#------------------------------------------------------------------------------ #$Date: 2019-07-20 06:59:05 +0300 (Sat, 20 Jul 2019) $ #$Revision: 217185 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/10/84/2108445.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108445 loop_ _publ_author_name 'Bodart, Laurie' 'Tumanov, Nikolay' 'Wouters, Johan' _publ_section_title ; Structural variety of clofaziminium salts: effect of the counter-ion on clofaziminium conformation and crystal packing ; _journal_coeditor_code AW5025 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first ; ; _journal_paper_doi 10.1107/S2052520619007649 _journal_volume 75 _journal_year 2019 _chemical_formula_moiety ; C27 H23 Cl2 N4 + , C7 H5 O4 - , C1 H4 O ; _chemical_formula_sum 'C35 H32 Cl2 N4 O5' _chemical_formula_weight 659.54 _chemical_name_common ; clofaziminium 2,4-dihydroxybenzoate methanol solvate ; _chemical_name_systematic ; N-[10-(4-chlorophenyl)-3-[(4-chlorophenyl)amino] -2,10-dihydrophenazin-2-ylidene]propan-2-aminium methanol 2,4-dihydroxybenzoate ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary dual _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 98.415(3) _cell_angle_beta 103.379(3) _cell_angle_gamma 110.450(4) _cell_formula_units_Z 2 _cell_length_a 9.4861(4) _cell_length_b 12.5322(5) _cell_length_c 15.3641(5) _cell_measurement_reflns_used 8225 _cell_measurement_temperature 295(2) _cell_measurement_theta_max 67.0100 _cell_measurement_theta_min 3.0300 _cell_volume 1612.41(13) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 295(2) _diffrn_detector_area_resol_mean 10.3712 _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur Ruby Gemini ultra' _diffrn_measurement_method \w _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0212 _diffrn_reflns_av_unetI/netI 0.0194 _diffrn_reflns_Laue_measured_fraction_full 0.989 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 15458 _diffrn_reflns_point_group_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_theta_full 67.001 _diffrn_reflns_theta_max 67.001 _diffrn_reflns_theta_min 3.053 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance Ultra (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 2.215 _exptl_absorpt_correction_T_max 0.991 _exptl_absorpt_correction_T_min 0.539 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'Metallic dark red' _exptl_crystal_density_diffrn 1.358 _exptl_crystal_description Plate _exptl_crystal_F_000 688 _exptl_crystal_size_max 0.485 _exptl_crystal_size_mid 0.122 _exptl_crystal_size_min 0.064 _refine_diff_density_max 0.243 _refine_diff_density_min -0.325 _refine_diff_density_rms 0.035 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 555 _refine_ls_number_reflns 5692 _refine_ls_number_restraints 66 _refine_ls_restrained_S_all 1.038 _refine_ls_R_factor_all 0.0422 _refine_ls_R_factor_gt 0.0374 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0640P)^2^+0.2274P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1054 _refine_ls_wR_factor_ref 0.1113 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4965 _reflns_number_total 5692 _reflns_threshold_expression I>2\s(I) _cod_data_source_file aw5025sup1.cif _cod_data_source_block lb0214_CLZ-24DHBA _cod_original_cell_volume 1612.41(12) _cod_database_code 2108445 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL lb0214_clz-24dhba_a.res in P-1 lb0214_CLZ-24DHBA.res created by SHELXL-2016/6 at 17:12:58 on 13-Jul-2018 REM Old TITL lb0214_clz-24dhba_a.res in P-1 REM SHELXT solution in P-1 REM R1 0.193, Rweak 0.013, Alpha 0.043, Orientation as input REM Formula found by SHELXT: C38 N4 O2 Cl2 CELL 1.54184 9.4861 12.5322 15.3641 98.415 103.379 110.45 ZERR 2 0.0004 0.0005 0.0005 0.003 0.003 0.004 LATT 1 SFAC C H N O Cl UNIT 70 64 8 10 4 L.S. 4 0 0 PLAN 20 CONF BOND $H list 4 fmap 2 53 ACTA TEMP 22 SADI O3A H3OA O3B H3OB EQIV $1 -x+1, -y+1, -z+1 HTAB C14 O1A_$1 HTAB C14 O1B_$1 EQIV $2 x+1, y+1, z HTAB C23 O4A_$2 HTAB C23 O4B_$2 HTAB O3A O2A EQIV $3 -x, -y+1, -z+1 HTAB O4A O5A_$3 HTAB O5A O3A_$1 HTAB O3B O2B EQIV $4 x, y-1, z+1 HTAB O4B O5B_$4 HTAB O5B O4B_$3 HTAB N4 O1A HTAB N4 O1B HTAB N3 O1A HTAB N3 O1B WGHT 0.064000 0.227400 FVAR 0.60796 0.63160 CL1 5 0.927785 0.646904 1.080275 11.00000 0.09939 0.10092 = 0.03764 0.00947 0.01197 0.03870 CL2 5 0.429746 0.252408 -0.011857 11.00000 0.08853 0.09094 = 0.04707 -0.00491 -0.00419 0.02299 N1 3 0.808807 0.527140 0.371698 11.00000 0.04421 0.04171 = 0.03595 0.01213 0.01298 0.01598 N2 3 1.000550 0.655038 0.550801 11.00000 0.04382 0.04573 = 0.03974 0.01021 0.01359 0.01255 N4 3 0.435679 0.292950 0.505112 11.00000 0.04663 0.04231 = 0.04337 0.01135 0.01530 0.01021 N3 3 0.629385 0.422849 0.680512 11.00000 0.05456 0.04558 = 0.04049 0.01179 0.01936 0.00948 C6 1 0.862922 0.568475 0.536656 11.00000 0.04243 0.04006 = 0.03738 0.01052 0.01313 0.01576 C11 1 0.756435 0.500494 0.444873 11.00000 0.04344 0.03963 = 0.03575 0.01197 0.01304 0.01788 C9 1 0.569455 0.382653 0.512903 11.00000 0.04306 0.03717 = 0.04183 0.01016 0.01389 0.01533 C8 1 0.676053 0.451953 0.606541 11.00000 0.04755 0.04015 = 0.03788 0.01226 0.01677 0.01785 C13 1 0.713742 0.458410 0.278129 11.00000 0.04374 0.04664 = 0.03529 0.01116 0.01343 0.01566 C7 1 0.816218 0.539622 0.613926 11.00000 0.04557 0.04416 = 0.03503 0.00902 0.01186 0.01378 AFIX 43 H7 2 0.884238 0.582415 0.672638 11.00000 -1.20000 AFIX 0 C12 1 0.953318 0.618121 0.384692 11.00000 0.04274 0.04290 = 0.04225 0.01629 0.01543 0.01973 C14 1 0.640316 0.509573 0.219170 11.00000 0.04716 0.04979 = 0.04508 0.01496 0.01324 0.01998 AFIX 43 H14 2 0.648524 0.585737 0.239635 11.00000 -1.20000 AFIX 0 C19 1 0.710672 0.480419 0.774683 11.00000 0.05123 0.04939 = 0.03907 0.01393 0.02085 0.01708 C5 1 1.045065 0.682740 0.476174 11.00000 0.04388 0.04432 = 0.04278 0.01411 0.01580 0.01765 C10 1 0.612418 0.412372 0.435456 11.00000 0.04381 0.04132 = 0.03657 0.00897 0.01008 0.01307 AFIX 43 H10 2 0.542748 0.372060 0.376658 11.00000 -1.20000 AFIX 0 C1 1 1.011261 0.645469 0.310995 11.00000 0.05150 0.05872 = 0.04254 0.02122 0.01832 0.02490 AFIX 43 H1 2 0.953983 0.600969 0.250864 11.00000 -1.20000 AFIX 0 C24 1 0.780598 0.602144 0.807890 11.00000 0.06190 0.04873 = 0.04135 0.01570 0.02095 0.01620 AFIX 43 H24 2 0.781350 0.649648 0.766675 11.00000 -1.20000 AFIX 0 C18 1 0.703251 0.345643 0.249682 11.00000 0.06515 0.05063 = 0.04324 0.01316 0.01310 0.02661 AFIX 43 H18 2 0.754710 0.313048 0.290148 11.00000 -1.20000 AFIX 0 C20 1 0.708061 0.410921 0.837527 11.00000 0.06693 0.05050 = 0.04890 0.01832 0.02588 0.02412 AFIX 43 H20 2 0.660565 0.329458 0.816225 11.00000 -1.20000 AFIX 0 C15 1 0.554271 0.445752 0.129104 11.00000 0.05139 0.06495 = 0.04350 0.01807 0.00937 0.02331 AFIX 43 H15 2 0.505144 0.479035 0.088101 11.00000 -1.20000 AFIX 0 C4 1 1.189608 0.778511 0.490949 11.00000 0.04677 0.05035 = 0.05205 0.01253 0.01488 0.01123 AFIX 43 H4 2 1.249615 0.823192 0.550681 11.00000 -1.20000 AFIX 0 C2 1 1.152743 0.738152 0.328289 11.00000 0.05406 0.06159 = 0.05627 0.03016 0.02793 0.02531 AFIX 43 H2 2 1.190395 0.756419 0.279274 11.00000 -1.20000 AFIX 0 C16 1 0.542176 0.333192 0.100965 11.00000 0.05303 0.06369 = 0.03948 0.00540 0.00825 0.01694 C3 1 1.241686 0.805838 0.418095 11.00000 0.04771 0.05358 = 0.06511 0.02389 0.02266 0.01394 AFIX 43 H3 2 1.336321 0.869475 0.428220 11.00000 -1.20000 AFIX 0 C25 1 0.321317 0.209305 0.418402 11.00000 0.04580 0.04590 = 0.05160 0.00831 0.00909 0.01232 AFIX 13 H25 2 0.292871 0.253720 0.374869 11.00000 -1.20000 AFIX 0 C21 1 0.775303 0.461619 0.931319 11.00000 0.07698 0.06914 = 0.04598 0.02701 0.02638 0.03622 AFIX 43 H21 2 0.773179 0.414730 0.973056 11.00000 -1.20000 AFIX 0 C22 1 0.845186 0.581815 0.962171 11.00000 0.06101 0.06969 = 0.03785 0.01230 0.01594 0.02688 C17 1 0.615084 0.281621 0.160079 11.00000 0.07260 0.05135 = 0.04925 0.00534 0.01375 0.02394 AFIX 43 H17 2 0.604941 0.204881 0.139826 11.00000 -1.20000 AFIX 0 C23 1 0.848891 0.653036 0.901509 11.00000 0.06197 0.05290 = 0.04539 0.00923 0.02002 0.01400 AFIX 43 H23 2 0.896850 0.734418 0.923422 11.00000 -1.20000 AFIX 0 C27 1 0.174273 0.137286 0.440884 11.00000 0.04886 0.06124 = 0.07446 0.00755 0.01603 0.00751 AFIX 137 H27A 2 0.198898 0.088269 0.479234 11.00000 -1.50000 H27B 2 0.092802 0.088933 0.384642 11.00000 -1.50000 H27C 2 0.138323 0.189207 0.472965 11.00000 -1.50000 AFIX 0 C26 1 0.389896 0.130410 0.374796 11.00000 0.05973 0.05527 = 0.07775 -0.00618 0.01725 0.01292 AFIX 137 H26A 2 0.480622 0.177625 0.359681 11.00000 -1.50000 H26B 2 0.311824 0.075790 0.319589 11.00000 -1.50000 H26C 2 0.420588 0.087949 0.417556 11.00000 -1.50000 AFIX 0 SADI C35A O5A C35B O5B SAME C28A > C35A SAME C28B > C35B REM FLAT C28A C29A C30A C31A C32A C33A C34A O4A O3A REM FLAT C28B C29B C30B C31B C32B C33B C34B O4B O3B SIMU C35A O5A C35B O5B DELU C35A O5A DELU C35B O5B PART 1 C28A 1 0.357837 0.147761 0.687459 21.00000 0.05557 0.06755 = 0.07067 -0.00815 0.01434 0.01778 O1A 4 0.353881 0.239941 0.665684 21.00000 0.07775 0.05233 = 0.06517 0.01370 0.03776 0.00917 O2A 4 0.453256 0.103370 0.668292 