#------------------------------------------------------------------------------
#$Date: 2018-12-07 05:37:15 +0200 (Fri, 07 Dec 2018) $
#$Revision: 212436 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/83/2108346.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108346
_cell_angle_alpha                90.000
_cell_angle_beta                 99.270
_cell_angle_gamma                90.000
_cell_length_a                   19.1455
_cell_length_b                   6.2686
_cell_length_c                   17.2963
_exptl_crystal_F_000             2671.20
_reflns_d_resolution_high        0.7570
_cod_data_source_file            ps5074CuPbOXO2sup8.hkl
_cod_data_source_block           CuPbOXO2
_shelx_title                     ' mo_r1233112_0m in C2/m'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1410.35
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 4815.43 3610.98 172.45 o
4 0 0 15549.77 14089.50 498.23 o
6 0 0 45493.72 41326.44 1434.96 o
8 0 0 90271.47 85063.11 2154.12 o
10 0 0 29094.77 28875.98 1116.61 o
12 0 0 107463.25 107060.81 2273.93 o
14 0 0 14504.38 15369.63 1348.57 o
16 0 0 23819.09 29781.66 2463.01 o
18 0 0 37228.21 34600.48 4178.97 o
20 0 0 5377.96 4668.05 2382.98 o
22 0 0 46997.78 51316.84 5397.53 o
24 0 0 3498.09 1489.87 2516.67 o
1 1 0 9232.73 12628.36 454.88 o
3 1 0 29159.01 28862.94 367.12 o
5 1 0 40233.17 45225.34 646.37 o
7 1 0 258148.62 245688.75 2204.55 o
9 1 0 120311.97 118273.66 1893.14 o
11 1 0 233355.31 224544.25 2513.46 o
13 1 0 17658.49 17158.23 1073.33 o
15 1 0 98463.09 98901.65 2268.13 o
17 1 0 2306.47 1838.97 723.57 o
19 1 0 70643.95 70813.39 4008.84 o
21 1 0 32181.26 36803.76 2913.10 o
23 1 0 9147.05 10037.32 1981.42 o
0 2 0 1648248.00 1732796.62 19321.18 o
2 2 0 25947.30 28804.43 504.33 o
4 2 0 53340.61 51093.65 819.14 o
6 2 0 111312.47 102410.62 1110.47 o
8 2 0 42158.47 43915.11 772.89 o
10 2 0 24824.01 26922.76 1115.61 o
12 2 0 130773.41 129648.19 3111.19 o
14 2 0 13282.95 13217.14 887.24 o
16 2 0 3046.41 1856.84 642.59 o
18 2 0 10988.43 9794.87 1877.13 o
20 2 0 10000.36 8081.93 2556.06 o
22 2 0 178645.75 184383.70 17498.37 o
24 2 0 2416.77 856.00 1800.81 o
1 3 0 6186.64 7146.27 430.97 o
3 3 0 83554.53 87668.31 1170.15 o
5 3 0 32119.97 33396.52 724.33 o
7 3 0 193639.56 191913.55 2250.85 o
9 3 0 102450.19 99710.95 1782.30 o
11 3 0 178616.44 181812.70 2531.80 o
13 3 0 14967.88 15608.43 768.62 o
15 3 0 91311.97 92892.70 2221.33 o
17 3 0 1168.34 2351.99 680.57 o
19 3 0 46606.59 40959.83 5377.45 o
21 3 0 32790.36 27074.11 9922.32 o
23 3 0 5034.18 4263.87 1377.13 o
0 4 0 1989080.50 2013393.00 23474.25 o
2 4 0 1443.19 1698.38 219.30 o
4 4 0 10464.24 11209.76 486.71 o
6 4 0 7001.47 6638.07 539.46 o
8 4 0 75436.73 74044.52 2060.64 o
10 4 0 13926.59 13376.12 1026.56 o
12 4 0 40445.62 42025.90 1457.14 o
14 4 0 4526.68 5167.58 785.18 o
16 4 0 14294.88 14145.84 1324.43 o
18 4 0 24771.70 27219.79 1879.98 o
