#------------------------------------------------------------------------------
#$Date: 2018-12-07 05:37:15 +0200 (Fri, 07 Dec 2018) $
#$Revision: 212436 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/83/2108345.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108345
_cell_angle_alpha                90.000
_cell_angle_beta                 109.843
_cell_angle_gamma                90.000
_cell_length_a                   19.0489
_cell_length_b                   6.2255
_cell_length_c                   12.7255
_exptl_crystal_F_000             1926.00
_reflns_d_resolution_high        0.6947
_cod_data_source_file            ps5074CuPbOXO1sup7.hkl
_cod_data_source_block           CuPbOXO1
_shelx_title                     ' shelxt_a.res in C2/m'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            997.22
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 7308.55 6612.98 370.66 o
4 0 0 41735.61 40773.89 1097.72 o
6 0 0 64057.64 62267.80 2128.98 o
8 0 0 38024.97 38031.91 1316.77 o
10 0 0 152960.97 157184.11 3194.15 o
12 0 0 14159.89 14907.86 1034.61 o
14 0 0 25967.78 24829.71 1469.83 o
16 0 0 63553.52 68464.45 5069.16 o
18 0 0 69501.07 67742.38 3161.29 o
20 0 0 16314.84 19145.82 1987.92 o
22 0 0 17560.78 17968.80 2067.31 o
24 0 0 5919.88 3798.49 1817.99 o
1 1 0 35.88 -76.21 124.38 o
3 1 0 2475.27 2806.08 272.70 o
5 1 0 28702.96 29969.43 797.42 o
7 1 0 185135.58 182060.38 3076.26 o
9 1 0 3717.89 3851.69 482.63 o
11 1 0 49080.16 49391.64 1375.82 o
13 1 0 75.00 671.56 469.56 o
15 1 0 48152.43 51400.71 1611.07 o
17 1 0 51987.93 51015.96 1990.75 o
19 1 0 9414.88 9481.27 1076.06 o
21 1 0 20999.82 20654.07 1472.27 o
23 1 0 258.42 -381.73 865.90 o
25 1 0 405.43 -839.22 1313.39 o
0 2 0 950617.88 1011138.00 13576.50 o
2 2 0 94019.14 93573.70 1300.18 o
4 2 0 8752.36 9518.75 420.51 o
6 2 0 27200.15 27436.18 814.89 o
8 2 0 5133.03 4843.56 472.26 o
10 2 0 507761.53 508804.88 6904.52 o
12 2 0 16438.59 18213.78 894.57 o
14 2 0 47848.25 51421.82 1573.20 o
16 2 0 55027.96 52403.41 1646.48 o
18 2 0 22844.78 23388.07 1236.45 o
20 2 0 1281.27 390.85 854.16 o
22 2 0 57.90 -1392.83 1392.83 o
24 2 0 587.23 1508.88 1514.60 o
1 3 0 581.82 654.84 296.18 o
3 3 0 11620.50 11907.49 589.74 o
5 3 0 20048.85 20021.90 655.15 o
7 3 0 82158.62 80639.44 1728.93 o
9 3 0 11383.08 12423.25 913.84 o
11 3 0 27795.80 26181.85 1345.97 o
13 3 0 1831.76 1063.46 1040.93 o
15 3 0 33368.96 29963.57 1883.63 o
17 3 0 47114.47 47555.95 2588.67 o