21.00000 0.07979 0.09182 = 0.10521 0.02974 0.05872 0.03932 C34A 1 0.136271 0.125701 0.753192 21.00000 0.04952 0.04308 = 0.05607 0.01226 0.02297 0.02020 AFIX 43 H34A 2 0.135193 0.193619 0.736008 21.00000 -1.20000 AFIX 0 C29A 1 0.246095 0.083852 0.734191 21.00000 0.05364 0.03245 = 0.04271 0.00996 0.01723 0.01339 C30A 1 0.236825 -0.023415 0.754443 21.00000 0.05867 0.05206 = 0.04790 0.00720 0.01127 0.02824 O3A 4 0.340284 -0.070272 0.736343 21.00000 0.07789 0.06790 = 0.08415 0.02265 0.02857 0.04664 AFIX 148 H3OA 2 0.409913 -0.019179 0.704048 21.00000 -1.50000 AFIX 0 C33A 1 0.028221 0.071456 0.796437 21.00000 0.06235 0.03825 = 0.06243 0.01808 0.03370 0.01729 AFIX 43 H33A 2 -0.037936 0.105349 0.812741 21.00000 -1.20000 AFIX 0 C31A 1 0.124005 -0.082271 0.793306 21.00000 0.07750 0.04673 = 0.06885 0.03142 0.02417 0.02536 AFIX 43 H31A 2 0.117285 -0.154325 0.805059 21.00000 -1.20000 AFIX 0 C32A 1 0.021677 -0.034759 0.814663 21.00000 0.07187 0.05286 = 0.06550 0.02203 0.03618 0.02269 O4A 4 -0.094546 -0.101017 0.847318 21.00000 0.10106 0.07600 = 0.12153 0.05409 0.07068 0.02984 AFIX 147 H4OA 2 -0.136155 -0.059926 0.867831 21.00000 0.09832 AFIX 0 C35A 1 0.301983 0.923995 0.061383 21.00000 0.14744 0.18095 = 0.15427 -0.03989 0.02747 0.01937 AFIX 137 H35A 2 0.225923 0.847255 0.056713 21.00000 -1.20000 H35B 2 0.403930 0.921390 0.068755 21.00000 -1.20000 H35C 2 0.271236 0.948527 0.006253 21.00000 -1.20000 AFIX 0 O5A 4 0.308734 1.000153 0.134230 21.00000 0.08136 0.14633 = 0.10196 0.00128 0.03257 0.03976 AFIX 147 H5OA 2 0.398751 1.029525 0.170189 21.00000 -1.50000 AFIX 0 PART 0 PART 2 C28B 1 0.370672 0.141692 0.688830 -21.00000 0.05238 0.03373 = 0.05339 0.01723 0.03540 -0.00126 O1B 4 0.364453 0.232397 0.666440 -21.00000 0.07912 0.04296 = 0.09747 0.03392 0.04364 0.01348 O2B 4 0.474125 0.101034 0.684478 -21.00000 0.06097 0.07243 = 0.15893 0.03068 0.05283 0.01906 C34B 1 0.153778 0.126026 0.757702 -21.00000 0.07622 0.03178 = 0.07077 0.02438 0.01901 0.00161 AFIX 43 H34B 2 0.158153 0.197994 0.746758 -21.00000 -1.20000 AFIX 0 C29B 1 0.256353 0.080079 0.734809 -21.00000 0.03936 0.06208 = 0.05454 0.00460 0.01384 0.00947 C30B 1 0.266106 -0.017177 0.764923 -21.00000 0.05682 0.05756 = 0.05643 0.02442 0.00798 0.01719 O3B 4 0.375692 -0.055772 0.749374 -21.00000 0.07590 0.10161 = 0.10947 0.02828 0.01547 0.04829 AFIX 148 H3OB 2 0.444748 -0.000636 0.719079 -21.00000 -1.50000 AFIX 0 C33B 1 0.044900 0.064823 0.796829 -21.00000 0.07658 0.08186 = 0.10188 0.01027 0.04799 0.03723 AFIX 43 H33B 2 -0.034319 0.089174 0.804819 -21.00000 -1.20000 AFIX 0 C31B 1 0.165261 -0.073209 0.809917 -21.00000 0.10516 0.07924 = 0.06838 0.03817 0.03462 0.05285 AFIX 43 H31B 2 0.172229 -0.137879 0.830571 -21.00000 -1.20000 AFIX 0 C32B 1 0.054270 -0.032898 0.824080 -21.00000 0.12209 0.06664 = 0.09513 0.05191 0.06766 0.02617 O4B 4 -0.038583 -0.084225 0.875464 -21.00000 0.14874 0.10197 = 0.12889 0.06541 0.09844 0.03388 AFIX 147 H4OB 2 0.010197 -0.056396 0.930586 -21.00000 0.30360 AFIX 0 C35B 1 0.291167 0.922889 0.058987 -21.00000 0.09187 0.15337 = 0.13008 0.02854 0.06135 0.04074 AFIX 137 H35D 2 0.248996 0.851786 0.010883 -21.00000 -1.20000 H35E 2 0.312159 0.904921 0.118059 -21.00000 -1.20000 H35F 2 0.387500 0.976280 0.052943 -21.00000 -1.20000 AFIX 0 O5B 4 0.188928 0.971426 0.052287 -21.00000 0.17241 0.20569 = 0.14654 0.07476 0.09267 0.11063 AFIX 147 H5OB 2 0.218144 1.025765 0.098031 -21.00000 -1.50000 AFIX 0 PART 0 H4N 2 0.417242 0.278095 0.554775 11.00000 0.05094 H3N 2 0.549108 0.355248 0.672464 11.00000 0.07375 HKLF 4 REM lb0214_clz-24dhba_a.res in P-1 REM R1 = 0.0374 for 4965 Fo > 4sig(Fo) and 0.0422 for all 5692 data REM 555 parameters refined using 66 restraints END WGHT 0.0644 0.2207 REM Highest difference peak 0.243, deepest hole -0.325, 1-sigma level 0.035 Q1 1 0.9048 0.5604 1.0727 11.00000 0.05 0.24 Q2 1 0.2790 0.9163 0.1637 11.00000 0.05 0.15 Q3 1 0.8028 0.5215 0.4830 11.00000 0.05 0.15 Q4 1 0.3741 0.2094 0.0240 11.00000 0.05 0.14 Q5 1 0.7180 0.4230 0.2608 11.00000 0.05 0.13 Q6 1 0.6489 0.4584 0.2609 11.00000 0.05 0.13 Q7 1 0.6154 0.4327 0.5620 11.00000 0.05 0.12 Q8 1 0.7141 0.5228 0.6034 11.00000 0.05 0.12 Q9 1 0.9883 0.6749 0.4340 11.00000 0.05 0.12 Q10 1 0.9289 0.7588 1.1007 11.00000 0.05 0.12 Q11 1 1.0245 0.6455 0.4351 11.00000 0.05 0.12 Q12 1 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7 64.66 2.44 1 -10 7 59.98 2.47 1 -10 7 62.70 2.64 1 -10 7 62.23 2.47 1 -10 8 4.69 0.75 1 -10 8 4.71 0.70 1 -10 8 4.59 0.65 1 -10 8 3.48 0.65 1 -10 8 4.11 0.76 1 -10 9 0.13 0.32 1 -10 9 0.17 0.43 1 -10 9 0.32 0.27 1 -10 10 8.79 0.92 1 -10 10 10.53 1.14 1 -10 10 10.11 1.06 1 -10 11 5.50 0.77 1 -10 11 5.26 0.82 1 -10 12 8.62 0.97 1 -10 12 9.09 0.91 1 -10 13 24.19 1.49 1 -10 14 6.01 0.70 1 -10 15 2.69 0.44 -1 9 11 2.61 0.43 -1 9 10 8.82 0.86 1 -9 -10 7.55 0.73 1 -9 -9 0.37 0.25 -1 9 9 -0.15 0.35 -1 9 8 3.09 0.64 1 -9 -8 3.54 0.62 1 -9 -7 8.51 1.00 1 -9 -7 8.14 0.89 1 -9 -6 9.52 1.08 1 -9 -6 9.69 1.03 1 -9 -5 13.74 1.30 1 -9 -5 11.51 1.14 1 -9 -4 2.88 0.62 1 -9 -4 3.78 0.73 1 -9 -4 3.02 0.51 1 -9 -3 20.90 1.54 1 -9 -3 17.87 1.26 1 -9 -3 17.58 1.26 1 -9 -3 17.28 1.41 1 -9 -3 18.99 1.35 -1 9 3 19.18 2.87 1 -9 -2 51.45 2.24 1 -9 -2 48.96 2.13 1 -9 -2 51.57 2.32 1 -9 -2 49.72 2.18 1 -9 -2 55.60 2.39 1 -9 -1 0.97 0.47 1 -9 -1 0.92 0.38 1 -9 -1 0.84 0.36 1 -9 -1 1.05 0.41 1 -9 -1 1.44 0.44 1 -9 0 94.30 2.97 1 -9 0 90.82 2.90 1 -9 0 95.04 3.04 1 -9 0 88.78 2.81 1 -9 0 91.37 2.81 1 -9 0 90.63 2.86 1 -9 0 86.94 5.85 1 -9 1 62.64 2.32 1 -9 1 60.99 2.35 1 -9 1 61.87 2.47 1 -9 1 55.70 2.21 1 -9 1 60.85 2.38 1 -9 1 56.80 4.82 1 -9 1 58.38 2.26 1 -9 2 172.95 3.77 1 -9 2 177.99 3.93 1 -9 2 177.23 4.01 1 -9 2 180.91 4.19 1 -9 2 175.84 3.89 1 -9 2 174.48 3.80 1 -9 3 210.59 4.47 1 -9 3 205.49 4.06 1 -9 3 208.65 4.25 1 -9 3 196.87 4.19 1 -9 3 205.31 4.24 1 -9 3 207.78 3.99 1 -9 3 199.82 4.26 1 -9 4 2.71 0.50 1 -9 4 2.40 0.50 1 -9 4 2.21 0.47 1 -9 4 2.62 0.53 1 -9 4 2.02 0.48 1 -9 4 2.69 0.57 1 -9 5 1.51 0.41 1 -9 5 2.53 0.53 1 -9 5 3.02 0.53 1 -9 5 2.20 0.56 1 -9 5 2.76 0.57 1 -9 5 2.11 0.47 1 -9 6 9.71 0.97 1 -9 6 11.12 1.07 1 -9 6 9.87 1.03 1 -9 6 10.37 0.98 1 -9 6 9.60 0.93 1 -9 7 2.62 0.61 1 -9 7 3.78 0.68 1 -9 7 2.89 0.55 1 -9 7 2.82 1.29 1 -9 7 2.27 0.48 1 -9 7 3.02 0.55 1 -9 8 0.66 0.29 1 -9 8 0.53 0.41 1 -9 8 0.92 0.40 1 -9 8 0.50 0.22 1 -9 8 0.92 0.44 1 -9 8 0.34 0.64 1 -9 9 8.03 0.90 1 -9 9 8.53 1.01 1 -9 9 4.85 1.38 1 -9 9 8.54 0.99 1 -9 9 8.21 0.83 1 -9 9 7.91 0.96 1 -9 10 23.67 1.68 1 -9 10 22.63 1.45 1 -9 10 23.28 1.58 1 -9 10 24.39 1.66 1 -9 11 6.57 0.94 1 -9 11 7.43 0.95 1 -9 11 5.91 0.84 1 -9 12 76.58 2.71 1 -9 12 75.31 2.87 1 -9 12 72.49 2.77 1 -9 13 46.77 2.13 1 -9 13 49.67 2.07 1 -9 13 51.70 2.29 1 -9 14 0.10 0.26 1 -9 14 0.43 0.31 1 -9 14 0.53 0.29 1 -9 15 8.13 0.77 -1 8 12 0.82 0.31 -1 8 12 0.21 0.20 -1 8 11 14.93 1.15 1 -8 -10 -0.18 0.24 -1 8 10 -0.23 0.37 1 -8 -9 0.44 0.30 -1 8 9 0.44 0.40 -1 8 8 -0.12 0.37 1 -8 -8 0.23 0.34 1 -8 -7 14.19 1.15 1 -8 -7 14.68 1.32 1 -8 -6 92.16 3.04 1 -8 -6 93.23 2.80 1 -8 -6 91.00 3.21 -1 8 6 88.82 6.40 1 -8 -5 151.74 3.58 1 -8 -5 150.33 4.05 1 -8 -4 28.60 1.54 1 -8 -4 30.08 1.78 1 -8 -4 28.71 1.47 -1 8 4 26.45 3.22 1 -8 -3 117.86 3.11 1 -8 -3 120.39 3.21 1 -8 -3 121.48 3.32 1 -8 -3 120.04 3.28 1 -8 -3 120.50 3.08 1 -8 -3 125.06 3.49 1 -8 -3 126.21 3.42 1 -8 -2 10.47 1.80 1 -8 -2 10.61 0.93 1 -8 -2 11.33 1.03 1 -8 -2 9.45 0.93 1 -8 -2 10.64 0.97 1 -8 -2 9.98 0.97 1 -8 -2 10.65 0.95 1 -8 -1 20.00 1.28 1 -8 -1 20.07 1.28 1 -8 -1 20.59 1.26 1 -8 -1 20.75 1.29 1 -8 -1 19.70 1.29 1 -8 -1 20.76 1.37 1 -8 -1 19.57 1.28 1 -8 -1 20.24 2.55 1 -8 0 41.55 1.87 1 -8 0 42.06 1.80 1 -8 0 41.92 1.87 1 -8 0 41.99 1.80 1 -8 0 40.07 1.83 1 -8 0 40.59 1.79 1 -8 0 43.95 1.81 1 -8 1 12.49 0.99 1 -8 1 11.05 0.93 1 -8 1 11.62 0.99 1 -8 1 12.63 1.06 1 -8 1 11.79 0.98 1 -8 1 12.32 0.97 1 -8 1 12.14 0.97 1 -8 2 16.69 1.09 1 -8 2 17.74 1.22 1 -8 2 17.54 1.13 1 -8 2 15.88 1.09 1 -8 2 16.81 1.15 1 -8 2 16.70 1.13 1 -8 3 36.54 1.66 1 -8 3 37.84 1.71 1 -8 3 36.80 1.60 1 -8 3 38.04 1.69 1 -8 3 37.48 1.69 1 -8 3 38.86 1.77 1 -8 4 84.35 2.47 1 -8 4 82.81 2.56 1 -8 4 83.26 2.36 1 -8 4 82.87 2.51 1 -8 4 79.75 2.54 1 -8 4 83.26 2.54 1 -8 4 83.93 2.49 1 -8 5 0.24 0.23 1 -8 5 0.19 0.18 1 -8 5 0.36 0.31 1 -8 5 0.29 0.30 1 -8 6 74.19 2.59 1 -8 6 72.72 2.37 1 -8 6 69.26 2.36 1 -8 6 69.55 2.46 1 -8 6 71.41 2.35 1 -8 6 71.96 2.48 1 -8 7 6.67 0.84 1 -8 7 6.51 0.77 1 -8 7 7.35 0.86 1 -8 7 7.58 0.79 1 -8 7 7.54 0.77 1 -8 7 7.02 0.81 1 -8 8 8.84 0.97 1 -8 8 9.63 0.91 1 -8 8 8.13 1.77 1 -8 8 8.45 0.82 1 -8 8 8.17 0.94 1 -8 8 9.38 1.01 1 -8 9 100.37 3.15 1 -8 9 102.94 2.98 1 -8 9 103.29 3.32 1 -8 9 100.64 3.23 1 -8 9 95.65 6.18 1 -8 10 0.16 0.24 1 -8 10 0.50 0.38 1 -8 10 0.41 0.35 1 -8 10 0.50 0.44 -1 8 -11 8.18 0.91 1 -8 11 6.56 0.87 1 -8 11 7.39 0.96 1 -8 11 7.40 0.97 1 -8 12 33.06 1.79 1 -8 12 30.54 1.87 1 -8 12 31.64 1.88 -1 8 -12 31.67 1.78 1 -8 13 7.56 0.96 1 -8 13 8.27 0.97 1 -8 13 6.80 0.80 -1 8 -13 8.11 0.90 1 -8 14 5.15 0.75 -1 8 -14 5.60 0.73 1 -8 14 5.24 0.73 1 -8 14 5.36 0.67 1 -8 15 3.86 0.62 1 -8 15 4.28 0.64 1 -8 15 3.07 0.46 -1 8 -15 3.66 0.57 1 -8 16 9.79 0.78 1 -8 16 10.19 0.82 -1 7 13 0.05 0.18 -1 7 13 0.25 0.23 -1 7 12 -0.05 0.27 -1 7 12 0.53 0.34 -1 7 11 0.29 0.32 -1 7 10 18.23 1.49 1 -7 -10 20.06 1.36 1 -7 -9 18.73 1.36 -1 7 9 19.95 1.55 1 -7 -8 0.52 0.34 -1 7 7 23.68 3.29 1 -7 -7 27.63 1.55 1 -7 -7 27.58 1.53 1 -7 -7 26.21 1.66 1 -7 -6 1.06 0.35 -1 7 6 0.32 0.57 1 -7 -6 0.42 0.30 -1 7 5 8.23 1.78 1 -7 -5 8.42 0.92 1 -7 -5 8.81 0.84 -1 7 4 83.47 5.29 1 -7 -4 88.34 2.59 1 -7 -4 85.86 2.64 1 -7 -4 92.33 2.90 1 -7 -4 86.08 2.63 1 -7 -3 7.43 0.72 1 -7 -3 8.24 0.78 1 -7 -3 9.83 0.91 1 -7 -3 7.78 1.41 1 -7 -3 8.95 0.87 1 -7 -3 9.11 0.89 1 -7 -3 9.08 0.85 1 -7 -2 28.05 2.66 1 -7 -2 30.18 1.44 1 -7 -2 30.10 1.45 1 -7 -2 29.24 1.50 1 -7 -2 30.53 1.46 1 -7 -2 29.86 1.46 1 -7 -2 32.34 1.61 1 -7 -1 32.98 1.50 1 -7 -1 36.94 1.58 1 -7 -1 36.53 1.59 1 -7 -1 37.03 1.57 1 -7 -1 35.66 1.60 1 -7 -1 36.80 1.54 1 -7 -1 39.18 1.74 1 -7 0 1086.41 8.38 1 -7 0 1083.53 8.21 1 -7 0 1081.69 17.47 1 -7 0 1088.21 8.23 1 -7 0 1087.00 8.79 1 -7 0 1074.97 8.25 1 -7 0 1070.56 8.68 1 -7 1 574.53 5.98 1 -7 1 577.09 13.06 1 -7 1 586.21 6.13 1 -7 1 576.96 6.12 1 -7 2 1.06 0.33 1 -7 2 0.87 0.27 1 -7 2 0.98 0.76 1 -7 2 1.14 0.29 1 -7 2 0.91 0.29 1 -7 2 0.79 0.28 1 -7 3 8.05 0.71 1 -7 3 8.05 0.74 1 -7 3 7.91 0.74 1 -7 3 7.93 1.50 1 -7 3 8.11 0.72 1 -7 3 7.72 0.71 1 -7 4 204.30 3.75 1 -7 4 203.21 3.67 1 -7 4 208.66 3.63 1 -7 4 208.77 3.64 1 -7 4 206.51 3.71 1 -7 5 1.37 0.40 1 -7 5 1.15 0.29 1 -7 5 0.86 0.28 1 -7 5 0.95 0.27 1 -7 5 1.08 0.34 1 -7 5 1.15 0.35 1 -7 6 41.80 1.77 1 -7 6 44.05 1.84 1 -7 6 44.92 1.77 1 -7 6 45.45 1.73 1 -7 6 44.19 1.86 1 -7 6 42.41 1.67 1 -7 7 156.79 3.69 1 -7 7 153.65 3.18 1 -7 7 159.11 3.61 1 -7 7 161.04 3.30 1 -7 7 157.45 3.39 1 -7 7 160.09 3.54 1 -7 8 93.30 5.65 -1 7 -8 89.39 2.64 1 -7 8 90.96 2.94 1 -7 8 92.86 2.81 1 -7 8 92.11 2.65 1 -7 8 93.22 2.89 1 -7 8 91.48 2.53 1 -7 9 27.50 3.08 1 -7 9 26.01 1.45 1 -7 9 25.87 1.53 1 -7 9 26.46 1.67 1 -7 9 25.77 1.60 -1 7 -9 25.50 1.49 -1 7 -10 8.13 0.90 1 -7 10 6.87 0.89 1 -7 10 7.37 0.92 1 -7 10 6.82 0.83 -1 7 -11 5.67 0.78 1 -7 11 6.17 0.90 1 -7 11 6.31 0.90 1 -7 11 6.21 0.82 -1 7 -12 31.31 1.84 1 -7 12 31.19 1.90 1 -7 12 32.09 1.90 1 -7 12 30.26 1.74 1 -7 13 24.74 1.51 1 -7 13 24.11 1.61 1 -7 13 23.43 1.61 -1 7 -13 24.38 1.62 -1 7 -14 5.75 0.82 1 -7 14 6.16 0.86 1 -7 14 6.31 0.82 1 -7 14 5.14 0.67 1 -7 15 18.48 1.29 1 -7 15 18.01 1.25 1 -7 15 17.23 1.07 -1 7 -15 18.67 1.32 1 -7 16 74.16 2.29 1 -7 16 74.70 2.20 -1 7 -16 78.81 2.39 -1 6 14 19.40 1.13 -1 6 13 16.27 1.11 -1 6 13 15.96 1.18 -1 6 12 63.36 2.54 -1 6 11 45.73 2.29 -1 6 10 37.40 2.14 1 -6 -10 36.94 1.83 1 -6 -9 0.15 0.27 1 -6 -9 0.36 0.31 -1 6 9 0.99 0.47 -1 6 8 36.72 4.15 1 -6 -8 34.04 1.78 1 -6 -8 37.03 1.77 1 -6 -7 0.25 0.26 1 -6 -7 0.17 0.25 1 -6 -7 0.17 0.21 -1 6 7 -0.22 0.85 -1 6 6 4.01 1.27 1 -6 -6 4.43 0.59 1 -6 -6 4.38 0.66 1 -6 -5 1.37 0.36 -1 6 5 0.96 0.52 1 -6 -5 1.91 0.44 1 -6 -5 0.90 0.28 1 -6 -4 1.82 0.41 1 -6 -4 1.23 0.30 1 -6 -4 1.35 0.41 1 -6 -4 1.02 0.26 1 -6 -4 2.00 0.48 1 -6 -3 190.95 6.05 1 -6 -3 193.53 3.52 1 -6 -3 194.16 3.64 1 -6 -3 197.62 3.73 1 -6 -2 12.34 1.61 1 -6 -1 122.40 5.24 1 -6 0 122.14 5.38 1 -6 1 164.73 6.36 1 -6 2 420.52 9.88 1 -6 3 284.67 7.89 1 -6 4 117.71 5.04 1 -6 5 271.17 7.01 1 -6 6 3.44 0.53 1 -6 6 3.53 0.53 1 -6 6 2.80 0.45 1 -6 6 3.53 0.92 1 -6 7 457.43 5.24 1 -6 7 449.67 5.76 1 -6 7 445.20 5.31 1 -6 7 466.93 10.37 1 -6 7 455.26 5.72 1 -6 8 317.55 4.66 1 -6 8 330.21 5.06 1 -6 8 346.82 9.84 1 -6 8 325.32 4.54 -1 6 -8 324.40 4.96 1 -6 8 350.83 9.59 1 -6 9 162.32 3.66 -1 6 -9 161.06 3.71 -1 6 -10 -0.41 0.26 1 -6 10 0.03 0.27 -1 6 -11 26.81 1.53 1 -6 11 27.22 1.60 -1 6 -11 26.11 1.65 -1 6 -12 52.04 2.21 -1 6 -12 49.83 2.35 1 -6 12 45.71 2.08 -1 6 -13 29.62 1.82 1 -6 13 31.75 1.82 1 -6 13 30.03 1.65 -1 6 -13 32.52 1.76 -1 6 -14 13.23 1.21 1 -6 14 14.21 1.25 1 -6 14 13.29 1.16 1 -6 14 14.34 1.10 -1 6 -14 15.70 1.20 -1 6 -15 1.44 0.44 -1 6 -15 1.82 0.43 1 -6 15 1.03 0.40 1 -6 15 1.26 0.39 1 -6 15 1.65 0.35 1 -6 16 12.57 0.94 -1 6 -16 14.96 1.12 1 -6 16 13.88 1.05 -1 6 -17 1.35 0.34 1 -6 17 0.43 0.24 -1 5 15 8.17 0.73 -1 5 14 64.12 2.29 -1 5 14 62.54 2.10 -1 5 13 38.75 1.96 -1 5 13 37.50 1.82 -1 5 12 0.12 0.49 -1 5 11 0.46 0.46 -1 5 10 9.03 1.09 1 -5 -10 10.21 0.93 -1 5 10 10.26 2.33 1 -5 -9 1.78 0.43 -1 5 9 1.94 1.05 1 -5 -9 1.74 0.47 -1 5 9 1.34 0.49 1 -5 -8 244.18 4.41 -1 5 8 234.26 9.95 1 -5 -8 241.72 4.45 1 -5 -7 23.36 1.32 1 -5 -7 23.96 1.38 -1 5 7 19.79 2.73 1 -5 -6 26.11 1.40 1 -5 -6 24.30 1.28 -1 5 6 25.53 2.91 -1 5 5 115.69 5.65 1 -5 -5 126.63 3.02 1 -5 -4 318.31 6.68 1 -5 -3 1.34 0.49 1 -5 -2 40.67 2.64 1 -5 -1 18.31 1.84 1 -5 0 267.42 7.24 1 -5 1 171.98 5.99 1 -5 2 205.82 6.23 1 -5 3 574.81 9.99 1 -5 4 885.32 12.13 1 -5 4 910.86 11.01 1 -5 5 75.67 3.47 1 -5 6 776.83 11.94 1 -5 7 125.70 5.22 1 -5 7 125.16 2.83 1 -5 8 13.02 1.72 1 -5 8 12.72 1.84 1 -5 8 11.82 0.95 -1 5 -9 23.91 1.32 1 -5 9 22.64 1.34 1 -5 9 24.71 2.72 1 -5 10 0.35 0.26 -1 5 -10 0.21 0.21 1 -5 11 22.20 1.42 -1 5 -11 22.04 1.43 -1 5 -12 96.08 3.09 -1 5 -12 95.46 3.25 1 -5 12 94.43 2.91 -1 5 -13 34.39 1.88 1 -5 13 31.84 1.69 -1 5 -13 33.40 1.98 1 -5 14 25.80 1.45 -1 5 -14 25.74 1.60 -1 5 -14 25.87 1.71 1 -5 15 0.18 0.22 -1 5 -15 0.15 0.27 1 -5 16 10.72 0.85 -1 5 -16 13.03 1.09 -1 5 -16 11.34 0.94 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0.37 2 -11 0 0.05 0.33 2 -11 0 -0.03 0.32 2 -11 0 0.04 0.28 2 -11 1 1.34 0.47 2 -11 1 1.35 0.51 2 -11 1 0.52 0.53 2 -11 1 1.13 0.39 2 -11 1 1.08 0.50 2 -11 2 0.35 0.34 2 -11 2 0.63 0.37 2 -11 2 0.48 0.36 2 -11 2 0.87 0.46 2 -11 2 0.31 0.29 2 -11 3 2.59 0.65 2 -11 3 2.20 0.54 2 -11 3 2.94 0.67 2 -11 3 1.87 0.54 2 -11 3 2.75 0.59 2 -11 4 0.20 0.35 2 -11 4 0.82 0.36 2 -11 4 0.38 0.34 2 -11 4 0.50 0.36 2 -11 4 0.71 0.39 2 -11 5 101.27 3.47 2 -11 5 102.38 3.13 2 -11 5 95.57 3.25 2 -11 5 101.22 3.35 2 -11 5 101.24 3.23 2 -11 6 233.30 4.82 2 -11 6 223.96 4.87 2 -11 6 238.96 5.21 2 -11 6 243.60 5.29 2 -11 7 6.04 0.81 2 -11 7 5.69 0.78 2 -11 7 6.89 0.95 2 -11 7 5.37 0.81 2 -11 8 23.37 1.46 2 -11 8 23.71 1.69 2 -11 8 22.12 1.53 2 -11 9 -0.21 0.36 2 -11 9 0.11 0.33 2 -11 9 0.16 0.25 2 -11 9 -0.03 0.22 2 -11 10 0.25 0.22 2 -11 10 0.26 0.34 2 -11 10 0.03 0.32 2 -11 11 -0.23 0.30 2 -11 11 -0.23 0.29 2 -11 12 0.34 0.29 2 -11 13 0.15 0.23 -2 10 10 6.63 0.72 -2 10 9 0.02 0.25 -2 10 8 2.17 0.54 2 -10 -8 1.89 0.48 2 -10 -7 11.78 1.05 2 -10 -7 11.68 1.14 2 -10 -6 3.04 0.56 2 -10 -6 3.65 0.67 2 -10 -6 3.41 0.74 2 -10 -5 0.95 0.43 2 -10 -5 0.61 0.32 2 -10 -5 0.79 0.38 2 -10 -4 1.32 0.47 2 -10 -4 0.86 0.34 2 -10 -4 1.63 0.43 2 -10 -4 1.85 0.54 2 -10 -3 4.37 0.76 2 -10 -3 3.87 0.72 2 -10 -3 3.90 0.66 2 -10 -3 3.23 0.60 2 -10 -2 0.17 0.28 2 -10 -2 0.20 0.38 2 -10 -2 0.24 0.32 2 -10 -2 1.36 0.63 2 -10 -2 0.15 0.28 2 -10 -1 17.80 1.39 2 -10 -1 16.33 1.44 2 -10 -1 16.16 1.34 2 -10 -1 16.13 1.28 2 -10 -1 14.91 2.51 2 -10 -1 16.76 1.36 2 -10 0 39.40 1.99 2 -10 0 36.02 1.87 2 -10 0 36.55 2.06 2 -10 0 36.15 1.88 2 -10 0 34.59 1.91 2 -10 0 38.89 4.23 2 -10 0 41.14 2.15 2 -10 0 36.59 2.01 2 -10 1 2.19 0.52 2 -10 1 0.62 0.70 2 -10 1 2.29 0.54 2 -10 1 1.75 0.53 2 -10 1 2.12 0.56 2 -10 1 1.98 0.54 2 -10 1 2.07 0.54 2 -10 1 1.93 0.53 2 -10 2 14.48 1.21 2 -10 2 15.32 1.31 2 -10 2 16.05 1.27 2 -10 2 15.92 1.33 2 -10 2 16.14 1.38 2 -10 2 16.31 1.22 2 -10 2 18.52 3.20 2 -10 3 1.66 0.46 2 -10 3 1.42 0.47 2 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37.74 1.92 2 -9 -6 214.71 5.09 2 -9 -6 204.28 4.67 2 -9 -6 205.35 4.42 2 -9 -5 3.76 0.75 2 -9 -5 4.37 0.67 2 -9 -5 4.08 0.71 2 -9 -4 0.20 0.27 2 -9 -4 -0.13 0.30 2 -9 -4 -0.11 0.25 2 -9 -3 29.56 1.68 2 -9 -3 29.18 1.64 2 -9 -3 31.14 1.87 2 -9 -3 30.97 1.77 2 -9 -3 29.83 1.73 2 -9 -3 32.28 1.95 2 -9 -2 5.92 0.77 2 -9 -2 6.52 1.52 2 -9 -2 6.53 0.84 2 -9 -2 6.25 0.88 2 -9 -2 5.75 0.71 2 -9 -2 6.48 0.83 2 -9 -1 -0.07 0.30 2 -9 -1 0.35 0.35 2 -9 -1 0.50 0.56 2 -9 -1 0.27 0.31 2 -9 -1 0.02 0.28 2 -9 -1 0.20 0.31 2 -9 -1 0.01 0.25 2 -9 0 16.48 1.24 2 -9 0 19.37 1.30 2 -9 0 17.83 1.27 2 -9 0 17.58 1.23 2 -9 0 16.82 2.64 2 -9 0 19.58 1.38 2 -9 0 18.70 1.40 2 -9 0 17.93 1.36 2 -9 1 -0.19 0.24 2 -9 1 0.03 0.26 2 -9 1 0.41 0.29 2 -9 1 0.23 0.24 2 -9 1 0.32 0.22 2 -9 1 0.33 0.31 2 -9 1 0.10 0.25 2 -9 2 0.15 0.22 2 -9 2 0.14 0.31 2 -9 2 -0.03 0.29 2 -9 2 0.13 0.23 2 -9 2 0.08 0.20 2 -9 2 0.16 0.24 2 -9 2 0.45 0.32 2 -9 2 -0.79 0.72 2 -9 3 135.18 3.38 2 -9 3 137.92 3.42 2 -9 3 140.15 3.69 2 -9 3 134.65 3.45 2 -9 3 137.41 3.53 2 -9 3 134.82 3.40 2 -9 4 83.48 2.84 2 -9 4 88.91 2.75 2 -9 4 84.74 2.73 2 -9 4 88.68 2.88 2 -9 4 89.41 2.77 2 -9 4 86.49 2.72 2 -9 4 93.03 6.54 2 -9 5 11.17 1.05 2 -9 5 12.11 2.38 2 -9 5 9.54 1.00 2 -9 5 10.93 1.02 2 -9 5 11.24 0.96 2 -9 5 10.64 0.97 2 -9 5 9.41 0.97 2 -9 6 4.65 0.70 2 -9 6 4.69 1.56 2 -9 6 4.90 0.70 2 -9 6 4.46 0.73 2 -9 6 4.65 0.69 2 -9 6 5.75 0.75 2 -9 7 1.09 0.44 2 -9 7 1.16 0.43 2 -9 7 1.20 0.39 2 -9 7 1.13 0.37 2 -9 7 1.63 0.44 2 -9 8 27.19 1.75 2 -9 