20 4 0 6403.34 6235.20 1794.90 o
1 5 0 6369.27 6947.50 384.50 o
3 5 0 18661.91 19542.57 655.92 o
5 5 0 21862.78 22190.33 787.27 o
7 5 0 89537.62 88260.34 1483.30 o
9 5 0 62884.22 61806.82 1292.07 o
11 5 0 80675.09 77451.52 1549.10 o
13 5 0 15290.65 14990.56 1111.80 o
15 5 0 58474.67 55099.77 2067.27 o
17 5 0 265.61 847.86 818.48 o
19 5 0 50680.36 54574.23 4883.96 o
0 6 0 386891.88 404423.34 9268.84 o
2 6 0 11349.62 12159.26 538.78 o
4 6 0 33287.58 34450.04 844.03 o
6 6 0 36182.00 36854.84 1133.86 o
8 6 0 1179.29 1409.78 404.04 o
10 6 0 8409.04 8041.70 787.56 o
12 6 0 37579.16 37522.25 1662.28 o
14 6 0 13093.59 11467.05 1079.08 o
16 6 0 4618.63 5657.79 1074.22 o
1 7 0 5665.72 5891.99 538.12 o
3 7 0 26788.89 27428.12 857.55 o
5 7 0 7006.64 7634.08 545.74 o
7 7 0 51171.89 51567.87 1315.97 o
9 7 0 26919.28 25403.11 1040.64 o
11 7 0 62328.53 59728.96 2836.23 o
13 7 0 7961.66 9189.82 1034.10 o
0 8 0 346516.38 345088.62 5842.62 o
2 8 0 1086.53 873.73 461.21 o
4 8 0 3846.15 3757.93 555.60 o
6 8 0 1931.81 2188.20 516.94 o
-24 0 1 3266.48 3503.20 2858.93 o
-22 0 1 26.25 422.04 1947.92 o
-20 0 1 11383.96 7832.14 2847.55 o
-18 0 1 1478.85 853.84 1015.33 o
-16 0 1 10917.78 8325.52 2399.12 o
-14 0 1 21354.89 19623.43 1247.16 o
-12 0 1 7388.13 6171.88 747.16 o
-10 0 1 16679.83 16058.54 990.71 o
-8 0 1 151149.53 146178.64 2377.01 o
-6 0 1 101668.25 103018.61 1866.45 o
-4 0 1 22536.25 21836.50 965.60 o
-2 0 1 51315.78 57083.04 1936.88 o
2 0 1 22817.96 20075.02 360.85 o
4 0 1 2913.54 2344.27 243.06 o
6 0 1 15956.24 13890.00 1145.38 o
8 0 1 9492.49 10035.63 659.27 o
10 0 1 37785.58 35512.52 1192.33 o
12 0 1 280059.69 285099.03 4439.17 o
14 0 1 40246.54 40542.95 1524.28 o
16 0 1 1518.87 1233.24 861.71 o
18 0 1 255732.31 270080.75 6925.86 o
20 0 1 131761.38 134677.70 4934.53 o
22 0 1 10502.49 11899.46 3261.78 o
24 0 1 6254.30 10066.87 3221.40 o
-23 1 1 1255.77 1038.18 1279.72 o
-21 1 1 9677.96 8212.46 1870.37 o
-19 1 1 18094.38 19147.32 1897.87 o
-17 1 1 22729.22 22295.25 1527.67 o
-15 1 1 1001.40 941.00 492.74 o
-13 1 1 11618.09 12303.20 692.26 o
-11 1 1 4114.53 3863.67 423.35 o
-9 1 1 112580.69 114364.91 1384.86 o
-7 1 1 79646.59 70090.18 1255.70 o
-5 1 1 56626.72 55312.21 721.51 o
-3 1 1 3642.21 3158.27 229.24 o
-1 1 1 7457.08 4967.60 210.24 o
1 1 1 86211.19 76803.60 864.08 o
3 1 1 26503.34 26515.81 381.65 o
5 1 1 132289.84 141542.59 1606.40 o
7 1 1 464.80 747.52 243.40 o
9 1 1 123388.59 118991.46 2734.98 o
11 1 1 84999.72 85285.70 1485.29 o
13 1 1 238.78 -15.18 361.76 o
15 1 1 3394.98 3908.09 620.19 o
17 1 1 8101.73 7699.22 1018.58 o
19 1 1 1161.61 790.16 1040.03 o
21 1 1 4523.21 1393.42 1221.42 o
23 1 1 1300.37 624.17 1301.01 o
-24 2 1 5075.05 3398.92 1496.71 o
-22 2 1 800.47 217.37 1151.87 o
-20 2 1 13721.50 11262.58 3812.61 o
-18 2 1 55602.86 48934.11 2598.90 o
-16 2 1 942.44 1821.17 646.55 o
-14 2 1 44246.97 44871.00 1387.18 o