19 3 0 6654.31 8067.59 1671.43 o
21 3 0 16058.91 18751.80 2325.94 o
23 3 0 122.58 3239.16 1593.44 o
0 4 0 994439.81 1028492.19 15462.34 o
2 4 0 799.28 1008.95 360.47 o
4 4 0 16223.87 16824.10 649.77 o
6 4 0 24678.99 26436.30 1042.41 o
8 4 0 18368.19 20986.49 1167.93 o
10 4 0 75597.61 75024.23 4225.06 o
12 4 0 7461.48 7205.12 1126.09 o
14 4 0 9225.21 9761.85 1526.16 o
16 4 0 34014.80 30054.16 2180.28 o
18 4 0 35474.85 35302.37 3372.32 o
20 4 0 7900.25 9140.08 3290.43 o
22 4 0 9720.23 12589.13 2231.72 o
1 5 0 2022.65 2130.57 610.43 o
3 5 0 141.65 -227.84 562.72 o
5 5 0 11177.55 10650.28 1954.59 o
7 5 0 70652.92 74702.00 3986.87 o
9 5 0 5757.93 9245.33 1915.77 o
11 5 0 19928.13 22990.61 4577.81 o
13 5 0 50.47 2101.61 1775.34 o
15 5 0 14747.69 12288.02 2467.52 o
17 5 0 17766.47 17285.24 2833.50 o
19 5 0 7095.32 11151.04 5849.44 o
21 5 0 8488.35 8132.21 3517.70 o
0 6 0 178175.98 168151.38 7224.45 o
2 6 0 23870.72 23944.57 2941.91 o
4 6 0 337.35 -104.48 1105.60 o
6 6 0 4704.05 6554.01 1817.69 o
8 6 0 191.60 568.18 1647.08 o
10 6 0 105816.95 113983.59 8597.89 o
12 6 0 3597.16 2259.99 1914.77 o
14 6 0 14163.78 12107.50 3375.27 o
16 6 0 16812.04 15356.42 2779.33 o
18 6 0 6037.02 2300.38 2248.33 o
1 7 0 17.38 1357.71 964.41 o
3 7 0 3193.25 3881.81 1329.26 o
5 7 0 4633.10 3729.61 2302.06 o
7 7 0 16761.85 15054.48 2386.62 o
9 7 0 10942.00 9670.45 3241.44 o
11 7 0 4812.91 2220.66 3611.15 o
13 7 0 2002.69 5635.08 2245.62 o
15 7 0 6002.96 4780.87 2370.16 o
0 8 0 113843.55 122661.89 8651.02 o
2 8 0 342.97 2882.66 2099.15 o
4 8 0 2227.07 5038.31 3052.62 o
6 8 0 3438.19 3626.29 1682.81 o
8 8 0 3710.78 1978.54 1827.11 o
10 8 0 12942.15 9180.41 2361.99 o
-26 0 1 1333.89 -1452.17 1531.19 o
-24 0 1 2135.03 118.55 1600.40 o
-22 0 1 248.78 1239.61 1679.31 o
-20 0 1 3067.74 1907.06 1247.79 o
-18 0 1 2061.18 420.93 2193.18 o
-16 0 1 925.10 1313.41 1010.13 o
-14 0 1 67475.25 68054.98 2595.66 o
-12 0 1 27.71 -153.87 604.09 o
-10 0 1 2683.38 2416.21 637.11 o
-8 0 1 143828.23 136678.89 2780.05 o
-6 0 1 308102.69 295353.56 5442.02 o
-4 0 1 13070.06 12396.56 1141.01 o
-2 0 1 76528.45 73389.06 1269.92 o
0 0 1 26140.94 24772.16 565.86 o
2 0 1 1623.67 1813.23 298.19 o
4 0 1 28693.53 29001.05 868.06 o
6 0 1 9467.67 8954.63 626.48 o
8 0 1 631.52 638.12 505.02 o
10 0 1 30575.55 31857.35 1439.07 o
12 0 1 88379.65 89432.71 3978.35 o
14 0 1 344.54 457.86 749.11 o
16 0 1 16562.82 15076.57 2348.01 o
18 0 1 7873.21 8348.01 1778.71 o
20 0 1 8858.43 10169.67 1511.72 o
