#------------------------------------------------------------------------------ #$Date: 2019-07-20 06:59:05 +0300 (Sat, 20 Jul 2019) $ #$Revision: 217185 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/10/84/2108443.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108443 loop_ _publ_author_name 'Bodart, Laurie' 'Tumanov, Nikolay' 'Wouters, Johan' _publ_section_title ; Structural variety of clofaziminium salts: effect of the counter-ion on clofaziminium conformation and crystal packing ; _journal_coeditor_code AW5025 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first ; ; _journal_paper_doi 10.1107/S2052520619007649 _journal_volume 75 _journal_year 2019 _chemical_formula_moiety ; C27 H23 Cl2 N4 + , C7 H4 N O3 S - , 1.393(C2 H3 N) ; _chemical_formula_sum 'C36.79 H31.18 Cl2 N6.39 O3 S' _chemical_formula_weight 713.78 _chemical_name_common ; Clofaziminium saccharinate acetonitrile solvate ; _chemical_name_systematic ; 1,1,3-trioxo-2,3-dihydro-1,2-benzothiazol-2-ide; N-[(2E)-10-(4-chlorophenyl)-3-[(4-chlorophenyl)amino] -2,10-dihydrophenazin-2-ylidene]propan-2-aminium; acetonitrile ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary dual _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 80.214(3) _cell_angle_beta 80.034(4) _cell_angle_gamma 83.036(3) _cell_formula_units_Z 2 _cell_length_a 7.9970(3) _cell_length_b 13.5824(3) _cell_length_c 16.6638(7) _cell_measurement_reflns_used 7454 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 66.9180 _cell_measurement_theta_min 3.3300 _cell_volume 1748.86(11) _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 5.1856 _diffrn_measured_fraction_theta_full 0.987 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur Ruby Gemini ultra' _diffrn_measurement_method \w _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0325 _diffrn_reflns_av_unetI/netI 0.0324 _diffrn_reflns_Laue_measured_fraction_full 0.987 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 17257 _diffrn_reflns_point_group_measured_fraction_full 0.987 _diffrn_reflns_point_group_measured_fraction_max 0.987 _diffrn_reflns_theta_full 67.226 _diffrn_reflns_theta_max 67.226 _diffrn_reflns_theta_min 2.724 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance Ultra (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 2.607 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.295 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'metallic dark red' _exptl_crystal_density_diffrn 1.355 _exptl_crystal_description plate _exptl_crystal_F_000 741 _exptl_crystal_size_max 0.700 _exptl_crystal_size_mid 0.257 _exptl_crystal_size_min 0.046 _refine_diff_density_max 0.607 _refine_diff_density_min -0.666 _refine_diff_density_rms 0.052 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 594 _refine_ls_number_reflns 6202 _refine_ls_number_restraints 137 _refine_ls_restrained_S_all 1.038 _refine_ls_R_factor_all 0.0601 _refine_ls_R_factor_gt 0.0528 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0656P)^2^+1.3374P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1342 _refine_ls_wR_factor_ref 0.1421 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5378 _reflns_number_total 6202 _reflns_threshold_expression I>2\s(I) _cod_data_source_file aw5025sup1.cif _cod_data_source_block lb0276_CLZ_SAC _cod_original_cell_volume 1748.87(11) _cod_database_code 2108443 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.263 _shelx_estimated_absorpt_t_max 0.889 _shelx_res_file ; TITL lb0276_clz_sac_a.res in P-1 lb0276_CLZ_SAC.res created by SHELXL-2016/6 at 14:20:33 on 17-Aug-2018 REM Old TITL lb0276_CLZ_SAC in P-1 REM SHELXT solution in P-1 REM R1 0.274, Rweak 0.029, Alpha 0.064, Orientation as input REM Formula found by SHELXT: C38 N4 O3 Cl3 CELL 1.54184 7.997 13.5824 16.6638 80.214 80.034 83.036 ZERR 2 0.0003 0.0003 0.0007 0.003 0.004 0.003 LATT 1 SFAC C H Cl N O S UNIT 73.5744 62.3617 4 12.7872 6 2 EQIV $1 -1+X,+Y,+Z EQIV $2 -X,1-Y,1-Z EQIV $3 1-X,1-Y,1-Z SADI N1 C13A N1 C13B L.S. 10 PLAN 15 SIZE 0.046 0.257 0.7 TEMP -173 HTAB C33 O3_$1 HTAB C24 O1_$2 HTAB N3 N5_$3 BOND $H list 4 CONF fmap 2 acta SIMU C25A > C26B DELU C25A > C26B ISOR 0.01 0.01 C27A WGHT 0.065600 1.337400 FVAR 6.39913 0.41052 0.43975 0.46406 0.48921 PART 1 C18A 1 -0.083353 0.756818 0.354294 21.00000 0.05826 0.03445 = 0.05769 -0.00425 -0.02468 -0.01023 AFIX 43 H18A 2 -0.009343 0.740921 0.394484 21.00000 -1.20000 AFIX 0 C17A 1 -0.083314 0.850014 0.301085 21.00000 0.08668 0.01766 = 0.08458 -0.00427 -0.03005 -0.01234 AFIX 43 H17A 2 -0.009993 0.898698 0.304484 21.00000 -1.20000 AFIX 0 C16A 1 -0.192638 0.867063 0.244824 21.00000 0.06499 0.02314 = 0.04836 -0.00242 -0.00562 0.00864 C15A 1 -0.294640 0.801178 0.233891 21.00000 0.03509 0.05193 = 0.03849 0.00159 -0.00329 0.00703 AFIX 43 H15A 2 -0.366024 0.817284 0.192566 21.00000 -1.20000 AFIX 0 C14A 1 -0.293974 0.708011 0.284620 21.00000 0.03315 0.03835 = 0.03786 -0.00051 -0.00703 -0.00187 AFIX 43 H14A 2 -0.361447 0.658946 0.275998 21.00000 -1.20000 AFIX 0 C13A 1 -0.198133 0.687012 0.345913 21.00000 0.02275 0.01896 = 0.04865 -0.00921 -0.00524 -0.00739 CL1A 3 -0.195587 0.986312 0.180209 21.00000 0.11468 0.02949 = 0.07355 0.01072 -0.00518 0.01416 REM SAME 0.02 0.04 C18A > Cl1A SIMU C18A > Cl1A DELU C18A > Cl1B PART 0 PART 2 C18B 1 -0.043523 0.745821 0.355661 -21.00000 0.02894 0.01830 = 0.04715 -0.00641 -0.00773 -0.00161 AFIX 43 H18B 2 0.044455 0.718926 0.387069 -21.00000 -1.20000 AFIX 0 C17B 1 -0.037621 0.838703 0.308988 -21.00000 0.03651 0.02356 = 0.04778 -0.00522 -0.00758 -0.00453 AFIX 43 H17B 2 0.057057 0.875862 0.306169 -21.00000 -1.20000 AFIX 0 C16B 1 -0.170767 0.879072 0.265396 -21.00000 0.04022 0.01363 = 0.05313 -0.00508 -0.00673 -0.00045 C15B 1 -0.308037 0.824578 0.267989 -21.00000 0.03858 0.03092 = 0.04791 0.00372 -0.01321 0.00320 AFIX 43 H15B 2 -0.398319 0.852104 0.238224 -21.00000 -1.20000 AFIX 0 C14B 1 -0.312558 0.730039 0.314133 -21.00000 0.03055 0.02536 = 0.04600 0.00132 -0.01279 -0.00327 AFIX 43 H14B 2 -0.405390 0.691379 0.317064 -21.00000 -1.20000 AFIX 0 C13B 1 -0.175716 0.693099 0.356447 -21.00000 0.02402 0.01618 = 0.04241 -0.00398 -0.01261 0.00132 CL1B 3 -0.164990 0.997332 0.208050 -21.00000 0.06038 0.02226 = 0.06526 0.01126 -0.00915 -0.00268 PART 0 CL2 3 0.268626 -0.157360 0.457608 11.00000 0.04806 0.02345 = 0.07522 0.00575 -0.01260 0.00517 S1 6 0.247120 0.691226 0.799204 11.00000 0.03842 0.06134 = 0.06783 -0.03626 -0.01319 0.01308 N2 4 -0.168546 0.406581 0.505187 11.00000 0.02625 0.02067 = 0.03930 -0.00701 -0.00687 -0.00313 N3 4 0.248598 0.268647 0.302226 11.00000 0.02904 0.02238 = 0.03944 -0.00567 -0.00343 0.00006 REM AFIX 43 H3 2 0.344730 0.285312 0.272364 11.00000 -1.20000 REM AFIX 0 N1 4 -0.185798 0.592426 0.403396 11.00000 0.02516 0.01836 = 0.04309 -0.00312 -0.00668 -0.00058 N4 4 0.203187 0.442579 0.195687 11.00000 0.05026 0.02357 = 0.04622 0.00144 0.00541 0.00388 H4N 2 0.262126 0.389025 0.183224 11.00000 -1.20000 O3 5 0.589506 0.736596 0.900210 11.00000 0.03566 0.10216 = 0.06707 0.01763 -0.02010 -0.01915 C12 1 -0.287851 0.580949 0.479920 11.00000 0.02484 0.02394 = 0.04147 -0.00789 -0.00917 -0.00222 C5 1 -0.275556 0.486001 0.529947 11.00000 0.02506 0.02201 = 0.04054 -0.00872 -0.00764 -0.00274 C6 1 -0.077759 0.418856 0.430780 11.00000 0.02524 0.01968 = 0.03751 -0.00424 -0.00844 -0.00436 N5 4 0.441093 0.691912 0.811136 11.00000 0.03066 0.05624 = 0.04974 -0.00414 -0.00255 0.01042 C7 1 0.034916 0.337406 0.404376 11.00000 0.02788 0.01777 = 0.03862 -0.00395 -0.00858 -0.00170 AFIX 43 H7 2 0.040969 0.275383 0.440520 11.00000 -1.20000 AFIX 0 C19 1 0.251949 0.168210 0.342246 11.00000 0.03377 0.02017 = 0.03728 -0.00787 -0.00864 0.00154 C10 1 0.017123 0.522532 0.298607 11.00000 0.02984 0.01852 = 0.04341 -0.00117 -0.00814 -0.00259 AFIX 43 H10 2 0.015667 0.585425 0.263477 11.00000 -1.20000 AFIX 0 C11 1 -0.081547 0.513905 0.374932 11.00000 0.02326 0.01884 = 0.04201 -0.00667 -0.00849 -0.00266 O1 5 0.215430 0.753068 0.723636 11.00000 0.06192 0.14816 = 0.05341 -0.04563 -0.02264 0.04580 C9 1 0.120285 0.439554 0.271735 11.00000 0.02882 0.02337 = 0.03957 -0.00283 -0.00413 -0.00419 C8 1 0.134271 0.345217 0.329207 11.00000 0.02746 0.01926 = 0.03784 -0.00634 -0.00866 -0.00118 C24 1 0.102862 0.120830 0.365019 11.00000 0.03181 0.02224 = 0.04430 -0.00801 -0.01120 0.00321 AFIX 43 H24 2 -0.003122 0.156834 0.355473 11.00000 -1.20000 AFIX 0 C34 1 0.151220 0.750299 0.883784 11.00000 0.02777 0.02579 = 0.04291 -0.00200 -0.00321 -0.00101 C29 1 0.281315 0.769836 0.921566 11.00000 0.03676 0.03274 = 0.03782 0.00379 -0.00832 -0.00552 C3 1 -0.488657 0.549222 0.635247 11.00000 0.02881 0.03466 = 0.04215 -0.01426 -0.00563 -0.00307 AFIX 43 H3A 2 -0.557790 0.539163 0.687848 11.00000 -1.20000 AFIX 0 C4 1 -0.376201 0.472452 0.608438 11.00000 0.03029 0.02571 = 0.04164 -0.00819 -0.00726 -0.00422 AFIX 43 H4A 2 -0.366250 0.409589 0.643216 11.00000 -1.20000 AFIX 0 C2 1 -0.500699 0.642656 0.584356 11.00000 0.02827 0.03041 = 0.04959 -0.01763 -0.01070 0.00297 AFIX 43 H2 2 -0.579359 0.695365 0.602906 11.00000 -1.20000 AFIX 0 C23 1 0.108065 0.021226 0.401618 11.00000 0.03488 0.02226 = 0.04666 -0.00648 -0.00941 -0.00082 AFIX 43 H23 2 0.005873 -0.010904 0.418443 11.00000 -1.20000 AFIX 0 C1 1 -0.401361 0.659475 0.508448 11.00000 0.02994 0.02334 = 0.04957 -0.01034 -0.01190 0.00202 AFIX 43 H1 2 -0.409208 0.723667 0.475426 11.00000 -1.20000 AFIX 0 C20 1 0.408547 0.114913 0.354608 11.00000 0.03098 0.02854 = 0.04605 -0.00622 -0.00924 -0.00014 AFIX 43 H20 2 0.510766 0.147163 0.338832 11.00000 -1.20000 AFIX 0 C21 1 0.414006 0.014529 0.390082 11.00000 0.03458 0.03029 = 0.05189 -0.00522 -0.01194 0.00818 AFIX 43 H21 2 0.520025 -0.022423 0.398206 11.00000 -1.20000 AFIX 0 C22 1 0.264324 -0.031139 0.413441 11.00000 0.04129 0.01946 = 0.04778 -0.00200 -0.01198 0.00260 O2 5 0.200868 0.589875 0.811011 11.00000 0.07556 0.07105 = 0.19769 -0.08880 -0.02448 0.00208 C28 1 0.452245 0.732402 0.877690 11.00000 0.02742 0.04918 = 0.04924 0.01578 -0.00848 -0.00659 C33 1 -0.018500 0.775004 0.911961 11.00000 0.02836 0.04609 = 0.05871 0.00151 -0.00074 0.00221 AFIX 43 H33 2 -0.106794 0.759927 0.885799 11.00000 -1.20000 AFIX 0 C30 1 0.245023 0.816747 0.990377 11.00000 0.07582 0.07743 = 0.04712 -0.01761 -0.02042 -0.00166 AFIX 43 H30 2 0.333496 0.830010 1.017297 11.00000 -1.20000 AFIX 0 C32 1 -0.052666 0.823144 0.980722 11.00000 0.05598 0.08532 = 0.05049 -0.00161 0.01282 0.02917 AFIX 43 H32 2 -0.167728 0.842433 1.002159 11.00000 -1.20000 AFIX 0 C31 1 0.076752 0.843842 1.018979 11.00000 0.09722 0.10752 = 0.04518 -0.02966 -0.00768 0.03131 AFIX 43 H31 2 0.048815 0.877363 1.065830 11.00000 -1.20000 AFIX 0 PART 2 N6 4 0.371972 0.714638 0.202478 31.00000 0.06482 0.08393 = 0.05418 0.00105 -0.01905 -0.02546 C36 1 0.499076 0.693768 0.160985 31.00000 0.07000 0.05885 = 0.04592 0.00041 -0.01898 -0.02274 C35 1 0.664403 0.669569 0.108721 31.00000 0.08764 0.05309 = 0.05163 -0.00866 -0.00262 -0.01476 AFIX 137 H35A 2 0.651742 0.687667 0.050450 31.00000 -1.50000 H35B 2 0.699050 0.597539 0.120559 31.00000 -1.50000 H35C 2 0.751454 0.707540 0.120684 31.00000 -1.50000 AFIX 0 C38 1 0.440840 0.976461 0.105526 41.00000 0.04526 0.05817 = 0.05090 -0.01412 -0.00244 -0.01008 N7 4 0.537777 0.940194 0.055298 41.00000 0.05318 0.11695 = 0.08260 -0.03652 0.00044 -0.01650 C37 1 0.328756 1.031875 0.168029 41.00000 0.05249 0.09041 = 0.02489 -0.01302 -0.00617 0.00810 AFIX 137 H37A 2 0.211662 1.013948 0.174130 41.00000 -1.50000 H37B 2 0.330988 1.104276 0.149812 41.00000 -1.50000 H37C 2 0.370137 1.013732 0.221121 41.00000 -1.50000 AFIX 0 PART 0 PART 1 N7A 4 0.314759 0.852406 0.184436 51.00000 0.07907 0.10911 = 0.13101 -0.05608 -0.05074 0.01433 C38A 1 0.325892 0.939248 0.173370 51.00000 0.06945 0.10585 = 0.08366 -0.04393 -0.03873 0.01696 C37A 1 0.325534 1.024056 0.164089 51.00000 0.16477 0.16536 = 0.19129 -0.09933 -0.07964 0.12266 AFIX 137 H37D 2 0.218547 1.053208 0.192962 51.00000 -1.50000 H37E 2 0.335909 1.050345 0.105096 51.00000 -1.50000 H37F 2 0.421836 1.041804 0.186201 51.00000 -1.50000 AFIX 0 PART 1 C25A 1 0.212852 0.537260 0.135167 -31.00000 0.09133 0.01861 = 0.03678 0.00518 0.01812 0.00555 AFIX 13 H25A 2 0.105698 0.581761 0.147950 -31.00000 -1.20000 AFIX 0 C27A 1 0.208883 0.500102 0.054243 -31.00000 0.08030 0.05556 = 0.04499 0.01031 -0.00682 -0.01194 AFIX 137 H27A 2 0.209451 0.557256 0.009553 -31.00000 -1.50000 H27B 2 0.105302 0.466343 0.058851 -31.00000 -1.50000 H27C 2 0.309343 0.452821 0.042306 -31.00000 -1.50000 AFIX 0 C26A 1 0.351449 0.589388 0.139507 -31.00000 0.18815 0.05532 = 0.05847 0.02039 -0.03086 -0.06411 AFIX 137 H26A 2 0.349964 0.651831 0.100170 -31.00000 -1.50000 H26B 2 0.458179 0.547645 0.125955 -31.00000 -1.50000 H26C 2 0.342965 0.605080 0.195424 -31.00000 -1.50000 AFIX 0 PART 0 PART 2 C25B 1 0.195313 0.523298 0.124069 31.00000 0.04179 0.01876 = 0.06210 -0.01300 0.00060 -0.00760 AFIX 13 H25B 2 0.205041 0.586718 0.145148 31.00000 -1.20000 AFIX 0 C26B 1 0.355362 0.510631 0.057757 31.00000 0.08566 0.04166 = 0.04952 0.00875 0.02878 0.00993 AFIX 137 H26D 2 0.353189 0.567388 0.012817 31.00000 -1.50000 H26E 2 0.355519 0.448001 0.035947 31.00000 -1.50000 H26F 2 0.458403 0.508508 0.082651 31.00000 -1.50000 AFIX 0 C27B 1 0.036059 0.540109 0.089678 31.00000 0.08966 0.03426 = 0.05925 0.01003 -0.02572 -0.00553 AFIX 137 H27D 2 0.040578 0.598774 0.046325 31.00000 -1.50000 H27E 2 -0.059811 0.551906 0.133379 31.00000 -1.50000 H27F 2 0.020726 0.480909 0.066293 31.