8 26.68 1.75 2 -9 8 27.04 1.55 2 -9 8 26.87 3.47 2 -9 8 27.07 1.68 2 -9 9 0.60 0.43 2 -9 9 0.32 0.27 2 -9 9 0.24 0.38 2 -9 9 0.13 0.35 2 -9 10 1.82 0.43 2 -9 10 3.14 0.70 2 -9 10 2.25 0.58 2 -9 10 2.79 0.62 2 -9 11 9.63 1.07 2 -9 11 10.37 1.05 2 -9 11 9.83 1.09 2 -9 12 7.57 0.92 2 -9 12 7.03 0.91 2 -9 12 7.70 0.91 2 -9 13 3.82 0.67 2 -9 13 3.20 0.55 2 -9 13 2.48 0.50 2 -9 14 0.67 0.35 2 -9 14 0.44 0.24 2 -9 14 0.30 0.27 2 -9 15 2.10 0.38 2 -9 15 2.24 0.38 -2 8 13 0.97 0.30 -2 8 12 16.12 1.14 2 -8 -12 14.77 1.02 -2 8 11 0.14 0.33 2 -8 -10 45.04 2.00 2 -8 -10 44.61 1.86 -2 8 10 45.08 2.21 2 -8 -9 8.72 0.91 2 -8 -9 7.09 0.86 -2 8 9 8.63 1.03 2 -8 -8 19.06 1.36 2 -8 -8 17.38 1.41 2 -8 -7 158.29 3.87 2 -8 -7 154.73 4.18 2 -8 -7 154.89 3.84 2 -8 -6 103.99 3.46 2 -8 -6 101.22 3.09 2 -8 -6 107.17 3.26 2 -8 -5 29.19 1.85 2 -8 -5 27.23 1.60 2 -8 -5 26.12 1.64 -2 8 5 24.51 3.07 2 -8 -4 2.57 0.55 2 -8 -4 2.61 0.56 2 -8 -4 2.51 0.48 2 -8 -4 2.69 0.51 -2 8 4 1.61 0.90 2 -8 -4 3.63 0.68 2 -8 -3 56.49 2.43 2 -8 -3 51.29 2.04 2 -8 -3 54.53 2.31 2 -8 -3 56.51 2.24 2 -8 -3 50.88 3.95 2 -8 -3 55.24 2.10 -2 8 3 51.43 3.99 2 -8 -2 3.95 0.60 2 -8 -2 3.05 0.51 2 -8 -2 4.23 0.73 2 -8 -2 3.01 0.95 2 -8 -2 4.23 0.63 2 -8 -1 15.79 1.17 2 -8 -1 17.08 1.16 2 -8 -1 17.31 1.31 2 -8 -1 15.40 1.11 2 -8 -1 15.99 1.17 2 -8 -1 17.29 1.14 2 -8 -1 17.35 2.41 2 -8 -1 15.95 1.18 2 -8 0 0.61 0.24 2 -8 0 0.48 0.44 2 -8 0 0.51 0.29 2 -8 0 0.65 0.28 2 -8 0 1.09 0.38 2 -8 0 0.69 0.36 2 -8 0 0.79 0.32 2 -8 0 0.64 0.28 2 -8 1 28.82 1.67 2 -8 1 27.79 1.53 2 -8 1 26.40 1.43 2 -8 1 28.03 1.42 2 -8 1 29.31 3.28 2 -8 1 26.37 1.43 2 -8 1 27.20 1.40 2 -8 1 27.95 1.51 2 -8 2 70.64 2.33 2 -8 2 69.26 2.33 2 -8 2 69.85 2.49 2 -8 2 65.85 2.13 2 -8 2 64.59 2.16 2 -8 2 65.89 2.16 2 -8 2 70.16 2.25 2 -8 2 67.27 2.20 2 -8 3 99.50 2.65 2 -8 3 102.15 2.74 2 -8 3 102.84 2.83 2 -8 3 99.84 2.90 2 -8 3 101.60 2.78 2 -8 3 106.01 6.61 2 -8 3 95.92 2.63 2 -8 4 51.15 2.03 2 -8 4 48.30 1.88 2 -8 4 50.87 1.97 2 -8 4 50.89 1.96 2 -8 4 46.43 1.83 2 -8 4 47.96 1.98 2 -8 4 45.79 4.32 2 -8 5 104.05 2.88 2 -8 5 108.93 2.92 2 -8 5 107.31 3.05 2 -8 5 106.86 6.55 2 -8 5 105.30 2.77 2 -8 5 107.37 3.01 2 -8 5 104.45 2.88 2 -8 6 0.27 0.48 2 -8 6 0.94 0.31 2 -8 6 0.49 0.32 2 -8 6 1.04 0.35 2 -8 6 0.11 0.26 2 -8 6 0.99 0.37 2 -8 6 0.57 0.30 2 -8 7 11.29 0.95 2 -8 7 10.51 1.03 2 -8 7 11.26 0.98 2 -8 7 11.05 2.11 2 -8 7 10.68 1.02 2 -8 7 10.47 1.04 2 -8 8 23.35 1.55 2 -8 8 22.11 1.54 2 -8 8 22.68 1.51 2 -8 8 22.90 3.01 2 -8 8 21.67 1.37 2 -8 9 2.30 0.50 2 -8 9 2.55 0.62 2 -8 9 2.53 0.62 2 -8 9 2.36 0.58 2 -8 10 82.92 3.06 2 -8 10 75.80 2.51 2 -8 10 83.69 3.06 2 -8 10 83.68 2.94 2 -8 11 24.89 1.73 2 -8 11 24.45 1.68 2 -8 11 25.23 1.64 -2 8 -11 25.37 1.56 2 -8 12 -0.48 0.41 2 -8 12 -0.18 0.33 2 -8 12 0.37 0.37 -2 8 -12 0.09 0.26 2 -8 13 0.32 0.36 2 -8 13 -0.17 0.27 2 -8 13 0.22 0.34 -2 8 -13 -0.23 0.27 2 -8 14 1.26 0.40 2 -8 14 2.01 0.50 2 -8 14 0.92 0.31 -2 8 -14 1.43 0.38 2 -8 15 1.99 0.38 -2 8 -15 1.91 0.39 2 -8 15 2.45 0.49 2 -8 15 2.05 0.39 2 -8 16 5.72 0.60 -2 7 14 0.07 0.19 -2 7 13 7.08 0.76 -2 7 12 0.65 0.31 -2 7 12 0.56 0.37 -2 7 11 8.92 1.04 2 -7 -10 8.68 0.92 2 -7 -10 6.62 0.80 -2 7 10 8.84 1.07 -2 7 9 0.82 0.45 2 -7 -9 0.75 0.37 2 -7 -9 0.82 0.38 -2 7 8 140.07 8.09 2 -7 -8 144.71 3.87 2 -7 -8 151.05 3.80 2 -7 -7 43.87 2.14 2 -7 -7 49.53 2.07 2 -7 -7 46.40 2.09 -2 7 7 43.70 4.32 2 -7 -6 54.10 2.21 2 -7 -6 53.00 2.16 2 -7 -6 52.45 2.34 -2 7 6 50.77 4.39 2 -7 -5 170.60 3.55 2 -7 -5 175.93 4.24 2 -7 -5 173.98 3.90 2 -7 -5 173.97 3.81 -2 7 5 173.41 7.68 2 -7 -4 3.01 0.57 2 -7 -4 2.38 0.47 2 -7 -4 2.26 0.43 2 -7 -4 2.32 0.47 2 -7 -4 2.07 0.43 -2 7 4 2.09 0.82 2 -7 -3 265.95 4.19 2 -7 -3 266.37 4.26 2 -7 -3 265.44 8.23 2 -7 -3 279.67 5.05 2 -7 -3 266.48 4.72 2 -7 -3 269.15 4.49 -2 7 3 262.37 8.21 2 -7 -2 2.47 0.43 2 -7 -2 1.90 0.39 2 -7 -2 1.79 0.39 2 -7 -2 1.37 0.34 2 -7 -2 1.90 0.43 2 -7 -2 1.75 0.39 2 -7 -2 1.44 0.71 2 -7 -2 1.92 0.44 2 -7 -1 107.16 2.62 2 -7 -1 107.57 2.56 2 -7 -1 103.72 5.32 2 -7 -1 105.23 2.77 2 -7 -1 103.43 2.70 2 -7 -1 103.01 2.63 2 -7 -1 106.35 3.00 2 -7 -1 104.37 2.68 2 -7 0 38.15 1.56 2 -7 0 37.05 1.50 2 -7 0 34.09 3.18 2 -7 0 37.21 1.69 2 -7 0 36.14 1.70 2 -7 0 36.71 1.58 2 -7 1 0.91 0.37 2 -7 1 1.67 0.37 2 -7 1 0.31 0.58 2 -7 1 0.90 0.31 2 -7 2 11.56 0.86 2 -7 2 10.89 2.07 2 -7 2 10.71 0.85 2 -7 2 11.53 0.98 2 -7 3 145.36 3.26 2 -7 3 148.02 3.14 2 -7 3 152.68 3.08 2 -7 3 150.40 3.03 2 -7 3 150.83 7.49 2 -7 4 38.38 1.64 2 -7 4 41.07 1.71 2 -7 4 39.64 1.67 2 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3.01 0.94 2 -5 2 59.93 3.67 2 -5 3 354.41 9.08 2 -5 4 19.10 2.10 2 -5 4 20.94 1.41 2 -5 5 50.22 3.35 2 -5 5 52.89 2.51 2 -5 6 322.57 8.56 2 -5 7 37.69 1.64 2 -5 7 40.54 3.06 2 -5 8 0.58 0.29 -2 5 -9 250.78 4.26 2 -5 9 252.96 4.61 -2 5 -10 242.41 4.50 2 -5 10 240.49 4.69 -2 5 -11 37.52 1.86 2 -5 11 34.01 1.83 -2 5 -12 866.34 9.17 2 -5 12 843.70 8.90 2 -5 12 862.95 9.09 -2 5 -13 69.05 2.60 2 -5 13 65.98 2.43 2 -5 13 65.12 2.48 2 -5 14 17.37 1.20 2 -5 14 16.87 1.21 -2 5 -14 17.89 1.39 -2 5 -14 17.28 1.28 -2 5 -15 3.25 0.55 2 -5 15 3.01 0.48 -2 5 -15 4.70 0.71 -2 5 -16 3.44 0.50 2 -5 16 3.14 0.51 -2 5 -16 3.39 0.53 -2 4 16 4.54 0.56 -2 4 15 68.97 2.08 -2 4 15 68.79 2.37 -2 4 14 24.08 1.39 -2 4 14 23.50 1.53 2 -4 -14 24.00 1.42 -2 4 13 4.00 0.64 -2 4 13 4.16 0.72 2 -4 -13 4.46 0.67 -2 4 12 0.33 0.34 2 -4 -12 0.01 0.31 -2 4 12 -0.42 0.50 2 -4 -11 23.84 1.50 -2 4 11 21.71 1.54 -2 4 11 24.85 3.58 -2 4 10 1.99 0.52 2 -4 -10 1.28 0.37 2 -4 -10 1.38 0.47 -2 4 9 3.95 0.67 2 -4 -9 2.79 0.53 2 -4 -9 2.95 0.57 -2 4 9 2.56 1.08 2 -4 -8 50.87 1.94 2 -4 -8 45.86 1.78 2 -4 -8 51.96 2.01 -2 4 8 47.20 4.10 2 -4 -7 140.06 3.09 -2 4 7 136.56 6.42 -2 4 6 156.21 6.42 2 -4 -5 40.64 2.27 -2 4 5 34.67 2.78 2 -4 -4 800.66 10.54 -2 4 4 765.37 11.65 2 -4 -3 33.32 2.16 -2 4 3 30.29 2.11 2 -4 -2 94.24 3.66 -2 4 2 94.13 3.25 2 -4 -1 5311.72 27.76 2 -4 0 2003.95 17.34 2 -4 1 563.74 9.57 2 -4 2 130.35 4.73 2 -4 3 39.39 2.68 2 -4 3 39.19 1.51 2 -4 4 4.42 0.95 2 -4 4 3.96 0.64 2 -4 5 31.41 2.39 2 -4 5 32.56 1.99 2 -4 6 265.39 7.00 2 -4 6 277.02 6.58 2 -4 7 58.20 3.28 2 -4 7 56.54 1.93 2 -4 7 58.35 3.34 -2 4 -8 266.73 4.12 2 -4 8 276.30 4.55 2 -4 8 274.34 4.31 2 -4 8 271.89 4.16 2 -4 8 276.00 7.99 2 -4 8 273.50 4.67 2 -4 9 1.16 0.44 -2 4 -9 1.38 0.36 2 -4 9 0.60 0.27 2 -4 9 0.93 0.37 2 -4 10 9.60 0.84 -2 4 -10 9.03 0.88 -2 4 -11 56.82 2.31 -2 4 -12 461.75 6.74 2 -4 12 442.61 6.47 -2 4 -13 158.05 3.99 2 -4 13 152.52 3.59 2 -4 13 150.18 3.72 -2 4 -14 1.37 0.45 2 -4 14 0.73 0.29 -2 4 -15 51.49 2.10 -2 4 -15 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130.06 4.33 2 -3 5 35.27 2.28 2 -3 5 36.36 2.18 2 -3 6 35.49 2.43 2 -3 6 38.72 2.40 2 -3 7 26.29 2.34 2 -3 8 6.37 0.73 2 -3 8 5.93 0.69 -2 3 -8 6.54 0.68 2 -3 8 7.41 0.73 2 -3 8 6.03 0.63 2 -3 8 7.20 1.33 2 -3 9 7.29 0.83 2 -3 9 7.37 0.84 2 -3 9 7.45 0.75 2 -3 9 7.84 1.52 -2 3 -9 8.56 0.83 2 -3 10 63.50 2.16 2 -3 10 63.40 2.44 2 -3 10 63.18 2.51 -2 3 -10 63.65 2.37 2 -3 11 5.32 0.82 -2 3 -11 6.45 0.80 2 -3 11 5.73 0.86 -2 3 -12 12.08 1.14 2 -3 12 12.54 1.26 2 -3 12 12.10 1.23 -2 3 -13 14.53 1.24 2 -3 13 15.66 1.20 2 -3 14 21.90 1.35 -2 3 -14 22.61 1.53 -2 3 -15 21.97 1.41 -2 3 -15 22.68 1.49 2 -3 15 20.46 1.16 -2 3 -16 37.48 1.63 -2 3 -16 39.93 1.75 -2 2 17 0.29 0.22 2 -2 -17 0.35 0.21 -2 2 16 6.25 0.74 2 -2 -16 7.03 0.78 -2 2 15 4.70 0.71 -2 2 15 4.04 0.60 2 -2 -15 4.28 0.67 -2 2 14 1.22 0.49 -2 2 14 0.83 0.37 2 -2 -14 1.18 0.49 2 -2 -14 1.13 0.38 -2 2 13 603.60 7.54 -2 2 13 609.90 8.07 2 -2 -13 629.92 7.78 2 -2 -13 602.45 8.09 -2 2 12 7.18 0.82 2 -2 -12 6.34 0.84 2 -2 -12 7.08 0.85 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0.80 2 3 -12 6.90 0.95 -2 -3 11 43.53 1.99 2 3 -11 42.03 2.12 -2 -3 11 40.43 4.24 2 3 -11 44.44 2.12 -2 -3 10 111.84 3.06 -2 -3 10 102.90 2.68 2 3 -10 109.17 3.25 -2 -3 10 103.01 6.39 2 3 -10 111.04 3.17 -2 -3 9 131.73 2.91 2 3 -9 138.74 3.46 2 3 -9 138.40 3.36 -2 -3 8 33.17 1.54 2 3 -8 29.73 1.50 -2 -3 8 29.05 3.03 2 3 -8 29.49 1.46 -2 -3 7 610.17 12.76 -2 -3 6 152.40 5.98 -2 -3 5 37.63 2.87 -2 -3 4 260.78 7.07 2 3 -3 76.55 3.52 -2 -3 3 70.60 3.56 2 3 -2 143.70 4.73 2 3 -1 352.73 7.40 2 3 0 413.79 8.08 2 3 1 42.26 2.62 2 3 2 1.56 0.64 2 3 3 307.38 7.84 2 3 4 16.64 1.96 2 3 5 2.82 0.47 2 3 5 2.93 0.91 -2 -3 -5 2.54 0.43 -2 -3 -6 124.99 2.80 2 3 6 125.95 6.05 -2 -3 -6 133.66 3.15 2 3 6 124.69 2.94 2 3 6 127.80 3.20 2 3 6 134.21 6.90 2 3 7 2.31 0.49 -2 -3 -7 2.31 0.48 2 3 7 2.06 1.02 2 3 8 284.26 5.26 -2 -3 -8 291.22 5.12 2 3 9 201.70 4.54 2 3 9 215.44 10.25 -2 -3 -9 200.96 4.39 -2 -3 -10 6.48 0.83 2 3 10 7.41 0.91 2 3 11 0.93 0.44 -2 -3 -11 0.69 0.34 2 3 12 55.78 2.26 2 3 12 55.93 2.35 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72.30 3.68 2 4 -1 0.97 0.56 2 4 0 163.74 5.47 2 4 1 0.57 0.41 2 4 2 25.97 2.29 -2 -4 -2 27.27 1.26 2 4 3 -0.24 0.34 -2 -4 -3 0.05 0.20 -2 -4 -4 38.53 1.64 -2 -4 -4 36.27 2.77 2 4 4 36.97 2.97 -2 -4 -4 35.15 1.49 -2 -4 -5 81.17 2.41 -2 -4 -5 81.49 2.35 2 4 5 83.95 4.78 2 