-12 2 1 24187.20 27474.43 793.02 o
-10 2 1 265573.25 275181.00 2814.85 o
-8 2 1 16291.02 17682.62 550.39 o
-6 2 1 31691.45 34193.66 678.26 o
-4 2 1 425.22 259.88 183.15 o
-2 2 1 176736.38 165548.59 1533.27 o
0 2 1 7435.59 9488.06 402.02 o
2 2 1 2432.99 3238.26 325.60 o
4 2 1 100510.25 93892.12 956.98 o
6 2 1 44480.39 42167.66 660.50 o
8 2 1 206.36 -50.73 204.43 o
10 2 1 59125.17 59720.20 1103.17 o
12 2 1 9864.85 10735.85 733.75 o
14 2 1 134.89 134.06 431.33 o
16 2 1 1328.16 1086.60 764.27 o
18 2 1 227258.31 218068.08 5777.01 o
20 2 1 1856.61 2175.29 1183.79 o
22 2 1 380.00 -872.97 1099.63 o
24 2 1 11430.78 10943.28 4150.10 o
-23 3 1 501.02 371.92 1065.18 o
-21 3 1 5978.50 3077.65 2231.08 o
-19 3 1 15147.00 12495.75 1451.46 o
-17 3 1 18240.53 16388.51 1180.38 o
-15 3 1 28.73 88.30 493.99 o
-13 3 1 24322.49 24174.63 959.13 o
-11 3 1 4491.91 4369.21 573.29 o
-9 3 1 67456.20 69633.88 1304.78 o
-7 3 1 93401.88 88046.70 1334.95 o
-5 3 1 17838.00 18730.91 584.58 o
-3 3 1 410.95 626.93 180.44 o
-1 3 1 8370.29 7522.77 315.17 o
1 3 1 32311.81 31210.10 1240.94 o
3 3 1 15339.39 16068.83 702.75 o
5 3 1 97151.09 98237.72 2188.40 o
7 3 1 478.19 569.20 268.08 o
9 3 1 104863.25 107773.37 1951.96 o
11 3 1 59627.95 59712.14 1203.59 o
13 3 1 8.43 -153.24 360.56 o
15 3 1 2724.44 2304.33 602.37 o
17 3 1 457.73 393.78 575.77 o
19 3 1 1361.09 1314.08 936.53 o
21 3 1 4934.09 3865.84 1258.92 o
23 3 1 47.82 -588.86 1467.50 o
-22 4 1 29.39 -1581.61 1299.61 o
-20 4 1 4301.60 4053.89 1551.95 o
-18 4 1 1640.46 2076.23 862.05 o
-16 4 1 13937.76 13778.37 1380.18 o
-14 4 1 13610.11 14338.41 1097.55 o
-12 4 1 1209.54 1314.68 516.93 o
-10 4 1 185.53 430.32 393.93 o
-8 4 1 35300.06 37586.48 858.75 o
-6 4 1 73717.11 77104.35 1244.23 o
-4 4 1 11550.14 11312.97 521.18 o
-2 4 1 23817.04 24523.40 552.78 o
0 4 1 2452.47 2387.30 237.84 o
2 4 1 4373.13 4846.41 401.25 o
4 4 1 1185.16 1447.09 282.60 o
6 4 1 4121.73 3990.98 369.99 o
8 4 1 9408.70 8081.38 629.27 o
10 4 1 13803.35 13569.10 1149.09 o
12 4 1 167846.94 161867.28 2942.27 o
14 4 1 32504.46 33249.70 1598.85 o
16 4 1 438.13 -481.62 675.90 o
18 4 1 145468.31 136531.58 5542.69 o
-19 5 1 7625.29 6882.43 1272.80 o
-17 5 1 19212.41 19196.97 1672.57 o
-15 5 1 114.04 82.46 612.84 o
-13 5 1 3864.48 3468.46 694.79 o
-11 5 1 2518.46 2429.13 450.64 o
-9 5 1 28817.67 28582.48 920.16 o
-7 5 1 14482.25 15012.38 674.57 o
-5 5 1 5078.70 5041.57 380.10 o
-3 5 1 89.87 203.27 222.23 o
-1 5 1 3266.81 3331.42 304.80 o
1 5 1 34245.38 32860.22 674.55 o
3 5 1 1083.39 1195.86 239.46 o
5 5 1 66207.69 67700.62 1106.86 o
7 5 1 1334.88 896.60 351.87 o
9 5 1 25253.45 25210.54 1044.77 o
11 5 1 46700.12 46524.63 2041.08 o
13 5 1 1281.83 1425.07 1030.79 o
15 5 1 4096.26 3668.84 881.29 o
17 5 1 2185.84 2483.47 885.59 o
19 5 1 58.65 736.93 888.43 o
-16 6 1 66.55 441.34 738.37 o
-14 6 1 20495.96 18248.21 1569.75 o
-12 6 1 2511.74 3965.54 710.54 o