22 0 1 66860.36 62338.97 3275.68 o
24 0 1 10127.58 9921.95 2371.64 o
-25 1 1 1853.35 1406.55 1020.88 o
-23 1 1 13569.72 13454.21 1509.23 o
-21 1 1 7991.75 8937.94 1177.85 o
-19 1 1 2212.52 3028.04 895.02 o
-17 1 1 2520.27 2751.91 773.26 o
-15 1 1 25738.68 27405.01 1270.31 o
-13 1 1 111939.75 115002.46 2523.69 o
-11 1 1 43007.34 44564.37 1400.27 o
-9 1 1 8582.97 8884.83 565.54 o
-7 1 1 85850.27 83728.02 1414.97 o
-5 1 1 45.69 312.15 294.79 o
-3 1 1 237.10 61.23 185.24 o
-1 1 1 1620.98 1775.58 170.83 o
1 1 1 111622.10 113254.23 1811.70 o
3 1 1 301840.34 300432.44 4618.02 o
5 1 1 206113.31 206627.03 2901.38 o
7 1 1 217958.94 213457.81 2899.10 o
9 1 1 4739.15 4540.40 468.54 o
11 1 1 521.13 751.61 497.52 o
13 1 1 41889.58 44149.84 1338.02 o
15 1 1 67501.67 67300.69 2135.85 o
17 1 1 22187.62 23115.71 1197.04 o
19 1 1 20824.12 20986.26 1194.47 o
21 1 1 20546.22 19631.45 1439.03 o
23 1 1 693.91 1598.25 1326.27 o
25 1 1 369.32 -1200.01 1200.01 o
-24 2 1 548.64 1525.39 2158.43 o
-22 2 1 3245.65 2366.51 1086.21 o
-20 2 1 12799.42 14996.05 1743.17 o
-18 2 1 37293.92 40255.23 1786.34 o
-16 2 1 35074.79 36313.26 2321.11 o
-14 2 1 8397.78 8006.31 964.21 o
-12 2 1 16080.83 16469.60 843.48 o
-10 2 1 6847.42 7213.72 586.77 o
-8 2 1 8217.37 8877.16 706.09 o
-6 2 1 76644.96 79317.22 1289.18 o
-4 2 1 104058.97 97281.80 1274.71 o
-2 2 1 2161.08 2048.66 252.04 o
0 2 1 50715.58 48517.47 837.89 o
2 2 1 23186.35 23047.77 718.73 o
4 2 1 121572.59 118820.70 2181.88 o
6 2 1 17635.60 17766.47 818.84 o
8 2 1 73990.24 74226.46 1810.62 o
10 2 1 1094.29 413.54 564.53 o
12 2 1 47871.44 46215.90 1734.15 o
14 2 1 19034.84 18333.70 1343.39 o
16 2 1 548.00 276.71 1054.73 o
18 2 1 7280.79 11051.21 1402.50 o
20 2 1 33768.08 38642.92 2827.18 o
22 2 1 61859.12 65591.07 3710.64 o
24 2 1 1946.17 1613.43 1543.83 o
-23 3 1 9810.83 9684.97 2033.62 o
-21 3 1 9046.15 8662.53 1877.79 o
-19 3 1 1737.84 2278.90 879.95 o
-17 3 1 1071.60 502.62 653.89 o
-15 3 1 22742.17 21440.90 1863.24 o
-13 3 1 88496.35 90172.70 2096.94 o
-11 3 1 19970.89 20627.04 950.98 o
-9 3 1 3303.70 3866.32 533.78 o
-7 3 1 56737.48 55520.42 1317.34 o
-5 3 1 759.59 849.08 304.71 o
-3 3 1 219.57 389.83 272.78 o
-1 3 1 354.82 412.03 272.63 o
1 3 1 80119.49 78683.29 1442.67 o
3 3 1 145571.22 144955.03 2273.42 o
5 3 1 110349.93 109750.62 2233.23 o
7 3 1 135913.39 134804.20 2723.34 o
9 3 1 3236.08 2576.27 844.02 o
11 3 1 39.91 244.90 621.27 o
13 3 1 39612.73 41425.86 1880.83 o
15 3 1 56274.07 55171.82 2495.99 o