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM lb0276_clz_sac_a.res in P-1 REM R1 = 0.0528 for 5378 Fo > 4sig(Fo) and 0.0601 for all 6202 data REM 594 parameters refined using 137 restraints END WGHT 0.0656 1.3374 REM Highest difference peak 0.607, deepest hole -0.666, 1-sigma level 0.052 Q1 1 0.5588 0.7983 0.9198 11.00000 0.05 0.61 Q2 1 0.1826 0.6335 0.7725 11.00000 0.05 0.50 Q3 1 0.2837 0.7800 0.2233 11.00000 0.05 0.48 Q4 1 0.2427 0.7298 0.7575 11.00000 0.05 0.43 Q5 1 0.2195 0.8044 0.7228 11.00000 0.05 0.42 Q6 1 0.1812 0.5812 0.8366 11.00000 0.05 0.39 Q7 1 0.2847 0.4584 0.2188 11.00000 0.05 0.35 Q8 1 0.2911 0.5913 0.8200 11.00000 0.05 0.34 Q9 1 0.1493 0.7311 0.7402 11.00000 0.05 0.33 Q10 1 0.3498 0.6975 0.8093 11.00000 0.05 0.33 Q11 1 0.4797 0.7389 0.8277 11.00000 0.05 0.25 Q12 1 0.6788 0.5828 0.1918 11.00000 0.05 0.24 Q13 1 0.5641 0.8573 0.0508 11.00000 0.05 0.22 Q14 1 0.5911 0.7562 0.0812 11.00000 0.05 0.21 Q15 1 0.3847 1.0436 0.0803 11.00000 0.05 0.20 ; 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1297.01 24 0 7 8 11253.6 652.751 23 0 7 8 10923.1 608.935 21 0 7 8 10868.6 572.116 4 0 7 8 11509.2 511.645 7 0 7 8 11374.0 601.249 6 0 -7 -9 7041.75 1035.22 24 0 7 9 8144.86 578.471 27 0 7 9 7859.08 452.532 4 0 7 9 7768.46 591.898 23 0 7 9 8270.40 584.950 26 0 7 9 8067.32 591.164 13 0 7 9 7418.44 532.004 15 0 7 9 7618.95 525.296 21 0 7 10 2547.25 380.056 23 0 7 10 2410.37 306.711 21 0 7 10 2449.96 359.386 13 0 7 10 2395.89 302.029 15 0 -7 -10 2104.94 603.169 24 0 7 10 2283.84 340.540 26 0 7 10 2469.07 337.558 27 0 7 11 10368.5 724.729 27 0 7 11 10179.3 624.807 21 0 7 11 11392.9 761.070 26 0 7 11 10305.4 778.175 13 0 7 11 9020.20 680.084 23 0 7 11 10915.9 631.459 15 0 -7 -11 9177.71 1260.65 24 0 7 12 7663.15 673.168 13 0 7 12 7536.38 553.958 21 0 7 12 7330.11 597.118 23 0 -7 -12 5766.83 1035.63 24 0 7 12 7561.11 530.350 15 0 7 12 7749.45 620.408 27 0 7 12 7499.83 644.305 26 0 7 13 18945.8 959.463 27 0 7 13 19177.3 1019.15 13 0 7 13 18719.6 914.968 23 0 7 13 19283.3 1013.70 26 0 7 13 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238.602 30 0 8 -4 1468.40 218.637 12 0 8 -4 1656.78 235.864 8 0 8 -4 1351.14 466.943 28 0 8 -4 1433.58 235.259 11 0 8 -3 1066.81 223.280 17 0 8 -3 1069.99 185.580 30 0 8 -3 1029.10 187.278 11 0 8 -3 1074.82 173.287 12 0 8 -3 1166.11 197.903 8 0 8 -3 992.653 187.316 1 0 8 -3 785.067 360.060 28 0 8 -2 12711.9 610.860 12 0 8 -2 12663.7 1210.84 28 0 8 -2 12961.3 612.188 11 0 8 -2 13017.5 636.463 17 0 8 -2 13138.7 619.773 30 0 8 -2 12879.0 619.441 1 0 8 -1 9535.87 497.554 11 0 8 -1 10413.4 568.743 12 0 8 -1 9760.84 511.012 30 0 8 -1 9653.55 481.044 4 0 8 -1 10283.7 538.579 1 0 8 -1 9709.34 941.799 28 0 8 0 8559.28 452.202 11 0 8 0 8095.19 443.374 4 0 8 0 8685.65 825.576 28 0 8 0 8945.04 559.745 12 0 8 1 36.4654 53.7164 15 0 8 1 41.1165 51.4218 23 0 8 1 249.526 221.640 28 0 8 1 47.4757 46.7707 7 0 8 1 74.1736 87.0001 12 0 8 1 65.8403 71.1944 11 0 8 1 190.592 82.3618 4 0 8 2 13352.1 595.852 12 0 8 2 12744.9 535.040 7 0 8 2 13422.8 566.867 15 0 8 2 12942.5 605.935 13 0 8 2 12534.9 580.699 23 0 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9194.05 591.332 26 0 8 7 8900.32 510.215 6 0 8 7 9635.04 601.345 13 0 8 7 8913.23 571.037 23 0 8 7 8581.46 556.003 21 0 8 7 9127.27 497.573 7 0 8 8 546.823 184.707 13 0 8 8 654.437 135.717 7 0 -8 -8 897.425 396.648 24 0 8 8 564.035 161.571 6 0 8 8 397.383 125.765 27 0 8 8 515.082 154.190 15 0 8 8 581.662 145.932 21 0 8 8 575.058 154.151 4 0 8 8 650.848 164.143 26 0 8 8 646.545 181.780 23 0 8 9 179.842 137.282 23 0 8 9 292.625 127.170 21 0 -8 -9-197.472 281.456 24 0 8 9 87.4894 89.1948 13 0 8 9 176.533 116.232 26 0 8 9 154.646 77.2817 7 0 8 9 144.502 88.9055 4 0 8 9 79.6250 104.886 15 0 8 9 462.836 173.488 27 0 8 10 3123.63 404.739 13 0 8 10 3695.07 442.328 23 0 8 10 3505.05 416.033 27 0 8 10 3428.34 414.920 26 0 -8 -10 2955.08 738.585 24 0 8 10 3220.62 329.646 4 0 8 10 3291.49 377.197 15 0 8 10 3010.01 364.739 21 0 -8 -11 3259.18 768.418 24 0 8 11 3831.47 412.427 21 0 8 11 3454.72 443.080 23 0 8 11 4383.92 493.874 27 0 8 11 4084.10 423.815 15 0 8 11 4080.58 473.566 26 0 8 11 4221.63 482.599 13 0 8 12 1590.99 328.284 26 0 8 12 1466.18 249.526 15 0 8 12 1655.43 305.993 27 0 8 12 1569.76 319.846 13 0 8 12 1407.06 273.140 23 0 8 12 1270.51 257.581 21 0 8 13 20101.3 1050.15 13 0 8 13 20092.9 1044.69 26 0 8 13 19811.4 948.094 23 0 8 13 19205.4 985.934 27 0 8 13 19218.1 847.507 15 0 8 14 3824.39 369.151 15 0 8 14 3863.60 451.416 26 0 8 14 3898.41 455.740 13 0 8 14 4042.71 436.766 27 0 8 14 3533.91 401.120 23 0 8 15 142.888 72.7916 15 0 8 15-75.8799 111.725 26 0 8 15-61.5883 109.684 27 0 8 15 196.896 113.654 13 0 8 15-55.7426 91.3722 23 0 8 16 26.8033 77.6173 13 0 8 16 217.821 107.503 27 0 8 16 67.9101 76.4101 26 0 8 16-50.8560 70.7593 23 0 8 17 3159.03 336.098 13 0 8 17 2684.32 288.911 27 0 8 18 117.502 66.4367 13 0 9 -14 258.202 97.7560 1 0 9 -13 1719.54 249.010 1 0 9 -13 1884.29 245.766 30 0 9 -12 82.8441 104.197 1 0 9 -12 197.056 122.426 30 0 9 -12-5.71886 90.2968 17 0 9 -11 350.224 169.349 30 0 9 -11 80.6099 79.9577 17 0 9 -11 188.951 135.679 1 0 9 -11 184.445 94.4646 11 0 9 -10 10578.1 597.957 11 0 9 -10 10835.4 751.652 1 0 9 -10 10588.8 722.229 30 0 9 -9-7.86061 64.6832 11 0 9 -9-34.0310 121.854 30 0 9 -9 30.2750 135.635 1 0 9 -9-81.8124 167.580 17 0 9 -8 332.505 159.023 17 0 9 -8 461.962 156.737 30 0 9 -8 620.488 164.558 11 0 9 -8 401.780 173.059 1 0 9 -7 73239.9 1961.75 30 0 9 -7 78977.5 3746.58 28 0 9 -7 71132.8 1583.44 12 0 9 -7 67135.0 1877.05 17 0 9 -7 76583.9 1721.19 11 0 9 -7 73003.0 1908.81 1 0 9 -6 4346.93 454.104 1 0 9 -6 3936.35 374.901 12 0 9 -6 3824.71 457.392 8 0 9 -6 3540.70 416.775 17 0 9 -6 4186.33 417.026 11 0 9 -6 4701.98 922.606 28 0 9 -6 4103.72 446.645 30 0 9 -5 6564.34 529.331 30 0 9 -5 7018.55 1134.54 28 0 9 -5 6300.41 525.186 17 0 9 -5 6271.46 518.811 1 0 9 -5 6494.13 477.472 12 0 9 -5 5861.63 489.871 8 0 9 -5 6553.75 549.345 11 0 9 -4 3183.38 359.473 30 0 9 -4 3753.15 841.455 28 0 9 -4 2798.10 332.770 17 0 9 -4 2839.85 372.409 11 0 9 -4 2914.25 330.904 12 0 9 -4 3078.79 347.100 1 0 9 -4 2985.33 336.317 8 0 9 -3 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4 0 9 3 16645.1 728.844 23 0 9 3 16269.5 736.509 13 0 9 3 17073.7 701.349 12 0 9 3 16445.5 684.291 7 0 9 3 15974.5 684.954 16 0 9 3 16021.8 654.872 11 0 9 3 16281.5 661.347 17 0 9 3 17091.2 705.699 15 0 9 3 16167.0 742.645 21 0 9 4 79581.8 1391.41 6 0 9 4 80801.9 1575.45 15 0 9 4 80789.0 1668.39 13 0 9 4 80305.0 1553.16 4 0 9 4 81976.5 1591.49 7 0 9 4 81517.2 1486.66 12 0 9 4 81264.9 1636.45 23 0 9 4 81670.2 1679.64 21 0 9 4 80605.8 1451.54 11 0 9 5 40037.9 1155.79 7 0 9 5 40503.0 1204.17 13 0 9 5 40383.3 1142.97 15 0 9 5 40473.8 1186.19 23 0 -9 -5 43233.2 2170.35 24 0 9 5 39369.8 1015.64 6 0 9 5 38506.3 1155.61 21 0 9 5 40331.1 1154.93 4 0 9 6 247.763 129.125 4 0 -9 -6 48.0523 166.572 24 0 9 6 178.263 106.764 7 0 9 6 267.363 115.611 15 0 9 6 199.306 136.152 27 0 9 6 260.559 112.547 13 0 9 6 208.096 126.145 21 0 9 6 180.930 91.3735 6 0 9 6 32.1215 76.9592 23 0 9 7 103.019 87.7821 7 0 9 7 34.7268 60.0650 6 0 9 7 162.431 125.023 4 0 9 7 52.3947 95.0468 15 0 9 7 192.670 93.5570 27 0 9 7 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782.589 179.067 11 0 12 -7 476.516 146.898 11 0 12 -7 439.934 187.770 16 0 12 -7 441.786 152.669 9 0 12 -6 1402.14 261.877 11 0 12 -6 906.361 247.860 16 0 12 -5 22.9741 104.812 16 0 12 -5 85.9787 135.829 11 0 12 -4 3829.16 453.844 11 0 12 -4 3363.08 433.568 8 0 12 -4 3449.73 428.367 16 0 12 -3 348.954 134.644 16 0 12 -3 424.926 134.003 12 0 12 -3 677.046 210.851 11 0 12 -3 710.120 199.383 8 0 12 -2 7962.00 618.866 11 0 12 -2 7654.08 565.782 8 0 12 -2 8036.65 607.768 12 0 12 -2 7718.79 602.036 16 0 12 -1 103.176 105.897 8 0 12 -1 221.883 161.620 12 0 12 -1-35.7685 85.5440 11 0 12 -1 63.6522 75.9135 16 0 12 0 40540.5 1304.73 11 0 12 0 41433.4 1498.30 12 0 12 0 41733.0 1210.89 15 0 12 0 40403.5 1293.95 16 0 12 1 43900.4 1498.06 12 0 12 1 46901.3 1359.71 16 0 12 1 47011.3 1307.39 15 0 12 1 45391.9 1354.54 11 0 12 2 94492.3 2062.50 12 0 12 2 92271.5 1886.38 11 0 12 2 93738.8 1872.71 16 0 12 2 90313.5 1862.63 15 0 12 3 44552.3 1324.13 15 0 12 3 45372.1 1365.94 12 0 12 3 44861.8 1300.84 11 0 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553.883 16 0 13 -7 8283.54 513.367 11 0 13 -6 751.054 202.987 16 0 13 -6 883.416 179.532 11 0 13 -6 753.045 176.912 9 0 13 -5 1927.83 298.752 16 0 13 -5 2656.69 348.561 11 0 13 -4 3986.93 428.608 16 0 13 -4 4273.87 462.878 11 0 13 -3 13783.5 772.748 16 0 13 -3 11535.4 727.835 8 0 13 -3 13844.9 827.666 11 0 13 -2-18.1510 103.621 11 0 13 -2 196.506 134.278 8 0 13 -2-35.7147 94.6607 16 0 13 -1 829.490 195.975 16 0 13 -1 791.096 211.152 11 0 13 -1 579.865 158.572 8 0 13 0 1378.66 258.323 11 0 13 0 1369.90 244.612 8 0 13 0 1350.89 240.579 16 0 13 1 21263.2 925.260 8 0 13 1 22695.2 952.801 11 0 13 1 21283.6 867.421 15 0 13 2 8718.49 579.920 15 0 13 2 9027.07 589.737 10 0 13 2 8709.41 581.885 11 0 13 3 4105.57 411.524 15 0 13 3 3833.62 384.123 11 0 13 4 55.6514 119.978 15 0 13 5 5796.03 492.491 15 0 13 6 117.389 105.867 21 0 13 6 56.1520 115.159 15 0 13 7 4392.92 396.603 21 0 13 7 4850.54 457.575 15 0 13 8 9955.58 592.842 21 0 13 8 10518.6 678.848 15 0 13 9 6118.77 449.104 21 0 13 9 6596.02 546.896 15 0 13 10 1666.47 284.001 15 0 13 11 12825.5 691.409 15 0 13 12 9743.21 556.300 15 0 13 13-40.0415 75.7981 15 0 14 -6 3925.57 319.933 9 0 14 -6 4034.66 339.221 11 0 14 -6 3094.84 312.753 16 0 14 -5 352.464 130.097 9 0 14 -5 298.168 106.875 11 0 14 -5 253.729 108.941 16 0 14 -4 13598.4 682.415 16 0 14 -4 15136.9 764.441 11 0 14 -3 8039.29 527.741 16 0 14 -3 7661.76 569.938 11 0 14 -2 332.134 119.549 16 0 14 -2 116.468 139.722 8 0 14 -2 284.186 128.715 11 0 14 -1 348.396 143.922 11 0 14 -1 203.684 146.000 8 0 14 0 88.6773 70.5703 11 0 14 0 198.512 117.768 10 0 14 0 208.524 101.195 8 0 14 1 1071.66 199.608 10 0 14 1 1137.79 205.480 11 0 14 1 1244.30 223.003 8 0 14 2 605.719 166.558 8 0 14 2 558.882 153.761 11 0 14 2 389.146 123.610 15 0 14 3 1236.09 216.390 15 0 14 4 6281.83 475.245 15 0 14 5 146.769 102.774 15 0 14 6 12310.0 681.042 15 0 14 7 6866.74 513.539 15 0 14 8 6786.35 511.236 15 0 14 9 310.804 114.798 15 0 14 10 1934.82 263.620 15 0 14 11 4728.69 382.986 15 0 14 12 892.717 155.327 15 0 15 -4 3655.96 302.236 9 0 15 -4 2952.19 290.235 11 0 15 -3 341.292 93.8371 11 0 15 -3 464.432 133.991 9 0 15 -3 150.130 102.250 10 0 15 -2 3473.14 341.234 11 0 15 -2 3123.66 315.138 10 0 15 -1 3546.11 333.520 8 0 15 -1 2805.13 285.239 10 0 15 -1 3982.70 359.781 11 0 15 0 487.904 136.383 10 0 15 0 376.773 151.946 8 0 15 1 7879.34 480.556 8 0 15 2 917.877 174.850 8 0 15 3 142.345 88.0880 8 0 15 4 4490.24 354.813 15 0 15 4 5028.51 391.739 8 0 15 5-221.339 113.643 15 0 15 6 204.462 107.252 15 0 15 7 5173.98 405.208 15 0 15 8-65.2575 89.8470 15 0 15 9-97.6910 97.4011 15 -1 15 7 831.742 153.738 15 -1 15 6 111.450 73.7208 8 -1 15 6 178.526 82.3362 15 -1 15 5 175.362 93.2311 8 -1 15 4 1409.65 194.688 8 -1 15 3 1678.57 220.248 9 -1 15 2 168.927 92.2223 9 -1 15 1 89.4016 62.2432 10 -1 15 1 386.081 145.063 9 -1 15 0 88.6416 92.6359 9 -1 15 0-7.55227 59.2203 10 -1 15 -1 3963.81 342.481 10 -1 15 -1 4602.56 373.450 9 -1 15 -2 8483.08 502.648 10 -1 15 -2 9452.38 512.555 9 -1 15 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294.049 23 1 11 8 1505.86 289.600 15 1 11 8 1503.72 259.407 21 1 11 8 1426.04 274.906 4 1 11 8 1729.07 303.058 13 1 11 9 5454.74 512.829 23 1 11 9 5465.34 529.837 13 1 11 9 4644.49 441.579 21 1 11 9 4985.11 503.703 15 1 11 9 5655.01 493.335 4 1 11 10 8489.32 661.524 13 1 11 10 7877.65 640.314 23 1 11 10 7584.14 543.962 4 1 11 10 7556.26 627.055 15 1 11 11 13172.5 790.805 15 1 11 11 13752.0 870.214 23 1 11 11 13847.2 695.341 4 1 11 11 13531.0 845.091 13 1 11 12 67.1927 95.3882 4 1 11 12 122.265 98.4344 15 1 11 12 121.997 176.550 23 1 11 12 178.970 153.103 13 1 11 13 1177.43 217.795 15 1 11 13 1220.02 237.939 13 1 11 13 1058.67 231.830 23 1 11 14 1003.21 202.023 23 1 11 14 736.840 171.461 15 1 11 14 821.142 197.206 13 1 11 15 4516.80 341.505 15 1 11 15 4396.28 375.805 23 1 11 15 4043.17 381.822 13 1 11 16 862.302 152.857 13 1 11 16 1052.36 176.667 23 1 12 -10 217.286 94.7578 16 1 12 -10 316.336 102.960 11 1 12 -9 4314.77 346.252 11 1 12 -8 939.863 182.046 11 1 12 -7 7181.61 513.108 11 1 12 -6 14880.4 778.277 11 1 12 -5 24574.4 1062.67 11 1 12 -5 23834.2 944.047 12 1 12 -4 122.536 112.835 11 1 12 -4-6.08144 187.616 8 1 12 -4 106.438 72.3168 12 1 12 -3 7667.03 618.033 11 1 12 -3 6842.65 577.007 16 1 12 -3 7109.15 580.076 8 1 12 -3 7161.69 540.986 12 1 12 -2 10385.1 679.694 8 1 12 -2 10211.9 671.330 16 1 12 -2 10397.7 701.022 11 1 12 -2 11393.7 701.377 12 1 12 -1 351.549 129.166 11 1 12 -1 348.508 133.141 8 1 12 -1 367.854 147.481 16 1 12 -1 878.543 203.171 15 1 12 -1 634.302 191.016 12 1 12 0 17556.8 854.681 8 1 12 0 18298.2 849.607 15 1 12 0 18963.1 946.605 12 1 12 0 17685.5 842.059 11 1 12 1 541.430 146.873 11 1 12 1 453.425 136.369 15 1 12 1 620.972 234.382 12 1 12 2 12973.4 770.665 12 1 12 2 12948.4 685.331 11 1 12 2 13000.4 733.625 15 1 12 3 44755.3 1314.06 4 1 12 3 46835.7 1399.55 12 1 12 3 45134.2 1371.17 15 1 12 3 45959.8 1248.75 11 1 12 4 40633.3 1319.01 15 1 12 4 42194.2 1270.11 12 1 12 4 41716.1 1294.42 4 1 12 5 429.085 142.623 4 1 12 5 460.489 166.512 15 1 12 5 495.669 148.808 12 1 12 5 342.158 149.086 23 1 12 6 960.876 214.922 21 1 12 6 883.865 194.384 4 1 12 6 967.773 233.468 23 1 12 6 897.556 215.301 15 1 12 7 937.900 220.432 23 1 12 7 1050.01 236.196 4 1 12 7 737.674 207.716 15 1 12 7 764.592 197.237 21 1 12 8 7986.07 628.960 15 1 12 8 8017.70 606.452 23 1 12 8 7423.53 583.661 4 1 12 9-11.8906 92.4592 15 1 12 9 116.589 84.7477 4 1 12 9 150.030 110.799 13 1 12 9-35.6201 138.275 23 1 12 10 3996.80 447.592 13 1 12 10 4004.66 386.636 4 1 12 10 4003.01 449.201 23 1 12 10 3669.47 425.658 15 1 12 11 1686.98 301.895 13 1 12 11 1340.59 258.536 15 1 12 11 1611.88 293.140 23 1 12 11 1480.23 232.565 4 1 12 12 7411.95 535.817 15 1 12 12 6908.00 447.645 4 1 12 12 6790.01 575.190 13 1 12 12 6761.86 557.468 23 1 12 13 138.768 100.984 15 1 12 13 283.966 120.257 23 1 12 13 107.754 109.036 13 1 12 14 391.160 116.222 15 1 12 14 278.583 115.064 23 1 12 14 495.847 155.334 13 1 12 15 1903.87 234.335 13 1 12 15 1990.46 234.951 23 1 13 -8 702.875 149.806 16 1 13 -8 776.457 152.805 11 1 13 -7 775.723 178.929 16 1 13 -7 843.073 172.373 11 1 13 -7 859.599 143.771 9 1 13 -6 15808.8 737.722 11 1 13 -6 12877.9 727.810 16 1 13 -5 570.224 173.209 11 1 13 -5 551.880 162.266 16 1 13 -4 30.9741 110.041 11 1 13 -4-0.36294 113.570 12 1 13 -4 63.5912 83.0045 16 1 13 -3 854.359 219.523 11 1 13 -3 574.059 198.260 8 1 13 -3 761.812 185.514 12 1 13 -3 754.384 186.593 16 1 13 -2 636.730 181.548 11 1 13 -2 194.281 139.366 8 1 13 -2 489.823 162.839 12 1 13 -2 332.455 117.577 16 1 13 -1 3236.70 392.649 11 1 13 -1 2879.77 359.458 8 1 13 -1 3065.42 372.302 12 1 13 0 2241.08 312.613 8 1 13 0 2450.15 312.405 15 1 13 0 2124.83 309.571 11 1 13 0 2172.74 327.909 12 1 13 1 24375.7 1008.28 8 1 13 1 25098.6 984.670 15 1 13 1 26931.2 1170.57 12 1 13 1 26027.9 994.473 11 1 13 2 2343.75 310.454 15 1 13 2 2142.69 324.376 12 1 13 2 2262.63 293.576 11 1 13 3 40340.7 1290.90 15 1 13 3 41992.5 1335.05 12 1 13 4 24961.2 1029.88 15 1 13 4 25558.3 987.599 12 1 13 5 43738.1 1345.53 4 1 13 5 40043.7 1323.34 15 1 13 5 41042.6 1197.76 12 1 13 6 20455.7 950.885 15 1 13 6 21832.1 977.587 4 1 13 7 2882.27 370.215 4 1 13 7 3112.84 369.387 15 1 13 7 3110.08 370.601 23 1 13 8 2023.25 321.645 15 1 13 8 1791.40 286.430 23 1 13 8 1521.83 268.232 4 1 13 9 2225.60 328.652 15 1 13 9 2036.92 289.397 4 1 13 9 2274.80 332.830 23 1 13 10 25.0163 69.9986 4 1 13 10 55.4239 100.650 15 1 13 10 139.941 97.1827 23 1 13 11 1957.70 317.138 23 1 13 11 1725.92 267.092 15 1 13 12 331.680 123.605 15 1 13 12 306.293 118.334 23 1 13 13 8465.00 495.220 15 1 13 13 8391.89 515.335 23 1 13 14 44.9004 49.3401 23 1 14 -6 11566.1 560.785 11 1 14 -5 386.663 114.947 16 1 14 -5 762.435 179.488 11 1 14 -4 6261.73 479.085 11 1 14 -3 129.538 97.9975 11 1 14 -2 1554.86 275.089 8 1 14 -2 1816.22 272.577 11 1 14 -1 6073.95 509.949 8 1 14 -1 6326.09 506.842 12 1 14 -1 6191.01 481.443 11 1 14 0 2623.99 316.294 8 1 14 0 2692.99 349.840 12 1 14 0 2598.05 317.478 11 1 14 1 369.746 141.754 8 1 14 1 227.119 115.592 12 1 14 1 212.638 111.082 15 1 14 1 197.393 103.306 11 1 14 2 1364.23 213.003 11 1 14 2 1544.70 251.505 8 1 14 2 1438.20 238.368 15 1 14 2 1525.03 258.797 12 1 14 3 527.569 171.797 15 1 14 4 38.1643 87.2693 15 1 14 5 1947.31 297.824 15 1 14 6 1136.99 234.400 15 1 14 7 278.895 114.487 15 1 14 8 1783.20 275.355 15 1 14 9 430.528 151.517 15 1 14 10 1383.77 235.303 15 1 14 11 160.945 104.943 15 1 14 12 6692.07 431.120 15 1 15 -4 10934.6 540.072 11 1 15 -3 107.360 79.9383 11 1 15 -2 730.857 165.536 11 1 15 -1 8607.32 537.614 8 1 15 -1 9258.01 535.341 11 1 15 0 2715.31 306.122 8 1 15 0 2510.51 285.371 11 1 15 1 567.903 133.055 11 1 15 1 663.297 164.032 8 1 15 2 1226.93 220.147 15 1 15 2 1296.15 217.499 8 1 15 3 2120.33 264.138 15 1 15 3 2298.05 275.303 8 1 15 4 655.876 147.694 15 1 15 4 687.163 171.378 8 1 15 5 3012.83 321.674 15 1 15 6 866.267 176.196 15 1 15 7-17.6382 96.5602 15 1 15 8 238.829 108.276 15 1 15 9 186.271 105.823 15 1 15 10 4744.50 373.325 15 1 16 2 84.7057 96.1416 8 1 16 3 2515.43 251.848 8 1 16 4 5825.53 380.636 8 1 16 5 116.089 62.0979 8 1 16 6 168.482 88.1182 8 -2 14 9 125.098 66.6909 21 -2 14 8 1786.08 206.088 21 -2 14 8 2013.62 244.288 15 -2 14 7 277.078 88.7456 15 -2 14 7 435.024 101.725 21 -2 14 6 640.325 139.550 21 -2 14 6 431.751 121.728 15 -2 14 5 2130.45 234.815 6 -2 14 5 1895.48 228.415 21 -2 14 3 2538.30 281.403 10 -2 14 2 896.976 183.141 9 -2 14 2 734.643 156.434 10 -2 14 1 