-10 6 1 85220.91 83872.66 2422.29 o
-8 6 1 735.48 825.37 366.58 o
-6 6 1 8523.11 8104.89 532.37 o
-4 6 1 1568.02 1451.74 339.88 o
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0 6 1 336.33 399.59 265.34 o
2 6 1 1046.20 694.77 268.48 o
4 6 1 45868.52 46943.86 970.33 o
6 6 1 32413.26 32543.89 948.50 o
8 6 1 1550.10 1676.27 414.70 o
10 6 1 9022.29 9030.98 895.09 o
12 6 1 9895.81 10529.43 798.22 o
14 6 1 36.96 42.43 623.92 o
16 6 1 2358.09 3860.97 995.32 o
-13 7 1 8538.34 8596.87 990.80 o
-11 7 1 232.08 901.19 617.48 o
-9 7 1 18298.98 17262.18 912.73 o
-7 7 1 18630.18 18894.55 1185.78 o
-5 7 1 3368.30 3046.68 484.75 o
-3 7 1 46.76 -160.56 352.86 o
-1 7 1 2642.18 3183.91 457.62 o
1 7 1 6054.60 6126.45 490.07 o
3 7 1 2430.76 2543.47 402.81 o
5 7 1 30661.30 31081.80 875.27 o
7 7 1 610.05 133.55 357.52 o
9 7 1 29521.88 30120.22 1097.66 o
11 7 1 13442.24 13576.58 1070.54 o
13 7 1 9.54 42.18 636.11 o
-6 8 1 15792.07 15195.60 862.24 o
-4 8 1 2780.94 1868.59 515.86 o
-2 8 1 2313.07 1553.53 484.62 o
0 8 1 805.49 781.75 456.23 o
2 8 1 1663.83 1617.52 483.48 o
4 8 1 0.08 96.51 414.34 o
6 8 1 4595.65 5217.47 770.93 o
-24 0 2 20695.03 25149.67 4429.89 o
-22 0 2 24961.45 14289.08 13300.30 o
-20 0 2 59290.48 65903.31 3607.13 o
-18 0 2 159589.34 167031.42 5191.87 o
-16 0 2 42818.78 40072.36 2485.47 o
-14 0 2 72563.50 69458.37 4134.79 o
-12 0 2 432.14 1363.81 501.15 o
-10 0 2 696.39 650.45 422.52 o
-8 0 2 532176.50 520010.94 8707.10 o
-6 0 2 245664.69 251975.09 9567.00 o
-4 0 2 2898.41 3031.56 234.46 o
-2 0 2 47796.00 41968.21 1884.03 o
0 0 2 32130.30 25631.14 496.03 o
2 0 2 132007.66 125779.24 1316.63 o
4 0 2 365855.88 377305.97 3658.50 o
6 0 2 58078.25 61049.66 1481.08 o
8 0 2 47963.72 46831.88 2928.78 o
10 0 2 45471.81 44056.09 1290.56 o
12 0 2 136830.69 136047.53 2558.03 o
14 0 2 42507.11 40258.63 1571.54 o
16 0 2 705.34 -228.78 807.04 o
18 0 2 112064.19 117937.53 4347.94 o
20 0 2 3971.50 3184.81 1359.33 o
22 0 2 28222.07 23338.91 4168.38 o
24 0 2 1635.00 -80.53 2194.51 o
-23 1 2 32372.19 39137.85 3224.08 o
-21 1 2 38393.54 36841.02 2545.98 o
-19 1 2 4722.72 4475.82 1499.52 o
-17 1 2 5930.70 5437.89 888.47 o
-15 1 2 174264.50 173172.89 2776.52 o
-13 1 2 4538.99 4595.41 574.82 o
-11 1 2 3708.83 3571.52 411.33 o
-9 1 2 24423.17 27291.49 689.11 o
-7 1 2 100885.34 102198.95 1688.15 o
-5 1 2 30643.23 31593.51 538.07 o
-3 1 2 67869.48 62849.61 1433.33 o
-1 1 2 166070.03 153548.59 1521.88 o
1 1 2 7525.34 10090.73 499.24 o
3 1 2 16552.03 16956.46 364.86 o
5 1 2 127231.28 131878.05 1498.99 o
7 1 2 137817.69 143856.59 1760.73 o
9 1 2 5362.51 5279.62 608.68 o
11 1 2 231446.88 226419.06 3017.05 o
13 1 2 47761.41 49668.58 1826.44 o
15 1 2 167097.81 166382.59 3373.38 o
17 1 2 1927.72 549.29 724.45 o
19 1 2 5086.83 3388.36 1896.84 o
21 1 2 1093.46 140.46 1088.98 o
23 1 2 2321.40 2434.66 1537.38 o
-24 2 2 11895.45 9464.78 3620.65 o
-22 2 2 15063.73 14155.71 2387.01 o