4 5 77.38 2.47 -2 -4 -5 79.94 2.37 -2 -4 -6 114.04 2.85 -2 -4 -6 113.82 3.02 2 4 6 111.22 3.13 2 4 6 114.19 6.84 2 4 7 40.71 1.99 -2 -4 -7 40.19 1.89 2 4 7 44.73 4.52 2 4 8 1.27 0.46 -2 -4 -8 1.29 0.34 2 4 9 1.60 0.49 -2 -4 -9 1.99 0.51 2 4 10 7.97 0.94 -2 -4 -10 7.28 0.85 -2 -4 -10 8.03 0.84 2 4 11 2.43 0.54 -2 -4 -11 3.11 0.57 -2 -4 -12 23.44 1.30 2 4 12 26.48 1.53 2 4 12 24.47 1.39 -2 -4 -13 22.35 1.11 2 4 13 25.90 1.33 2 4 13 25.54 1.23 2 5 -17 2.48 0.46 -2 -5 17 2.05 0.46 -2 -5 16 1.00 0.32 2 5 -16 1.00 0.42 2 5 -16 1.15 0.41 2 5 -15 6.68 0.85 -2 -5 15 6.17 0.72 -2 -5 15 5.91 0.76 2 5 -15 5.81 0.86 2 5 -14 7.33 0.90 2 5 -14 6.95 0.98 -2 -5 14 6.92 0.82 -2 -5 14 6.05 0.83 -2 -5 13 -0.08 0.28 2 5 -13 0.24 0.40 -2 -5 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-2 -5 -1 76.11 2.21 -2 -5 -2 17.51 1.16 -2 -5 -2 17.05 1.07 -2 -5 -2 20.40 1.20 2 5 2 17.80 1.96 -2 -5 -2 17.15 2.18 -2 -5 -3 17.85 1.19 -2 -5 -3 19.95 1.19 2 5 3 19.04 2.14 -2 -5 -3 19.02 2.21 -2 -5 -4 8.70 0.84 -2 -5 -4 8.23 0.80 -2 -5 -5 5.46 0.67 2 5 5 5.12 0.68 -2 -5 -5 5.64 0.67 -2 -5 -5 5.83 0.71 -2 -5 -6 94.02 2.75 2 5 6 93.07 2.98 -2 -5 -6 93.86 2.79 2 5 6 99.95 6.81 2 5 7 -0.03 0.29 -2 -5 -7 0.46 0.24 2 5 7 -0.42 0.66 -2 -5 -8 40.07 1.89 2 5 8 40.31 2.04 2 5 9 47.17 2.19 -2 -5 -9 48.08 2.04 -2 -5 -9 47.58 2.09 2 5 10 17.84 1.28 -2 -5 -10 17.74 1.21 -2 -5 -10 19.70 1.24 -2 -5 -11 64.28 2.06 2 5 11 62.66 2.21 2 5 12 44.20 1.78 2 5 12 39.16 1.54 -2 -6 17 17.08 1.08 -2 -6 16 49.79 1.85 -2 -6 16 53.37 2.11 2 6 -16 55.00 2.06 2 6 -15 0.22 0.33 -2 -6 15 0.03 0.24 -2 -6 14 68.61 2.55 2 6 -14 72.85 2.71 2 6 -13 0.19 0.26 -2 -6 13 0.99 0.46 2 6 -13 0.57 0.38 2 6 -12 1.10 0.45 -2 -6 12 0.96 0.46 2 6 -12 1.53 0.51 -2 -6 11 83.23 2.92 2 6 -11 78.64 3.04 -2 -6 11 76.90 6.05 2 6 -11 80.99 2.87 -2 -6 10 25.16 1.41 -2 -6 10 24.42 1.58 2 6 -10 23.94 1.53 -2 -6 10 21.07 3.12 -2 -6 9 208.85 4.05 -2 -6 9 220.09 4.54 -2 -6 9 204.07 9.30 2 6 -9 215.53 4.35 2 6 -8 25.16 1.42 -2 -6 8 26.62 1.41 -2 -6 8 26.54 2.76 -2 -6 8 27.16 1.58 -2 -6 8 24.83 1.39 -2 -6 8 27.02 3.27 -2 -6 7 66.66 4.51 -2 -6 7 75.33 2.35 -2 -6 7 73.24 2.47 -2 -6 7 73.37 2.37 -2 -6 6 30.11 1.49 -2 -6 6 29.32 1.42 -2 -6 6 32.85 3.15 -2 -6 6 31.48 1.59 2 6 -6 30.79 3.12 -2 -6 5 0.26 0.25 -2 -6 5 0.19 0.23 -2 -6 5 1.04 0.69 -2 -6 5 0.52 0.24 2 6 -5 -0.12 0.44 -2 -6 4 194.49 3.53 2 6 -4 192.82 7.22 -2 -6 4 200.99 3.78 -2 -6 4 194.74 3.39 -2 -6 4 203.41 3.78 -2 -6 4 203.37 8.16 -2 -6 3 172.09 3.47 -2 -6 3 178.47 3.51 2 6 -3 166.17 6.54 -2 -6 3 168.01 3.41 -2 -6 3 174.89 3.28 -2 -6 3 177.59 3.52 -2 -6 2 38.83 1.70 -2 -6 2 36.84 3.53 -2 -6 2 38.39 1.64 -2 -6 2 38.94 1.66 -2 -6 2 38.16 1.66 -2 -6 2 39.63 1.59 2 6 -2 38.06 3.00 -2 -6 1 230.86 4.26 -2 -6 1 227.34 4.03 -2 -6 1 229.32 8.71 -2 -6 1 230.90 4.00 -2 -6 1 220.44 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19.12 1.33 3 -10 9 19.65 1.51 3 -10 10 0.77 0.33 3 -10 10 1.12 0.46 3 -10 10 0.12 0.38 3 -10 11 3.21 0.63 3 -10 11 3.50 0.54 3 -10 11 3.51 0.64 3 -10 12 0.70 0.34 3 -10 12 0.68 0.32 3 -10 13 2.29 0.42 3 -10 13 2.43 0.47 3 -10 14 3.23 0.47 -3 9 12 4.31 0.55 -3 9 11 11.80 1.01 3 -9 -11 12.38 0.95 -3 9 10 5.32 0.77 3 -9 -10 5.80 0.70 3 -9 -10 5.35 0.69 -3 9 9 -0.30 0.40 3 -9 -9 0.21 0.26 3 -9 -9 0.87 0.42 3 -9 -8 2.78 0.60 3 -9 -8 3.24 0.65 3 -9 -8 2.05 0.49 3 -9 -7 0.71 0.34 3 -9 -7 2.27 0.55 3 -9 -7 1.81 0.54 3 -9 -7 1.49 0.45 3 -9 -6 13.62 1.38 3 -9 -6 11.12 1.14 3 -9 -6 12.22 1.16 3 -9 -5 0.79 0.43 3 -9 -5 1.17 0.45 3 -9 -5 0.91 0.48 3 -9 -4 3.61 0.64 3 -9 -4 2.52 0.62 3 -9 -4 2.70 0.62 3 -9 -4 1.88 0.51 3 -9 -3 28.16 3.25 3 -9 -3 29.34 1.69 3 -9 -3 28.33 1.82 3 -9 -3 29.78 1.95 3 -9 -3 27.82 1.55 3 -9 -2 7.74 1.01 3 -9 -2 6.61 0.82 3 -9 -2 5.47 1.49 3 -9 -2 6.31 0.76 3 -9 -2 5.98 0.83 3 -9 -2 6.92 0.85 3 -9 -1 28.17 1.69 3 -9 -1 28.74 3.46 3 -9 -1 29.99 1.58 3 -9 -1 28.95 1.75 3 -9 -1 28.78 1.65 3 -9 -1 28.92 1.84 3 -9 -1 28.61 1.71 3 -9 0 86.37 2.67 3 -9 0 86.10 2.80 3 -9 0 86.06 3.03 3 -9 0 82.71 5.98 3 -9 0 87.49 3.12 3 -9 0 87.25 2.93 3 -9 1 0.33 0.28 3 -9 1 0.93 0.47 3 -9 1 0.21 0.26 3 -9 1 0.48 0.26 3 -9 1 0.14 0.46 3 -9 1 0.47 0.28 3 -9 2 19.61 1.31 3 -9 2 18.79 1.34 3 -9 2 19.60 1.39 3 -9 2 17.13 1.28 3 -9 2 18.02 1.21 3 -9 2 17.61 3.04 3 -9 2 19.13 1.48 3 -9 3 261.20 4.76 3 -9 3 252.32 4.88 3 -9 3 248.67 4.77 3 -9 3 255.47 5.07 3 -9 3 265.38 11.77 3 -9 3 251.22 5.08 3 -9 3 246.29 4.53 3 -9 4 92.59 2.98 3 -9 4 93.84 3.06 3 -9 4 99.51 7.09 3 -9 4 89.37 2.83 3 -9 4 90.93 2.84 3 -9 4 95.92 3.12 3 -9 4 91.17 2.81 3 -9 5 0.04 0.53 3 -9 5 0.84 0.33 3 -9 5 1.19 0.45 3 -9 5 2.12 0.45 3 -9 5 0.78 0.36 3 -9 5 1.36 0.46 3 -9 5 0.74 0.35 3 -9 6 35.09 4.10 3 -9 6 33.39 1.78 3 -9 6 30.21 1.79 3 -9 6 30.43 1.72 3 -9 6 30.57 1.82 3 -9 7 47.07 4.78 3 -9 7 47.93 2.14 3 -9 7 47.80 2.14 3 -9 7 48.13 2.33 3 -9 7 45.54 2.23 3 -9 7 46.35 2.17 3 -9 8 72.52 2.87 3 -9 8 73.53 2.63 3 -9 8 68.62 5.62 3 -9 8 70.95 2.85 3 -9 8 74.78 2.81 3 -9 9 56.80 2.57 3 -9 9 55.07 2.49 3 -9 9 51.08 2.18 3 -9 9 57.40 2.51 3 -9 10 3.78 0.62 3 -9 10 3.76 0.69 3 -9 10 4.05 0.79 3 -9 10 4.81 0.79 3 -9 11 5.05 0.82 3 -9 11 5.10 0.77 3 -9 11 4.50 0.62 3 -9 11 4.65 0.73 3 -9 12 35.03 1.92 3 -9 12 32.55 1.76 3 -9 12 36.08 1.86 3 -9 13 1.47 0.44 3 -9 13 1.72 0.43 3 -9 13 2.16 0.47 3 -9 14 0.34 0.24 3 -9 14 0.87 0.30 3 -9 14 0.59 0.29 -3 8 13 14.07 0.97 3 -8 -13 13.78 0.96 3 -8 -12 22.28 1.36 -3 8 12 21.62 1.36 -3 8 11 35.46 1.87 -3 8 10 0.84 0.37 3 -8 -10 1.75 0.53 3 -8 -9 3.53 0.65 3 -8 -9 4.30 0.74 3 -8 -8 109.78 3.37 3 -8 -8 104.79 3.43 3 -8 -7 0.35 0.28 3 -8 -7 -0.22 0.36 3 -8 -7 0.88 0.46 3 -8 -6 1.51 0.47 3 -8 -6 1.62 0.47 3 -8 -6 2.33 0.64 3 -8 -5 16.61 1.35 3 -8 -5 16.75 1.45 3 -8 -5 16.96 1.30 3 -8 -5 18.06 1.23 3 -8 -4 84.28 3.01 3 -8 -4 86.42 3.11 3 -8 -4 88.73 2.64 3 -8 -4 81.97 2.50 3 -8 -4 85.77 2.83 3 -8 -3 17.71 1.24 3 -8 -3 18.31 1.44 3 -8 -3 18.52 1.17 3 -8 -3 17.40 1.35 3 -8 -3 17.96 2.41 3 -8 -2 18.94 1.29 3 -8 -2 19.25 1.51 3 -8 -2 18.60 1.17 3 -8 -2 17.87 1.31 3 -8 -2 19.50 2.61 3 -8 -2 19.59 1.34 3 -8 -1 22.16 1.45 3 -8 -1 21.18 1.48 3 -8 -1 21.39 1.32 3 -8 -1 21.76 1.38 3 -8 -1 20.67 1.37 3 -8 -1 21.53 1.26 3 -8 -1 19.65 2.67 3 -8 0 133.18 7.06 3 -8 0 131.29 3.53 3 -8 0 131.83 3.34 3 -8 0 131.18 3.30 3 -8 0 131.90 3.07 3 -8 0 138.81 3.75 3 -8 0 135.84 3.27 3 -8 1 3.03 1.14 3 -8 1 2.63 0.51 3 -8 1 1.86 0.43 3 -8 1 3.20 0.67 3 -8 1 2.37 0.46 3 -8 1 1.95 0.38 3 -8 2 98.89 6.70 3 -8 2 93.85 2.73 3 -8 2 91.97 3.00 3 -8 2 93.15 2.63 3 -8 2 93.27 2.80 3 -8 2 92.40 2.80 3 -8 2 91.79 2.50 3 -8 3 5.43 1.63 3 -8 3 5.11 0.72 3 -8 3 4.96 0.65 3 -8 3 4.14 0.62 3 -8 3 3.75 0.58 3 -8 3 4.81 0.68 3 -8 3 4.67 0.61 3 -8 3 5.08 0.62 3 -8 4 37.13 4.11 3 -8 4 39.64 1.84 3 -8 4 38.70 1.82 3 -8 4 38.70 1.75 3 -8 4 39.40 1.78 3 -8 4 38.12 1.88 3 -8 4 37.93 1.72 3 -8 5 0.72 0.28 3 -8 5 0.98 0.76 3 -8 5 1.41 0.38 3 -8 5 1.39 0.41 3 -8 5 1.77 0.47 3 -8 5 1.45 0.41 3 -8 5 1.03 0.30 3 -8 6 107.13 3.06 3 -8 6 103.38 3.12 3 -8 6 108.57 3.21 3 -8 6 115.06 6.93 3 -8 6 105.67 3.07 3 -8 6 106.55 3.16 3 -8 7 2.59 1.12 3 -8 7 1.10 0.37 3 -8 7 1.66 0.47 3 -8 7 1.15 0.43 3 -8 7 1.28 0.40 3 -8 8 17.19 2.77 3 -8 8 17.93 1.32 3 -8 8 19.96 1.48 3 -8 8 16.51 1.36 3 -8 8 17.38 1.33 3 -8 9 13.16 1.13 3 -8 9 13.22 1.24 3 -8 9 14.63 1.28 3 -8 9 14.56 1.25 3 -8 10 0.39 0.39 3 -8 10 0.74 0.43 3 -8 10 0.69 0.35 3 -8 10 0.31 0.35 3 -8 11 8.41 1.05 3 -8 11 8.32 0.84 3 -8 11 8.70 0.97 3 -8 11 8.59 1.01 3 -8 12 96.67 3.25 3 -8 12 96.28 3.01 3 -8 12 99.31 3.11 3 -8 13 26.07 1.60 3 -8 13 24.30 1.42 3 -8 13 25.46 1.50 3 -8 14 -0.04 0.29 3 -8 14 0.01 0.24 3 -8 15 1.00 0.33 3 -8 15 0.72 0.25 3 -7 -14 9.83 0.84 -3 7 14 10.58 0.83 -3 7 13 -0.09 0.28 -3 7 12 11.87 1.12 -3 7 11 6.63 0.88 3 -7 -11 5.72 0.78 -3 7 10 12.48 1.22 3 -7 -10 14.36 1.26 3 -7 -10 11.91 1.08 3 -7 -9 144.37 3.63 3 -7 -9 139.48 3.83 3 -7 -9 139.65 3.77 3 -7 -8 221.02 4.74 3 -7 -8 212.64 4.76 3 -7 -7 116.55 3.21 3 -7 -7 111.32 3.48 3 -7 -7 110.84 3.30 -3 7 7 107.17 6.46 3 -7 -6 9.31 1.04 3 -7 -6 9.54 0.93 3 -7 -6 9.37 0.94 -3 7 6 7.96 1.68 3 -7 -5 30.84 1.87 3 -7 -5 28.98 1.63 3 -7 -5 30.41 1.45 3 -7 -5 31.49 1.67 -3 7 5 31.78 3.13 3 -7 -4 24.45 1.43 3 -7 -4 27.47 1.62 3 -7 -4 28.50 1.68 3 -7 -4 25.61 1.29 -3 7 4 25.87 2.65 3 -7 -4 24.33 2.63 3 -7 -3 19.94 1.12 3 -7 -3 19.83 1.43 3 -7 -3 20.50 1.34 3 -7 -3 21.42 1.25 3 -7 -3 18.85 1.12 3 -7 -3 17.41 2.20 3 -7 -2 39.81 1.70 3 -7 -2 35.00 3.24 3 -7 -2 37.43 1.68 3 -7 -2 38.49 1.96 3 -7 -2 36.14 1.71 3 -7 -2 37.40 1.50 3 -7 -2 38.64 1.70 3 -7 -1 2.42 0.97 3 -7 -1 3.35 0.48 3 -7 -1 2.84 0.50 3 -7 -1 3.33 0.53 3 -7 -1 2.63 0.49 3 -7 -1 3.09 0.51 3 -7 -1 3.29 0.52 3 -7 0 226.52 8.47 3 -7 0 228.77 4.24 3 -7 0 241.08 4.11 3 -7 0 233.66 3.72 3 -7 0 230.18 4.40 3 -7 0 232.04 3.97 3 -7 0 230.60 4.05 3 -7 1 39.68 3.72 3 -7 1 42.49 1.71 3 -7 1 44.01 1.97 3 -7 1 43.09 1.64 3 -7 1 42.59 1.78 3 -7 1 42.91 1.75 3 -7 2 7.12 1.72 3 -7 2 8.58 0.78 3 -7 2 8.12 0.83 3 -7 2 8.63 0.78 3 -7 2 9.52 0.82 3 -7 2 8.69 0.79 3 -7 3 177.99 8.37 3 -7 3 168.91 3.41 3 -7 3 176.93 3.47 3 -7 3 168.97 3.59 3 -7 3 