17 3 1 11629.14 12942.35 1727.78 o
19 3 1 16953.22 19801.59 2322.96 o
21 3 1 11113.46 9950.04 2772.00 o
23 3 1 928.67 2202.91 1512.38 o
-22 4 1 568.14 -103.38 1468.43 o
-20 4 1 3270.32 2977.64 1328.19 o
-18 4 1 784.53 -628.36 1033.06 o
-16 4 1 652.58 997.58 1054.54 o
-14 4 1 38172.00 39177.88 3146.45 o
-12 4 1 9.63 719.49 804.15 o
-10 4 1 953.72 231.44 541.97 o
-8 4 1 45492.77 45917.65 1272.05 o
-6 4 1 169913.33 169487.17 2551.46 o
-4 4 1 4084.67 4179.44 470.99 o
-2 4 1 33821.37 33506.09 932.19 o
0 4 1 11349.00 12294.95 629.61 o
2 4 1 65.17 147.67 383.62 o
4 4 1 9513.12 10139.27 878.18 o
6 4 1 10545.05 10444.43 829.17 o
8 4 1 189.77 -534.81 534.81 o
10 4 1 16157.74 14146.20 1349.71 o
12 4 1 49931.77 50697.27 2397.86 o
14 4 1 179.56 -410.94 913.02 o
16 4 1 12625.07 16137.69 1718.51 o
18 4 1 3256.78 1658.27 1297.66 o
20 4 1 5749.59 5503.35 3043.14 o
22 4 1 39822.21 36813.59 3239.56 o
-21 5 1 2696.63 -136.41 2697.01 o
-19 5 1 446.73 1217.01 2078.16 o
-17 5 1 1366.94 1643.79 1907.25 o
-15 5 1 6961.95 7996.14 2460.39 o
-13 5 1 44869.71 44879.83 3644.58 o
-11 5 1 16654.01 14629.73 2308.46 o
-9 5 1 1652.22 876.88 1362.58 o
-7 5 1 24561.98 25311.50 1317.17 o
-5 5 1 111.81 206.17 607.40 o
-3 5 1 63.51 516.47 571.19 o
-1 5 1 440.49 619.81 544.69 o
1 5 1 18867.89 18689.50 1711.33 o
3 5 1 85282.64 85764.88 5062.26 o
5 5 1 70235.99 69560.68 3799.60 o
7 5 1 46328.70 44789.38 3251.80 o
9 5 1 2303.18 976.88 1069.09 o
11 5 1 1809.23 3836.50 1135.50 o
13 5 1 16977.40 16455.46 2075.16 o
15 5 1 23368.61 23264.32 2039.24 o
17 5 1 10128.52 10551.68 1658.91 o
19 5 1 7399.39 4728.52 1613.89 o
-18 6 1 7743.83 7486.58 3947.45 o
-16 6 1 15973.37 10496.38 2588.80 o
-14 6 1 1399.59 -226.49 2094.30 o
-12 6 1 3962.76 5940.35 2022.25 o
-10 6 1 622.38 2012.77 1742.78 o
-8 6 1 785.50 556.02 2099.19 o
-6 6 1 22663.57 25110.33 2557.44 o
-4 6 1 41587.40 41529.16 1540.91 o
-2 6 1 534.37 382.14 576.22 o
0 6 1 9330.03 8809.11 1176.22 o
2 6 1 5758.39 2632.99 1260.71 o
4 6 1 41697.10 37534.57 3145.96 o
6 6 1 4636.72 1936.90 1675.44 o
8 6 1 16006.15 14146.40 2385.51 o
10 6 1 2173.06 2400.00 1804.86 o
12 6 1 17957.53 20675.44 2863.70 o
14 6 1 8321.07 7595.98 2332.63 o
16 6 1 98.30 1173.19 2111.78 o
18 6 1 2349.81 1022.00 2176.46 o
-15 7 1 6554.03 3943.78 4130.07 o
-13 7 1 22434.29 17440.16 2857.18 o
-11 7 1 3652.41 3363.77 1973.78 o
-9 7 1 524.95 125.59 1631.41 o
-7 7 1 8085.27 6386.29 1741.73 o
-5 7 1 681.16 -880.05 1235.71 o
-3 7 1 408.82 355.06 1582.66 o