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-18 2 2 58572.89 57938.93 2991.72 o
-16 2 2 11982.92 12954.01 1120.55 o
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-12 2 2 196999.38 198290.81 2294.19 o
-10 2 2 13436.86 14642.88 573.57 o
-8 2 2 196769.94 202794.56 2072.33 o
-6 2 2 64173.16 69185.60 1284.91 o
-4 2 2 132470.62 125200.70 1409.42 o
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0 2 2 3700.41 2531.14 280.09 o
2 2 2 83133.00 86925.88 1979.81 o
4 2 2 685441.88 680396.06 5409.39 o
6 2 2 98919.62 101009.83 1126.90 o
8 2 2 22047.52 24254.31 656.18 o
10 2 2 122427.12 124204.87 1804.81 o
12 2 2 4760.51 4481.43 507.10 o
14 2 2 55717.14 58500.93 1611.27 o
16 2 2 5374.86 5105.21 1427.25 o
18 2 2 3509.22 2084.96 1202.71 o
20 2 2 11224.01 7436.60 2817.36 o
22 2 2 53213.31 50820.82 4098.62 o
-23 3 2 21353.05 18924.07 5594.76 o
-21 3 2 31007.06 19901.75 5754.09 o
-19 3 2 4564.10 3074.01 793.44 o
-17 3 2 3284.32 2410.13 670.96 o
-15 3 2 130438.41 130904.95 2319.40 o
-13 3 2 1155.30 1358.33 516.86 o
-11 3 2 10557.31 11228.12 822.47 o
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-5 3 2 36549.59 36123.34 696.59 o
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1 3 2 1824.47 2091.35 323.29 o
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7 3 2 158283.72 163823.00 1842.56 o
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11 3 2 195560.56 196899.22 3427.11 o
13 3 2 51402.77 51374.29 1538.96 o
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19 3 2 4189.67 3544.15 1158.97 o
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12 4 2 36671.28 37873.14 1534.50 o
14 4 2 14432.48 13688.90 1275.92 o
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18 4 2 74173.89 72018.80 4703.66 o
20 4 2 871.69 -865.72 1382.29 o
-19 5 2 2507.61 1097.26 953.83 o
-17 5 2 14109.11 12689.63 1224.53 o
-15 5 2 80472.47 82052.87 2301.39 o
-13 5 2 671.53 813.29 561.86 o
-11 5 2 5623.94 5502.64 555.25 o
-9 5 2 9367.79 9340.52 621.10 o
-7 5 2 38474.70 38255.30 1189.33 o
-5 5 2 24704.41 24141.26 868.17 o
-3 5 2 10337.79 10195.44 472.47 o
-1 5 2 26715.38 25823.23 635.28 o
1 5 2 681.95 675.26 225.25 o
3 5 2 2241.93 1837.77 400.23 o
5 5 2 64023.53 62828.47 1963.30 o
7 5 2 56746.50 56324.66 1306.04 o
9 5 2 4226.51 3087.35 545.90 o
11 5 2 98573.78 100120.38 2223.35 o
13 5 2 15018.64 15554.59 1500.08 o
15 5 2 72318.30 71473.47 2478.34 o
17 5 2 2640.09 1922.25 896.55 o
19 5 2 3623.15 3080.41 1610.67 o
-16 6 2 6743.37 6685.73 1021.50 o
-14 6 2 8428.97 7303.58 937.07 o
-12 6 2 70839.70 71027.91 1967.40 o
-10 6 2 587.66 564.89 423.06 o
-8 6 2 49289.00 46789.48 1535.45 o
-6 6 2 21882.84 20350.60 766.23 o
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0 6 2 15500.38 16160.74 585.29 o
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4 6 2 195101.81 192916.09 2601.10 o
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