178.643 109.676 10 -2 14 1-3.31082 130.231 9 -2 14 0 2467.36 298.953 10 -2 14 0 2589.07 323.399 9 -2 14 -1 183.180 105.334 9 -2 14 -1 143.918 92.3978 10 -2 14 -2 45.5000 108.552 9 -2 14 -2 9.87648 65.4678 10 -2 14 -3 4454.52 373.790 9 -2 14 -3 4580.87 413.467 10 -2 14 -4 2240.91 255.936 9 -2 14 -4 1739.48 260.564 10 -2 14 -5 733.935 177.180 10 -2 14 -5 568.101 122.925 9 -2 13 11 7814.26 456.799 15 -2 13 11 7205.08 402.039 21 -2 13 10-6.16073 66.8155 15 -2 13 10 25.5055 57.8312 21 -2 13 9 2799.20 290.065 21 -2 13 9 2858.26 328.870 15 -2 13 8 548.489 142.552 15 -2 13 8 512.571 134.490 21 -2 13 7 38.0680 79.5706 15 -2 13 7 88.3616 77.4721 21 -2 13 7-24.4381 64.0081 6 -2 13 6 667.116 162.660 21 -2 13 6 728.701 169.753 6 -2 13 6 544.464 137.014 15 -2 13 5 1009.02 192.050 15 -2 13 5 1025.58 182.529 21 -2 13 5 1049.62 181.940 6 -2 13 4 2230.52 274.842 21 -2 13 4 2952.33 298.855 6 -2 13 4 2677.86 318.563 10 -2 13 3 11966.3 683.586 9 -2 13 3 11716.9 671.434 10 -2 13 3 12830.4 608.381 6 -2 13 2 465.619 153.043 10 -2 13 2 392.547 133.830 9 -2 13 2 346.130 111.366 6 -2 13 1 238.772 125.603 9 -2 13 1 423.802 155.625 10 -2 13 1 493.948 125.834 6 -2 13 0 6061.26 516.885 10 -2 13 0 6934.51 577.901 9 -2 13 0 6753.06 490.789 17 -2 13 -1 3911.21 370.767 17 -2 13 -1 4003.67 432.425 9 -2 13 -1 3729.87 405.924 10 -2 13 -2 988.875 222.660 10 -2 13 -2 1062.22 242.159 9 -2 13 -2 993.659 194.872 17 -2 13 -3 20197.9 953.462 10 -2 13 -3 19508.6 871.413 9 -2 13 -3 19032.8 895.598 16 -2 13 -3 18725.4 806.333 17 -2 13 -4 22245.6 868.204 17 -2 13 -4 22775.5 914.601 9 -2 13 -4 23177.1 1040.57 10 -2 13 -4 24045.1 1007.06 16 -2 13 -5 2185.97 306.614 16 -2 13 -5 1954.94 257.881 17 -2 13 -5 2050.99 271.767 9 -2 13 -5 2599.22 355.641 10 -2 13 -6 441.803 139.382 9 -2 13 -6 221.701 74.9905 17 -2 13 -6 667.870 163.091 16 -2 13 -6 508.642 163.011 10 -2 13 -7 6141.03 472.647 16 -2 13 -7 6003.85 444.076 10 -2 13 -7 5585.17 385.361 9 -2 13 -8 1266.62 191.711 10 -2 13 -8 1312.84 194.813 16 -2 12 13 461.067 110.573 15 -2 12 12 39.8873 59.5345 15 -2 12 12-55.8229 81.3983 21 -2 12 11 14801.4 699.057 15 -2 12 11 13322.3 623.466 21 -2 12 10 1470.92 242.823 15 -2 12 10 1627.18 229.060 21 -2 12 9 9852.05 591.850 21 -2 12 9 10554.6 669.973 15 -2 12 8 514.185 174.547 15 -2 12 8 246.063 122.380 21 -2 12 8 279.445 128.929 6 -2 12 7 8355.77 586.095 15 -2 12 7 8716.52 578.945 21 -2 12 7 7834.55 533.675 6 -2 12 6 20704.0 847.293 6 -2 12 6 20949.3 914.671 21 -2 12 6 20452.0 901.217 15 -2 12 5 4357.56 411.431 15 -2 12 5 4650.10 448.547 21 -2 12 5 4413.04 412.189 10 -2 12 5 4805.28 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5629.71 437.152 7 -2 11 8 5038.41 458.208 6 -2 11 8 6151.13 507.134 13 -2 11 7 1151.46 217.446 6 -2 11 7 1334.96 258.580 15 -2 11 7 1157.16 254.966 21 -2 11 7 1420.47 240.877 7 -2 11 6 17372.7 843.790 15 -2 11 6 17774.2 898.659 21 -2 11 6 17136.0 828.677 7 -2 11 6 17748.4 803.253 6 -2 11 5 27132.7 1047.38 10 -2 11 5 26733.0 975.725 6 -2 11 5 27446.4 1062.39 7 -2 11 5 26778.1 1086.57 21 -2 11 5 25342.3 999.519 15 -2 11 4 9631.84 622.058 7 -2 11 4 9762.97 598.467 15 -2 11 4 9291.78 624.603 10 -2 11 4 9330.33 573.036 6 -2 11 4 9364.49 623.253 21 -2 11 3 2163.12 282.680 15 -2 11 3 1980.14 302.332 10 -2 11 3 2043.55 264.660 6 -2 11 3 2200.19 304.327 21 -2 11 3 2058.89 289.492 7 -2 11 3 1975.01 281.549 17 -2 11 2 2135.21 284.602 7 -2 11 2 1928.32 307.778 10 -2 11 2 2018.06 277.518 21 -2 11 2 1660.12 244.965 6 -2 11 2 1779.21 270.636 17 -2 11 1 3966.04 431.625 10 -2 11 1 4096.36 387.039 7 -2 11 1 3821.98 408.953 11 -2 11 1 4046.18 391.007 21 -2 11 1 3329.39 348.195 6 -2 11 1 4271.39 415.213 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504.802 6 -2 10 9 6335.50 564.406 23 -2 10 8 3699.20 425.311 23 -2 10 8 4126.25 460.999 27 -2 10 8 3953.39 439.934 15 -2 10 8 3866.50 426.588 21 -2 10 8 3807.78 414.401 13 -2 10 8 3742.99 406.040 6 -2 10 8 3568.46 359.370 7 -2 10 7 23641.5 1037.93 21 -2 10 7 23236.1 900.853 7 -2 10 7 23625.6 995.138 13 -2 10 7 24240.3 1035.83 23 -2 10 7 23455.8 940.942 6 -2 10 7 24001.4 1024.66 15 -2 10 6 34337.0 1171.99 15 -2 10 6 34774.1 1125.90 7 -2 10 6 35201.9 1189.01 13 -2 10 6 34053.3 1112.89 6 -2 10 6 34837.7 1205.59 21 -2 10 5 2454.11 319.036 15 -2 10 5 2428.09 287.187 6 -2 10 5 2552.76 318.895 21 -2 10 5 2488.54 310.520 13 -2 10 5 2628.13 329.933 7 -2 10 5 2461.46 324.620 10 -2 10 4 3265.32 371.344 10 -2 10 4 3504.56 356.705 21 -2 10 4 3482.06 365.529 7 -2 10 4 3462.74 346.717 6 -2 10 4 3055.51 337.384 15 -2 10 3 1949.37 273.213 17 -2 10 3 1898.71 263.664 15 -2 10 3 2057.12 260.779 21 -2 10 3 1887.62 256.574 7 -2 10 3 1860.61 253.274 6 -2 10 3 2314.21 320.862 10 -2 10 2 11038.3 685.201 10 -2 10 2 11482.6 621.321 7 -2 10 2 11510.4 609.564 21 -2 10 2 11023.9 590.597 15 -2 10 2 11257.4 664.380 17 -2 10 2 10262.3 657.711 11 -2 10 1 13418.8 776.287 16 -2 10 1 14174.5 676.602 7 -2 10 1 14249.5 667.809 21 -2 10 1 13672.2 766.670 10 -2 10 1 13286.0 741.673 11 -2 10 1 13997.6 747.053 17 -2 10 0 1973.99 291.153 16 -2 10 0 2181.57 263.093 21 -2 10 0 1741.05 242.323 20 -2 10 0 1777.10 241.879 7 -2 10 0 2006.70 292.522 17 -2 10 0 1677.41 276.594 11 -2 10 -1 22613.4 1018.91 16 -2 10 -1 22743.7 972.193 17 -2 10 -1 21990.3 818.700 7 -2 10 -1 21909.1 877.264 20 -2 10 -1 22236.8 983.575 11 -2 10 -2 27113.6 983.321 20 -2 10 -2 27538.8 1091.60 17 -2 10 -2 27593.4 1118.60 11 -2 10 -2 28286.6 1157.50 16 -2 10 -3 102.462 110.000 17 -2 10 -3-359.227 623.624 28 -2 10 -3 162.257 96.1696 11 -2 10 -3 134.191 102.281 20 -2 10 -3 55.0700 106.436 16 -2 10 -4 897.211 245.127 16 -2 10 -4 601.584 165.896 17 -2 10 -4 854.077 223.231 11 -2 10 -4 681.080 155.591 20 -2 10 -5 16464.0 971.649 16 -2 10 -5 16951.7 875.603 9 -2 10 -5 18360.0 1039.21 11 -2 10 -5 16535.0 911.382 17 -2 10 -5 17221.6 808.799 20 -2 10 -6 7022.18 529.527 20 -2 10 -6 7414.57 596.582 9 -2 10 -6 6857.61 609.808 17 -2 10 -6 7807.79 622.412 11 -2 10 -6 7002.02 647.984 16 -2 10 -7 3000.21 451.251 16 -2 10 -7 2670.58 363.318 9 -2 10 -7 2536.31 383.489 17 -2 10 -7 2950.63 371.106 11 -2 10 -8 127.440 153.526 16 -2 10 -8 288.486 188.449 9 -2 10 -8-86.0163 100.030 11 -2 10 -8 65.2449 84.6630 17 -2 10 -9 2357.64 368.064 16 -2 10 -9 1711.35 354.023 17 -2 10 -9 2508.07 367.116 1 -2 10 -9 2089.70 303.717 9 -2 10 -9 2145.83 276.826 11 -2 10 -10 1586.64 275.670 16 -2 10 -10 1593.60 255.224 9 -2 10 -10 1711.70 284.286 1 -2 10 -10 1859.39 243.284 11 -2 10 -10 1373.28 278.382 17 -2 10 -11 3862.02 381.483 16 -2 10 -11 3311.09 369.215 17 -2 10 -12 50.3646 51.3555 17 -2 10 -12 143.916 82.4398 16 -2 9 16 2863.18 271.671 27 -2 9 15 100.945 58.7378 27 -2 9 15 345.636 102.608 13 -2 9 15 182.292 82.1340 15 -2 9 14 1814.87 262.387 13 -2 9 14 1989.24 258.173 15 -2 9 14 1819.63 271.606 27 -2 9 13 4091.41 389.125 15 -2 9 13 4103.65 432.907 27 -2 9 13 3772.51 376.877 21 -2 9 13 3943.70 421.535 13 -2 9 12 152.230 142.365 27 -2 9 12 160.360 96.8066 15 -2 9 12 24.5066 99.9824 13 -2 9 12 82.8210 90.3492 21 -2 9 11 1130.39 215.804 23 -2 9 11 1293.20 286.796 27 -2 9 11 1287.55 203.064 7 -2 9 11 1319.99 233.673 15 -2 9 11 1256.19 234.348 21 -2 9 11 954.321 255.695 13 -2 9 10 7910.89 607.312 15 -2 9 10 8436.50 655.648 13 -2 9 10 8066.45 591.816 21 -2 9 10 7431.20 470.661 7 -2 9 10 7646.75 643.676 27 -2 9 10 7807.52 608.629 23 -2 9 9 95.2872 102.194 27 -2 9 9 100.380 116.030 15 -2 9 9 112.198 91.5030 6 -2 9 9 106.587 121.745 21 -2 9 9 151.707 98.1908 7 -2 9 9-1.39716 79.0724 13 -2 9 9-41.5508 94.4875 23 -2 9 8 1442.23 280.161 21 -2 9 8 1254.28 253.954 27 -2 9 8 1589.10 287.121 23 -2 9 8 1357.60 276.806 15 -2 9 8 1497.42 260.322 6 -2 9 8 1388.80 261.053 13 -2 9 8 748.105 356.562 29 -2 9 8 1672.36 238.584 7 -2 9 7 7975.20 580.288 15 -2 9 7 7671.22 510.681 7 -2 9 7 8186.53 571.375 21 -2 9 7 8033.58 596.416 27 -2 9 7 7851.55 570.973 13 -2 9 7 7961.27 539.672 6 -2 9 7 8124.46 580.932 23 -2 9 6 14751.4 757.987 23 -2 9 6 14506.7 742.717 10 -2 9 6 15035.4 762.940 13 -2 9 6 14613.3 783.486 27 -2 9 6 15176.9 744.056 21 -2 9 6 14581.4 703.830 7 -2 9 6 14641.3 750.616 15 -2 9 6 14907.8 721.839 6 -2 9 5 3806.04 379.052 23 -2 9 5 3886.42 384.572 10 -2 9 5 4030.90 385.604 13 -2 9 5 3638.96 352.301 21 -2 9 5 4002.39 378.386 7 -2 9 5 3314.70 367.746 27 -2 9 5 3896.15 367.301 6 -2 9 5 3929.47 373.644 15 -2 9 4 45549.2 1308.16 10 -2 9 4 48177.4 1282.13 13 -2 9 4 47200.8 1235.41 15 -2 9 4 46781.7 1285.79 7 -2 9 4 46966.4 1207.16 21 -2 9 4 46316.8 1319.69 17 -2 9 4 45366.6 1226.57 6 -2 9 3 3587.54 327.026 15 -2 9 3 3378.49 360.041 10 -2 9 3 3613.49 353.379 7 -2 9 3 3680.37 325.672 21 -2 9 3 2996.36 311.717 6 -2 9 3 3699.05 365.603 17 -2 9 2 875.681 166.440 21 -2 9 2 852.132 173.912 10 -2 9 2 672.188 171.966 11 -2 9 2 825.889 181.399 7 -2 9 2 953.452 208.072 16 -2 9 2 735.360 147.646 15 -2 9 2 735.019 171.278 17 -2 9 1 100548. 2000.17 16 -2 9 1 101800. 1944.16 17 -2 9 1 102989. 1676.41 21 -2 9 1 105876. 1748.56 7 -2 9 1 100867. 1921.53 11 -2 9 1 102641. 1812.55 20 -2 9 0 38409.2 1247.51 16 -2 9 0 38529.0 1205.72 17 -2 9 0 39387.2 1023.60 21 -2 9 0 37287.3 1094.72 20 -2 9 0 37321.1 1176.73 11 -2 9 0 38205.9 1031.08 7 -2 9 -1 62923.3 1570.61 17 -2 9 -1 58930.5 2742.25 28 -2 9 -1 62174.9 1294.68 7 -2 9 -1 61992.7 1420.94 20 -2 9 -1 62568.3 1610.68 16 -2 9 -1 62088.5 1545.44 11 -2 9 -2 53176.2 2729.89 28 -2 9 -2 57908.5 1233.49 7 -2 9 -2 56907.8 1533.91 17 -2 9 -2 55192.7 1368.11 20 -2 9 -2 56156.6 1498.21 11 -2 9 -2 55816.9 1553.68 16 -2 9 -3 135.862 137.614 16 -2 9 -3 91.4471 70.2916 17 -2 9 -3 129.411 98.9683 20 -2 9 -3 163.599 122.861 11 -2 9 -4 31472.6 1241.27 16 -2 9 -4 31386.6 2388.40 28 -2 9 -4 31107.0 1216.78 17 -2 9 -4 31132.6 1078.05 20 -2 9 -4 32185.0 1253.71 11 -2 9 -5 236.529 194.691 11 -2 9 -5 106.109 132.467 16 -2 9 -5 209.497 99.3314 20 -2 9 -5 406.044 164.995 17 -2 9 -5 298.182 150.855 1 -2 9 -6 2100.40 324.003 1 -2 9 -6 1603.57 690.161 28 -2 9 -6 1775.45 276.555 20 -2 9 -6 1786.02 300.176 11 -2 9 -6 1933.68 318.921 9 -2 9 -6 1870.79 354.451 17 -2 9 -7 5513.98 514.904 9 -2 9 -7 5213.38 476.102 20 -2 9 -7 5194.58 570.233 17 -2 9 -7 5585.39 543.455 1 -2 9 -7 5694.58 505.597 11 -2 9 -8 1278.85 312.380 17 -2 9 -8 1425.36 263.101 9 -2 9 -8 972.233 232.717 20 -2 9 -8 1621.74 290.026 1 -2 9 -8 1306.62 233.812 11 -2 9 -9 70.4567 135.471 1 -2 9 -9 163.422 144.013 9 -2 9 -9 53.2822 125.666 17 -2 9 -9 71.4862 67.1434 11 -2 9 -10 1134.50 301.924 17 -2 9 -10 1372.14 295.239 1 -2 9 -10 1629.19 243.379 11 -2 9 -10 1997.20 298.722 9 -2 9 -11 1716.43 289.500 16 -2 9 -11 1189.47 270.989 17 -2 9 -12 633.620 172.477 16 -2 9 -12 477.298 158.360 17 -2 9 -12 871.302 205.166 1 -2 9 -13 1593.70 224.512 16 -2 9 -13 1381.28 235.799 17 -2 9 -13 2043.68 267.720 1 -2 9 -14 1904.55 237.919 17 -2 9 -14 3707.10 301.684 1 -2 8 16 1424.08 186.980 15 -2 8 16 1191.39 188.535 13 -2 8 16 1099.44 182.615 27 -2 8 15 5062.83 429.647 27 -2 8 15 5854.39 406.097 15 -2 8 15 5108.88 423.485 13 -2 8 14 4721.25 445.213 27 -2 8 14 5422.98 427.265 15 -2 8 14 4771.31 444.716 13 -2 8 13 3848.47 428.133 27 -2 8 13 3423.42 371.448 15 -2 8 13 3417.49 361.233 21 -2 8 13 3201.58 396.146 13 -2 8 12 5633.64 534.966 27 -2 8 12 5657.97 494.680 15 -2 8 12 5728.44 541.234 13 -2 8 12 6198.67 503.711 21 -2 8 11 3241.56 378.409 15 -2 8 11 3073.08 408.431 13 -2 8 11 3568.07 391.263 21 -2 8 11 3313.38 428.826 27 -2 8 10 16828.3 957.457 27 -2 8 10 16690.6 881.670 23 -2 8 10 17231.7 854.906 15 -2 8 10 16513.7 890.678 6 -2 8 10 16956.3 857.215 21 -2 8 10 17063.4 933.422 13 -2 8 10 17340.0 690.921 7 -2 8 9 5776.23 536.890 21 -2 8 9 6585.20 557.297 23 -2 8 9 5787.44 411.001 7 -2 8 9 5886.41 529.626 13 -2 8 9 5843.69 539.738 27 -2 8 9 5876.09 511.622 6 -2 8 9 6016.65 510.742 15 -2 8 9 4858.11 828.172 29 -2 8 8 460.175 143.964 15 -2 8 8 183.293 80.6323 23 -2 8 8 219.494 122.986 21 -2 8 8 316.248 123.422 7 -2 8 8 232.956 128.292 13 -2 8 8 236.941 142.244 27 -2 8 8 221.063 112.631 6 -2 8 7 3674.12 408.837 15 -2 8 7 3974.31 406.337 27 -2 8 7 4445.99 412.817 13 -2 8 7 4027.28 392.377 23 -2 8 7 4223.51 387.813 21 -2 8 7 4017.82 353.004 7 -2 8 7 3856.34 374.889 6 -2 8 7 3835.46 695.062 29 -2 8 6 6208.17 485.702 15 -2 8 6 6358.66 449.361 21 -2 8 6 6445.87 482.148 10 -2 8 6 6775.70 493.989 13 -2 8 6 5897.07 474.350 27 -2 8 6 6187.81 469.248 23 -2 8 6 6346.52 458.789 6 -2 8 6 5752.63 445.916 7 -2 8 6 5109.15 764.418 29 -2 8 5 1966.05 262.730 27 -2 8 5 1718.28 232.316 15 -2 8 5 1828.39 253.318 7 -2 8 5 1838.92 247.312 23 -2 8 5 1925.91 251.218 21 -2 8 5 1924.41 255.517 13 -2 8 5 1702.95 254.721 10 -2 8 5 1862.34 237.809 6 -2 8 5 1425.43 390.292 29 -2 8 4 4985.36 365.072 21 -2 8 4 4576.20 398.864 10 -2 8 4 4638.36 375.866 6 -2 8 4 4847.92 380.803 15 -2 8 4 4680.15 382.426 13 -2 8 4 4458.97 389.255 7 -2 8 4 4831.50 397.355 27 -2 8 4 4552.00 394.200 17 -2 8 4 4224.89 628.802 29 -2 8 4 4609.83 386.660 23 -2 8 3 3571.02 324.478 13 -2 8 3 3857.85 329.623 15 -2 8 3 3996.12 360.466 7 -2 8 3 4081.83 321.375 21 -2 8 3 3842.49 363.146 10 -2 8 3 3972.61 363.046 17 -2 8 2 1741.96 246.179 16 -2 8 2 1851.58 217.977 15 -2 8 2 1739.61 251.135 10 -2 8 2 1902.00 219.141 21 -2 8 2 1922.35 239.386 7 -2 8 2 1901.21 243.584 20 -2 8 2 1888.96 259.365 17 -2 8 2 1751.84 247.318 11 -2 8 1 32439.4 1062.08 16 -2 8 1 33573.9 925.025 7 -2 8 1 32172.6 1034.09 17 -2 8 1 31748.2 960.831 20 -2 8 1 32379.2 878.814 21 -2 8 1 30592.5 992.034 11 -2 8 0 971.195 160.396 21 -2 8 0 1205.69 177.248 7 -2 8 0 861.810 163.797 20 -2 8 0 913.884 182.525 16 -2 8 0 1126.92 205.103 11 -2 8 0 1009.76 194.624 17 -2 8 -1 26363.3 1717.62 28 -2 8 -1 26262.1 799.354 21 -2 8 -1 25376.3 879.280 20 -2 8 -1 26520.1 804.742 7 -2 8 -1 26570.9 989.432 16 -2 8 -1 27075.5 980.639 17 -2 8 -1 26031.4 929.202 11 -2 8 -2 78.9615 62.2439 17 -2 8 -2 116.010 56.7481 7 -2 8 -2 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4067.57 822.848 24 2 4 14 3630.95 391.295 2 2 4 14 3537.48 414.723 13 2 4 15 778.120 204.166 26 2 4 15 508.936 142.637 13 2 4 15 688.986 173.846 2 2 4 16 937.087 232.316 26 2 4 16 742.602 193.753 13 2 4 16 1094.23 210.908 2 2 4 17 1816.47 270.896 13 2 4 17 1509.76 263.981 26 2 4 17 1437.26 223.273 2 2 4 18 1702.07 265.458 26 2 4 18 1476.86 234.180 13 2 4 18 1353.86 197.601 2 2 4 19 84.7505 70.0908 26 2 4 19-7.61997 57.1497 23 2 4 19-40.6659 70.1047 2 2 5 -16 215.355 85.4616 30 -2 -5 16 65.5941 66.1651 19 -2 -5 15 120.596 93.4953 19 2 5 -15 71.3227 76.7105 30 2 5 -14 2696.53 314.055 30 -2 -5 14 2608.47 298.055 19 -2 -5 13 4341.48 393.853 19 -2 -5 12 1444.88 241.577 19 -2 -5 11 2083.19 278.281 19 2 5 -10 1405.11 438.091 28 -2 -5 10 874.591 191.237 19 2 5 -9 41428.2 2226.30 28 -2 -5 9 41641.9 1193.02 19 2 5 -8 5268.05 756.145 28 -2 -5 8 5177.25 418.535 19 -2 -5 7 970.103 202.890 19 2 5 -7 1328.71 375.826 28 2 5 -6 137.376 212.423 28 2 5 -5 62485.6 2470.03 28 2 5 -5 61064.4 1327.81 8 2 5 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27 2 5 14 43.0254 120.526 2 2 5 14 91.2309 84.1509 13 2 5 14 197.145 160.320 26 2 5 15 1033.14 235.050 26 2 5 15 913.192 224.720 13 2 5 15 1183.68 226.566 2 2 5 16 67.0714 126.003 26 2 5 16 70.3546 88.1500 2 2 5 17 4226.56 368.779 2 2 5 17 4283.36 429.095 26 2 5 17 4215.92 403.223 13 2 5 18-84.4752 83.4095 26 2 5 18-129.671 116.855 13 2 5 18 163.669 82.0801 2 2 5 19 137.034 84.4832 26 2 5 19 133.717 70.4206 23 2 6 -15 27.3293 64.7792 1 -2 -6 15 263.907 99.7044 19 2 6 -15 147.601 97.2368 30 2 6 -14-63.0748 84.5016 30 -2 -6 14 52.1155 63.4004 19 -2 -6 13 8405.57 526.025 19 2 6 -13 8250.54 568.127 30 -2 -6 12 1933.98 269.676 19 2 6 -12 1571.85 283.768 30 -2 -6 11 8996.36 571.095 19 -2 -6 10 57012.3 1417.37 19 -2 -6 9 124303. 2042.29 19 2 6 -9 117631. 