171.13 3.48 3 -7 3 173.33 3.44 3 -7 3 173.73 3.56 3 -7 3 174.07 3.29 3 -7 4 162.16 3.43 3 -7 4 160.75 3.48 3 -7 4 159.85 3.28 3 -7 4 160.97 3.44 3 -7 4 167.93 7.88 3 -7 4 160.28 3.30 3 -7 4 160.33 3.43 3 -7 4 161.16 3.38 3 -7 4 157.41 3.52 3 -7 5 149.03 7.31 3 -7 5 141.08 3.33 3 -7 5 141.22 3.37 3 -7 5 144.57 3.28 3 -7 5 143.47 3.43 3 -7 6 102.08 6.03 3 -7 6 96.68 2.89 3 -7 6 96.39 2.87 3 -7 6 102.38 2.89 3 -7 7 1.03 0.37 3 -7 7 1.33 0.41 3 -7 7 1.82 0.50 3 -7 8 41.78 1.99 3 -7 8 37.43 1.96 3 -7 8 38.35 1.97 3 -7 9 1.58 0.49 3 -7 9 1.06 0.42 3 -7 9 1.88 0.52 3 -7 10 4.82 0.80 3 -7 10 3.22 0.63 3 -7 10 3.25 0.68 3 -7 11 27.30 1.66 3 -7 11 29.23 1.58 3 -7 11 30.47 1.81 3 -7 11 30.24 1.85 -3 7 -11 29.80 1.72 3 -7 12 87.21 2.84 3 -7 12 86.78 3.07 3 -7 12 91.95 3.02 -3 7 -12 90.97 2.99 3 -7 13 75.33 2.47 3 -7 13 73.71 2.73 3 -7 13 72.18 2.54 -3 7 -13 74.20 2.60 -3 7 -14 4.16 0.59 3 -7 14 5.19 0.73 3 -7 14 4.35 0.63 3 -7 15 35.60 1.60 -3 7 -15 33.52 1.49 -3 6 15 1.37 0.35 3 -6 -15 1.71 0.39 -3 6 14 3.68 0.58 -3 6 13 20.06 1.39 -3 6 12 31.46 1.84 -3 6 11 0.52 0.43 3 -6 -11 0.73 0.42 -3 6 10 1.15 0.52 3 -6 -10 1.20 0.60 3 -6 -9 110.63 3.16 3 -6 -9 106.79 3.29 3 -6 -9 109.41 3.19 -3 6 9 101.83 6.76 3 -6 -8 -0.18 0.25 3 -6 -8 -0.08 0.36 -3 6 8 -0.92 0.76 3 -6 -7 50.11 1.97 3 -6 -7 50.60 2.23 3 -6 -7 50.41 2.13 -3 6 7 45.37 4.03 3 -6 -6 49.31 1.97 3 -6 -6 55.21 2.38 3 -6 -6 51.19 2.04 -3 6 6 51.40 4.02 3 -6 -5 28.22 1.50 3 -6 -5 30.51 1.76 3 -6 -5 29.52 2.62 3 -6 -5 30.95 1.54 -3 6 5 32.24 2.93 3 -6 -4 25.06 1.41 3 -6 -4 27.32 1.53 3 -6 -4 26.78 2.53 3 -6 -4 27.15 1.39 -3 6 4 25.70 2.43 3 -6 -3 104.91 5.06 -3 6 3 109.22 4.59 3 -6 -2 5.08 1.19 -3 6 2 4.59 0.92 3 -6 -1 96.95 5.00 3 -6 0 14.70 1.99 3 -6 1 0.76 0.73 3 -6 2 94.53 5.38 3 -6 3 34.30 3.29 3 -6 4 5.10 1.35 3 -6 5 167.11 3.41 3 -6 5 176.19 3.48 3 -6 5 173.08 7.20 3 -6 5 173.64 3.46 3 -6 5 172.05 3.50 3 -6 6 61.16 4.31 3 -6 6 56.32 2.11 3 -6 6 58.81 2.11 3 -6 6 60.98 2.15 3 -6 6 61.00 2.27 3 -6 7 65.78 2.34 3 -6 7 65.92 4.51 3 -6 7 71.82 2.44 3 -6 8 20.42 1.37 3 -6 8 22.70 1.46 3 -6 9 2.58 0.50 3 -6 9 2.34 0.58 3 -6 10 11.91 1.09 3 -6 10 9.99 1.07 3 -6 11 3.36 0.59 3 -6 11 3.39 0.69 3 -6 12 66.04 2.41 3 -6 12 69.26 2.64 3 -6 13 33.90 1.78 -3 6 -13 36.54 1.94 3 -6 13 35.57 1.93 3 -6 14 24.91 1.52 3 -6 14 22.98 1.37 -3 6 -14 25.34 1.51 3 -6 15 13.21 1.01 3 -6 15 11.96 0.87 -3 6 -15 13.64 1.01 3 -5 -16 1.88 0.37 -3 5 15 3.12 0.50 -3 5 14 0.88 0.38 -3 5 13 -0.19 0.36 -3 5 12 42.32 2.13 -3 5 11 0.63 0.40 3 -5 -11 0.23 0.35 -3 5 10 105.85 3.31 3 -5 -10 113.27 3.40 -3 5 10 99.53 6.82 3 -5 -10 116.26 3.18 -3 5 9 208.43 4.45 3 -5 -9 206.18 4.43 -3 5 9 200.95 9.21 3 -5 -9 204.98 4.19 3 -5 -8 49.63 2.10 3 -5 -8 45.80 1.95 -3 5 8 48.29 4.25 3 -5 -7 144.62 3.44 3 -5 -7 140.18 3.41 -3 5 7 143.77 6.83 3 -5 -6 658.69 7.45 -3 5 6 666.28 13.65 3 -5 -5 91.20 4.26 3 -5 -5 91.23 2.46 -3 5 5 85.61 4.52 3 -5 -4 1.62 0.64 -3 5 4 2.79 0.74 3 -5 -3 34.86 2.69 -3 5 3 40.07 2.53 3 -5 -2 113.06 4.88 -3 5 2 124.65 3.89 3 -5 -1 131.51 5.28 -3 5 1 140.86 3.27 3 -5 0 35.53 2.87 3 -5 1 17.70 2.08 3 -5 2 52.86 3.65 3 -5 3 733.66 13.65 3 -5 4 42.12 3.28 3 -5 5 7.32 0.71 3 -5 5 7.57 1.43 3 -5 6 6.34 0.68 3 -5 6 5.45 1.21 3 -5 6 5.50 0.67 3 -5 7 59.63 2.29 3 -5 7 62.87 4.00 3 -5 7 60.13 2.13 3 -5 7 59.93 2.10 3 -5 7 61.35 2.10 3 -5 7 56.25 2.01 3 -5 8 141.39 3.32 3 -5 8 144.99 3.48 3 -5 8 144.64 3.36 3 -5 9 2.33 0.48 -3 5 -9 2.35 0.45 3 -5 9 1.61 0.42 3 -5 10 9.09 0.94 3 -5 10 7.95 0.81 -3 5 -10 9.04 0.89 -3 5 -11 6.54 0.81 3 -5 11 5.88 0.83 -3 5 -12 112.30 3.24 3 -5 12 109.00 3.32 -3 5 -13 3.40 0.58 3 -5 13 3.52 0.61 -3 5 -14 2.16 0.48 3 -5 14 2.30 0.48 -3 5 -14 2.93 0.57 3 -5 15 0.56 0.28 -3 5 -15 0.46 0.25 3 -5 15 0.80 0.27 -3 5 -15 1.17 0.36 3 -5 16 0.77 0.27 -3 4 16 2.57 0.43 -3 4 15 1.85 0.43 -3 4 14 10.59 1.03 3 -4 -14 10.41 0.95 -3 4 13 107.71 3.33 3 -4 -13 110.03 3.24 3 -4 -12 49.71 2.23 -3 4 12 47.18 2.24 3 -4 -11 111.43 3.31 -3 4 11 107.38 3.32 3 -4 -11 110.27 3.38 -3 4 11 105.70 7.16 3 -4 -10 65.31 2.50 -3 4 10 60.50 2.41 3 -4 -10 61.64 2.46 3 -4 -10 65.06 2.34 3 -4 -9 105.00 3.10 -3 4 9 102.68 2.99 3 -4 -9 101.12 3.00 -3 4 9 95.10 6.15 3 -4 -9 103.12 2.89 3 -4 -8 188.66 3.76 3 -4 -8 188.13 3.89 -3 4 8 181.21 7.90 3 -4 -7 325.75 4.84 -3 4 7 313.07 9.57 -3 4 6 2.57 0.89 -3 4 5 115.16 4.91 3 -4 -4 10.04 1.36 -3 4 4 9.78 1.34 3 -4 -3 19.30 1.87 -3 4 3 20.61 1.67 3 -4 -2 4.52 0.93 3 -4 -2 5.13 0.42 -3 4 2 4.85 0.66 3 -4 -1 3.57 0.47 3 -4 -1 3.86 0.91 -3 4 1 2.92 0.36 3 -4 0 7.25 1.21 3 -4 0 7.81 0.79 3 -4 1 691.64 11.62 3 -4 1 656.92 8.45 3 -4 2 173.36 4.76 3 -4 2 182.05 6.06 3 -4 3 542.20 9.26 3 -4 3 563.21 10.85 3 -4 4 91.71 4.41 3 -4 5 15.32 1.81 3 -4 6 2.01 0.65 3 -4 6 1.87 0.39 3 -4 6 2.32 0.43 -3 4 -7 20.00 1.12 3 -4 7 20.11 1.21 3 -4 7 22.40 1.36 3 -4 7 20.72 1.31 3 -4 7 21.91 1.28 3 -4 7 20.91 1.22 3 -4 8 105.33 2.92 3 -4 8 105.47 2.96 3 -4 8 114.54 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10 29.37 1.71 4 -10 11 24.53 1.45 4 -10 11 22.71 1.29 4 -10 11 25.57 1.53 4 -10 12 1.16 0.37 4 -10 12 1.35 0.40 4 -10 13 0.32 0.26 -4 9 12 0.44 0.26 4 -9 -12 -0.01 0.17 -4 9 11 3.30 0.60 4 -9 -11 2.87 0.51 -4 9 10 0.80 0.40 4 -9 -10 0.14 0.23 4 -9 -10 0.64 0.39 -4 9 9 38.36 2.00 4 -9 -9 38.09 1.97 4 -9 -9 39.80 2.02 4 -9 -9 41.84 1.94 4 -9 -8 20.32 1.40 4 -9 -8 20.99 1.50 4 -9 -8 21.26 1.50 4 -9 -7 40.98 2.08 4 -9 -7 42.43 2.16 4 -9 -7 42.70 2.09 4 -9 -6 10.20 1.11 4 -9 -6 10.74 1.13 4 -9 -6 10.58 1.03 4 -9 -5 659.80 7.32 4 -9 -5 625.83 8.67 4 -9 -5 648.71 7.77 4 -9 -5 625.32 8.23 4 -9 -4 20.92 1.68 4 -9 -4 19.98 1.49 4 -9 -4 20.94 1.33 4 -9 -3 0.78 0.46 4 -9 -3 1.16 0.33 4 -9 -3 1.27 0.76 4 -9 -2 1.89 0.95 4 -9 -2 1.12 0.57 4 -9 -2 0.91 0.32 4 -9 -1 7.26 1.88 4 -9 -1 6.15 0.73 4 -9 -1 7.12 1.03 4 -9 -1 6.19 0.85 4 -9 0 2.29 0.53 4 -9 0 2.65 1.29 4 -9 0 1.86 0.57 4 -9 0 2.40 0.48 4 -9 1 62.82 2.31 4 -9 1 64.11 2.46 4 -9 1 64.09 2.59 4 -9 1 66.45 5.89 4 -9 1 63.41 2.15 4 -9 1 66.20 2.60 4 -9 2 -0.14 0.61 4 -9 2 0.31 0.28 4 -9 2 0.84 0.38 4 -9 2 0.69 0.41 4 -9 2 0.62 0.36 4 -9 2 0.61 0.29 4 -9 3 41.54 5.00 4 -9 3 42.13 2.14 4 -9 3 40.20 1.92 4 -9 3 37.83 1.93 4 -9 3 38.02 1.93 4 -9 3 38.75 1.79 4 -9 3 40.22 1.85 4 -9 4 1.80 0.75 4 -9 4 1.32 0.46 4 -9 4 1.47 0.43 4 -9 4 1.59 0.43 4 -9 4 2.90 0.59 4 -9 4 1.91 0.46 4 -9 4 2.54 0.53 4 -9 5 13.33 2.63 4 -9 5 15.52 1.26 4 -9 5 14.09 1.24 4 -9 5 15.91 1.32 4 -9 5 15.57 1.22 4 -9 6 0.21 0.30 4 -9 6 1.04 0.47 4 -9 6 0.66 0.33 4 -9 7 13.16 2.63 4 -9 7 13.37 1.23 4 -9 7 14.71 1.25 4 -9 7 13.88 1.26 4 -9 7 15.74 1.30 4 -9 8 17.06 1.40 4 -9 8 16.76 1.33 4 -9 8 19.27 1.49 4 -9 8 16.56 1.33 4 -9 9 0.97 0.46 4 -9 9 1.66 0.49 4 -9 9 1.65 0.47 4 -9 9 0.62 0.34 4 -9 10 10.65 1.14 4 -9 10 11.26 1.04 4 -9 10 12.95 1.17 4 -9 10 12.10 1.16 4 -9 11 77.55 2.82 4 -9 11 74.41 2.43 4 -9 11 77.56 2.62 4 -9 11 81.33 2.80 4 -9 12 49.88 2.14 4 -9 12 46.84 1.74 4 -9 12 48.44 1.89 4 -9 13 0.09 0.29 4 -9 13 -0.06 0.26 4 -9 14 6.17 0.62 -4 8 13 0.39 0.26 4 -8 -13 0.03 0.19 -4 8 12 1.16 0.37 4 -8 -12 0.56 0.26 -4 8 11 3.59 0.62 4 -8 -11 3.91 0.67 4 -8 -11 3.59 0.67 4 -8 -10 2.38 0.50 4 -8 -10 2.23 0.55 -4 8 10 2.37 0.56 4 -8 -10 3.69 0.73 4 -8 -9 44.99 2.12 4 -8 -9 46.17 2.32 4 -8 -9 44.35 2.23 4 -8 -8 77.57 2.93 4 -8 -8 78.16 2.98 4 -8 -7 28.30 1.70 4 -8 -7 28.86 1.78 4 -8 -7 27.54 1.72 4 -8 -6 2.31 0.56 4 -8 -6 2.55 0.56 4 -8 -6 3.54 0.63 4 -8 -5 59.75 2.60 4 -8 -5 63.13 2.42 4 -8 -5 65.23 2.59 4 -8 -4 1.88 0.52 4 -8 -4 2.50 0.47 4 -8 -4 2.72 0.55 4 -8 -4 2.03 0.43 4 -8 -4 0.73 0.65 4 -8 -3 68.31 5.04 4 -8 -3 65.18 2.14 4 -8 -3 68.24 2.94 4 -8 -3 65.53 2.27 4 -8 -2 34.43 3.67 4 -8 -2 30.29 1.48 4 -8 -2 32.25 1.96 4 -8 -2 33.16 1.56 4 -8 -1 373.90 12.19 4 -8 -1 367.84 5.10 4 -8 -1 382.53 5.64 4 -8 -1 366.28 6.22 4 -8 -1 373.78 5.85 4 -8 0 21.37 1.27 4 -8 0 23.67 1.41 4 -8 0 22.64 1.50 4 -8 0 19.37 2.85 4 -8 0 22.67 1.44 4 -8 1 21.54 1.41 4 -8 1 23.89 3.34 4 -8 1 20.45 1.25 4 -8 1 24.31 1.45 4 -8 1 21.15 1.42 4 -8 1 19.79 1.13 4 -8 1 21.33 1.14 4 -8 2 100.10 7.07 4 -8 2 94.35 2.95 4 -8 2 97.59 2.83 4 -8 2 106.37 3.11 4 -8 2 92.85 2.52 4 -8 2 92.95 2.52 4 -8 2 97.04 2.75 4 -8 3 97.83 6.98 4 -8 3 88.29 2.94 4 -8 3 91.88 2.72 4 -8 3 89.16 2.75 4 -8 3 86.97 2.75 4 -8 3 89.79 2.56 4 -8 3 88.43 2.61 4 -8 4 22.23 3.21 4 -8 4 22.69 1.54 4 -8 4 22.04 1.38 4 -8 4 21.29 1.38 4 -8 4 22.32 1.41 4 -8 4 20.68 1.30 4 -8 4 21.90 1.38 4 -8 5 -0.24 0.42 4 -8 5 0.38 0.30 4 -8 5 0.13 0.32 4 -8 5 0.22 0.26 4 -8 5 0.16 0.26 4 -8 5 0.26 0.32 4 -8 6 15.95 2.62 4 -8 6 12.42 1.14 4 -8 6 14.00 1.19 4 -8 6 13.46 1.17 4 -8 6 12.22 1.10 4 -8 7 6.43 1.70 4 -8 7 6.91 0.88 4 -8 7 6.85 0.86 4 -8 7 7.15 0.89 4 -8 7 6.97 0.87 4 -8 8 3.66 0.66 4 -8 8 3.28 0.68 4 -8 8 4.52 0.69 4 -8 8 3.40 0.66 4 -8 9 32.26 1.91 4 -8 9 37.01 1.98 4 -8 9 33.97 1.83 4 -8 9 35.28 1.95 4 -8 10 29.63 1.85 4 -8 10 30.67 1.76 4 -8 10 29.20 1.66 4 -8 10 30.64 1.81 4 -8 11 8.54 1.00 4 -8 11 9.05 0.90 4 -8 11 8.44 0.90 4 -8 11 8.11 0.97 4 -8 12 169.87 4.03 4 -8 12 171.96 3.97 4 -8 13 35.93 1.74 4 -8 13 36.02 1.69 4 -8 14 95.82 