#------------------------------------------------------------------------------ #$Date: 2019-03-16 05:21:04 +0200 (Sat, 16 Mar 2019) $ #$Revision: 214143 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/83/2108383.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108383 _cell_angle_alpha 90.000 _cell_angle_beta 102.634 _cell_angle_gamma 90.000 _cell_length_a 23.2416 _cell_length_b 5.2305 _cell_length_c 25.4061 _exptl_crystal_F_000 1424.00 _reflns_d_resolution_high 0.8058 _cod_data_source_file um5023Isup2.hkl _cod_data_source_block I _shelx_title DVK _shelx_refln_list_code 4 _shelx_f_calc_maximum 330.18 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -6 0 211.81 242.32 141.07 o 2 -6 0 385.99 466.36 150.53 o 4 -6 0 347.65 255.96 148.96 o 6 -6 0 490.40 620.97 159.23 o 8 -6 0 303.67 431.73 155.92 o 10 -6 0 158.97 141.97 144.77 o 1 -5 0 670.09 682.85 92.25 o 3 -5 0 320.31 338.19 127.28 o 5 -5 0 49.27 22.34 124.55 o 7 -5 0 395.82 430.98 134.78 o 9 -5 0 221.60 241.90 138.63 o 11 -5 0 138.30 135.38 141.81 o 13 -5 0 92.22 77.32 142.06 o 15 -5 0 274.66 327.32 139.71 o 17 -5 0 75.44 53.44 136.42 o 0 -4 0 2680.32 2680.94 148.53 o 2 -4 0 491.68 508.85 78.49 o 4 -4 0 233.49 217.11 112.90 o 6 -4 0 273.35 213.05 118.81 o 8 -4 0 1197.52 1177.22 139.62 o 10 -4 0 1406.73 1434.05 147.46 o 12 -4 0 28.47 166.48 119.36 o 14 -4 0 103.04 255.78 125.32 o 1 -3 0 570.09 616.81 68.26 o 3 -3 0 756.68 732.91 70.49 o 5 -3 0 5476.87 5512.77 172.17 o 7 -3 0 1441.18 1548.99 122.49 o 11 -3 0 334.37 231.64 75.55 o 13 -3 0 607.75 635.93 87.78 o 15 -3 0 13.09 2.51 79.34 o 17 -3 0 1850.02 1907.87 122.82 o 19 -3 0 200.15 212.35 95.57 o 21 -3 0 641.41 603.92 113.58 o 0 -2 0 5766.69 4944.18 129.24 o 2 -2 0 768.70 817.84 62.25 o 4 -2 0 4007.14 4088.24 128.76 o 6 -2 0 3810.88 4371.95 107.33 o 8 -2 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