3935.30 28 2 6 -8 43185.4 2276.96 28 -2 -6 8 43559.2 1202.56 19 2 6 -7 1155.71 388.405 28 -2 -6 7 1442.26 229.469 19 2 6 -6 405.789 205.623 28 -2 -6 6 581.860 168.752 19 2 6 -6 579.408 137.819 12 2 6 -5 193.786 178.180 28 2 6 -5 153.237 112.315 8 2 6 -5 298.796 125.521 12 2 6 -4 1630.37 429.221 28 2 6 -4 2201.76 268.646 12 2 6 -4 2088.46 253.684 8 2 6 -3 8632.27 921.279 28 2 6 -3 9451.03 493.217 8 2 6 -2 9230.79 934.189 28 2 6 -1 1586.50 365.863 28 -2 -6 1 1091.67 249.231 24 2 6 0 1519.17 354.520 28 -2 -6 0 1448.24 298.383 24 2 6 1 32002.7 1682.62 28 -2 -6 -1 28914.1 1297.78 24 -2 -6 -2 25764.6 1284.35 24 -2 -6 -3 3756.06 496.233 24 -2 -6 -4 9700.84 875.560 24 2 6 4 11060.8 770.043 28 -2 -6 -5 1723.47 413.187 24 -2 -6 -6 2799.20 558.827 24 2 6 7 24012.7 829.696 26 -2 -6 -7 21799.9 1601.68 24 2 6 7 24335.0 824.058 13 2 6 8 7827.14 467.798 27 2 6 8 7117.70 438.895 2 2 6 8 7484.19 472.238 15 2 6 8 7723.25 489.158 13 -2 -6 -8 7524.14 1064.75 24 2 6 8 7499.42 487.388 26 2 6 9 3286.32 326.514 27 2 6 9 3534.39 372.839 26 -2 -6 -9 2700.78 781.301 24 2 6 9 3023.10 304.355 2 2 6 9 3728.23 360.796 13 2 6 9 3389.01 345.566 15 2 6 10-84.8285 96.0207 27 2 6 10 82.6841 77.5680 26 -2 -6 -10-232.034 391.530 24 2 6 10 46.4801 83.6021 15 2 6 10-6.62480 83.1091 13 2 6 10 180.083 80.8975 2 2 6 11 8526.10 593.455 27 2 6 11 8270.68 568.229 2 -2 -6 -11 8760.47 1227.55 24 2 6 11 8984.32 658.408 26 2 6 11 8601.26 639.407 13 2 6 12 43.1513 102.761 26 -2 -6 -12 1.70819 259.025 24 2 6 12 182.206 128.388 2 2 6 12 215.131 117.066 13 2 6 12 138.205 85.2918 27 2 6 13 483.421 160.388 26 2 6 13 589.261 151.611 2 2 6 13 684.642 192.768 13 -2 -6 -13 559.828 351.243 24 2 6 13 566.592 153.096 27 2 6 14 1219.94 267.614 26 2 6 14 1157.51 214.806 27 2 6 14 1462.19 287.542 13 2 6 14 1538.87 254.112 2 2 6 15 6256.36 568.417 26 2 6 15 5903.63 471.484 2 2 6 15 5388.99 501.350 13 2 6 16 585.923 148.011 2 2 6 16 601.125 173.344 13 2 6 16 529.222 188.825 26 2 6 17 50.2068 80.8486 23 2 6 17 4.11933 75.8437 26 2 6 17 0.36690 69.9609 13 2 6 18-77.0288 67.9075 23 2 6 18 194.051 103.952 26 2 6 18 83.8493 62.0889 13 2 6 19 579.277 137.571 26 2 6 19 426.895 114.324 23 -2 -7 15 462.610 109.812 19 2 7 -15 389.179 120.066 30 -2 -7 14 868.516 169.396 19 2 7 -14 1205.52 205.524 30 2 7 -13 225.565 90.9965 1 -2 -7 13 244.388 97.5508 19 2 7 -13 298.425 123.471 30 2 7 -12 73.7188 73.5561 11 2 7 -12-3.47351 75.6474 1 -2 -7 12 9.36301 61.4521 19 2 7 -12-101.246 135.195 30 -2 -7 11 574.503 155.370 19 2 7 -11 424.030 149.247 30 2 7 -10 33402.4 1224.75 30 -2 -7 10 32889.2 1067.75 19 2 7 -9 11418.0 725.640 30 -2 -7 9 11575.1 622.836 19 -2 -7 8 31901.2 1031.62 19 2 7 -8 31353.2 2090.57 28 2 7 -7 1582.90 481.371 28 2 7 -7 1080.20 191.053 12 -2 -7 7 1042.67 195.619 19 2 7 -6 17678.1 1442.99 28 2 7 -6 17053.7 716.018 12 -2 -7 6 16163.6 736.554 19 2 7 -5 691.007 319.354 28 2 7 -5 209.400 134.959 8 2 7 -5 395.818 125.520 1 2 7 -5 507.352 131.848 12 2 7 -4 5172.82 752.835 28 2 7 -4 4602.00 397.198 8 2 7 -4 4766.63 376.142 12 2 7 -3 39255.6 1080.39 8 2 7 -3 38679.3 908.467 25 2 7 -3 36827.9 1081.25 15 2 7 -3 37654.4 1076.31 12 2 7 -3 40196.4 2002.15 28 2 7 -3 38766.9 1023.50 30 2 7 -2 7865.55 886.506 28 2 7 -2 7055.68 456.846 15 2 7 -2 7442.95 454.705 8 2 7 -2 7461.44 485.172 12 2 7 -2 6648.68 373.971 25 2 7 -1 7739.45 458.788 15 2 7 -1 7711.20 389.998 25 2 7 -1 7745.04 874.586 28 -2 -7 0 187879. 3236.20 24 2 7 0 190350. 4207.93 28 2 7 1 87822.0 2885.95 28 -2 -7 -1 87289.8 2355.22 24 2 7 2 43701.1 1837.36 28 -2 -7 -2 41727.3 1705.99 24 2 7 3 10197.7 784.716 28 -2 -7 -3 8927.46 834.718 24 2 7 4 7223.27 420.231 15 -2 -7 -4 6333.36 736.350 24 -2 -7 -5 30057.8 1684.24 24 2 7 5 30456.8 881.819 23 2 7 5 31255.1 921.172 13 2 7 5 32978.8 880.351 25 2 7 5 30610.7 886.050 15 2 7 6 1200.55 192.961 26 2 7 6 1189.85 196.278 21 -2 -7 -6 1024.56 334.571 24 2 7 6 1175.75 179.205 23 2 7 6 1059.65 158.051 2 2 7 6 1225.98 202.177 13 2 7 6 1165.48 162.515 25 2 7 6 1052.24 171.505 15 2 7 7 11253.1 592.616 13 2 7 7 10579.2 527.898 2 2 7 7 11071.1 597.234 26 2 7 7 11112.7 537.421 25 -2 -7 -7 10881.8 1167.16 24 2 7 7 11126.5 577.742 21 2 7 7 11368.8 578.502 27 2 7 7 10788.3 558.070 15 2 7 8 5844.83 436.179 27 2 7 8 5318.37 387.062 2 2 7 8 5756.44 376.929 25 -2 -7 -8 5955.71 964.366 24 2 7 8 5789.25 441.100 15 2 7 8 5578.78 442.079 13 2 7 8 5768.21 452.542 26 2 7 9 28970.7 953.813 2 2 7 9 31078.9 1111.66 26 -2 -7 -9 27932.8 2291.83 24 2 7 9 30199.8 1079.13 15 2 7 9 30778.1 1077.04 13 2 7 9 31091.5 1055.68 27 -2 -7 -10 11.3628 269.523 24 2 7 10 358.465 126.213 27 2 7 10 434.560 164.647 13 2 7 10 390.111 142.426 2 2 7 10 475.748 177.030 26 2 7 10 309.885 127.417 15 2 7 11 225.297 105.027 26 -2 -7 -11-110.637 164.749 24 2 7 11 209.842 87.6132 15 2 7 11 208.641 100.778 27 2 7 11 168.064 81.6906 2 2 7 11 166.839 122.471 13 2 7 12 3481.58 371.724 2 2 7 12 3452.56 439.966 26 2 7 12 3383.16 395.804 27 2 7 12 3631.72 373.551 15 -2 -7 -12 2700.03 727.216 24 2 7 12 3591.93 452.997 13 2 7 13 2524.28 344.472 27 2 7 13 2483.89 338.261 2 2 7 13 2922.08 404.558 26 2 7 13 2225.88 358.491 13 2 7 14 402.041 127.618 27 2 7 14 716.284 229.191 26 2 7 14 310.584 143.702 13 2 7 14 497.558 147.709 2 2 7 15 3888.17 457.399 26 2 7 15 3356.03 363.531 27 2 7 15 3908.22 366.716 2 2 7 15 3502.30 411.730 13 2 7 16 2749.45 334.359 13 2 7 16 2825.06 351.424 23 2 7 16 3056.39 373.092 26 2 7 17 10.0194 87.9550 23 2 7 17 96.8074 68.4992 13 2 7 17-20.0857 97.7392 26 2 7 18 808.681 161.591 23 2 7 18 984.602 174.688 13 2 7 18 865.701 186.466 26 2 7 19 64.5250 63.6530 26 -2 -8 14 1710.54 189.783 19 2 8 -14 1767.94 214.682 30 -2 -8 13 416.575 116.644 19 2 8 -13 217.010 106.204 30 2 8 -12-109.658 78.2015 11 2 8 -12 97.0375 97.5944 30 2 8 -12-55.5030 74.2186 1 -2 -8 12 103.867 74.4185 19 2 8 -11 24.8941 61.4430 11 2 8 -11 176.884 103.507 30 -2 -8 11 87.2931 97.1055 19 2 8 -11-3.90300 89.2006 1 2 8 -10 14.1584 74.9261 11 2 8 -10 100.279 120.644 1 -2 -8 10 49.9415 85.1293 19 2 8 -10-52.2791 109.302 30 2 8 -9 184.553 151.468 1 -2 -8 9 376.625 148.873 19 2 8 -9 525.040 192.949 30 2 8 -8 2215.71 356.035 1 -2 -8 8 2621.63 297.483 19 2 8 -8 2370.87 347.707 30 2 8 -7 15.7112 73.4411 1 2 8 -7 45.2638 227.572 28 2 8 -7-15.7294 66.2024 12 -2 -8 7 8.35455 79.1647 19 2 8 -7-83.3020 157.219 30 2 8 -6 8018.82 1028.30 28 2 8 -6 7802.39 596.444 30 2 8 -6 7969.08 498.686 12 -2 -8 6 8166.93 518.438 19 2 8 -6 8182.10 573.944 1 2 8 -5 7910.23 996.736 28 2 8 -5 7569.05 521.134 1 2 8 -5 7440.80 575.569 8 2 8 -5 8142.79 508.600 12 -2 -8 5 6798.25 476.621 19 2 8 -5 7679.61 564.331 30 2 8 -4 9179.95 1046.15 28 2 8 -4 9378.35 598.285 8 2 8 -4 9653.15 582.037 30 2 8 -4 9079.40 552.158 12 2 8 -3 55648.2 2473.86 28 2 8 -3 51201.6 1318.21 15 2 8 -3 50558.0 1320.49 8 2 8 -3 51331.5 1246.62 30 2 8 -3 51250.0 1292.09 12 2 8 -2 11978.2 1129.19 28 2 8 -2 11754.9 614.345 15 2 8 -2 11121.8 598.516 8 2 8 -2 11556.1 554.552 30 2 8 -2 11475.5 615.619 12 2 8 -2 10911.5 524.794 25 2 8 -1 55103.9 1308.89 15 2 8 -1 58706.1 2502.25 28 2 8 -1 53814.9 1066.84 4 2 8 -1 56884.9 1395.18 12 2 8 -1 55987.9 1149.60 25 2 8 0 8421.90 445.248 25 2 8 0 8945.85 534.307 15 2 8 0 8695.76 427.505 4 2 8 0 7979.06 892.618 28 2 8 0 8932.06 557.905 12 2 8 1 12318.9 1032.91 28 2 8 1 11406.5 581.895 15 2 8 1 12361.3 517.135 4 2 8 1 12432.0 532.896 25 2 8 1 12408.3 684.227 12 2 8 1 11658.0 529.332 23 2 8 2 13477.6 622.947 15 2 8 2 14077.6 568.342 25 -2 -8 -2 13486.4 1007.05 24 2 8 2 13896.3 580.957 23 2 8 2 13905.2 561.724 4 2 8 2 15450.7 1059.11 28 2 8 2 13740.8 749.999 12 2 8 3 8214.19 482.129 15 2 8 3 8300.09 443.565 25 -2 -8 -3 7464.34 807.984 24 2 8 3 8436.62 462.429 23 2 8 3 7783.25 528.359 12 2 8 4 142.083 79.2718 13 2 8 4 129.062 61.6912 25 2 8 4 298.420 95.2416 15 2 8 4 301.443 109.149 21 2 8 4 217.884 75.9721 12 -2 -8 -4 22.9716 96.0175 24 2 8 4 228.174 101.904 23 2 8 5 69.5137 82.8138 25 2 8 5 90.2987 63.7749 15 2 8 5 82.5046 99.9685 23 2 8 5 169.571 126.295 21 2 8 5-2.53758 81.9375 13 2 8 5 146.817 76.8561 12 -2 -8 -5 165.185 108.368 24 2 8 6 39009.4 1144.35 21 2 8 6 41457.6 1097.35 25 2 8 6 38575.5 1100.27 15 -2 -8 -6 39234.0 2138.25 24 2 8 6 38472.8 1112.68 23 2 8 6 40624.1 1153.95 13 2 8 7 33844.7 1064.29 15 2 8 7 33588.2 979.378 25 -2 -8 -7 33969.5 2146.92 24 2 8 7 33781.4 1089.42 13 2 8 7 32599.2 1078.94 23 2 8 7 33762.4 1043.88 21 2 8 8 99.5091 80.8701 23 2 8 8 145.628 133.933 26 2 8 8 195.787 73.5032 2 2 8 8 117.759 94.9404 13 2 8 8 148.302 108.880 15 2 8 8 195.361 82.2617 25 2 8 9 663.111 191.841 27 2 8 9 515.306 160.539 26 2 8 9 536.442 173.511 23 2 8 9 584.120 142.088 2 2 8 9 597.176 175.690 13 -2 -8 -9 426.639 419.957 24 2 8 9 820.160 193.882 15 2 8 10 3367.19 339.429 2 2 8 10 3536.24 391.826 27 -2 -8 -10 3600.99 901.152 24 2 8 10 3010.34 415.269 23 2 8 10 3541.04 403.447 26 2 8 10 3891.37 423.297 13 2 8 10 3927.33 416.139 15 2 8 11 11243.8 650.792 2 2 8 11 10882.3 728.291 27 2 8 11 11192.3 776.089 26 -2 -8 -11 10724.4 1513.45 24 2 8 11 10838.4 734.298 13 2 8 11 10249.6 783.023 23 2 8 11 10869.4 671.160 15 2 8 12 4846.28 450.068 2 2 8 12 4811.09 495.285 27 2 8 12 4559.94 533.225 23 2 8 12 4792.34 523.672 26 2 8 12 5649.34 462.660 15 2 8 12 4808.57 523.487 13 2 8 13 1887.07 315.717 27 2 8 13 1999.09 355.231 23 2 8 13 1844.15 249.343 4 2 8 13 2005.92 265.909 15 2 8 13 1744.50 329.873 26 2 8 13 1635.68 310.316 13 2 8 14 700.678 202.980 23 2 8 14 1018.74 243.768 13 2 8 14 923.879 214.957 27 2 8 14 1067.66 253.281 26 2 8 15 2654.93 359.272 23 2 8 15 2634.25 373.393 26 2 8 15 2587.25 349.005 13 2 8 16 228.858 96.3807 23 2 8 16 23.7026 83.9405 26 2 8 16 233.890 140.053 13 2 8 17 3109.76 327.030 23 2 8 17 3197.65 326.664 13 2 8 17 3240.59 352.289 26 2 8 18 6.18771 48.6588 13 2 8 18-77.2438 72.8556 23 -2 -9 13 2037.34 202.986 19 2 9 -13 2163.08 242.405 30 2 9 -12 157.379 79.8522 11 2 9 -12-23.4023 88.3274 30 -2 -9 12 147.350 74.8991 19 2 9 -11 229.553 91.0950 11 -2 -9 11 123.826 88.1405 19 2 9 -11 193.973 112.356 30 2 9 -10 4018.95 410.299 1 2 9 -10 3560.57 337.464 11 -2 -9 10 4263.40 355.334 19 2 9 -10 4337.27 425.813 30 2 9 -9 468.441 160.162 1 2 9 -9 479.726 165.617 11 -2 -9 9 499.657 137.234 19 2 9 -9 477.221 189.747 30 2 9 -8 681.094 177.325 11 2 9 -8 443.434 171.621 1 -2 -9 8 678.210 153.114 19 2 9 -8 601.335 205.356 30 2 9 -7 3324.54 398.178 1 2 9 -7 3536.39 428.725 30 2 9 -7 3201.45 325.438 12 -2 -9 7 3839.34 347.370 19 2 9 -6 1364.44 267.150 30 2 9 -6 1432.59 245.947 1 2 9 -6 1265.73 212.805 12 -2 -9 6 1427.98 214.228 19 2 9 -5 3278.11 380.096 30 2 9 -5 3645.68 758.276 28 2 9 -5 3453.72 366.522 1 2 9 -5 3136.99 418.089 8 2 9 -5 3603.21 348.929 12 -2 -9 5 3484.76 329.778 19 2 9 -4 22391.3 984.637 8 2 9 -4 23812.0 938.796 30 2 9 -4 26131.6 1877.07 28 2 9 -4 24926.0 932.462 12 2 9 -3 18352.8 1544.67 28 2 9 -3 18976.3 813.477 12 2 9 -3 18626.9 855.143 8 2 9 -3 18855.2 799.815 30 2 9 -3 17251.4 830.318 15 2 9 -2 14472.3 743.595 15 2 9 -2 14993.3 745.846 8 2 9 -2 14903.9 674.280 30 2 9 -2 15588.4 743.065 12 2 9 -2 15360.5 1375.51 28 2 9 -1 220.957 246.091 28 2 9 -1 156.322 79.4063 25 2 9 -1 231.874 107.770 4 2 9 -1 248.639 134.606 15 2 9 -1 387.789 131.136 12 2 9 0 1176.90 184.751 25 2 9 0 1396.16 243.572 15 2 9 0 564.659 219.247 28 2 9 0 1131.58 166.826 4 2 9 0 1352.32 224.604 12 2 9 1 26077.7 860.331 23 2 9 1 25828.9 840.080 25 2 9 1 28647.5 1627.98 28 2 9 1 25423.5 805.087 4 2 9 1 25444.6 923.373 15 2 9 1 28022.5 1047.47 12 2 9 2 3827.34 366.515 15 2 9 2 3965.32 316.506 11 2 9 2 3798.88 316.680 4 2 9 2 3733.96 327.249 23 2 9 2 3440.99 300.748 25 2 9 2 3959.28 409.396 12 2 9 3 2213.18 271.364 15 2 9 3 2354.07 276.702 23 2 9 3 2041.71 240.674 4 2 9 3 2130.85 283.921 12 2 9 3 2316.88 255.358 25 2 9 4 21423.3 848.537 15 -2 -9 -4 22653.3 1520.42 24 2 9 4 21369.2 812.962 23 2 9 4 22049.2 804.502 4 2 9 4 22828.6 872.560 12 2 9 4 22941.3 815.942 25 -2 -9 -5 8955.31 1018.58 24 2 9 5 8485.32 521.695 23 2 9 5 9066.31 543.806 4 2 9 5 8215.31 549.522 21 2 9 5 8663.98 559.574 13 2 9 5 9070.42 531.152 25 2 9 5 8757.40 519.563 12 2 9 5 8365.85 537.511 15 2 9 6 2195.61 273.022 25 -2 -9 -6 1703.52 477.105 24 2 9 6 2169.12 290.672 15 2 9 6 1900.97 263.083 23 2 9 6 1895.65 268.596 4 2 9 6 2187.66 290.247 13 2 9 6 1602.68 252.866 21 2 9 7 2107.74 266.693 25 2 9 7 1919.46 282.980 23 -2 -9 -7 2026.66 544.948 24 2 9 7 2277.20 308.778 13 2 9 7 1845.10 285.918 4 2 9 7 2172.78 289.345 15 2 9 8 4076.32 418.424 15 -2 -9 -8 3766.33 790.563 24 2 9 8 4401.50 433.717 13 2 9 8 4085.90 419.706 4 2 9 8 3892.56 416.792 23 2 9 8 4041.27 357.760 25 2 9 9 11696.1 736.548 23 2 9 9 12401.5 754.834 15 2 9 9 11348.4 681.272 4 2 9 9 12286.5 736.524 13 -2 -9 -9 11006.1 1496.44 24 2 9 10 1311.03 270.050 23 -2 -9 -10 2004.86 768.941 24 2 9 10 1789.12 297.831 15 2 9 10 1335.54 233.761 4 2 9 10 1965.59 326.270 13 2 9 11-63.9060 143.421 15 2 9 11 61.2800 110.033 23 2 9 11 19.9900 79.2580 4 2 9 11-36.4000 88.6610 13 2 9 12 624.563 183.510 23 2 9 12 1055.44 222.953 15 2 9 12 948.810 250.223 13 2 9 12 954.476 248.761 26 2 9 12 764.065 179.291 4 2 9 13-40.5704 114.027 26 2 9 13 103.657 145.051 23 2 9 13-92.2324 81.5801 4 2 9 13 71.2470 110.578 13 2 9 13 15.6796 82.9580 15 2 9 14 2223.56 370.055 26 2 9 14 1818.29 327.189 23 2 9 14 2134.42 334.297 13 2 9 15 2067.10 300.727 23 2 9 15 2352.24 330.289 13 2 9 16 15948.5 755.049 23 2 9 16 14652.3 733.818 13 2 9 17 3411.24 319.968 23 2 9 17 2860.95 295.052 13 2 9 18 15.8993 50.0204 23 2 10 -12 2809.37 273.926 30 2 10 -11 283.810 84.9312 11 -2 -10 11 357.631 102.356 19 2 10 -11 549.642 152.700 30 2 10 -10 5891.80 460.554 30 -2 -10 10 5778.80 376.876 19 2 10 -10 5714.86 403.050 11 2 10 -9 882.802 187.473 11 -2 -10 9 741.146 151.804 19 2 10 -9 950.455 222.346 30 2 10 -8 441.596 144.378 11 -2 -10 8 310.224 101.616 19 2 10 -8 475.304 167.477 30 2 10 -7 604.580 166.177 11 2 10 -7 494.110 142.662 12 2 10 -7 459.408 142.016 30 2 10 -6 251.753 136.591 11 2 10 -6 95.6339 76.1309 12 2 10 -6 176.644 111.728 30 2 10 -5 3659.76 408.600 30 2 10 -5 2893.05 463.325 8 2 10 -5 3456.59 352.175 12 2 10 -5 3069.81 383.211 11 2 10 -4 9684.02 1207.81 28 2 10 -4 10731.6 722.931 8 2 10 -4 10837.3 635.826 12 2 10 -4 10958.6 713.582 11 2 10 -4 11117.3 666.218 30 2 10 -3-24.0331 178.823 28 2 10 -3 409.086 176.701 11 2 10 -3 342.907 116.157 30 2 10 -3 245.769 146.963 8 2 10 -3 377.678 183.398 15 2 10 -3 212.495 128.095 12 2 10 -2 1643.59 446.232 28 2 10 -2 1635.42 281.201 11 2 10 -2 1530.05 278.621 15 2 10 -2 1758.32 274.127 8 2 10 -2 1611.67 255.920 30 2 10 -2 1685.99 266.073 12 2 10 -1 13408.1 1409.46 28 2 10 -1 13810.5 742.164 15 2 10 -1 13877.3 719.680 11 2 10 -1 14322.3 758.312 8 2 10 -1 14197.6 743.261 12 2 10 -1 14242.9 627.337 4 2 10 0 16353.0 679.244 4 2 10 0 15487.6 771.623 15 2 10 0 15368.2 704.936 25 2 10 0 17178.3 838.279 12 2 10 0 16106.0 738.922 11 2 10 1 1966.02 259.688 11 2 10 1 2182.89 315.871 15 2 10 1 1911.78 272.339 25 2 10 1 1771.66 239.580 4 2 10 1 2150.78 327.528 12 2 10 2 70735.6 1629.57 15 2 10 2 73287.1 1523.63 25 2 10 2 73477.8 1542.19 23 2 10 2 72325.4 1464.38 4 2 10 2 70914.2 1762.08 12 2 10 2 73021.3 1437.43 11 2 10 3 6191.23 485.535 15 2 10 3 6389.71 453.627 25 2 10 3 6068.27 434.910 4 2 10 3 6091.58 457.882 23 2 10 3 6314.34 505.538 12 2 10 4 7340.26 510.529 23 2 10 4 7217.64 489.190 4 2 10 4 8066.00 519.112 25 2 10 4 6976.37 508.589 15 2 10 4 7861.81 531.061 12 2 10 5 4187.00 401.238 15 2 10 5 3975.85 391.767 23 2 10 5 4246.54 390.159 4 2 10 5 4680.93 410.146 25 2 10 5 4144.65 373.182 12 2 10 6 8054.35 572.050 13 2 10 6 7757.61 550.662 23 2 10 6 8487.58 566.562 25 2 10 6 8346.15 571.987 15 2 10 6 8004.90 559.855 4 2 10 6 7988.21 492.118 12 -2 -10 -7 13389.1 1440.18 24 2 10 7 