-1 7 1 82.07 -554.56 827.05 o
1 7 1 10322.80 5667.02 1473.62 o
3 7 1 29996.80 28644.64 2720.93 o
5 7 1 19243.46 13418.73 2306.05 o
7 7 1 20992.81 18934.43 2757.07 o
9 7 1 444.36 1582.40 1846.67 o
11 7 1 53.06 -1814.06 1814.06 o
13 7 1 12019.96 10609.02 2622.04 o
15 7 1 15048.14 15980.08 10436.95 o
-12 8 1 15.88 632.21 2400.41 o
-10 8 1 11.03 -1148.56 1546.04 o
-8 8 1 3604.75 3118.18 2504.46 o
-6 8 1 40869.07 38761.67 5490.74 o
-4 8 1 1317.60 345.75 2677.13 o
-2 8 1 7827.51 4464.26 2969.28 o
0 8 1 2126.62 2612.05 1978.83 o
2 8 1 15.50 -681.32 1250.89 o
4 8 1 1650.65 352.75 1597.41 o
6 8 1 4487.06 3817.65 1978.53 o
8 8 1 170.16 877.98 1858.37 o
10 8 1 3681.38 1056.95 2021.31 o
-24 0 2 12035.53 10268.14 2332.32 o
-22 0 2 2674.29 2933.26 1379.15 o
-20 0 2 20524.48 18653.84 3124.33 o
-18 0 2 2339.16 980.57 3008.25 o
-16 0 2 19953.99 19356.00 1656.08 o
-14 0 2 1429.54 1296.03 757.27 o
-12 0 2 149687.88 140596.92 4242.68 o
-10 0 2 1692.27 2174.79 675.07 o
-8 0 2 583191.75 580888.88 10193.89 o
-6 0 2 2385.40 2291.65 554.87 o
-4 0 2 1534.02 1688.62 336.45 o
-2 0 2 1142.66 1120.55 209.65 o
0 0 2 41378.30 41504.86 807.77 o
2 0 2 61681.89 59889.75 1404.24 o
4 0 2 5939.24 6333.94 467.91 o
6 0 2 46834.58 45494.84 1386.02 o
8 0 2 77095.98 74512.47 1897.59 o
10 0 2 171238.92 168367.16 3561.59 o
12 0 2 3256.38 3805.39 725.06 o
14 0 2 61337.87 61279.13 4442.49 o
16 0 2 52303.98 55647.89 4057.45 o
18 0 2 25059.68 23026.27 1920.29 o
20 0 2 6169.69 8646.99 1892.15 o
22 0 2 30516.49 31934.46 2257.41 o
24 0 2 2993.70 3131.73 2420.42 o
-25 1 2 523.11 1212.53 1206.91 o
-23 1 2 130.38 77.98 1026.35 o
-21 1 2 86.97 -689.27 933.75 o
-19 1 2 96810.04 102589.30 3136.19 o
-17 1 2 755.68 1648.94 724.71 o
-15 1 2 11079.49 11002.05 892.94 o
-13 1 2 12901.01 13877.64 804.22 o
-11 1 2 1559.38 926.38 516.40 o
-9 1 2 90269.13 85768.62 1551.23 o
-7 1 2 29797.94 28749.21 857.82 o
-5 1 2 26257.41 27411.93 627.91 o
-3 1 2 38435.46 36860.32 654.62 o
-1 1 2 36237.38 36192.34 745.20 o
1 1 2 5631.24 4923.37 386.61 o
3 1 2 22375.84 20484.57 760.93 o
5 1 2 5594.02 6610.99 470.60 o
7 1 2 56414.16 58373.29 1376.06 o
9 1 2 76909.50 76960.06 2026.61 o
11 1 2 12609.88 11936.54 623.19 o
13 1 2 10901.94 10768.09 700.94 o
15 1 2 25363.61 26503.44 1108.81 o
17 1 2 6262.84 5867.03 1265.80 o
19 1 2 1066.88 -850.39 850.39 o
21 1 2 12182.25 10400.51 1718.23 o
23 1 2 15665.08 15589.61 1681.36 o
-26 2 2 38249.52 36577.37 2514.96 o
-24 2 2 4750.45 5066.83 1266.28 o