2.53 4 -8 14 94.67 2.42 -4 7 14 9.01 0.76 4 -7 -14 9.45 0.86 -4 7 13 5.96 0.71 4 -7 -13 5.86 0.77 -4 7 12 1.39 0.44 4 -7 -12 1.71 0.52 -4 7 11 0.88 0.41 4 -7 -11 2.37 0.50 4 -7 -11 2.64 0.63 -4 7 10 0.46 0.35 4 -7 -10 0.00 0.35 4 -7 -9 17.33 1.33 4 -7 -9 18.29 1.46 4 -7 -8 42.61 2.13 4 -7 -7 4.99 0.76 4 -7 -7 4.75 0.67 4 -7 -6 0.53 0.23 4 -7 -6 0.97 0.40 4 -7 -6 0.75 0.36 4 -7 -5 12.82 1.98 4 -7 -5 11.38 1.09 4 -7 -5 11.69 1.02 4 -7 -5 11.80 1.05 4 -7 -4 47.23 3.90 4 -7 -4 48.60 1.72 4 -7 -4 49.23 2.23 4 -7 -4 47.73 1.96 4 -7 -4 48.44 2.07 4 -7 -3 4.25 1.22 4 -7 -3 4.59 0.53 4 -7 -3 4.78 0.77 4 -7 -3 3.84 0.53 4 -7 -2 70.83 2.07 4 -7 -2 68.42 2.62 4 -7 -2 69.94 2.22 4 -7 -2 70.46 4.89 4 -7 -1 1326.16 21.33 4 -7 -1 1357.89 9.10 4 -7 -1 1341.98 9.92 4 -7 -1 1334.06 10.92 4 -7 -1 1313.05 9.19 4 -7 -1 1336.50 10.21 4 -7 0 477.97 13.07 4 -7 0 484.16 5.51 4 -7 0 483.10 5.92 4 -7 0 466.60 6.27 4 -7 0 475.40 6.04 4 -7 1 938.33 19.01 4 -7 1 956.82 8.27 4 -7 1 963.50 7.96 4 -7 1 968.56 8.83 4 -7 1 945.58 7.35 4 -7 1 944.94 8.44 4 -7 2 50.47 4.58 4 -7 2 53.08 2.01 4 -7 2 53.28 2.08 4 -7 2 54.48 1.95 4 -7 2 54.55 1.98 4 -7 2 57.25 1.83 4 -7 2 53.14 1.81 4 -7 3 1.95 0.42 4 -7 3 2.64 1.13 4 -7 3 2.36 0.45 4 -7 3 1.59 0.39 4 -7 3 1.65 0.38 4 -7 3 2.24 0.44 4 -7 3 2.59 0.45 4 -7 4 11.79 2.23 4 -7 4 8.94 0.86 4 -7 4 9.01 0.85 4 -7 4 9.78 0.86 4 -7 4 9.02 0.86 4 -7 5 3.18 1.15 4 -7 5 2.65 0.52 4 -7 5 2.69 0.50 4 -7 5 3.25 0.56 4 -7 5 2.29 0.48 4 -7 6 0.99 0.69 4 -7 6 0.00 0.24 4 -7 6 0.29 0.26 4 -7 6 0.06 0.28 4 -7 6 0.38 0.33 4 -7 7 3.30 1.20 4 -7 7 4.52 0.69 4 -7 7 4.70 0.69 4 -7 7 3.92 0.68 4 -7 8 44.66 2.15 4 -7 8 49.91 2.26 4 -7 8 47.16 2.18 4 -7 9 31.53 1.77 4 -7 9 29.76 1.81 4 -7 9 30.08 1.80 4 -7 10 43.38 2.19 4 -7 10 44.42 2.18 4 -7 11 11.53 1.14 4 -7 11 11.64 1.14 4 -7 12 73.19 2.36 4 -7 12 75.64 2.76 4 -7 12 80.29 2.78 -4 7 -12 81.84 2.70 4 -7 13 51.82 2.14 4 -7 13 56.94 2.17 -4 7 -13 57.87 2.14 4 -7 14 42.38 1.74 4 -7 14 40.53 1.64 -4 7 -14 40.69 1.62 4 -6 -15 17.29 1.11 -4 6 14 34.18 1.60 4 -6 -14 33.13 1.74 -4 6 13 3.86 0.62 -4 6 12 0.02 0.31 4 -6 -11 26.17 1.73 -4 6 11 25.72 1.65 4 -6 -11 27.95 1.61 4 -6 -10 16.62 1.40 -4 6 10 13.88 1.23 4 -6 -10 14.38 1.21 4 -6 -9 1.63 0.48 4 -6 -9 1.38 0.36 4 -6 -8 3.72 0.61 -4 6 8 5.85 1.57 4 -6 -7 65.17 2.32 4 -6 -7 67.01 2.49 -4 6 7 65.84 4.82 4 -6 -6 39.76 1.85 4 -6 -6 41.13 1.88 4 -6 -5 1.41 0.39 4 -6 -5 1.63 0.41 4 -6 -4 20.95 2.41 4 -6 -4 19.60 1.29 4 -6 -4 18.11 1.17 4 -6 -4 20.18 1.24 4 -6 -3 41.99 3.46 4 -6 -3 46.43 1.98 4 -6 -3 47.20 1.80 4 -6 -2 49.42 2.03 4 -6 -2 49.82 3.84 4 -6 -1 1292.18 19.61 4 -6 0 2218.29 26.31 4 -6 1 1138.77 19.26 4 -6 2 1158.35 19.87 4 -6 3 287.57 10.00 4 -6 3 286.24 4.19 4 -6 3 283.45 4.17 4 -6 4 26.34 3.01 4 -6 4 23.88 1.28 4 -6 4 25.32 1.30 4 -6 4 24.28 1.24 4 -6 4 24.94 1.33 4 -6 4 24.85 1.32 4 -6 5 -0.67 0.56 4 -6 5 0.25 0.19 4 -6 5 -0.27 0.25 4 -6 5 0.08 0.19 4 -6 5 -0.01 0.25 4 -6 5 0.30 0.31 4 -6 6 3.18 0.55 4 -6 6 3.28 0.49 4 -6 6 4.19 0.64 4 -6 6 3.67 0.59 4 -6 6 3.22 0.54 4 -6 6 3.47 1.16 4 -6 6 3.18 0.55 4 -6 6 3.27 0.61 4 -6 7 0.42 0.37 4 -6 7 -0.02 0.24 4 -6 7 0.07 0.24 4 -6 7 -0.10 0.24 4 -6 7 0.45 0.37 4 -6 7 0.00 0.27 4 -6 7 0.02 0.39 4 -6 8 0.00 0.36 4 -6 8 0.02 0.23 4 -6 8 1.04 0.52 4 -6 8 0.70 0.41 4 -6 9 1.05 0.43 4 -6 9 0.71 0.44 4 -6 10 7.38 0.97 4 -6 10 6.49 0.90 4 -6 11 35.10 1.96 4 -6 11 36.40 1.97 4 -6 12 8.45 0.94 4 -6 12 8.01 0.93 4 -6 13 22.38 1.44 4 -6 13 23.70 1.44 4 -6 14 13.23 0.99 4 -6 14 14.41 1.01 -4 6 -14 15.02 1.06 4 -5 -16 7.79 0.72 -4 5 15 2.54 0.45 4 -5 -15 3.00 0.56 -4 5 14 0.30 0.24 -4 5 13 113.90 3.26 -4 5 12 6.53 0.84 -4 5 11 288.91 5.37 4 -5 -11 301.57 5.71 4 -5 -11 307.39 5.41 -4 5 10 32.97 1.80 4 -5 -10 34.42 1.93 -4 5 10 29.12 3.62 4 -5 -10 34.04 1.83 4 -5 -9 0.68 0.45 4 -5 -9 0.38 0.26 -4 5 9 0.78 0.41 4 -5 -8 38.39 1.90 -4 5 8 38.80 3.71 4 -5 -7 56.35 2.17 -4 5 7 57.34 4.36 4 -5 -6 8.09 0.79 4 -5 -6 8.72 0.83 -4 5 6 10.88 1.81 4 -5 -5 509.65 5.96 -4 5 5 495.05 10.87 4 -5 -4 239.23 7.82 -4 5 4 246.11 6.45 4 -5 -3 639.44 12.74 4 -5 -2 163.66 6.55 4 -5 -1 38.46 3.23 4 -5 0 253.17 8.26 4 -5 0 276.41 5.42 4 -5 1 23.68 1.78 4 -5 1 15.60 2.15 4 -5 2 1118.09 13.48 4 -5 2 1051.47 17.44 4 -5 3 281.70 9.15 4 -5 4 39.97 3.46 4 -5 4 44.75 1.73 4 -5 4 42.10 1.59 4 -5 4 43.08 1.64 4 -5 5 68.47 4.51 4 -5 5 63.76 2.07 4 -5 5 67.38 2.23 4 -5 5 68.89 2.12 4 -5 5 68.99 2.20 4 -5 6 62.70 4.26 4 -5 6 55.66 2.14 4 -5 6 60.53 2.21 4 -5 6 59.67 2.09 4 -5 6 59.88 2.23 4 -5 7 13.99 1.16 4 -5 7 13.78 1.12 4 -5 7 13.53 1.11 4 -5 7 13.88 1.18 4 -5 8 31.45 1.74 -4 5 -8 29.64 1.48 4 -5 8 29.14 1.64 4 -5 8 31.10 1.71 -4 5 -9 11.59 0.96 4 -5 9 10.40 1.02 4 -5 9 10.78 1.04 4 -5 10 24.31 1.55 -4 5 -10 24.80 1.47 -4 5 -11 0.62 0.28 4 -5 11 0.37 0.37 -4 5 -12 7.21 0.79 4 -5 12 6.55 0.84 4 -5 13 1.55 0.43 -4 5 -13 1.61 0.42 4 -5 13 0.95 0.36 4 -5 14 5.36 0.65 4 -5 14 4.91 0.63 -4 5 -15 -0.01 0.17 4 -4 -16 13.80 1.02 -4 4 15 0.67 0.29 -4 4 14 3.54 0.60 -4 4 13 84.25 2.81 4 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4 -6 415.46 5.13 4 -4 6 414.50 5.65 4 -4 7 1.18 0.37 -4 4 -7 1.47 0.36 4 -4 7 1.10 0.40 4 -4 7 1.50 0.46 4 -4 7 1.20 0.45 4 -4 7 1.83 0.47 4 -4 8 19.77 1.32 4 -4 8 19.18 1.42 4 -4 8 20.27 1.38 -4 4 -8 20.52 1.30 4 -4 9 14.78 1.26 4 -4 9 15.93 1.26 -4 4 -9 14.06 1.11 -4 4 -10 1.96 0.50 4 -4 10 1.86 0.48 -4 4 -11 0.12 0.23 4 -4 11 0.57 0.40 -4 4 -12 11.84 1.05 4 -4 12 10.67 0.96 -4 4 -13 0.35 0.27 4 -4 13 0.33 0.30 -4 4 -14 7.00 0.71 4 -4 14 6.17 0.68 4 -4 14 6.60 0.70 -4 4 -15 26.62 1.27 4 -3 -16 17.27 1.20 4 -3 -16 16.12 1.07 4 -3 -15 0.48 0.32 -4 3 14 5.34 0.74 4 -3 -14 5.07 0.74 4 -3 -13 6.11 0.84 -4 3 13 7.35 0.88 4 -3 -12 2.79 0.59 -4 3 12 3.26 0.60 -4 3 12 3.55 1.40 -4 3 11 14.17 1.11 4 -3 -11 15.40 1.23 -4 3 11 13.69 2.65 4 -3 -11 13.59 1.28 -4 3 10 94.11 2.73 4 -3 -10 92.30 2.99 4 -3 -10 97.63 2.98 -4 3 10 91.87 6.29 4 -3 -10 89.93 3.27 4 -3 -9 336.20 5.37 -4 3 9 333.06 11.18 4 -3 -9 332.88 5.34 4 -3 -9 335.27 5.79 4 -3 -8 148.13 3.39 -4 3 8 140.64 6.82 4 -3 -8 149.20 3.43 4 -3 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5 -7 34.55 3.84 -4 -5 7 31.22 1.72 -4 -5 7 33.53 1.74 -4 -5 6 5.28 0.66 4 5 -6 5.59 1.52 -4 -5 6 7.19 0.83 -4 -5 6 6.09 0.75 -4 -5 5 14.32 1.09 -4 -5 5 15.43 1.17 4 5 -5 14.05 2.32 -4 -5 5 15.64 1.13 -4 -5 4 5.98 0.78 4 5 -4 6.18 1.60 -4 -5 4 6.38 0.76 -4 -5 4 6.71 0.74 -4 -5 3 0.04 0.32 -4 -5 3 0.19 0.26 -4 -5 3 0.23 0.24 4 5 -3 -0.16 0.50 -4 -5 3 0.39 0.32 -4 -5 2 23.17 1.50 4 5 -2 21.46 2.72 -4 -5 2 22.65 1.28 -4 -5 2 23.74 1.40 -4 -5 2 22.33 1.35 -4 -5 1 32.89 1.83 4 5 -1 33.93 3.49 -4 -5 1 33.70 1.68 -4 -5 1 32.96 1.67 -4 -5 0 43.00 2.10 4 5 0 42.28 3.80 -4 -5 0 43.15 1.89 -4 -5 0 44.60 1.97 -4 -5 -1 133.30 3.73 -4 -5 -1 131.84 3.29 4 5 1 122.95 6.69 -4 -5 -1 136.86 3.50 -4 -5 -2 20.65 1.50 -4 -5 -2 20.91 1.31 -4 -5 -2 20.52 2.92 4 5 2 19.25 2.62 -4 -5 -3 32.86 1.84 -4 -5 -3 37.63 1.74 -4 -5 -4 21.82 1.47 -4 -5 -4 21.22 1.42 -4 -5 -5 203.22 4.30 -4 -5 -5 198.97 4.27 -4 -5 -6 0.93 0.32 -4 -5 -6 0.19 0.25 -4 -5 -7 -0.34 0.27 -4 -5 -8 2.68 0.46 4 5 9 -0.16 0.28 -4 -5 -9 -0.04 0.20 -4 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3.67 5 -10 0 147.32 4.37 5 -10 1 4.26 0.75 5 -10 1 3.75 0.74 5 -10 1 5.02 0.74 5 -10 1 4.25 1.67 5 -10 2 24.58 1.58 5 -10 2 25.45 1.68 5 -10 2 25.16 1.74 5 -10 2 24.45 4.22 5 -10 2 25.44 1.45 5 -10 3 18.91 3.68 5 -10 3 18.92 1.43 5 -10 3 18.16 1.42 5 -10 3 19.10 1.30 5 -10 3 17.54 1.33 5 -10 4 2.26 0.55 5 -10 4 1.94 0.48 5 -10 4 1.90 0.44 5 -10 5 7.66 0.94 5 -10 5 6.95 0.92 5 -10 5 6.54 0.82 5 -10 6 6.66 0.92 5 -10 6 6.25 0.87 5 -10 6 6.55 0.84 5 -10 7 1.86 0.50 5 -10 7 1.23 0.50 5 -10 7 1.62 0.44 5 -10 8 1.04 0.43 5 -10 8 1.67 0.46 5 -10 8 1.67 0.51 5 -10 9 0.62 0.30 5 -10 9 0.53 0.30 5 -10 9 0.54 0.34 5 -10 10 0.97 0.34 5 -10 10 1.13 0.40 5 -10 11 9.62 0.81 5 -10 11 11.17 0.95 5 -10 12 7.68 0.73 -5 9 12 0.50 0.24 5 -9 -12 0.23 0.21 5 -9 -11 0.63 0.28 -5 9 11 0.49 0.30 5 -9 -11 0.58 0.33 5 -9 -11 1.08 0.41 5 -9 -10 -0.44 0.33 -5 9 10 0.62 0.38 5 -9 -10 0.39 0.28 -5 9 9 13.97 1.17 5 -9 -9 12.44 1.20 5 -9 -9 13.66 1.23 5 -9 -9 11.82 1.08 5 -9 -8 13.97 1.24 5 -9 -8 15.94 1.36 5 -9 -7 42.66 2.15 5 -9 -7 43.33 2.22 5 -9 -7 42.10 2.13 5 -9 -6 5.22 0.81 5 -9 -6 4.86 0.80 5 -9 -6 6.19 0.85 5 -9 -5 0.50 0.39 5 -9 -5 0.16 0.30 5 -9 -5 0.23 0.29 5 -9 -4 0.25 0.35 5 -9 -4 0.07 0.21 5 -9 -4 0.25 0.28 5 -9 -4 0.32 0.28 5 -9 -3 5.80 1.65 5 -9 -3 5.83 0.69 5 -9 -3 5.83 1.06 5 -9 -3 4.89 0.67 5 -9 -3 5.36 0.81 5 -9 -2 145.27 3.41 5 -9 -2 146.96 4.57 5 -9 -2 149.28 3.55 5 -9 -1 6.62 1.73 5 -9 -1 9.51 0.92 5 -9 -1 9.70 1.15 5 -9 0 145.14 8.83 5 -9 0 137.25 3.44 5 -9 0 142.76 3.75 5 -9 0 138.20 4.08 5 -9 1 49.75 5.44 5 -9 1 48.07 2.08 5 -9 1 48.02 2.19 5 -9 1 48.48 2.35 5 -9 1 49.52 1.95 5 -9 2 385.94 5.96 5 -9 2 382.83 6.12 5 -9 2 374.12 6.44 5 -9 2 399.79 5.49 5 -9 2 393.05 5.73 5 -9 3 61.14 2.42 5 -9 3 61.73 6.13 5 -9 3 54.77 2.35 5 -9 3 58.37 2.20 5 -9 3 58.43 2.33 5 -9 4 41.86 4.91 5 -9 4 39.15 2.00 5 -9 4 37.05 1.97 5 -9 4 37.18 1.81 5 -9 4 