13902.5 689.427 25 2 10 7 14403.5 764.394 23 2 10 7 13979.1 773.945 4 2 10 7 14521.1 790.536 13 2 10 7 14072.8 773.757 15 2 10 8 3207.21 378.986 23 2 10 8 3047.48 312.816 25 2 10 8 3259.91 385.159 4 2 10 8 3433.01 400.158 13 2 10 8 2986.70 387.089 15 -2 -10 -8 2134.82 641.473 24 2 10 9 256.600 144.201 15 2 10 9 348.275 154.111 23 2 10 9 263.394 132.094 4 2 10 9 152.910 105.725 13 2 10 10 7685.78 625.569 15 2 10 10 8146.15 649.919 23 2 10 10 7982.33 564.954 4 2 10 10 7952.36 631.113 13 2 10 11 746.514 206.292 13 2 10 11 673.566 212.293 23 2 10 11 986.059 236.472 15 2 10 11 702.775 187.588 4 2 10 12 679.290 172.085 15 2 10 12 746.395 262.442 23 2 10 12 835.702 186.578 4 2 10 12 832.325 234.201 13 2 10 13 1738.18 308.884 23 2 10 13 1867.13 275.417 15 2 10 13 1625.93 315.518 13 2 10 13 1475.54 241.664 4 2 10 14 7716.26 507.992 15 2 10 14 8051.68 592.715 23 2 10 14 7684.65 600.506 13 2 10 15 5741.23 466.181 23 2 10 15 5341.64 471.648 13 2 10 16 17817.1 748.923 23 2 10 16 16299.7 725.730 13 2 10 17 925.559 158.137 23 2 10 17 678.490 135.647 13 2 11 -11 3474.91 291.714 30 2 11 -10 247.507 87.3955 11 2 11 -10 348.726 124.603 30 2 11 -9 432.792 141.897 11 2 11 -9 316.634 144.594 30 2 11 -8 5364.01 432.539 11 2 11 -8 5927.72 499.130 30 2 11 -7 707.793 172.526 11 2 11 -7 630.152 191.075 30 2 11 -7 575.658 134.252 12 2 11 -6 189.948 176.807 11 2 11 -6 66.2549 80.2691 12 2 11 -6 107.436 120.741 30 2 11 -5 19655.7 846.793 12 2 11 -5 19997.5 932.462 30 2 11 -5 20977.7 961.457 11 2 11 -4 8709.68 590.633 30 2 11 -4 9274.86 660.408 11 2 11 -4 8146.57 676.807 8 2 11 -4 9287.02 602.517 12 2 11 -3 387.268 138.919 11 2 11 -3 100.334 191.249 8 2 11 -3 162.363 84.9892 30 2 11 -3 172.867 136.701 12 2 11 -2 308.496 140.251 11 2 11 -2 426.526 201.320 15 2 11 -2 351.569 132.995 8 2 11 -2 220.973 133.129 12 2 11 -1 183.097 149.402 11 2 11 -1-17.4700 119.311 15 2 11 -1-57.0884 105.652 8 2 11 -1 35.3714 73.6760 12 2 11 0 331.758 133.672 11 2 11 0 359.327 146.438 15 2 11 0 323.253 122.881 12 2 11 0 422.782 147.678 4 2 11 1 8951.64 546.578 4 2 11 1 10136.8 682.122 12 2 11 1 9031.46 603.377 15 2 11 1 9363.80 564.692 11 2 11 2 5805.77 461.516 25 2 11 2 5574.48 436.791 4 2 11 2 5537.96 518.441 12 2 11 2 5743.13 428.244 11 2 11 2 5798.39 500.490 15 2 11 3 200.481 94.5244 23 2 11 3 95.5272 98.5093 25 2 11 3 344.570 187.596 15 2 11 3 180.837 120.866 4 2 11 3 142.501 115.981 12 2 11 4 10866.1 678.186 15 2 11 4 11393.2 657.049 25 2 11 4 10978.9 636.673 23 2 11 4 11254.1 640.358 4 2 11 4 11384.1 654.042 12 2 11 5 8493.54 598.683 15 2 11 5 7755.12 558.085 25 2 11 5 7684.80 538.252 23 2 11 5 8085.37 554.696 4 2 11 5 7727.69 520.013 12 2 11 6 177.117 113.254 25 2 11 6 157.471 122.857 15 2 11 6 170.993 77.6489 23 2 11 6 58.7104 86.9696 4 2 11 6 270.138 118.216 12 2 11 7 21.9748 73.4949 25 2 11 7 64.6403 106.981 15 2 11 7-161.022 91.4109 23 2 11 8 12623.5 775.047 15 2 11 8 12456.7 644.600 25 2 11 8 12376.0 741.962 23 2 11 8 12777.3 767.904 4 2 11 8 12187.3 761.121 13 2 11 9 480.022 169.763 13 2 11 9 400.365 143.640 15 2 11 9 563.246 174.238 23 2 11 9 515.120 150.923 4 2 11 10 1908.09 315.936 13 2 11 10 1624.31 302.385 15 2 11 10 1701.37 267.029 4 2 11 10 2010.94 332.819 23 2 11 11 9634.03 668.567 15 2 11 11 8584.14 682.354 23 2 11 11 9282.42 596.864 4 2 11 11 8822.39 674.141 13 2 11 12 407.455 148.261 15 2 11 12 463.961 157.622 23 2 11 12 322.877 129.191 4 2 11 12 668.205 198.869 13 2 11 13 2365.92 303.621 15 2 11 13 2214.02 260.295 4 2 11 13 2285.01 334.999 23 2 11 13 2264.38 336.495 13 2 11 14 1164.31 193.469 15 2 11 14 1156.97 232.498 23 2 11 14 1325.22 240.701 13 2 11 15 1449.32 225.748 13 2 11 15 1950.43 254.948 23 2 11 16 192.051 78.2281 23 2 11 16 302.488 106.155 13 2 12 -9 2919.66 267.307 11 2 12 -8 12581.5 608.682 11 2 12 -7 786.804 171.671 11 2 12 -7 850.860 165.289 12 2 12 -6 220.882 120.110 11 2 12 -6 151.837 88.6547 12 2 12 -5 18.6444 93.3921 11 2 12 -5 175.869 95.3451 12 2 12 -4 286.995 240.998 8 2 12 -4 160.541 112.898 12 2 12 -4 67.2034 120.869 11 2 12 -3 2094.50 351.026 8 2 12 -3 2260.41 347.721 11 2 12 -3 2137.70 295.895 12 2 12 -2 548.250 197.856 15 2 12 -2 734.061 221.982 8 2 12 -2 661.121 181.351 11 2 12 -2 651.784 175.088 12 2 12 -1 583.568 178.077 11 2 12 -1 548.326 197.684 15 2 12 -1 950.226 234.414 8 2 12 -1 870.742 206.798 12 2 12 0 3849.84 398.497 8 2 12 0 3888.15 417.998 15 2 12 0 3301.58 387.673 12 2 12 0 3450.87 365.516 11 2 12 1 239.025 118.686 11 2 12 1 106.061 101.036 4 2 12 1 153.874 104.199 12 2 12 1 65.9028 109.120 15 2 12 2 150.018 89.4349 11 2 12 2 47.4757 105.857 15 2 12 2 259.739 124.062 4 2 12 2 181.076 128.437 12 2 12 3 19723.5 928.279 12 2 12 3 19809.9 850.417 4 2 12 3 19580.8 928.715 15 2 12 4 15929.0 843.220 15 2 12 4 15994.6 783.456 4 2 12 4 15495.2 782.712 12 2 12 5 4776.71 460.697 15 2 12 5 4949.04 451.986 4 2 12 5 5339.09 438.554 12 2 12 5 5094.04 458.571 23 2 12 6 18007.0 906.716 15 2 12 6 17996.0 770.861 12 2 12 6 18751.0 879.830 23 2 12 6 19674.8 913.300 4 2 12 7 4748.95 463.728 4 2 12 7 4101.24 417.687 23 2 12 7 4384.28 463.387 15 2 12 8 1114.13 245.565 15 2 12 8 1390.16 260.292 23 2 12 8 1443.97 268.830 4 2 12 9 1557.39 275.242 15 2 12 9 1420.93 262.377 23 2 12 9 1743.26 279.267 4 2 12 10-74.0321 137.215 15 2 12 10-14.0885 104.666 23 2 12 10-8.51619 82.8144 4 2 12 11 488.834 186.113 23 2 12 11 496.273 171.363 15 2 12 11 561.374 161.109 4 2 12 12 354.030 144.122 15 2 12 12 97.4729 93.2151 23 2 12 12 157.899 90.1587 4 2 12 13 206.841 92.2506 15 2 12 13 206.922 112.487 23 2 12 13 164.336 92.0435 4 2 12 14 2099.68 243.659 15 2 12 14 2293.82 289.316 23 2 12 15 2388.02 265.805 23 2 13 -8 5036.01 338.024 11 2 13 -7 169.795 80.8769 11 2 13 -7-42.8498 56.0488 16 2 13 -6 999.586 196.972 11 2 13 -6 541.129 155.600 16 2 13 -5 3097.71 345.209 11 2 13 -5 2691.12 297.331 12 2 13 -4 74.6952 101.550 11 2 13 -4 180.682 101.237 12 2 13 -3 9133.79 666.867 8 2 13 -3 10361.7 681.169 11 2 13 -3 10591.8 626.382 12 2 13 -2 253.608 134.807 11 2 13 -2 112.874 143.331 8 2 13 -2 89.4853 85.1414 12 2 13 -1-16.3819 73.6920 11 2 13 -1 127.427 132.386 8 2 13 -1 145.059 142.570 15 2 13 -1 71.5223 103.147 12 2 13 0 4854.14 447.632 15 2 13 0 5065.17 487.855 12 2 13 0 4219.16 430.118 8 2 13 0 4647.27 420.841 11 2 13 1 13937.7 771.639 15 2 13 1 14246.0 778.410 8 2 13 1 14208.0 828.028 12 2 13 1 13624.2 697.242 11 2 13 2 12028.9 718.015 15 2 13 2 11373.2 727.592 12 2 13 2 11588.8 631.306 11 2 13 3 988.052 229.756 15 2 13 3 1007.29 202.218 4 2 13 3 1040.70 224.917 12 2 13 4 28485.7 1115.62 15 2 13 4 30437.4 1070.94 4 2 13 4 28676.4 1050.12 12 2 13 5 59443.7 1526.07 4 2 13 5 57229.0 1594.30 15 2 13 5 56129.1 1401.42 12 2 13 6 7327.98 555.122 4 2 13 6 7971.34 604.677 15 2 13 7 5041.57 458.717 23 2 13 7 4835.59 466.373 15 2 13 7 5023.78 469.858 4 2 13 8-60.0051 95.9743 23 2 13 8 62.9613 120.977 4 2 13 8 161.694 126.582 15 2 13 9 4250.08 421.728 23 2 13 9 4227.97 455.242 15 2 13 9 4313.51 415.046 4 2 13 10 2396.11 295.916 4 2 13 10 2586.18 342.081 23 2 13 10 2354.67 337.290 15 2 13 11 158.772 106.098 15 2 13 11 210.241 110.804 23 2 13 11 105.159 90.4690 4 2 13 12 4671.64 353.608 4 2 13 12 4712.24 426.309 23 2 13 12 4711.45 399.903 15 2 13 13 1291.54 193.689 15 2 13 13 1474.23 219.579 23 2 13 14 276.222 98.7780 23 2 14 -6 8646.92 460.437 11 2 14 -5 660.247 136.732 11 2 14 -4 2019.99 265.810 11 2 14 -3 9428.88 591.541 11 2 14 -3 9421.81 550.186 12 2 14 -2 4458.78 460.155 8 2 14 -2 4782.81 425.860 11 2 14 -2 5176.82 423.005 12 2 14 -1-10.3840 82.6283 11 2 14 -1 100.587 135.938 8 2 14 -1 39.1205 79.8328 12 2 14 0 4463.73 428.899 8 2 14 0 4632.70 435.245 12 2 14 0 4034.64 369.286 11 2 14 0 3786.73 398.123 15 2 14 1 500.643 149.553 11 2 14 1 643.463 201.094 15 2 14 1 572.692 169.251 8 2 14 1 639.380 191.980 12 2 14 2 5612.99 471.803 15 2 14 2 5705.14 464.762 8 2 14 2 5613.10 491.491 12 2 14 3 4210.62 404.454 8 2 14 3 3909.14 403.730 15 2 14 3 3911.78 390.947 12 2 14 4 28263.9 1070.49 15 2 14 4 26422.5 972.140 12 2 14 5 8944.24 593.530 15 2 14 5 8322.90 518.142 12 2 14 6 742.097 182.929 15 2 14 6 879.689 193.129 4 2 14 7 1917.51 292.481 15 2 14 7 2021.81 285.555 4 2 14 8 425.513 142.354 15 2 14 8 581.016 167.559 4 2 14 9 2959.72 356.760 15 2 14 9 3000.01 324.170 4 2 14 10 984.694 212.873 15 2 14 10 1147.60 196.362 4 2 14 11 135.778 118.741 15 2 14 12 278.375 109.576 15 2 15 -3 9668.29 513.047 11 2 15 -2 1410.67 205.948 11 2 15 -1 3071.72 352.189 8 2 15 -1 3155.37 302.578 11 2 15 0-109.787 126.950 8 2 15 0-83.3450 80.0876 11 2 15 0-22.4186 67.9728 12 2 15 1 2042.16 277.113 8 2 15 1 1720.97 253.275 12 2 15 2 5023.93 407.910 8 2 15 2 4432.06 392.136 12 2 15 2 4223.11 376.019 15 2 15 3 14629.8 687.412 8 2 15 3 14425.4 671.305 15 2 15 4 14329.8 684.022 8 2 15 4 14462.4 689.846 15 2 15 5 1376.12 221.021 15 2 15 5 1572.21 219.398 8 2 15 6 5116.44 419.970 15 2 15 7 11086.2 621.006 15 2 15 8 3126.13 332.166 15 2 15 9 248.405 101.305 15 2 15 10 4753.06 378.129 15 2 16 1 3859.55 320.110 8 2 16 2 8592.43 467.654 8 2 16 3 168.739 88.5424 8 2 16 4 623.946 134.270 8 2 16 5 44.5040 63.0205 8 2 16 6 1054.90 165.971 8 -3 14 5 467.922 120.286 6 -3 14 4 232.006 82.4952 6 -3 14 3 1227.20 165.388 6 -3 14 2 1532.42 180.844 6 -3 14 0 925.615 170.916 10 -3 14 0 949.104 196.493 9 -3 14 -1 361.990 116.238 10 -3 14 -1 545.999 135.737 9 -3 14 -2 9924.26 563.226 10 -3 14 -2 10205.3 543.554 9 -3 14 -3 942.084 181.641 10 -3 14 -3 989.097 174.522 9 -3 13 9 6683.76 387.098 21 -3 13 8 278.556 93.7326 21 -3 13 8 239.053 96.5187 15 -3 13 7 4.65939 60.2390 15 -3 13 7 5.34159 52.1387 21 -3 13 6 343.246 109.685 21 -3 13 6 540.688 145.169 6 -3 13 5 372.100 101.039 21 -3 13 5 513.334 115.370 6 -3 13 4 2709.71 299.583 21 -3 13 4 3155.50 295.366 6 -3 13 3 450.577 130.793 21 -3 13 3 445.237 113.493 6 -3 13 2 13732.6 715.549 10 -3 13 2 13714.6 617.508 6 -3 13 1 4030.76 399.401 10 -3 13 1 3570.28 394.371 9 -3 13 1 3841.37 328.746 6 -3 13 0 1463.77 250.026 10 -3 13 0 1319.83 262.193 9 -3 13 0 1151.91 183.080 6 -3 13 -1 1059.93 189.142 17 -3 13 -1 1054.70 218.037 10 -3 13 -1 1404.58 271.099 9 -3 13 -1 877.905 158.191 6 -3 13 -2 1308.23 223.374 9 -3 13 -2 852.307 162.242 6 -3 13 -2 1148.92 201.166 17 -3 13 -2 1114.25 225.460 10 -3 13 -3 1180.23 240.835 10 -3 13 -3 1101.07 215.767 9 -3 13 -3 1264.35 210.618 17 -3 13 -4 4604.78 446.935 10 -3 13 -4 5242.70 425.032 9 -3 13 -4 4622.12 383.696 17 -3 13 -5 578.175 148.232 10 -3 13 -5 557.296 152.528 9 -3 13 -5 508.134 129.955 17 -3 13 -6 2000.08 260.019 10 -3 13 -6 1936.07 235.709 9 -3 13 -6 1517.67 212.032 17 -3 12 11 398.096 117.602 15 -3 12 11 354.484 95.2482 21 -3 12 10 794.138 164.227 15 -3 12 10 961.017 176.516 21 -3 12 9 4621.38 384.098 21 -3 12 9 4948.13 418.158 15 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320.102 9 -3 12 -1 1672.41 296.301 10 -3 12 -1 1510.26 236.570 6 -3 12 -2 394.121 169.407 10 -3 12 -2 549.228 162.192 17 -3 12 -2 398.029 209.817 9 -3 12 -3 20923.6 940.664 9 -3 12 -3 21858.6 1026.79 10 -3 12 -3 20243.2 898.388 17 -3 12 -4 5942.85 522.473 16 -3 12 -4 5498.53 472.022 9 -3 12 -4 5771.71 543.925 10 -3 12 -4 5528.92 473.840 17 -3 12 -5 1496.57 251.082 17 -3 12 -5 1680.63 282.521 16 -3 12 -5 1594.58 299.776 10 -3 12 -5 1359.00 254.349 9 -3 12 -6 5837.64 522.940 16 -3 12 -6 5491.23 448.047 9 -3 12 -6 5843.83 517.514 10 -3 12 -6 5143.81 449.453 17 -3 12 -7 19253.7 901.938 16 -3 12 -7 17340.0 797.531 17 -3 12 -7 19880.7 851.318 10 -3 12 -7 18262.3 745.681 9 -3 12 -8 532.449 129.426 17 -3 12 -8 613.270 155.073 16 -3 12 -8 604.142 142.428 10 -3 11 13 31.3231 47.1166 15 -3 11 12 2641.11 266.461 21 -3 11 12 3363.66 302.990 15 -3 11 11 1569.95 228.404 15 -3 11 11 1205.75 209.566 21 -3 11 10 1026.06 191.741 21 -3 11 10 947.657 183.703 15 -3 11 10 826.071 144.989 7 -3 11 9 100.660 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25 4 10 3 15751.7 700.525 4 4 10 3 15750.3 929.786 12 4 10 4 1950.16 263.248 25 4 10 4 1916.46 293.057 15 4 10 4 1858.12 246.872 4 4 10 4 2086.35 325.468 12 4 10 5-70.6209 81.8957 25 4 10 5 168.792 148.114 15 4 10 5 33.7643 74.6755 4 4 10 5 48.4800 86.0848 12 4 10 6-37.1830 103.650 25 4 10 6-64.0841 150.558 15 -4 -10 -6 153.226 85.6560 22 4 10 6 16.6959 90.1560 12 4 10 7 4505.79 465.717 15 4 10 7 4491.09 415.350 25 4 10 7 4109.42 394.836 23 -4 -10 -7 4260.91 396.929 22 4 10 7 4224.25 389.456 12 4 10 8 12679.8 803.329 15 4 10 8 10430.9 625.190 25 4 10 8 11363.4 670.873 23 4 10 9 10972.6 774.866 15 4 10 9 10870.2 618.140 25 4 10 9 11024.7 667.144 23 4 10 10 1271.35 194.716 25 4 10 10 1527.77 280.403 15 4 10 10 1560.35 272.630 23 4 10 11 2680.73 276.313 25 4 10 11 3125.20 383.905 23 4 10 12 486.160 173.334 23 4 10 12 402.936 141.600 4 4 10 13 77.5411 82.7820 23 4 10 13 145.378 91.2089 4 4 10 14 713.241 182.151 23 4 10 14 838.125 159.757 4 4 10 15 1442.43 228.992 23 4 10 15 1499.84 194.552 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798.558 4 4 12 6 15293.6 722.304 12 4 12 7 10484.8 711.865 15 4 12 7 9745.12 628.742 25 4 12 7 9537.27 614.087 4 4 12 8 345.193 125.414 25 4 12 8 78.9304 120.720 15 4 12 8 285.780 106.251 23 4 12 8 317.470 138.394 4 4 12 9 502.238 129.512 25 4 12 9 466.416 123.790 23 4 12 9 503.614 155.259 4 4 12 10 3711.90 413.874 15 4 12 10 3204.68 309.552 25 4 12 10 3428.40 356.523 23 4 12 10 3815.08 379.624 4 4 12 11 1041.91 211.966 15 4 12 11 1076.27 211.248 23 4 12 11 1047.26 192.821 4 4 12 12 64.0088 80.3106 15 4 12 12-51.9026 67.9259 23 4 12 12 4.32601 68.6034 4 4 12 13 123.007 70.8394 23 4 12 13 255.369 65.4023 4 4 12 14 2411.46 262.803 23 4 12 14 2622.19 238.199 4 4 13 -6 3468.74 275.369 11 4 13 -5 1037.00 162.091 11 4 13 -5 616.624 119.265 12 4 13 -4 184.862 92.8598 11 4 13 -4 37.1286 52.5562 12 4 13 -3 1745.43 229.372 12 4 13 -3 1799.29 248.496 11 4 13 -2 520.877 143.319 11 4 13 -2 472.407 133.633 12 4 13 -1 106.373 85.9161 11 4 13 -1 79.9500 77.9776 12 4 13 0 2249.27 333.620 8 4 13 0 1912.84 269.837 12 4 13 0 2221.71 259.092 11 4 13 1 3384.17 379.299 8 4 13 1 3591.15 373.888 12 4 13 2 366.499 151.099 8 4 13 2 289.683 111.537 12 4 13 3 745.229 234.715 15 4 13 3 707.324 165.214 4 4 13 3 662.859 166.989 8 4 13 3 643.154 168.523 12 4 13 4 64.2704 185.755 15 4 13 4 173.435 89.9009 4 4 13 4 5.12261 80.3085 8 4 13 4 10.1829 66.2332 12 4 13 5 239.632 80.7749 25 4 13 5 338.669 180.368 15 4 13 5 279.686 110.624 8 4 13 5 126.597 75.3984 4 4 13 5 77.8040 73.2605 12 4 13 6 1694.08 261.631 25 4 13 6 2082.56 318.598 15 4 13 6 1766.81 245.906 4 4 13 6 1358.27 213.963 12 4 13 7 5587.17 498.669 15 4 13 7 5265.55 444.120 25 4 13 7 5328.80 432.055 4 4 13 8 284.222 104.823 25 4 13 8 243.412 147.117 15 4 13 8 135.678 82.4910 4 4 13 9 298.375 147.977 15 4 13 9 75.7408 64.5417 23 4 13 9 262.490 143.046 4 4 13 10 2055.45 285.957 15 4 13 10 1681.13 233.362 23 4 13 10 1733.67 242.632 4 4 13 11 4852.67 395.385 15 4 13 11 4067.73 351.113 23 4 13 11 4630.94 365.472 4 4 13 12 5041.11 352.175 4 4 13 12 4366.46 363.445 23 4 13 13 731.431 130.906 4 4 14 -3 6982.92 397.846 12 4 14 -2 10968.3 526.806 12 4 14 -2 9468.84 498.391 11 4 14 -1 264.594 98.9250 11 4 14 -1 296.373 102.656 12 4 14 0 970.573 175.567 12 4 14 1 2068.85 295.322 8 4 14 1 2031.76 265.767 12 4 14 2 6.69905 131.050 8 4 14 2 117.040 80.8933 12 4 14 3 198.521 133.293 8 4 14 3 174.633 116.706 12 4 14 4 5062.25 435.933 15 4 14 4 4593.68 383.357 8 4 14 4 3827.97 345.653 12 4 14 5 2313.08 257.104 4 4 14 5 2601.04 322.718 15 4 14 5 2690.29 297.397 8 4 14 5 1795.00 236.257 12 4 14 6 2731.01 286.227 4 4 14 6 3116.89 361.269 15 4 14 6 2752.29 291.498 8 4 14 7 10515.0 631.084 15 4 14 7 10253.4 549.143 4 4 14 7 8995.32 521.869 8 4 14 8 30667.9 1074.43 15 4 14 8 30453.1 949.647 4 4 14 8 27852.1 922.206 