 o
15 3 2 57956.75 62453.33 1470.44 o
17 3 2 2796.79 2347.91 520.28 o
19 3 2 1720.88 1469.88 531.96 o
21 3 2 24863.39 28622.87 1245.66 o
-20 4 2 31854.17 34165.62 2330.88 o
-18 4 2 2049.69 3634.59 1220.04 o
-16 4 2 23509.21 28283.52 1578.17 o
-14 4 2 4351.72 4360.31 804.88 o
-12 4 2 1183.13 1227.55 356.44 o
-10 4 2 87645.36 94303.64 1672.62 o
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-6 4 2 5437.29 7180.71 430.50 o
-4 4 2 7286.50 8391.37 413.90 o
-2 4 2 1314.41 1445.11 172.23 o
0 4 2 5394.53 5972.52 354.21 o
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4 4 2 5839.20 6747.76 345.69 o
6 4 2 42025.16 48148.56 1443.40 o
8 4 2 11712.13 11812.47 826.93 o
10 4 2 156068.00 147852.28 3386.13 o
12 4 2 853.49 1276.81 808.72 o
14 4 2 12354.10 10386.46 744.91 o
16 4 2 44948.77 43647.85 1467.89 o
18 4 2 4214.36 4812.37 717.35 o
-17 5 2 90.12 462.37 871.39 o
-15 5 2 1412.39 2473.69 1001.54 o
-13 5 2 8532.94 9724.62 1002.69 o
-11 5 2 2947.37 2000.13 647.52 o
-9 5 2 30376.89 27837.97 1497.55 o
-7 5 2 12282.89 13484.10 419.37 o
-5 5 2 93000.74 94282.18 1291.65 o
-3 5 2 6265.94 7354.07 386.57 o
-1 5 2 7766.46 10182.50 486.90 o
1 5 2 7315.42 7176.00 436.77 o
3 5 2 10071.07 14728.93 989.04 o
5 5 2 65307.65 55816.93 1957.17 o
7 5 2 4927.76 9194.77 2036.74 o
9 5 2 992.28 1538.14 689.61 o
11 5 2 103.12 -150.26 666.15 o
13 5 2 977.56 2214.92 1033.92 o
15 5 2 20242.87 22559.45 1894.20 o
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0 6 2 222.01 595.59 322.67 o
2 6 2 1609.26 2625.56 405.02 o
4 6 2 168.59 713.87 573.28 o
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8 0 3 315776.38 337037.94 6423.88 o
10 0 3 147223.00 135803.52 2903.44 o
12 0 3 52981.71 52163.06 1923.44 o
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16 0 3 11609.62 10829.49 907.44 o
18 0 3 16222.55 23715.47 4261.98 o
20 0 3 12336.34 13701.25 1726.14 o
22 0 3 39119.86 42172.57 2914.66 o
24 0 3 128.15 -71.90 1222.30 o
-25 1 3 473.24 1923.96 364.94 o
-23 1 3 15499.30 15907.45 585.63 o
-21 1 3 15829.69 17478.22 737.33 o
-19 1 3 143.05 436.85 254.04 o
-17 1 3 11966.37 11852.10 412.18 o
-15 1 3 67935.91 65450.16 937.88 o
-13 1 3 99962.52 98985.70 1195.60 o
-11 1 3 102759.45 103459.13 1198.40 o
-9 1 3 2399.70 3048.94 223.16 o
-7 1 3 49110.52 45527.62 575.94 o
-5 1 3 675885.00 687627.50 6117.38 o
-3 1 3 81544.25 86827.91 940.08 o
-1 1 3 194919.56 194812.39 2123.97 o
1 1 3 2835.89 4818.41 208.57 o
3 1 3 460389.53 468925.78 5832.20 o
5 1 3 55326.64 47631.20 705.59 o
7 1 3 44829.05 50315.97 822.19 o
9 1 3 20091.21 19972.45 511.16 o
11 1 3 72.42 127.83 181.94 o
13 1 3 65957.42 65090.04 1088.03 o
15 1 3 7175.81 7571.76 355.35 o
17 1 3 5948.55 6131.35 366.44 o
19 1 3 24536.25 23997.44 679.11 o
21 1 3 20524.76 20582.63 1354.32 o
23 1 3 6193.63 7703.79 1135.12 o
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