-22 2 2 3990.44 3170.51 1139.02 o
-20 2 2 2390.96 3170.19 1187.32 o
-18 2 2 36132.11 39075.46 1990.27 o
-16 2 2 30110.05 30551.56 1528.90 o
-14 2 2 4902.23 4688.58 729.27 o
-12 2 2 20651.06 20095.62 953.72 o
-10 2 2 145445.33 142578.66 2323.65 o
-8 2 2 111468.18 104873.10 1639.64 o
-6 2 2 6189.99 6931.81 474.99 o
-4 2 2 3191.39 3501.30 308.89 o
-2 2 2 55511.30 53525.91 969.67 o
0 2 2 115904.45 116376.14 2192.07 o
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4 2 2 34580.15 32131.35 923.58 o
6 2 2 40427.03 39867.15 1173.39 o
8 2 2 151125.70 152882.25 3089.76 o
10 2 2 7153.19 7160.73 741.77 o
12 2 2 33126.16 33817.29 1582.54 o
14 2 2 14433.38 15844.21 2051.22 o
16 2 2 31605.04 32447.91 1971.69 o
18 2 2 13496.34 16599.81 2121.17 o
20 2 2 32812.72 31380.14 2205.24 o
22 2 2 3258.27 2224.04 1409.82 o
-25 3 2 352.31 -182.13 1641.54 o
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-13 3 2 4783.75 4796.04 995.38 o
-11 3 2 30.23 121.10 509.81 o
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-7 3 2 32529.62 34691.11 911.54 o
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-1 3 2 14244.03 14850.66 653.26 o
1 3 2 163.70 735.28 356.36 o
3 3 2 6000.94 6069.48 596.87 o
5 3 2 5793.90 5794.08 576.10 o
7 3 2 25583.91 25354.97 1103.72 o
9 3 2 63412.04 62057.83 2381.13 o
11 3 2 6930.99 7224.07 878.65 o
13 3 2 11958.32 12629.38 1587.15 o
15 3 2 17750.21 20314.63 1647.90 o
17 3 2 6064.51 1766.26 1244.97 o
19 3 2 1362.36 2424.98 1440.05 o
21 3 2 10006.88 13820.50 2076.69 o
23 3 2 10378.54 7592.75 1847.74 o
-22 4 2 1673.66 1519.61 3650.22 o
-20 4 2 11867.12 10225.74 2494.65 o
-18 4 2 1312.24 1750.70 1146.05 o
-16 4 2 8012.56 9247.78 1091.66 o
-14 4 2 222.39 476.41 804.20 o
-12 4 2 66780.30 68743.51 3428.04 o
-10 4 2 1665.03 1334.72 604.55 o
-8 4 2 215052.27 207826.88 3491.14 o
-6 4 2 1064.68 1551.27 382.01 o
-4 4 2 299.54 -383.89 383.89 o
-2 4 2 276.36 169.95 340.80 o
0 4 2 14724.54 16216.17 742.38 o
2 4 2 21251.02 22051.74 1063.69 o
4 4 2 393.51 298.87 466.34 o
6 4 2 20285.49 22481.81 1108.77 o
8 4 2 32808.22 33664.09 1429.23 o
10 4 2 68013.78 70433.13 2094.97 o
12 4 2 1246.07 380.03 967.40 o
14 4 2 29441.21 29962.14 2093.44 o
16 4 2 31858.61 28465.00 2387.89 o
18 4 2 16746.99 15136.08 2016.64 o
20 4 2 3479.86 3507.21 2963.84 o
-21 5 2 63.82 -1972.27 1972.27 o
-19 5 2 46732.61 45768.95 9668.05 o
-17 5 2 1184.22 2120.31 3916.89 o
-15 5 2 2389.08 2578.14 1861.99 o
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