8 4 14 9 3469.57 318.792 4 4 14 9 3235.34 337.906 15 4 14 10 73.0127 105.401 15 4 14 10 122.029 79.8580 4 4 14 11 781.569 137.634 4 4 15 0 2299.71 231.899 12 4 15 1 105.019 66.1200 12 4 15 2 4728.72 370.538 8 4 15 2 3762.98 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7935.30 500.974 20 -5 0 -5 7806.36 506.640 18 -5 0 -6 21622.4 1642.07 24 -5 0 -6 20875.5 800.334 22 -5 0 -6 20527.3 854.520 18 5 0 7 2450.12 266.149 2 -5 0 -7 2099.61 533.148 24 -5 0 -7 2662.01 323.874 18 5 0 8 4208.61 375.896 2 -5 0 -8 4478.30 836.588 24 -5 0 -8 4342.21 434.324 18 5 0 9 6208.61 486.910 2 5 0 10 13132.6 766.506 2 5 0 11 1578.81 307.527 2 5 0 12 966.720 227.451 2 5 0 13 9149.34 654.192 2 5 0 14 1740.49 282.161 2 5 0 15 85.3360 88.6373 2 -5 0 -16 439.935 131.921 18 5 0 16 769.546 172.959 2 5 0 17 1662.07 212.349 2 -5 0 -17 1084.21 169.876 18 -5 0 -18-6.56847 61.4497 20 -5 -1 14 146.047 81.6882 27 -5 -1 14 283.102 80.7164 15 -5 -1 13 226.618 98.0057 27 -5 -1 13 312.437 94.2200 15 -5 -1 12-27.1511 86.1433 15 -5 -1 11 21554.0 909.318 15 -5 -1 11 24673.1 810.157 19 -5 -1 10 4089.22 350.203 19 -5 -1 9 2098.33 332.760 22 -5 -1 9 2872.30 307.256 19 -5 -1 9 2539.52 328.877 5 -5 -1 8 12049.4 789.488 22 -5 -1 8 10895.5 633.272 14 -5 -1 8 12872.5 696.063 19 -5 -1 8 12545.3 758.155 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4799.46 421.478 19 -5 -2 8 609.406 166.860 5 -5 -2 8 778.313 214.263 22 -5 -2 8 865.438 198.931 19 -5 -2 7 4007.94 423.373 22 -5 -2 7 4392.02 432.823 5 -5 -2 7 3311.81 627.256 29 -5 -2 6 3094.09 338.838 22 -5 -2 6 3130.49 324.849 5 -5 -2 5 204.593 83.8720 5 -5 -2 5 231.426 106.789 22 -5 -2 5 71.7220 116.820 29 -5 -2 4 168.476 73.1745 5 -5 -2 4 338.481 113.988 22 -5 -2 4 214.012 142.687 29 -5 -2 3 8650.74 441.398 5 -5 -2 3 8380.88 491.456 22 -5 -2 3 9036.32 976.849 29 -5 -2 2 976.758 341.023 29 -5 -2 2 1073.85 188.948 22 -5 -2 1 7405.38 444.753 22 -5 -2 1 7483.84 868.528 29 -5 -2 0 315.353 163.352 29 -5 -2 0 402.293 106.772 22 -5 -2 -1 30065.8 891.405 22 5 2 1 31043.4 915.256 3 -5 -2 -1 29088.8 830.000 18 -5 -2 -1 30799.8 1791.47 29 -5 -2 -2 19776.4 1537.07 24 -5 -2 -2 18875.4 719.340 22 5 2 2 20190.7 745.732 3 -5 -2 -2 18777.3 673.593 18 -5 -2 -2 19062.3 1438.56 29 -5 -2 -3 3540.35 658.429 24 -5 -2 -3 3188.41 301.581 22 5 2 3 2954.86 293.777 3 -5 -2 -3 3217.93 287.052 18 5 2 4 35333.2 936.676 2 -5 -2 -4 36742.3 2130.71 24 -5 -2 -4 34440.8 1008.48 22 5 2 4 34973.6 1021.92 3 -5 -2 -4 34024.2 950.191 18 -5 -2 -5 1250.08 414.922 24 5 2 5 1359.00 188.985 2 -5 -2 -5 1334.12 205.089 18 5 2 5 1360.91 208.474 3 5 2 6 7469.11 456.639 2 -5 -2 -6 8957.66 1100.28 24 -5 -2 -6 7582.46 478.873 18 5 2 7 3777.21 344.139 2 -5 -2 -7 4042.20 368.028 18 5 2 8 2394.52 297.613 2 -5 -2 -8 2581.05 664.347 24 -5 -2 -8 2478.65 294.142 18 -5 -2 -9 1601.10 254.765 18 5 2 9 1458.59 238.258 2 5 2 10 5337.64 484.741 2 -5 -2 -10 4427.88 966.454 24 -5 -2 -10 5583.60 486.399 18 5 2 11 4689.94 498.598 2 -5 -2 -11 4073.72 865.766 24 5 2 12 6326.95 598.682 2 5 2 13 27752.5 1186.35 2 -5 -2 -14 1161.48 252.160 18 5 2 14 1941.56 318.385 2 5 2 15 1970.67 290.977 2 5 2 16 912.656 188.310 2 5 2 17 78.7939 67.7516 2 5 2 18-99.3875 94.0201 2 -5 -3 14 151.553 65.6048 27 -5 -3 13-1.10138 57.4336 15 -5 -3 13 137.157 74.0422 19 -5 -3 12 5155.76 388.611 15 -5 -3 12 6400.58 402.169 19 -5 -3 11 6519.24 441.416 19 -5 -3 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459.503 14 -7 -4 5 107.257 89.2987 22 -7 -4 4 2330.91 296.024 22 -7 -4 3 172.252 83.7636 22 -7 -4 2 597.207 154.175 22 -7 -4 1 4271.52 401.638 22 -7 -4 0 1044.02 192.419 22 -7 -4 -1 64.0796 65.0912 22 -7 -4 -2 17975.3 805.182 22 -7 -4 -3 394.345 141.877 22 -7 -4 -4 40.6636 63.6395 22 -7 -4 -5 3597.37 382.098 22 7 4 5 3816.84 384.912 3 -7 -4 -6 6664.93 524.231 22 7 4 6 6626.21 519.304 3 -7 -4 -7 274.251 116.445 22 7 4 7 133.900 65.8843 3 -7 -4 -8 11544.5 692.982 22 7 4 8 11974.9 713.563 3 -7 -4 -9 3503.07 387.098 22 7 4 9 3776.65 408.818 3 -7 -4 -10 14595.1 815.476 22 7 4 10 15947.9 833.780 3 -7 -4 -11 540.437 183.309 22 7 4 11 298.101 125.591 3 -7 -4 -12 648.099 224.371 22 7 4 12 402.347 163.424 3 -7 -4 -13 8634.89 603.056 22 7 4 13 6947.79 552.784 3 -7 -4 -14 5248.07 408.586 22 7 4 14 4356.30 388.767 3 -7 -4 -15 465.596 119.015 22 7 4 15 610.493 138.699 3 -7 -5 9 1658.34 195.213 15 -7 -5 8 101.376 63.9705 19 -7 -5 7 441.738 141.188 22 -7 -5 7 572.802 127.171 19 -7 -5 6 12713.9 674.897 22 -7 -5 5 982.303 198.088 22 -7 -5 4 7021.53 492.228 22 -7 -5 3 4262.12 390.308 22 -7 -5 2 1947.12 271.429 22 -7 -5 1 316.939 114.188 22 -7 -5 0 7091.08 502.829 22 7 5 1 3158.88 302.552 25 -7 -5 -1 3339.46 350.770 22 7 5 2 443.793 112.215 25 -7 -5 -2 523.629 154.618 22 -7 -5 -3 21034.0 888.424 22 -7 -5 -4 4850.10 426.166 22 -7 -5 -5 1558.72 251.135 22 -7 -5 -6 126.496 126.306 22 7 5 6 104.186 63.4443 3 -7 -5 -7 6782.76 529.500 22 7 5 7 6968.77 527.047 3 -7 -5 -8 5411.67 486.880 22 7 5 8 5481.19 476.790 3 -7 -5 -9 9967.43 660.091 22 7 5 9 10781.2 674.202 3 -7 -5 -10 5557.80 508.727 22 7 5 10 5699.57 488.962 3 -7 -5 -11 1915.18 320.077 22 7 5 11 2287.81 318.924 3 -7 -5 -12 6527.00 627.159 22 7 5 12 7267.22 580.094 3 -7 -5 -13 1959.93 310.317 22 7 5 13 1727.53 268.410 3 -7 -5 -14 7761.19 514.577 22 7 5 14 7041.58 473.536 3 -7 -5 -15 1988.87 226.832 22 7 5 15 1446.32 197.426 3 -7 -6 8 275.537 84.0342 19 -7 -6 7 418.026 128.285 22 -7 -6 7 471.156 124.968 14 -7 -6 7 719.988 143.865 19 -7 -6 6 330.391 122.010 22 -7 -6 6 387.778 119.502 19 -7 -6 5 4097.00 372.415 22 -7 -6 4 14569.8 685.287 22 -7 -6 3 2217.20 273.260 22 -7 -6 2 11.6391 67.3512 22 -7 -6 1 10572.6 596.015 22 -7 -6 0 591.555 155.658 22 7 6 1 14815.0 637.781 25 -7 -6 -1 16669.6 765.340 22 7 6 2 2805.02 294.574 25 -7 -6 -2 3037.89 329.611 22 7 6 3 1732.63 234.292 25 -7 -6 -3 2310.07 303.043 22 7 6 4 274.136 109.530 25 -7 -6 -4 231.742 104.763 22 -7 -6 -5 14767.1 754.282 22 -7 -6 -6 2211.88 304.006 22 -7 -6 -7 690.041 159.453 22 7 6 7 630.938 169.160 3 -7 -6 -8 11588.3 701.050 22 7 6 8 12548.2 693.872 3 -7 -6 -9 9233.71 629.037 22 7 6 9 9195.54 603.909 3 -7 -6 -10 63.2553 137.214 22 7 6 10-56.0544 90.9905 3 -7 -6 -11 1678.47 307.775 22 7 6 11 1639.39 264.362 3 7 6 12 1688.41 218.359 25 -7 -6 -12 1950.37 326.778 22 7 6 12 2268.58 305.130 3 7 6 13 266.057 92.6844 25 -7 -6 -13 303.273 142.421 22 7 6 13 192.207 88.7070 3 7 6 14 516.492 102.325 25 -7 -6 -14 958.924 190.026 22 7 6 14 654.434 147.067 3 -7 -6 -15 4671.99 344.793 22 7 6 15 4072.75 301.222 3 -7 -7 7 907.723 150.991 19 -7 -7 6 73.4010 57.7913 22 -7 -7 6 62.4589 65.9862 19 -7 -7 5 769.678 165.800 22 -7 -7 4 75.3681 50.5962 22 -7 -7 3 1798.27 237.050 22 -7 -7 2 630.635 141.148 22 -7 -7 1 17060.8 730.915 22 -7 -7 0 3326.82 329.728 22 7 7 1 5912.85 397.968 25 -7 -7 -1 7132.11 487.568 22 7 7 2 48.1498 97.0288 25 -7 -7 -2 16.1430 79.2535 22 7 7 3 6196.24 444.815 25 -7 -7 -3 7781.11 527.954 22 7 7 4 1254.65 207.946 25 -7 -7 -4 1132.22 214.727 22 7 7 5 201.770 75.7391 25 -7 -7 -5 389.528 113.502 22 7 7 6 11607.4 653.246 25 -7 -7 -6 11575.1 677.320 22 7 7 7 161.445 95.4728 25 -7 -7 -7 53.0315 64.6918 22 7 7 8 490.489 155.450 25 -7 -7 -8 448.300 152.524 22 7 7 9 2212.50 284.888 25 -7 -7 -9 2555.93 341.537 22 7 7 9 2556.04 310.539 3 7 7 10 609.867 125.639 25 -7 -7 -10 461.874 156.002 22 7 7 10 795.117 183.899 3 7 7 11 208.857 102.060 25 -7 -7 -11 142.222 123.907 22 7 7 11 147.732 93.9179 3 7 7 12 1916.48 223.803 25 -7 -7 -12 1836.70 315.227 22 7 7 12 1982.07 267.874 3 7 7 13 41.4096 42.7878 25 -7 -7 -13-65.7556 80.2722 22 7 7 13-53.7038 72.5950 3 -7 -7 -14 84.1458 82.5503 22 7 7 14-120.070 51.1744 3 -7 -8 6 189.078 79.3468 19 -7 -8 5 744.873 139.989 22 -7 -8 5 832.988 172.257 19 -7 -8 4 553.026 135.091 22 7 8 -4 59.4472 75.1750 12 -7 -8 3 5345.85 385.150 22 7 8 -3 4935.32 413.096 12 -7 -8 2 112.988 80.0845 22 -7 -8 1 743.673 150.326 22 -7 -8 0 596.684 139.003 22 7 8 1 18352.0 687.103 25 -7 -8 -1 20903.7 797.884 22 7 8 2-38.0450 53.5566 25 -7 -8 -2 24.1971 66.7918 22 7 8 3 465.614 139.394 25 -7 -8 -3 574.587 135.642 22 7 8 4 16931.4 732.728 25 -7 -8 -4 18795.6 800.055 22 7 8 5-11.0994 84.9475 25 -7 -8 -5 9.15297 60.8516 22 7 8 6 210.447 108.677 25 -7 -8 -6 312.266 118.222 22 7 8 7 120.870 118.572 25 -7 -8 -7 16.6054 73.9120 22 7 8 8 2678.38 324.468 25 -7 -8 -8 2836.64 337.770 22 7 8 9 214.044 100.352 25 -7 -8 -9 208.325 108.606 22 7 8 10 2040.22 257.278 25 -7 -8 -10 2034.83 289.334 22 7 8 11 2575.15 265.146 25 -7 -8 -11 2866.44 348.537 22 7 8 12 333.961 98.2015 25 -7 -8 -12 445.673 148.074 22 7 8 13 51.1954 41.3730 25 -7 -8 -13 25.7016 67.2493 22 -7 -8 -14 746.249 146.003 22 -7 -9 5 172.727 79.9368 19 -7 -9 4 368.539 121.348 19 7 9 -4 240.488 83.5741 12 -7 -9 3 14254.7 580.858 22 7 9 -3 12231.9 580.274 12 -7 -9 2 1808.73 203.023 22 7 9 -2 2636.58 300.768 12 -7 -9 1 7615.12 437.084 22 -7 -9 0 2748.49 265.469 22 7 9 1 136.696 70.0803 25 -7 -9 -1 168.848 65.2310 22 7 9 2 3334.92 301.189 25 -7 -9 -2 4047.39 335.659 22 7 9 3 87.6320 76.6160 25 -7 -9 -3 247.321 102.331 22 7 9 4 5765.23 412.342 25 -7 -9 -4 6236.97 429.659 22 7 9 5 1306.11 199.000 25 -7 -9 -5 1330.42 199.880 22 7 9 6 158.366 79.6466 25 -7 -9 -6 292.021 119.447 22 7 9 7 1494.82 228.470 25 -7 -9 -7 1674.53 242.724 22 7 9 8 990.812 192.240 25 -7 -9 -8 979.636 184.698 22 7 9 9 1398.88 220.682 25 -7 -9 -9 1199.57 203.900 22 7 9 10 2136.23 242.150 25 -7 -9 -10 2353.43 297.352 22 7 9 11 1836.17 212.150 25 -7 -9 -11 2673.26 318.454 22 7 9 12 12.3702 54.2086 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74.1144 12 7 11 1 931.025 165.445 12 7 11 2 1413.80 177.271 25 7 11 2 1604.57 229.693 12 7 11 3 648.168 141.727 25 7 11 3 723.027 146.121 12 7 11 4 395.907 90.2584 25 7 11 4 410.739 120.352 12 7 11 5 366.709 96.4287 25 -7 -11 -5 560.838 107.113 22 7 11 5 492.031 143.507 12 7 11 6 3756.84 313.173 25 7 11 6 3250.61 299.131 12 7 11 7 2124.69 244.015 25 -7 -11 -7 2730.13 244.811 22 7 11 8 670.836 157.669 25 -7 -11 -8 895.913 140.990 22 7 11 8 359.226 98.4865 4 7 11 9 1048.70 171.080 25 7 11 9 773.699 140.195 4 7 11 10 9.15218 49.7699 25 7 12 2 2191.33 231.008 12 7 12 3 20.0992 74.8115 12 7 12 4 16.2458 50.9483 25 7 12 4 285.372 70.2677 12 7 12 5 1469.75 179.429 25 7 12 6 718.047 126.168 25 7 12 7 874.279 151.625 25 -8 7 0 2528.21 214.725 21 -8 7 -1 5607.76 327.605 21 -8 7 -2-2.72398 57.2301 21 -8 6 3 461.698 93.7747 5 -8 6 3 546.920 116.247 7 -8 6 2 300.209 85.1855 5 -8 6 2 416.404 98.3449 21 -8 6 1 1968.69 189.706 5 -8 6 1 2143.59 200.771 21 -8 6 1 1494.60 178.442 7 -8 6 0 4470.17 295.804 5 -8 6 0 4657.76 305.902 7 -8 6 -1 19156.8 643.778 21 -8 6 -2 8097.96 429.809 21 -8 6 -3 1299.63 177.001 21 -8 6 -4 580.282 134.533 21 -8 6 -5 117.386 63.8346 21 -8 6 -6 233.108 92.3283 21 -8 5 5 4907.97 322.897 5 -8 5 4 915.748 142.588 5 -8 5 3 415.658 94.9619 5 -8 5 3 343.035 89.8740 21 -8 5 2 553.449 115.323 5 -8 5 2 522.344 113.126 21 -8 5 1 249.580 79.6941 5 -8 5 1 207.321 86.2361 21 -8 5 0 5675.84 364.267 21 -8 5 -1 87.8550 74.5769 21 -8 5 -2 2894.32 290.398 21 -8 5 -3 353.271 117.608 21 -8 5 -4 544.232 127.733 21 -8 5 -5 2268.97 262.155 21 -8 5 -6 1707.29 224.760 21 -8 5 -7 3020.31 274.222 21 -8 4 6 824.669 146.409 5 -8 4 5 533.407 120.484 5 -8 4 4 9224.95 450.148 5 -8 4 3 213.936 76.9694 5 -8 4 3 52.5206 45.6333 21 -8 4 2 160.257 67.2941 5 -8 4 2 161.012 68.3524 21 -8 4 1 4962.55 365.405 5 -8 4 1 5164.69 345.797 21 -8 4 0 2264.14 242.032 21 -8 4 -1 72.4441 75.4964 21 -8 4 -2 141.672 77.9292 21 -8 4 -3 340.351 124.789 21 -8 4 -4 2522.95 275.535 21 -8 4 -5 325.174 98.2769 21 -8 4 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52.4808 15 -8 0 4 35.3830 58.4613 22 -8 0 4-28.9190 87.9834 14 -8 0 3 8213.94 469.431 5 -8 0 3 8104.30 499.977 22 -8 0 2 4125.01 329.204 5 -8 0 2 4040.19 345.334 22 -8 0 2 3166.05 348.933 14 -8 0 1 628.102 135.185 5 -8 0 1 562.406 131.900 22 -8 0 1 476.689 188.388 14 -8 0 0 536.038 128.179 5 -8 0 0 686.055 151.246 22 -8 0 0 706.011 192.955 14 -8 0 0 657.291 130.829 21 -8 0 -1 5403.92 387.722 22 -8 0 -1 4806.35 369.296 21 -8 0 -2 2104.63 240.760 22 -8 0 -2 1407.21 239.969 14 -8 0 -2 1682.27 232.742 21 -8 0 -3 2923.27 283.459 22 -8 0 -3 2357.71 284.141 21 -8 0 -4 1519.69 229.894 14 -8 0 -4 1799.19 263.572 21 -8 0 -5 923.121 193.832 21 -8 0 -6 2209.45 307.058 21 -8 0 -7 369.726 144.971 21 -8 0 -7 491.186 136.893 18 -8 0 -8 509.185 165.019 21 8 0 8 478.009 120.121 3 -8 0 -8 861.440 167.529 18 8 0 9 1653.67 227.409 3 -8 0 -9 1745.97 317.144 21 -8 0 -9 2000.94 255.844 18 -8 0 -10 742.338 209.771 21 8 0 10 159.226 61.0043 3 -8 0 -10 484.131 139.324 18 -8 0 -11 210.217 89.1162 21 8 0 11 267.662 109.839 3 -8 0 -11 376.310 115.605 18 -8 0 -12 787.742 144.573 21 8 0 12 436.822 126.638 3 -8 -1 7 42.8315 43.1961 15 -8 -1 7 140.901 71.7816 14 -8 -1 6 167.034 86.1701 5 -8 -1 6 405.219 112.967 15 -8 -1 6 157.968 76.2738 14 -8 -1 5 60.7529 61.1402 5 -8 -1 5 110.284 53.1036 15 -8 -1 5 254.422 94.7854 22 -8 -1 5 155.799 87.6785 14 -8 -1 4 1149.82 188.375 15 -8 -1 4 1383.07 219.335 22 -8 -1 4 1136.19 202.368 14 -8 -1 4 1396.35 212.699 5 -8 -1 3 2430.37 283.886 15 -8 -1 3 3016.51 310.435 22 -8 -1 3 2309.54 293.174 14 -8 -1 3 3156.81 296.524 5 -8 -1 2 1817.34 224.787 5 -8 -1 2 1707.75 228.143 22 -8 -1 2 1202.92 248.031 14 -8 -1 1 232.288 76.4153 5 -8 -1 1 232.406 96.4994 22 -8 -1 1 218.862 81.1197 14 -8 -1 0 3412.32 305.234 5 -8 -1 0 3146.31 300.592 22 -8 -1 0 2430.59 358.585 14 -8 -1 -1 10122.5 550.569 22 -8 -1 -1 8166.17 662.612 14 -8 -1 -1 8768.90 479.316 21 -8 -1 -2 23613.8 831.383 22 -8 -1 -2 20962.2 780.517 21 -8 -1 -3 418.023 120.996 22 -8 -1 -3 269.051 108.702 14 -8 -1 -3 207.446 87.1055 21 -8 -1 -4 5151.44 421.862 14 -8 -1 -4 5726.23 441.256 21 -8 -1 -5 1396.92 214.162 22 -8 -1 -5 1070.14 211.139 21 -8 -1 -6 1591.24 228.826 22 -8 -1 -6 1460.92 251.376 21 -8 -1 -7-28.4071 89.8627 21 -8 -1 -8 118.613 86.0005 21 8 1 8 189.182 82.6566 3 -8 -1 -9 294.365 145.473 21 8 1 9 425.013 113.218 3 -8 -1 -9 254.827 92.2308 18 -8 -1 -10 3638.19 399.749 21 8 1 10 4346.63 388.859 3 -8 -1 -11 57.9854 76.2842 21 8 1 11-107.203 112.604 3 -8 -1 -12 517.598 129.252 21 8 1 12 423.740 124.099 3 -8 -1 -13 867.923 144.608 21 -8 -2 7 315.467 85.9447 15 -8 -2 6 864.577 162.204 22 -8 -2 6 605.725 134.434 15 -8 -2 6 896.069 158.906 14 -8 -2 5 527.268 127.548 15 -8 -2 5 277.612 108.594 22 -8 -2 5 356.151 104.996 14 -8 -2 4 448.100 141.055 5 -8 -2 4 431.855 131.140 22 -8 -2 4 212.543 80.4803 14 -8 -2 3 72.2357 51.1007 5 -8 -2 3 17.3258 52.2611 22 -8 -2 3 103.788 96.4226 14 -8 -2 2 2119.71 253.444 22 -8 -2 2 1433.26 256.603 14 -8 -2 2 2045.33 230.151 5 -8 -2 1 12723.8 565.103 5 -8 -2 1 12122.8 607.503 22 -8 -2 0 257.570 85.9912 5 -8 -2 0 120.378 51.7611 22 -8 -2 0 284.862 171.393 14 -8 -2 -1 1080.68 168.164 5 -8 -2 -1 1030.92 182.292 22 -8 -2 -1 793.415 218.101 14 -8 -2 -2 4124.16 359.063 22 -8 -2 -2 3083.12 396.965 14 -8 -2 -3 1544.65 227.438 22 -8 -2 -3 1097.45 210.513 14 -8 -2 -3 1244.53 202.551 21 -8 -2 -4 7430.15 486.032 22 -8 -2 -4 6478.00 459.504 21 -8 -2 -5 32.3512 71.8764 22 -8 -2 -5 5.07682 79.2436 21 -8 -2 -6 2424.96 284.347 22 -8 -2 -6 1906.01 283.239 21 -8 -2 -7 4152.85 366.770 22 -8 -2 -7 3480.44 377.887 21 -8 -2 -8 345.152 121.072 22 8 2 8 261.312 106.309 3 -8 -2 -9 1818.08 251.591 22 8 2 9 1971.85 263.446 3 8 2 10 262.500 103.033 3 8 2 11 1272.43 226.704 3 8 2 12 93.5032 77.5630 3 -8 -2 -13 253.992 84.2152 21 8 2 13 63.8046 52.0362 3 -8 -3 7 3686.16 277.877 15 -8 -3 6 149.751 80.2238 22 -8 -3 6 41.5220 54.9082 15 -8 -3 6 192.148 75.2079 14 -8 -3 5 146.883 79.2955 22 -8 -3 5 116.088 91.6845 14 -8 -3 5 36.4055 54.1717 19 -8 -3 4 1248.74 213.342 22 -8 -3 4 1010.53 184.545 14 -8 -3 3 295.325 110.016 22 -8 -3 3 150.177 97.6021 14 -8 -3 2 191.529 80.5633 22 -8 -3 2 68.0507 72.2585 14 -8 -3 1 120.799 87.7060 22 -8 -3 0 428.553 129.335 22 -8 -3 -1 2740.92 294.212 22 -8 -3 -2 4203.27 363.511 22 -8 -3 -3 2076.88 255.760 22 -8 -3 -4 122.528 66.6592 22 -8 -3 -4-12.6984 74.4588 21 -8 -3 -5 3167.47 320.017 22 -8 -3 -5 2907.15 316.065 21 -8 -3 -6 2703.34 303.413 22 -8 -3 -6 2290.08 296.444 21 -8 -3 -7 6981.78 478.844 22 -8 -3 -8 6184.52 456.380 22 8 3 8 6530.07 473.628 3 -8 -3 -9 1202.05 203.327 22 8 3 9 1108.27 200.769 3 -8 -3 -10 4110.30 374.959 22 8 3 10 4270.65 381.816 3 -8 -3 -11 7.90048 59.3107 22 8 3 11 41.2880 65.6908 3 8 3 12 165.471 114.269 3 8 3 13 7037.66 444.446 3 -8 -4 6 2213.71 239.768 22 -8 -4 6 1471.52 185.836 14 -8 -4 5 59.3544 72.7429 22 -8 -4 5 82.2867 64.8450 14 -8 -4 5 54.8785 53.1125 19 -8 -4 4 397.491 118.253 22 -8 -4 4 301.998 91.2657 14 -8 -4 3 441.322 126.292 22 -8 -4 3 112.358 82.5652 14 -8 -4 2 108.840 89.3755 22 -8 -4 1 1107.31 187.775 22 -8 -4 0 3811.61 346.854 22 -8 -4 -1 147.875 87.3724 22 -8 -4 -2 13.4429 70.9336 22 -8 -4 -3 1202.83 199.115 22 -8 -4 -4 1240.39 202.353 22 -8 -4 -5 212.308 98.1579 22 -8 -4 -5 298.424 120.247 21 -8 -4 -6 2403.87 286.047 22 -8 -4 -7 644.709 152.689 22 -8 -4 -8 13.5986 54.1473 22 -8 -4 -9 95.1520 59.6375 22 8 4 9 133.581 85.6340 3 -8 -4 -10 2641.77 312.540 22 8 4 10 2493.49 298.566 3 -8 -4 -11 11988.1 680.701 22 8 4 11 12457.5 665.455 3 -8 -4 -12 658.525 149.389 22 8 4 12 542.941 143.205 3 8 4 13 600.264 132.672 3 -8 -5 5 27.7654 59.8320 22 -8 -5 5 127.890 66.5784 14 -8 -5 5 72.4594 73.8152 19 -8 -5 4-0.28327 63.2795 22 -8 -5 4 16.5015 70.8643 14 -8 -5 3 6651.98 434.323 22 -8 -5 2 356.085 106.580 22 -8 -5 1 1607.31 221.718 22 -8 -5 0 356.923 118.975 22 -8 -5 -1 3953.53 356.692 22 -8 -5 -2 92.8623 77.1714 22 8 5 3 7317.44 442.083 25 -8 -5 -3 8948.99 534.897 22 8 5 4 5041.75 381.832 25 -8 -5 -4 6070.50 442.575 22 -8 -5 -5 3231.03 323.641 22 -8 -5 -6 3294.56 336.459 22 -8 -5 -7 525.615 152.342 22 -8 -5 -8 245.298 89.4864 22 -8 -5 -9 5562.65 434.578 22 -8 -5 -10 17.8187 59.1977 22 -8 -5 -11-22.7621 69.6168 22 8 5 11-75.8050 80.5871 3 8 5 12 1372.80 172.601 25 -8 -5 -12 2057.92 267.444 22 8 5 12 1695.36 236.102 3 8 5 13 326.696 95.4728 3 -8 -6 5 242.449 81.7265 22 -8 -6 5 265.571 77.9133 19 -8 -6 4 3525.38 313.811 22 -8 -6 4 2727.20 276.392 14 -8 -6 3 1784.29 219.198 22 -8 -6 2 101.316 67.1255 22 -8 -6 1 903.049 158.748 22 -8 -6 0 3990.72 341.601 22 -8 -6 -1 1528.52 218.385 22 -8 -6 -2 8896.14 519.280 22 8 6 3 14818.2 610.211 25 -8 -6 -3 17799.4 737.515 22 8 6 4 1535.03 207.357 25 -8 -6 -4 1591.89 227.064 22 8 6 5 47.8268 65.2603 25 -8 -6 -5-56.2436 93.0962 22 8 6 6 3087.13 305.685 25 -8 -6 -6 3805.84 356.508 22 8 6 7 180.580 91.8942 25 -8 -6 -7 316.409 118.769 22 8 6 8 1399.54 213.950 25 -8 -6 -8 1963.21 248.749 22 8 6 9 45.5118 77.4993 25 -8 -6 -9 5.75074 59.2016 22 8 6 10 3676.78 320.365 25 -8 -6 -10 4283.64 382.310 22 8 6 11 4625.57 328.082 25 -8 -6 -11 6004.78 458.401 22 8 6 12 10047.5 447.499 25 -8 -6 -12 13987.7 657.209 22 -8 -7 4 401.555 100.170 22 -8 -7 4 337.759 105.434 14 -8 -7 4 340.459 115.894 19 -8 -7 3 511.414 122.299 22 8 7 -3 363.926 114.996 12 -8 -7 2 2243.57 241.233 22 -8 -7 1 1250.15 179.397 22 -8 -7 0 71.6836 57.6262 22 -8 -7 -1-67.1286 80.7828 22 -8 -7 -2 4086.62 332.604 22 8 7 3 194.855 96.5749 25 -8 -7 -3 251.691 104.767 22 8 7 4 68.5121 72.7707 25 -8 -7 -4 14.1023 72.7538 22 8 7 5 399.930 105.867 25 -8 -7 -5 287.616 104.335 22 8 7 6 726.358 156.673 25 -8 -7 -6 1120.92 185.655 22 8 7 7 98.0294 90.3693 25 -8 -7 -7-41.6782 59.7392 22 8 7 8 1859.86 246.312 25 -8 -7 -8 2088.69 253.483 22 8 7 9 120.976 68.5344 25 -8 -7 -9 407.971 116.113 22 8 7 10 9358.35 486.168 25 -8 -7 -10 12748.1 618.740 22 8 7 11 14378.6 550.037 25 -8 -7 -11 17268.6 730.025 22 8 7 12 18609.4 572.067 25 -8 -7 -12 24271.6 826.092 22 -8 -8 3 1567.58 198.479 19 -8 -8 2 5.54845 52.3221 22 8 8 -2 52.8099 50.3565 12 -8 -8 1 2468.43 232.889 22 -8 -8 0 344.214 87.4711 22 -8 -8 -1 4462.82 325.567 22 -8 -8 -2 12393.2 549.111 22 8 8 3-62.0575 84.8726 25 -8 -8 -3 251.076 92.3304 22 8 8 4 732.380 136.088 25 -8 -8 -4 1142.41 179.072 22 8 8 5 271.943 95.1195 25 -8 -8 -5 265.976 95.6205 22 8 8 6 80.2740 80.9631 25 -8 -8 -6 29.9315 61.1514 22 8 8 7 1285.63 184.384 25 -8 -8 -7 1657.99 210.662 22 8 8 8 636.884 143.478 25 -8 -8 -8 989.876 167.159 22 8 8 9 574.419 126.511 25 -8 -8 -9 603.394 129.497 22 8 8 10 1527.58 190.223 25 -8 -8 -10 2015.35 238.268 22 8 8 11 9232.40 417.963 25 -8 -8 -11 10733.4 539.362 22 8 9 -1 2265.95 215.642 12 -8 -9 0 3164.20 245.234 22 8 9 0 2642.13 265.154 12 -8 -9 -1 86.6030 53.8597 22 8 9 1 33.3021 60.4898 12 -8 -9 -2 55.9829 37.7133 22 8 9 3 332.911 94.3037 25 -8 -9 -3 433.638 100.654 22 8 9 4 3255.29 260.027 25 -8 -9 -4 4582.66 322.694 22 8 9 5 1686.12 206.755 25 -8 -9 -5 2788.97 254.197 22 8 9 6 341.653 107.985 25 -8 -9 -6 284.947 90.3426 22 8 9 7 280.791 92.0702 25 -8 -9 -7 572.401 125.214 22 8 9 8 955.829 159.061 25 -8 -9 -8 1326.17 177.249 22 8 9 9 38.2129 54.0959 25 -8 -9 -9-61.4611 56.3736 22 8 10 2 1574.01 208.211 12 8 10 3 210.231 76.1674 12 8 10 4 299.698 109.302 12 8 10 5 252.541 84.2959 25 8 10 5 590.263 132.168 12 8 10 6 216.235 75.2153 25 8 10 7 539.068 114.022 25 -9 3 0 962.307 126.637 5 -9 3 -1 2590.18 206.584 5 -9 3 -2-78.3163 58.3149 5 -9 3 -3 932.115 137.759 21 -9 3 -4 809.678 122.124 21 -9 2 1 3639.64 251.362 5 -9 2 0 29.0459 41.7609 5 -9 2 -1 645.495 113.408 5 -9 2 -2 2291.79 212.300 5 -9 2 -2 3398.95 247.451 21 -9 2 -3 488.504 109.525 21 -9 2 -4 288.789 78.8387 21 -9 2 -5 157.269 81.5514 21 -9 2 -6 1376.81 173.390 21 -9 2 -7 90.7107 59.3776 21 -9 1 2 24218.1 684.408 5 -9 1 1 18761.7 582.808 5 -9 1 0 1253.39 152.016 5 -9 1 -1 695.268 115.080 5 -9 1 -2 598.490 108.427 5 -9 1 -2 692.765 105.680 21 -9 1 -3 2341.57 217.920 5 -9 1 -3 5161.18 319.941 21 -9 1 -4 2884.22 249.788 21 -9 1 -5 1619.22 191.311 21 -9 1 -6 360.248 96.2730 21 -9 1 -7 105.390 59.4898 21 -9 1 -8 833.453 159.151 21 -9 0 2 29274.6 839.883 14 -9 0 1 12563.8 594.182 14 -9 0 1 17192.7 569.111 5 -9 0 0 6934.59 356.501 5 -9 0 0 4826.49 396.783 14 -9 0 -1 2367.94 211.746 5 -9 0 -1 2232.47 261.549 14 -9 0 -2 552.533 108.830 5 -9 0 -2 520.426 116.780 14 -9 0 -3 107.659 59.5686 5 -9 0 -3 33.0129 49.1645 21 -9 0 -4 2324.83 224.782 21 -9 0 -5 518.601 116.773 21 -9 0 -6 2676.79 249.060 21 -9 0 -7 1038.25 170.380 21 -9 0 -8 2539.10 264.144 21 -9 -1 3 8781.34 438.324 14 -9 -1 2 9128.16 477.514 14 -9 -1 1 1827.78 201.537 22 -9 -1 1 1435.67 206.655 14 -9 -1 1 1980.45 197.314 5 -9 -1 0 5505.16 343.270 22 -9 -1 0 5216.45 314.603 5 -9 -1 -1 1582.74 164.798 5 -9 -1 -1 2108.45 207.808 22 -9 -1 -1 1788.45 252.348 14 -9 -1 -2 184.982 83.7918 5 -9 -1 -2 120.560 70.8664 14 -9 -1 -3 54.7893 46.6118 14 -9 -1 -4 587.981 123.381 21 -9 -1 -5-1.12159 49.9865 21 -9 -1 -6 1802.37 214.631 21 -9 -1 -7 12212.7 551.359 21 -9 -1 -8 12707.9 582.787 21 -9 -1 -9 1136.91 189.710 21 -9 -2 3 5966.58 361.488 14 -9 -2 2 10.3277 46.6528 22 -9 -2 2 46.0145 65.3744 14 -9 -2 1-74.9299 69.4581 22 -9 -2 1-19.7888 59.4678 14 -9 -2 0-1.33819 45.4676 22 -9 -2 0-89.4203 75.3357 14 -9 -2 -1 787.614 133.670 22 -9 -2 -1 399.160 126.273 14 -9 -2 -2 1074.51 152.958 22 -9 -2 -2 820.340 169.444 14 -9 -2 -3 37.4488 49.4343 22 -9 -2 -3-76.6169 68.9658 14 -9 -2 -4 1481.48 173.651 22 -9 -2 -5 2768.51 238.004 22 -9 -2 -5 1920.07 209.052 21 -9 -2 -6 719.656 140.807 21 -9 -2 -7 8367.19 447.539 21 -9 -2 -8 108.943 61.2035 21 -9 -2 -9 326.670 122.920 21 -9 -3 2 246.245 74.7723 22 -9 -3 2 122.787 55.3609 14 -9 -3 1 5428.89 348.785 22 -9 -3 1 4038.31 332.980 14 -9 -3 0 404.021 99.3164 22 -9 -3 0 199.447 115.239 14 -9 -3 -1 122.660 53.0589 22 -9 -3 -1-3.25372 64.7785 14 -9 -3 -2 3415.34 271.856 22 -9 -3 -2 1958.85 263.785 14 -9 -3 -3 60.7724 55.9835 22 -9 -3 -3 12.6524 54.2231 14 -9 -3 -4 1298.28 170.695 22 9 3 5 7.66086 66.7147 25 -9 -3 -5 64.7863 55.4036 22 -9 -3 -6 2053.31 209.400 22 -9 -3 -6 1482.78 180.632 21 -9 -3 -7-8.11330 40.0496 22 -9 -3 -7-79.2173 71.4980 21 -9 -3 -8 858.325 148.056 21 -9 -3 -9 306.007 100.939 21 -9 -4 2-129.622 81.5783 22 -9 -4 2 144.881 72.0859 14 -9 -4 1 34.0299 61.0114 22 -9 -4 1 177.288 93.9456 14 -9 -4 0 2353.14 227.781 22 -9 -4 0 1665.85 225.543 14 -9 -4 -1 965.268 148.982 22 -9 -4 -1 278.924 97.0844 14 -9 -4 -2 66.1663 63.1553 22 -9 -4 -2-66.5741 89.7749 14 -9 -4 -3 370.689 100.351 22 -9 -4 -3 106.957 72.3641 14 -9 -4 -4 1444.51 179.803 22 -9 -4 -4 950.167 152.957 14 9 4 5 2540.58 225.054 25 -9 -4 -5 3328.13 271.527 22 9 4 6 2047.38 206.764 25 -9 -4 -6 3046.51 258.377 22 9 4 7 221.747 89.1170 25 -9 -4 -7 225.365 81.7542 22 9 4 8 1519.20 195.171 25 -9 -4 -8 1763.86 195.427 22 9 4 9 1050.72 153.174 25 -9 -5 1 516.167 106.311 22 -9 -5 1 461.011 111.843 14 -9 -5 0 184.221 71.3621 22 -9 -5 0 140.001 79.3454 14 -9 -5 -1 180.319 68.6864 22 -9 -5 -1 43.0136 55.4058 14 -9 -5 -2 1444.98 175.247 22 -9 -5 -2 737.458 188.602 14 -9 -5 -3 1449.78 179.776 22 -9 -5 -3 750.273 158.657 14 -9 -5 -4-56.4044 46.0991 22 -9 -5 -4-4.87888 44.1379 14 9 5 5 767.626 124.897 25 -9 -5 -5 1074.97 153.456 22 9 5 6 1924.67 199.323 25 -9 -5 -6 2755.98 241.802 22 9 5 7 1874.91 202.691 25 -9 -5 -7 2510.79 236.538 22 9 5 8 457.294 120.289 25 -9 -5 -8 598.384 123.917 22 -9 -6 0 4780.77 303.730 22 -9 -6 -1 868.175 136.872 22 -9 -6 -1 446.444 121.939 14 -9 -6 -2 2276.70 211.018 22 -9 -6 -2 721.190 172.044 14 -9 -6 -3 156.738 59.5136 22 -9 -6 -3-108.180 93.6283 14 -9 -6 -4 3243.32 257.837 22 -9 -6 -5 1027.84 142.460 22 -9 -6 -6 49.8354 44.2685 22 -9 -6 -7 3232.13 255.562 22 -9 -7 -3 481.943 99.1710 22 -9 -7 -4 4177.16 279.762 22 -9 -7 -5-1.33445 45.8900 22 -9 -7 -6 918.812 131.392 22 0 0 0 0.00 0.00 0 TITL lb0276_CLZ_SAC in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 7.997032 13.582410 16.663788 80.2141 80.0340 83.0359 ZERR 2.00 0.000342 0.000311 0.000681 0.0026 0.0036 0.0027 LATT 1 SFAC C H N O S Cl UNIT 73.62 62.42 12.80 6.00 2.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 5601 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C18A C -0.083(3) 0.757(2) 0.354(2) 0.048(5) Uani 0.411(18) 1 d . U P A 1 H18A H -0.009343 0.740921 0.394484 0.058 Uiso 0.411(18) 1 calc R U P A 1 C17A C -0.083(3) 0.8500(14) 0.3011(13) 0.061(5) Uani 0.411(18) 1 d . U P A 1 H17A H -0.009993 0.898698 0.304484 0.073 Uiso 0.411(18) 1 calc R U P A 1 C16A C -0.193(3) 0.8671(14) 0.2448(12) 0.047(3) Uani 0.411(18) 1 d . U P A 1 C15A C -0.2946(11) 0.8012(9) 0.2339(8) 0.044(2) Uani 0.411(18) 1 d . U P A 1 H15A H -0.366024 0.817284 0.192566 0.053 Uiso 0.411(18) 1 calc R U P A 1 C14A C -0.2940(13) 0.7080(10) 0.2846(8) 0.037(2) Uani 0.411(18) 1 d . U P A 1 H14A H -0.361447 0.658946 0.275998 0.044 Uiso 0.411(18) 1 calc R U P A 1 C13A C -0.198(5) 0.6870(17) 0.346(2) 0.029(3) Uani 0.411(18) 1 d D U P A 1 Cl1A Cl -0.1956(14) 0.9863(4) 0.1802(6) 0.0777(19) Uani 0.411(18) 1 d . U P A 1 C18B C -0.0435(18) 0.7458(13) 0.3557(12) 0.031(2) Uani 0.589(18) 1 d . U P A 2 H18B H 0.044455 0.718926 0.387069 0.037 Uiso 0.589(18) 1 calc R U P A 2 C17B C -0.0376(13) 0.8387(9) 0.3090(6) 0.0357(18) Uani 0.589(18) 1 d . U P A 2 H17B H 0.057057 0.875862 0.306169 0.043 Uiso 0.589(18) 1 calc R U P A 2 C16B C -0.1708(16) 0.8791(8) 0.2654(8) 0.036(2) Uani 0.589(18) 1 d . U P A 2 C15B C -0.3080(8) 0.8246(5) 0.2680(6) 0.0401(17) Uani 0.589(18) 1 d . U P A 2 H15B H -0.398319 0.852104 0.238224 0.048 Uiso 0.589(18) 1 calc R U P A 2 C14B C -0.3126(9) 0.7300(5) 0.3141(6) 0.0339(16) Uani 0.589(18) 1 d . U P A 2 H14B H -0.405390 0.691379 0.317064 0.041 Uiso 0.589(18) 1 calc R U P A 2 C13B C -0.176(3) 0.6931(11) 0.3564(14) 0.027(3) Uani 0.589(18) 1 d D U P A 2 Cl1B Cl -0.1650(3) 0.9973(2) 0.2081(4) 0.0516(10) Uani 0.589(18) 1 d . U P A 2 Cl2 Cl 0.26863(8) -0.15736(4) 0.45761(5) 0.0508(2) Uani 1 1 d . . . . . S1 S 0.24712(8) 0.69123(6) 0.79920(5) 0.0536(2) Uani 1 1 d . . . . . N2 N -0.1685(2) 0.40658(12) 0.50519(11) 0.0282(4) Uani 1 1 d . . . . . N3 N 0.2486(2) 0.26865(13) 0.30223(12) 0.0306(4) Uani 1 1 d . . . . . H3 H 0.345(4) 0.285(2) 0.2724(17) 0.037 Uiso 1 1 d . U . . . N1 N -0.1858(2) 0.59243(12) 0.40340(12) 0.0290(4) Uani 1 1 d D . . . . N4 N 0.2032(3) 0.44258(15) 0.19569(14) 0.0430(5) Uani 1 1 d . . . . . H4N H 0.262(4) 0.389(3) 0.1832(19) 0.052 Uiso 1 1 d . U . . . O3 O 0.5895(3) 0.7366(2) 0.90021(14) 0.0694(7) Uani 1 1 d . . . . . C12 C -0.2879(3) 0.58095(15) 0.47992(14) 0.0293(5) Uani 1 1 d . . . . . C5 C -0.2756(3) 0.48600(15) 0.52995(14) 0.0284(4) Uani 1 1 d . . . . . C6 C -0.0778(3) 0.41886(15) 0.43078(13) 0.0269(4) Uani 1 1 d . . . . . N5 N 0.4411(3) 0.69191(18) 0.81114(14) 0.0477(5) Uani 1 1 d . . . . . C7 C 0.0349(3) 0.33741(15) 0.40438(13) 0.0278(4) Uani 1 1 d . . . . . H7 H 0.040969 0.275383 0.440520 0.033 Uiso 1 1 calc R U . . . C19 C 0.2519(3) 0.16821(15) 0.34225(14) 0.0300(5) Uani 1 1 d . . . . . C10 C 0.0171(3) 0.52253(15) 0.29861(14) 0.0307(5) Uani 1 1 d . . . . . H10 H 0.015667 0.585425 0.263477 0.037 Uiso 1 1 calc R U . . . C11 C -0.0815(3) 0.51390(15) 0.37493(14) 0.0273(4) Uani 1 1 d . . . . . O1 O 0.2154(3) 0.7531(2) 0.72364(14) 0.0873(9) Uani 1 1 d . . . . . C9 C 0.1203(3) 0.43955(16) 0.27174(14) 0.0308(5) Uani 1 1 d . . . . . C8 C 0.1343(3) 0.34522(15) 0.32921(13) 0.0276(4) Uani 1 1 d . . . . . C24 C 0.1029(3) 0.12083(16) 0.36502(14) 0.0323(5) Uani 1 1 d . . . . . H24 H -0.003122 0.156834 0.355473 0.039 Uiso 1 1 calc R U . . . C34 C 0.1512(3) 0.75030(16) 0.88378(15) 0.0329(5) Uani 1 1 d . . . . . C29 C 0.2813(3) 0.76984(17) 0.92157(15) 0.0364(5) Uani 1 1 d . . . . . C3 C -0.4887(3) 0.54922(17) 0.63525(15) 0.0342(5) Uani 1 1 d . . . . . H3A H -0.557790 0.539163 0.687848 0.041 Uiso 1 1 calc R U . . . C4 C -0.3762(3) 0.47245(16) 0.60844(14) 0.0319(5) Uani 1 1 d . . . . . H4A H -0.366250 0.409589 0.643216 0.038 Uiso 1 1 calc R U . . . C2 C -0.5007(3) 0.64266(17) 0.58436(15) 0.0346(5) Uani 1 1 d . . . . . H2 H -0.579359 0.695365 0.602906 0.042 Uiso 1 1 calc R U . . . C23 C 0.1081(3) 0.02123(16) 0.40162(15) 0.0342(5) Uani 1 1 d . . . . . H23 H 0.005873 -0.010904 0.418443 0.041 Uiso 1 1 calc R U . . . C1 C -0.4014(3) 0.65948(16) 0.50845(15) 0.0334(5) Uani 1 1 d . . . . . H1 H -0.409208 0.723667 0.475426 0.040 Uiso 1 1 calc R U . . . C20 C 0.4085(3) 0.11491(17) 0.35461(15) 0.0350(5) Uani 1 1 d . . . . . H20 H 0.510766 0.147163 0.338832 0.042 Uiso 1 1 calc R U . . . C21 C 0.4140(3) 0.01453(17) 0.39008(16) 0.0394(5) Uani 1 1 d . . . . . H21 H 0.520025 -0.022423 0.398206 0.047 Uiso 1 1 calc R U . . . C22 C 0.2643(3) -0.03114(16) 0.41344(15) 0.0364(5) Uani 1 1 d . . . . . O2 O 0.2009(4) 0.5899(2) 0.8110(2) 0.1070(12) Uani 1 1 d . . . . . C28 C 0.4522(3) 0.7324(2) 0.87769(17) 0.0442(6) Uani 1 1 d . . . . . C33 C -0.0185(3) 0.7750(2) 0.91196(18) 0.0467(6) Uani 1 1 d . . . . . H33 H -0.106794 0.759927 0.885799 0.056 Uiso 1 1 calc R U . . . C30 C 0.2450(5) 0.8167(3) 0.99038(19) 0.0650(8) Uani 1 1 d . . . . . H30 H 0.333496 0.830010 1.017297 0.078 Uiso 1 1 calc R U . . . C32 C -0.0527(4) 0.8231(3) 0.9807(2) 0.0705(10) Uani 1 1 d . . . . . H32 H -0.167728 0.842433 1.002159 0.085 Uiso 1 1 calc R U . . . C31 C 0.0768(6) 0.8438(3) 1.0190(2) 0.0850(13) Uani 1 1 d . . . . . H31 H 0.048815 0.877363 1.065830 0.102 Uiso 1 1 calc R U . . . N6 N 0.3720(9) 0.7146(5) 0.2025(4) 0.0663(18) Uani 0.440(5) 1 d . . P B 2 C36 C 0.4991(10) 0.6938(5) 0.1610(4) 0.0567(18) Uani 0.440(5) 1 d . . P B 2 C35 C 0.6644(11) 0.6696(6) 0.1087(5) 0.064(2) Uani 0.440(5) 1 d . . P B 2 H35A H 0.651742 0.687667 0.050450 0.097 Uiso 0.440(5) 1 calc R U P B 2 H35B H 0.699050 0.597539 0.120559 0.097 Uiso 0.440(5) 1 calc R U P B 2 H35C H 0.751454 0.707540 0.120684 0.097 Uiso 0.440(5) 1 calc R U P B 2 C38 C 0.4408(8) 0.9765(5) 0.1055(4) 0.0509(18) Uani 0.464(7) 1 d . . P C 2 N7 N 0.5378(8) 0.9402(6) 0.0553(5) 0.082(2) Uani 0.464(7) 1 d . . P C 2 C37 C 0.3288(14) 1.0319(11) 0.1680(5) 0.057(3) Uani 0.464(7) 1 d . . P C 2 H37A H 0.211662 1.013948 0.174130 0.085 Uiso 0.464(7) 1 calc R U P C 2 H37B H 0.330988 1.104276 0.149812 0.085 Uiso 0.464(7) 1 calc R U P C 2 H37C H 0.370137 1.013732 0.221121 0.085 Uiso 0.464(7) 1 calc R U P C 2 N7A N 0.3148(10) 0.8524(7) 0.1844(6) 0.100(3) Uani 0.489(7) 1 d . . P D 1 C38A C 0.3259(11) 0.9392(9) 0.1734(5) 0.082(3) Uani 0.489(7) 1 d . . P D 1 C37A C 0.326(3) 1.0241(19) 0.1641(14) 0.171(12) Uani 0.489(7) 1 d . . P D 1 H37D H 0.218547 1.053208 0.192962 0.256 Uiso 0.489(7) 1 calc R U P D 1 H37E H 0.335909 1.050345 0.105096 0.256 Uiso 0.489(7) 1 calc R U P D 1 H37F H 0.421836 1.041804 0.186201 0.256 Uiso 0.489(7) 1 calc R U P D 1 C25A C 0.213(2) 0.5373(11) 0.1352(9) 0.054(3) Uani 0.560(5) 1 d . U P B 1 H25A H 0.105698 0.581761 0.147950 0.065 Uiso 0.560(5) 1 calc R U P B 1 C27A C 0.2089(9) 0.5001(4) 0.0542(3) 0.0623(16) Uani 0.560(5) 1 d . U P B 1 H27A H 0.209451 0.557256 0.009553 0.093 Uiso 0.560(5) 1 calc R U P B 1 H27B H 0.105302 0.466343 0.058851 0.093 Uiso 0.560(5) 1 calc R U P B 1 H27C H 0.309343 0.452821 0.042306 0.093 Uiso 0.560(5) 1 calc R U P B 1 C26A C 0.3514(13) 0.5894(5) 0.1395(4) 0.098(3) Uani 0.560(5) 1 d . U P B 1 H26A H 0.349964 0.651831 0.100170 0.147 Uiso 0.560(5) 1 calc R U P B 1 H26B H 0.458179 0.547645 0.125955 0.147 Uiso 0.560(5) 1 calc R U P B 1 H26C H 0.342965 0.605080 0.195424 0.147 Uiso 0.560(5) 1 calc R U P B 1 C25B C 0.195(2) 0.5233(16) 0.1241(12) 0.041(3) Uani 0.440(5) 1 d . U P B 2 H25B H 0.205041 0.586718 0.145148 0.049 Uiso 0.440(5) 1 calc R U P B 2 C26B C 0.3554(12) 0.5106(5) 0.0578(4) 0.067(2) Uani 0.440(5) 1 d . U P B 2 H26D H 0.353189 0.567388 0.012817 0.100 Uiso 0.440(5) 1 calc R U P B 2 H26E H 0.355519 0.448001 0.035947 0.100 Uiso 0.440(5) 1 calc R U P B 2 H26F H 0.458403 0.508508 0.082651 0.100 Uiso 0.440(5) 1 calc R U P B 2 C27B C 0.0361(11) 0.5401(5) 0.0897(5) 0.061(2) Uani 0.440(5) 1 d . . P B 2 H27D H 0.040578 0.598774 0.046325 0.092 Uiso 0.440(5) 1 calc R U P B 2 H27E H -0.059811 0.551906 0.133379 0.092 Uiso 0.440(5) 1 calc R U P B 2 H27F H 0.020726 0.480909 0.066293 0.092 Uiso 0.440(5) 1 calc R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C18A 0.058(12) 0.034(8) 0.058(7) -0.004(5) -0.025(9) -0.010(8) C17A 0.087(13) 0.018(5) 0.085(8) -0.004(4) -0.030(8) -0.012(7) C16A 0.065(8) 0.023(5) 0.048(8) -0.002(5) -0.006(5) 0.009(4) C15A 0.035(4) 0.052(5) 0.038(5) 0.002(4) -0.003(3) 0.007(3) C14A 0.033(4) 0.038(5) 0.038(5) -0.001(3) -0.007(3) -0.002(3) C13A 0.023(8) 0.019(4) 0.049(9) -0.009(4) -0.005(4) -0.007(4) Cl1A 0.115(3) 0.0295(14) 0.074(3) 0.0107(16) -0.005(3) 0.0142(16) C18B 0.029(4) 0.018(3) 0.047(4) -0.006(3) -0.008(3) -0.002(3) C17B 0.037(3) 0.024(3) 0.048(4) -0.005(3) -0.008(3) -0.005(3) C16B 0.040(4) 0.014(3) 0.053(6) -0.005(3) -0.007(4) 0.000(2) C15B 0.039(3) 0.031(3) 0.048(4) 0.004(3) -0.013(3) 0.003(2) C14B 0.031(3) 0.025(3) 0.046(4) 0.001(2) -0.013(3) -0.003(2) C13B 0.024(6) 0.016(4) 0.042(5) -0.004(3) -0.013(3) 0.001(3) Cl1B 0.0604(11) 0.0223(7) 0.0653(19) 0.0113(8) -0.0091(9) -0.0027(6) Cl2 0.0481(4) 0.0235(3) 0.0752(5) 0.0058(3) -0.0126(3) 0.0052(2) S1 0.0384(4) 0.0613(4) 0.0678(5) -0.0363(4) -0.0132(3) 0.0131(3) N2 0.0263(9) 0.0207(8) 0.0393(10) -0.0070(7) -0.0069(7) -0.0031(7) N3 0.0290(9) 0.0224(9) 0.0394(10) -0.0057(7) -0.0034(8) 0.0001(7) N1 0.0252(9) 0.0184(8) 0.0431(10) -0.0031(7) -0.0067(8) -0.0006(7) N4 0.0503(13) 0.0236(10) 0.0462(12) 0.0014(9) 0.0054(10) 0.0039(9) O3 0.0357(10) 0.1022(18) 0.0671(14) 0.0176(12) -0.0201(10) -0.0191(11) C12 0.0248(10) 0.0239(10) 0.0415(12) -0.0079(9) -0.0092(9) -0.0022(8) C5 0.0251(10) 0.0220(10) 0.0405(12) -0.0087(8) -0.0076(9) -0.0027(8) C6 0.0252(10) 0.0197(10) 0.0375(11) -0.0042(8) -0.0084(9) -0.0044(8) N5 0.0307(11) 0.0562(13) 0.0497(13) -0.0041(10) -0.0025(9) 0.0104(9) C7 0.0279(10) 0.0178(9) 0.0386(12) -0.0039(8) -0.0086(9) -0.0017(8) C19 0.0338(11) 0.0202(10) 0.0373(11) -0.0079(8) -0.0086(9) 0.0015(8) C10 0.0298(11) 0.0185(10) 0.0434(12) -0.0012(8) -0.0081(9) -0.0026(8) C11 0.0233(10) 0.0188(10) 0.0420(12) -0.0067(8) -0.0085(9) -0.0027(7) O1 0.0619(14) 0.148(3) 0.0534(13) -0.0456(15) -0.0226(11) 0.0458(15) C9 0.0288(11) 0.0234(10) 0.0396(12) -0.0028(9) -0.0041(9) -0.0042(8) C8 0.0275(10) 0.0193(10) 0.0378(11) -0.0063(8) -0.0087(9) -0.0012(8) C24 0.0318(11) 0.0222(10) 0.0443(13) -0.0080(9) -0.0112(10) 0.0032(8) C34 0.0278(11) 0.0258(11) 0.0429(13) -0.0020(9) -0.0032(9) -0.0010(8) C29 0.0368(12) 0.0327(12) 0.0378(12) 0.0038(9) -0.0083(10) -0.0055(9) C3 0.0288(11) 0.0347(12) 0.0421(13) -0.0143(10) -0.0056(9) -0.0031(9) C4 0.0303(11) 0.0257(11) 0.0416(12) -0.0082(9) -0.0073(9) -0.0042(8) C2 0.0283(11) 0.0304(11) 0.0496(14) -0.0176(10) -0.0107(10) 0.0030(9) C23 0.0349(12) 0.0223(10) 0.0467(13) -0.0065(9) -0.0094(10) -0.0008(9) C1 0.0299(11) 0.0233(10) 0.0496(14) -0.0103(9) -0.0119(10) 0.0020(8) C20 0.0310(11) 0.0285(11) 0.0460(13) -0.0062(9) -0.0092(10) -0.0001(9) C21 0.0346(12) 0.0303(12) 0.0519(14) -0.0052(10) -0.0119(11) 0.0082(9) C22 0.0413(13) 0.0195(10) 0.0478(13) -0.0020(9) -0.0120(10) 0.0026(9) O2 0.0756(17) 0.0711(17) 0.198(3) -0.089(2) -0.0245(19) 0.0021(13) C28 0.0274(12) 0.0492(15) 0.0492(15) 0.0158(12) -0.0085(10) -0.0066(10) C33 0.0284(12) 0.0461(14) 0.0587(16) 0.0015(12) -0.0007(11) 0.0022(10) C30 0.076(2) 0.077(2) 0.0471(17) -0.0176(15) -0.0204(15) -0.0017(17) C32 0.0560(19) 0.085(2) 0.0505(17) -0.0016(16) 0.0128(15) 0.0292(17) C31 0.097(3) 0.108(3) 0.0452(18) -0.0297(19) -0.0077(19) 0.031(2) N6 0.065(4) 0.084(5) 0.054(4) 0.001(3) -0.019(3) -0.025(3) C36 0.070(5) 0.059(4) 0.046(4) 0.000(3) -0.019(4) -0.023(3) C35 0.088(6) 0.053(4) 0.052(4) -0.009(3) -0.003(4) -0.015(4) C38 0.045(3) 0.058(4) 0.051(4) -0.014(3) -0.002(3) -0.010(3) N7 0.053(4) 0.117(6) 0.083(5) -0.037(4) 0.000(3) -0.016(4) C37 0.052(6) 0.090(9) 0.025(3) -0.013(4) -0.006(3) 0.008(6) N7A 0.079(5) 0.109(7) 0.131(7) -0.056(5) -0.051(5) 0.014(4) C38A 0.069(5) 0.106(8) 0.084(6) -0.044(5) -0.039(4) 0.017(5) C37A 0.165(19) 0.165(19) 0.19(2) -0.099(15) -0.080(14) 0.123(15) C25A 0.091(8) 0.019(5) 0.037(4) 0.005(4) 0.018(4) 0.006(4) C27A 0.080(4) 0.056(3) 0.045(3) 0.010(2) -0.007(3) -0.012(3) C26A 0.188(9) 0.055(4) 0.058(4) 0.020(3) -0.031(5) -0.064(5) C25B 0.042(4) 0.019(5) 0.062(8) -0.013(4) 0.001(4) -0.008(3) C26B 0.086(6) 0.042(4) 0.050(4) 0.009(3) 0.029(4) 0.010(4) C27B 0.090(6) 0.034(3) 0.059(4) 0.010(3) -0.026(4) -0.006(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C17A C18A C13A 118.3(19) C17A C18A H18A 120.9 C13A C18A H18A 120.9 C16A C17A C18A 117.4(18) C16A C17A H17A 121.3 C18A C17A H17A 121.3 C15A C16A C17A 125.0(16) C15A C16A Cl1A 118.2(12) C17A C16A Cl1A 116.8(13) C16A C15A C14A 118.5(11) C16A C15A H15A 120.8 C14A C15A H15A 120.8 C13A C14A C15A 120.6(11) C13A C14A H14A 119.7 C15A C14A H14A 119.7 C14A C13A C18A 120.0(15) C14A C13A N1 126.1(15) C18A C13A N1 113.7(17) C13B C18B C17B 119.0(10) C13B C18B H18B 120.5 C17B C18B H18B 120.5 C18B C17B C16B 120.0(10) C18B C17B H17B 120.0 C16B C17B H17B 120.0 C15B C16B C17B 120.4(10) C15B C16B Cl1B 119.7(8) C17B C16B Cl1B 120.0(8) C14B C15B C16B 119.6(7) C14B C15B H15B 120.2 C16B C15B H15B 120.2 C15B C14B C13B 117.8(7) C15B C14B H14B 121.1 C13B C14B H14B 121.1 C18B C13B C14B 123.3(9) C18B C13B N1 121.2(12) C14B C13B N1 115.5(11) O1 S1 O2 116.2(2) O1 S1 N5 110.38(15) O2 S1 N5 110.66(15) O1 S1 C34 110.34(12) O2 S1 C34 110.14(16) N5 S1 C34 97.59(11) C6 N2 C5 118.30(18) C8 N3 C19 123.59(19) C8 N3 H3 117.2(18) C19 N3 H3 114.9(18) C11 N1 C12 121.68(18) C11 N1 C13B 119.4(13) C12 N1 C13B 118.6(13) C11 N1 C13A 117.0(19) C12 N1 C13A 121.0(19) C9 N4 C25B 129.2(8) C9 N4 C25A 122.8(7) C9 N4 H4N 117(2) C25B N4 H4N 113(2) C25A N4 H4N 120(2) N1 C12 C1 122.4(2) N1 C12 C5 117.74(18) C1 C12 C5 119.9(2) N2 C5 C4 118.52(19) N2 C5 C12 122.5(2) C4 C5 C12 119.01(19) N2 C6 C7 119.01(19) N2 C6 C11 123.14(18) C7 C6 C11 117.80(19) C28 N5 S1 111.61(17) C8 C7 C6 122.18(19) C8 C7 H7 118.9 C6 C7 H7 118.9 C24 C19 C20 120.1(2) C24 C19 N3 120.59(19) C20 C19 N3 119.3(2) C11 C10 C9 120.8(2) C11 C10 H10 119.6 C9 C10 H10 119.6 N1 C11 C10 122.86(19) N1 C11 C6 116.57(19) C10 C11 C6 120.56(18) N4 C9 C10 122.2(2) N4 C9 C8 118.53(19) C10 C9 C8 119.2(2) C7 C8 N3 123.86(19) C7 C8 C9 119.16(18) N3 C8 C9 116.97(19) C23 C24 C19 120.2(2) C23 C24 H24 119.9 C19 C24 H24 119.9 C33 C34 C29 123.0(2) C33 C34 S1 130.2(2) C29 C34 S1 106.79(17) C30 C29 C34 120.2(3) C30 C29 C28 129.0(3) C34 C29 C28 110.8(2) C4 C3 C2 119.5(2) C4 C3 H3A 120.2 C2 C3 H3A 120.2 C3 C4 C5 120.7(2) C3 C4 H4A 119.7 C5 C4 H4A 119.7 C1 C2 C3 121.4(2) C1 C2 H2 119.3 C3 C2 H2 119.3 C24 C23 C22 119.3(2) C24 C23 H23 120.4 C22 C23 H23 120.4 C2 C1 C12 119.5(2) C2 C1 H1 120.3 C12 C1 H1 120.3 C21 C20 C19 119.7(2) C21 C20 H20 120.2 C19 C20 H20 120.2 C22 C21 C20 119.6(2) C22 C21 H21 120.2 C20 C21 H21 120.2 C21 C22 C23 121.2(2) C21 C22 Cl2 120.24(18) C23 C22 Cl2 118.55(18) O3 C28 N5 122.3(3) O3 C28 C29 124.4(3) N5 C28 C29 113.2(2) C34 C33 C32 116.0(3) C34 C33 H33 122.0 C32 C33 H33 122.0 C31 C30 C29 118.0(3) C31 C30 H30 121.0 C29 C30 H30 121.0 C31 C32 C33 121.6(3) C31 C32 H32 119.2 C33 C32 H32 119.2 C30 C31 C32 121.2(3) C30 C31 H31 119.4 C32 C31 H31 119.4 N6 C36 C35 178.2(8) C36 C35 H35A 109.5 C36 C35 H35B 109.5 H35A C35 H35B 109.5 C36 C35 H35C 109.5 H35A C35 H35C 109.5 H35B C35 H35C 109.5 N7 C38 C37 173.9(8) C38 C37 H37A 109.5 C38 C37 H37B 109.5 H37A C37 H37B 109.5 C38 C37 H37C 109.5 H37A C37 H37C 109.5 H37B C37 H37C 109.5 C37A C38A N7A 175.6(15) C38A C37A H37D 109.5 C38A C37A H37E 109.5 H37D C37A H37E 109.5 C38A C37A H37F 109.5 H37D C37A H37F 109.5 H37E C37A H37F 109.5 C26A C25A N4 112.6(12) C26A C25A C27A 117.5(11) N4 C25A C27A 102.1(9) C26A C25A H25A 108.1 N4 C25A H25A 108.1 C27A C25A H25A 108.1 C25A C27A H27A 109.5 C25A C27A H27B 109.5 H27A C27A H27B 109.5 C25A C27A H27C 109.5 H27A C27A H27C 109.5 H27B C27A H27C 109.5 C25A C26A H26A 109.5 C25A C26A H26B 109.5 H26A C26A H26B 109.5 C25A C26A H26C 109.5 H26A C26A H26C 109.5 H26B C26A H26C 109.5 C27B C25B N4 116.3(10) C27B C25B C26B 112.9(13) N4 C25B C26B 110.3(14) C27B C25B H25B 105.5 N4 C25B H25B 105.5 C26B C25B H25B 105.5 C25B C26B H26D 109.5 C25B C26B H26E 109.5 H26D C26B H26E 109.5 C25B C26B H26F 109.5 H26D C26B H26F 109.5 H26E C26B H26F 109.5 C25B C27B H27D 109.5 C25B C27B H27E 109.5 H27D C27B H27E 109.5 C25B C27B H27F 109.5 H27D C27B H27F 109.5 H27E C27B H27F 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance C18A C17A 1.42(3) C18A C13A 1.44(3) C18A H18A 0.9500 C17A C16A 1.36(2) C17A H17A 0.9500 C16A C15A 1.335(19) C16A Cl1A 1.786(19) C15A C14A 1.397(13) C15A H15A 0.9500 C14A C13A 1.35(2) C14A H14A 0.9500 C13A N1 1.470(12) C18B C13B 1.34(2) C18B C17B 1.366(19) C18B H18B 0.9500 C17B C16B 1.397(12) C17B H17B 0.9500 C16B C15B 1.387(11) C16B Cl1B 1.725(12) C15B C14B 1.381(8) C15B H15B 0.9500 C14B C13B 1.400(15) C14B H14B 0.9500 C13B N1 1.459(8) Cl2 C22 1.746(2) S1 O1 1.433(3) S1 O2 1.441(3) S1 N5 1.599(2) S1 C34 1.755(2) N2 C6 1.319(3) N2 C5 1.368(3) N3 C8 1.380(3) N3 C19 1.412(3) N3 H3 0.87(3) N1 C11 1.370(3) N1 C12 1.385(3) N4 C9 1.321(3) N4 C25B 1.48(2) N4 C25A 1.494(14) N4 H4N 0.85(3) O3 C28 1.230(3) C12 C1 1.406(3) C12 C5 1.414(3) C5 C4 1.408(3) C6 C7 1.420(3) C6 C11 1.458(3) N5 C28 1.339(4) C7 C8 1.357(3) C7 H7 0.9500 C19 C24 1.388(3) C19 C20 1.398(3) C10 C11 1.371(3) C10 C9 1.403(3) C10 H10 0.9500 C9 C8 1.469(3) C24 C23 1.385(3) C24 H24 0.9500 C34 C33 1.378(3) C34 C29 1.378(3) C29 C30 1.376(4) C29 C28 1.508(4) C3 C4 1.374(3) C3 C2 1.404(3) C3 H3A 0.9500 C4 H4A 0.9500 C2 C1 1.372(3) C2 H2 0.9500 C23 C22 1.389(3) C23 H23 0.9500 C1 H1 0.9500 C20 C21 1.390(3) C20 H20 0.9500 C21 C22 1.381(4) C21 H21 0.9500 C33 C32 1.385(5) C33 H33 0.9500 C30 C31 1.375(5) C30 H30 0.9500 C32 C31 1.384(6) C32 H32 0.9500 C31 H31 0.9500 N6 C36 1.160(10) C36 C35 1.486(11) C35 H35A 0.9800 C35 H35B 0.9800 C35 H35C 0.9800 C38 N7 1.169(9) C38 C37 1.495(13) C37 H37A 0.9800 C37 H37B 0.9800 C37 H37C 0.9800 N7A C38A 1.174(13) C38A C37A 1.14(3) C37A H37D 0.9800 C37A H37E 0.9800 C37A H37F 0.9800 C25A C26A 1.404(16) C25A C27A 1.525(15) C25A H25A 1.0000 C27A H27A 0.9800 C27A H27B 0.9800 C27A H27C 0.9800 C26A H26A 0.9800 C26A H26B 0.9800 C26A H26C 0.9800 C25B C27B 1.46(2) C25B C26B 1.55(2) C25B H25B 1.0000 C26B H26D 0.9800 C26B H26E 0.9800 C26B H26F 0.9800 C27B H27D 0.9800 C27B H27E 0.9800 C27B H27F 0.9800 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C33 H33 O3 0.95 2.45 3.283(3) 146.0 1_455 C24 H24 O1 0.95 2.42 3.314(3) 157.3 2_566 N3 H3 N5 0.87(3) 2.03(3) 2.893(3) 170(3) 2_666 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C13A C18A C17A C16A 0(4) C18A C17A C16A C15A -3(3) C18A C17A C16A Cl1A 178.2(18) C17A C16A C15A C14A 2(3) Cl1A C16A C15A C14A -179.5(10) C16A C15A C14A C13A 3(3) C15A C14A C13A C18A -6(5) C15A C14A C13A N1 -180(3) C17A C18A C13A C14A 5(5) C17A C18A C13A N1 179(2) C13B C18B C17B C16B 2(3) C18B C17B C16B C15B -1.2(19) C18B C17B C16B Cl1B 178.8(12) C17B C16B C15B C14B 0.1(14) Cl1B C16B C15B C14B -179.8(6) C16B C15B C14B C13B -0.3(18) C17B C18B C13B C14B -3(4) C17B C18B C13B N1 178.3(18) C15B C14B C13B C18B 2(3) C15B C14B C13B N1 -179.3(14) C18B C13B N1 C11 -74(3) C14B C13B N1 C11 107(2) C18B C13B N1 C12 99(3) C14B C13B N1 C12 -80(2) C14A C13A N1 C11 79(4) C18A C13A N1 C11 -95(3) C14A C13A N1 C12 -95(4) C18A C13A N1 C12 91(3) C11 N1 C12 C1 -176.96(19) C13B N1 C12 C1 9.9(7) C13A N1 C12 C1 -3.3(11) C11 N1 C12 C5 2.8(3) C13B N1 C12 C5 -170.3(7) C13A N1 C12 C5 176.5(10) C6 N2 C5 C4 178.28(19) C6 N2 C5 C12 -2.1(3) N1 C12 C5 N2 -0.4(3) C1 C12 C5 N2 179.42(19) N1 C12 C5 C4 179.24(19) C1 C12 C5 C4 -1.0(3) C5 N2 C6 C7 179.51(18) C5 N2 C6 C11 2.3(3) O1 S1 N5 C28 116.5(2) O2 S1 N5 C28 -113.5(2) C34 S1 N5 C28 1.4(2) N2 C6 C7 C8 -178.87(19) C11 C6 C7 C8 -1.5(3) C8 N3 C19 C24 48.1(3) C8 N3 C19 C20 -135.5(2) C12 N1 C11 C10 178.2(2) C13B N1 C11 C10 -8.8(7) C13A N1 C11 C10 4.2(10) C12 N1 C11 C6 -2.7(3) C13B N1 C11 C6 170.4(7) C13A N1 C11 C6 -176.6(10) C9 C10 C11 N1 -179.16(19) C9 C10 C11 C6 1.7(3) N2 C6 C11 N1 0.1(3) C7 C6 C11 N1 -177.22(18) N2 C6 C11 C10 179.3(2) C7 C6 C11 C10 2.0(3) C25B N4 C9 C10 -6.2(7) C25A N4 C9 C10 8.1(8) C25B N4 C9 C8 172.4(7) C25A N4 C9 C8 -173.3(7) C11 C10 C9 N4 172.9(2) C11 C10 C9 C8 -5.7(3) C6 C7 C8 N3 178.19(19) C6 C7 C8 C9 -2.5(3) C19 N3 C8 C7 12.9(3) C19 N3 C8 C9 -166.40(19) N4 C9 C8 C7 -172.5(2) C10 C9 C8 C7 6.2(3) N4 C9 C8 N3 6.8(3) C10 C9 C8 N3 -174.51(19) C20 C19 C24 C23 1.3(3) N3 C19 C24 C23 177.7(2) O1 S1 C34 C33 64.9(3) O2 S1 C34 C33 -64.6(3) N5 S1 C34 C33 -180.0(2) O1 S1 C34 C29 -115.3(2) O2 S1 C34 C29 115.1(2) N5 S1 C34 C29 -0.23(18) C33 C34 C29 C30 -0.5(4) S1 C34 C29 C30 179.7(2) C33 C34 C29 C28 178.9(2) S1 C34 C29 C28 -0.9(2) C2 C3 C4 C5 -1.2(3) N2 C5 C4 C3 -178.39(19) C12 C5 C4 C3 2.0(3) C4 C3 C2 C1 -0.6(3) C19 C24 C23 C22 -1.5(4) C3 C2 C1 C12 1.6(3) N1 C12 C1 C2 179.0(2) C5 C12 C1 C2 -0.8(3) C24 C19 C20 C21 -0.3(3) N3 C19 C20 C21 -176.7(2) C19 C20 C21 C22 -0.6(4) C20 C21 C22 C23 0.5(4) C20 C21 C22 Cl2 179.66(19) C24 C23 C22 C21 0.6(4) C24 C23 C22 Cl2 -178.62(18) S1 N5 C28 O3 176.9(2) S1 N5 C28 C29 -2.2(3) C30 C29 C28 O3 2.2(4) C34 C29 C28 O3 -177.1(2) C30 C29 C28 N5 -178.7(3) C34 C29 C28 N5 2.0(3) C29 C34 C33 C32 1.2(4) S1 C34 C33 C32 -179.1(2) C34 C29 C30 C31 -0.6(5) C28 C29 C30 C31 -179.9(3) C34 C33 C32 C31 -0.7(5) C29 C30 C31 C32 1.1(6) C33 C32 C31 C30 -0.4(6) C9 N4 C25A C26A 88.5(12) C9 N4 C25A C27A -144.6(7) C9 N4 C25B C27B -69.2(14) C9 N4 C25B C26B 160.6(6) _cod_database_fobs_code 2108443