35.39 1.92 5 -9 5 11.31 2.55 5 -9 5 14.14 1.25 5 -9 5 13.72 1.25 5 -9 5 12.49 1.08 5 -9 5 13.44 1.26 5 -9 6 1.02 0.41 5 -9 6 1.16 0.49 5 -9 6 1.13 0.40 5 -9 7 14.86 1.31 5 -9 7 13.16 1.19 5 -9 7 12.43 1.16 5 -9 8 26.88 1.72 5 -9 8 28.23 1.72 5 -9 8 25.02 1.62 5 -9 8 25.83 1.63 5 -9 9 1.76 0.51 5 -9 9 1.52 0.49 5 -9 9 1.47 0.45 5 -9 10 0.46 0.37 5 -9 10 -0.03 0.28 5 -9 10 -0.09 0.34 5 -9 11 3.27 0.59 5 -9 11 3.51 0.55 5 -9 11 3.70 0.64 5 -9 12 5.32 0.58 5 -9 12 7.36 0.77 5 -9 13 12.27 0.87 5 -8 -13 0.35 0.25 -5 8 12 41.27 1.73 5 -8 -12 41.99 1.99 -5 8 11 23.85 1.45 5 -8 -11 28.25 1.68 5 -8 -11 24.66 1.65 5 -8 -11 25.46 1.48 -5 8 10 36.61 1.88 5 -8 -10 43.43 2.16 5 -8 -10 40.66 2.21 5 -8 -10 38.38 1.96 5 -8 -9 -0.38 0.51 5 -8 -9 -0.01 0.42 -5 8 9 0.13 0.30 5 -8 -9 0.36 0.32 5 -8 -8 13.53 1.23 5 -8 -8 15.17 1.34 5 -8 -7 4.02 0.73 5 -8 -7 4.14 0.67 5 -8 -7 3.71 0.69 5 -8 -6 19.50 1.49 5 -8 -6 18.51 1.44 5 -8 -6 18.66 1.43 5 -8 -5 5.36 0.82 5 -8 -5 5.66 0.81 5 -8 -5 5.26 0.75 5 -8 -4 4.77 1.46 5 -8 -4 5.09 0.82 5 -8 -4 4.65 0.70 5 -8 -4 4.82 0.68 5 -8 -3 3.08 1.22 5 -8 -3 3.75 0.74 5 -8 -3 3.09 0.49 5 -8 -3 2.94 0.53 5 -8 -2 40.27 4.18 5 -8 -2 37.36 1.64 5 -8 -2 35.10 2.09 5 -8 -2 39.04 1.80 5 -8 -1 136.34 3.21 5 -8 -1 142.35 4.02 5 -8 -1 139.65 3.31 5 -8 0 34.44 4.06 5 -8 0 35.77 1.66 5 -8 0 33.96 1.73 5 -8 0 35.06 1.94 5 -8 0 35.30 1.65 5 -8 0 35.57 1.56 5 -8 1 0.25 0.21 5 -8 1 0.52 1.02 5 -8 1 0.59 0.31 5 -8 1 0.59 0.37 5 -8 1 0.54 0.30 5 -8 1 0.33 0.23 5 -8 2 10.35 2.49 5 -8 2 8.45 0.88 5 -8 2 7.82 0.84 5 -8 2 8.38 0.80 5 -8 2 7.68 0.75 5 -8 2 8.69 0.85 5 -8 3 25.83 3.66 5 -8 3 30.24 1.64 5 -8 3 31.08 1.67 5 -8 3 27.02 1.41 5 -8 3 28.18 1.47 5 -8 3 28.92 1.56 5 -8 4 37.17 4.35 5 -8 4 40.64 1.93 5 -8 4 37.58 1.78 5 -8 4 39.06 1.91 5 -8 5 6.43 1.86 5 -8 5 6.93 0.83 5 -8 5 7.96 0.89 5 -8 5 7.84 0.85 5 -8 5 7.04 0.91 5 -8 6 25.15 3.47 5 -8 6 27.71 1.67 5 -8 6 29.06 1.73 5 -8 6 27.82 1.66 5 -8 6 28.60 1.84 5 -8 7 17.26 1.36 5 -8 7 20.09 1.48 5 -8 7 16.65 1.33 5 -8 8 51.76 2.34 5 -8 8 55.70 2.42 5 -8 9 3.24 0.62 5 -8 9 4.01 0.71 5 -8 10 2.79 0.61 5 -8 10 2.66 0.56 5 -8 10 2.90 0.61 5 -8 11 14.55 1.17 5 -8 11 13.69 1.08 5 -8 11 15.56 1.23 5 -8 12 8.24 0.82 5 -8 12 7.72 0.73 5 -8 12 8.23 0.83 5 -8 13 0.11 0.21 5 -8 13 0.12 0.23 5 -7 -14 11.74 0.95 5 -7 -13 8.51 0.93 -5 7 12 80.67 2.57 5 -7 -12 80.85 3.03 5 -7 -12 84.97 2.61 -5 7 11 71.53 2.56 5 -7 -11 75.89 2.82 5 -7 -11 75.39 3.08 5 -7 -11 70.40 2.61 -5 7 10 117.47 3.36 5 -7 -10 115.30 3.61 5 -7 -10 121.19 3.97 5 -7 -10 111.59 3.43 -5 7 9 113.45 3.29 5 -7 -9 108.93 3.49 5 -7 -9 115.72 3.81 5 -7 -9 110.55 3.50 5 -7 -8 11.77 1.12 5 -7 -8 14.00 1.30 5 -7 -7 81.96 2.82 5 -7 -7 78.49 2.87 5 -7 -7 77.44 2.92 5 -7 -6 63.77 2.55 5 -7 -6 61.13 2.47 5 -7 -6 65.34 2.59 5 -7 -5 0.17 0.30 5 -7 -5 0.35 0.32 5 -7 -5 0.20 0.26 5 -7 -4 6.00 1.57 5 -7 -4 5.86 0.82 5 -7 -4 5.95 0.77 5 -7 -4 7.45 0.84 5 -7 -3 24.81 1.67 5 -7 -3 25.53 1.46 5 -7 -2 30.46 3.46 5 -7 -2 30.68 1.40 5 -7 -2 29.27 1.76 5 -7 -2 29.26 1.54 5 -7 -1 6.55 1.62 5 -7 -1 5.80 0.64 5 -7 -1 5.26 0.78 5 -7 -1 5.24 0.65 5 -7 0 171.26 8.47 5 -7 0 168.53 3.61 5 -7 0 167.90 4.05 5 -7 0 170.23 3.44 5 -7 0 173.27 3.55 5 -7 1 15.44 2.58 5 -7 1 14.92 1.07 5 -7 1 14.86 1.06 5 -7 1 15.85 1.09 5 -7 1 15.37 1.04 5 -7 2 23.59 3.32 5 -7 2 24.82 1.38 5 -7 2 22.68 1.29 5 -7 2 23.01 1.23 5 -7 2 23.45 1.32 5 -7 3 31.95 3.84 5 -7 3 31.13 1.55 5 -7 3 29.97 1.49 5 -7 3 31.17 1.50 5 -7 3 30.04 1.54 5 -7 4 14.34 2.63 5 -7 4 11.76 1.00 5 -7 4 12.64 1.01 5 -7 4 12.27 0.98 5 -7 4 11.59 0.99 5 -7 4 12.76 1.05 5 -7 5 9.68 0.93 5 -7 5 8.98 0.88 5 -7 5 9.75 0.95 5 -7 5 9.76 0.99 5 -7 5 11.09 2.19 5 -7 6 11.13 2.16 5 -7 6 11.01 1.03 5 -7 6 9.97 0.94 5 -7 6 11.94 1.09 5 -7 6 10.71 1.10 5 -7 7 0.59 0.36 5 -7 7 0.34 0.29 5 -7 7 0.72 0.41 5 -7 7 0.98 0.43 5 -7 7 0.40 0.44 5 -7 8 5.85 0.81 5 -7 8 5.98 0.76 5 -7 8 5.77 0.81 5 -7 8 7.06 0.91 5 -7 9 11.21 1.12 5 -7 9 12.37 1.21 5 -7 10 17.57 1.35 5 -7 10 18.42 1.43 5 -7 11 18.48 1.32 5 -7 11 20.31 1.43 5 -7 12 0.65 0.32 5 -7 12 0.01 0.20 5 -7 12 0.16 0.27 -5 7 -12 0.39 0.24 5 -7 13 -0.04 0.20 5 -7 13 0.48 0.32 5 -6 -15 0.21 0.27 5 -6 -14 8.98 0.93 5 -6 -13 82.72 3.03 5 -6 -12 323.60 6.40 5 -6 -12 314.63 5.35 -5 6 11 170.94 3.95 5 -6 -11 173.95 4.43 5 -6 -11 180.12 4.98 5 -6 -11 169.86 4.18 -5 6 10 16.95 1.26 5 -6 -10 19.03 1.49 5 -6 -10 16.69 1.58 5 -6 -10 16.28 1.34 5 -6 -9 5.62 0.84 -5 6 9 6.05 0.74 5 -6 -9 4.57 0.73 5 -6 -9 5.83 0.92 5 -6 -8 11.03 1.11 5 -6 -8 12.14 1.12 5 -6 -8 12.75 1.25 5 -6 -7 13.75 1.17 5 -6 -7 14.68 1.26 5 -6 -6 4.99 0.70 5 -6 -6 5.05 0.69 5 -6 -6 5.05 0.73 5 -6 -5 5.73 0.76 5 -6 -5 6.64 0.74 5 -6 -5 6.61 0.78 5 -6 -4 32.81 1.76 5 -6 -4 35.33 1.71 5 -6 -4 35.25 1.66 5 -6 -3 31.28 3.31 5 -6 -3 33.05 1.77 5 -6 -3 33.14 1.62 5 -6 -3 32.91 1.56 5 -6 -2 507.36 6.82 5 -6 -2 513.68 6.16 5 -6 -1 0.01 0.76 5 -6 -1 0.30 0.30 5 -6 -1 0.56 0.27 5 -6 -1 0.25 0.19 5 -6 0 0.19 0.71 5 -6 0 0.85 0.27 5 -6 0 1.05 0.31 5 -6 1 14.38 2.40 5 -6 1 13.77 0.93 5 -6 1 12.75 0.96 5 -6 2 165.89 8.08 5 -6 2 164.82 3.40 5 -6 2 152.04 3.04 5 -6 2 158.42 3.31 5 -6 3 8.52 1.90 5 -6 3 8.01 0.75 5 -6 3 7.20 0.67 5 -6 3 8.03 0.78 5 -6 3 8.89 0.80 5 -6 3 8.38 0.82 5 -6 4 11.30 2.15 5 -6 4 12.37 0.96 5 -6 4 13.98 1.08 5 -6 4 13.74 0.99 5 -6 4 12.83 1.01 5 -6 4 12.85 1.01 5 -6 4 13.48 1.05 5 -6 5 4.03 0.59 5 -6 5 4.71 0.70 5 -6 5 4.20 0.60 5 -6 5 3.38 0.58 5 -6 5 4.74 1.41 5 -6 5 4.02 0.63 5 -6 6 91.37 2.81 5 -6 6 90.72 2.90 5 -6 6 93.57 2.96 5 -6 6 87.12 2.75 5 -6 6 91.34 3.01 5 -6 7 34.27 1.82 5 -6 7 33.77 1.87 5 -6 7 35.57 1.90 5 -6 7 35.56 1.85 5 -6 7 36.11 2.00 5 -6 8 55.28 2.34 5 -6 8 54.89 2.33 5 -6 8 54.14 2.39 5 -6 8 55.52 2.38 5 -6 9 90.81 3.03 5 -6 9 93.72 3.02 5 -6 9 95.11 3.18 5 -6 10 146.61 3.79 5 -6 10 150.46 3.95 5 -6 11 8.84 0.92 5 -6 11 8.70 0.97 5 -6 12 3.35 0.57 5 -6 12 3.91 0.62 5 -6 13 0.27 0.21 5 -6 13 0.32 0.20 5 -6 13 0.44 0.29 5 -6 14 0.44 0.19 5 -5 -16 38.23 1.54 5 -5 -15 8.76 0.87 5 -5 -14 11.22 1.09 5 -5 -13 63.27 2.76 5 -5 -12 181.83 4.95 5 -5 -11 36.47 2.04 5 -5 -11 37.68 2.04 5 -5 -10 32.97 1.95 5 -5 -10 31.57 1.85 5 -5 -9 5.26 0.78 5 -5 -9 5.50 0.85 5 -5 -8 19.65 1.39 5 -5 -8 19.07 1.47 5 -5 -8 18.83 1.36 5 -5 -7 156.30 3.44 5 -5 -7 149.22 3.59 5 -5 -7 150.04 3.88 5 -5 -6 2.04 0.42 5 -5 -6 1.85 0.39 5 -5 -6 2.32 0.50 5 -5 -5 0.65 0.29 5 -5 -5 0.42 0.24 5 -5 -5 0.69 0.36 5 -5 -4 656.11 7.12 5 -5 -4 650.29 6.67 5 -5 -3 306.57 4.73 5 -5 -2 198.04 3.72 5 -5 -1 22.00 2.71 5 -5 -1 24.79 1.30 5 -5 0 106.73 5.96 5 -5 0 107.44 4.26 5 -5 0 103.17 2.62 5 -5 1 -0.09 0.49 5 -5 1 0.54 0.43 5 -5 1 0.51 0.31 5 -5 1 0.60 0.27 5 -5 2 2.06 0.89 5 -5 2 1.52 0.71 5 -5 2 3.12 0.49 5 -5 2 2.67 0.46 5 -5 2 3.10 0.47 5 -5 3 48.94 4.15 5 -5 3 49.79 3.59 5 -5 3 52.10 2.00 5 -5 3 51.93 1.84 5 -5 3 51.39 1.92 5 -5 3 49.47 1.85 5 -5 4 102.81 5.50 5 -5 4 109.59 2.97 5 -5 4 107.14 2.75 5 -5 4 107.02 2.84 5 -5 4 106.53 2.81 5 -5 5 32.64 1.70 5 -5 5 30.20 1.56 5 -5 5 32.85 1.65 5 -5 5 30.51 1.60 5 -5 6 135.34 3.33 5 -5 6 131.56 3.50 5 -5 6 133.01 3.54 5 -5 6 131.97 3.43 5 -5 6 131.71 3.50 5 -5 7 1.07 0.32 5 -5 7 0.12 0.36 5 -5 7 0.45 0.39 5 -5 7 0.25 0.36 5 -5 8 20.26 1.42 5 -5 8 19.98 1.50 5 -5 8 20.47 1.46 5 -5 8 20.44 1.54 -5 5 -9 95.22 2.81 5 -5 9 95.75 3.05 5 -5 9 93.21 3.13 5 -5 9 96.85 3.14 -5 5 -10 74.13 2.49 5 -5 10 72.81 2.64 5 -5 10 71.27 2.63 5 -5 11 -0.06 0.27 -5 5 -11 0.03 0.20 5 -5 11 -0.26 0.36 5 -5 12 18.55 1.21 5 -5 12 19.03 1.31 5 -5 13 2.12 0.39 5 -5 13 3.03 0.51 5 -5 14 5.41 0.56 -5 4 16 -0.16 0.24 5 -4 -16 -0.27 0.25 5 -4 -15 8.93 0.93 5 -4 -14 43.22 2.16 5 -4 -13 0.62 0.50 5 -4 -11 5.08 0.81 5 -4 -11 4.34 0.81 5 -4 -10 24.51 1.62 5 -4 -10 21.10 1.50 -5 4 10 23.26 3.29 5 -4 -9 135.16 3.63 5 -4 -9 147.01 3.63 -5 4 9 145.37 7.71 5 -4 -9 140.34 3.74 5 -4 -8 0.24 0.28 5 -4 -8 0.37 0.25 5 -4 -8 0.25 0.28 5 -4 -8 0.58 0.39 -5 4 8 0.82 0.50 5 -4 -7 201.62 4.04 5 -4 -7 215.86 4.15 5 -4 -7 210.42 4.43 -5 4 7 224.70 8.15 5 -4 -7 217.39 4.36 5 -4 -6 120.53 3.00 5 -4 -6 117.58 2.90 5 -4 -6 122.49 3.22 5 -4 -5 59.75 2.05 5 -4 -5 58.33 1.94 5 -4 -5 56.25 2.08 5 -4 -4 80.23 2.32 5 -4 -4 80.00 2.38 5 -4 -3 51.15 2.79 5 -4 -3 49.85 1.84 5 -4 -2 23.79 1.98 5 -4 -1 240.73 6.43 5 -4 0 863.25 12.84 5 -4 1 134.96 5.35 5 -4 1 135.71 2.96 5 -4 2 2.22 0.82 5 -4 2 3.23 0.51 5 -4 2 3.82 0.56 5 -4 2 3.42 0.48 5 -4 3 1.65 0.40 5 -4 3 1.00 0.76 5 -4 3 1.25 0.34 5 -4 3 1.45 0.36 5 -4 3 1.52 0.36 5 -4 4 13.88 2.04 5 -4 4 14.82 1.11 5 -4 4 13.43 1.00 5 -4 4 13.93 1.07 5 -4 4 13.49 0.97 5 -4 5 36.35 3.50 -5 4 -5 36.20 1.56 5 -4 5 37.92 1.81 5 -4 5 34.98 1.70 5 -4 5 36.04 1.77 5 -4 5 35.96 1.68 5 -4 6 56.33 2.32 5 -4 6 55.34 2.29 5 -4 6 59.56 2.35 -5 4 -6 57.36 2.08 5 -4 6 56.50 2.22 -5 4 -7 33.65 1.67 5 -4 7 33.25 1.93 5 -4 7 33.70 1.84 5 -4 7 34.67 1.92 5 -4 7 34.03 1.86 -5 4 -8 62.68 2.35 5 -4 8 63.09 2.70 5 -4 8 63.38 2.55 -5 4 -9 2.04 0.48 5 -4 9 1.89 0.55 5 -4 9 1.60 0.53 -5 4 -10 0.30 0.25 5 -4 10 0.06 0.39 -5 4 -11 6.09 0.76 5 -4 11 5.75 0.75 -5 4 -12 35.79 1.66 5 -4 12 37.23 1.67 5 -4 12 36.21 1.77 -5 4 -13 7.68 0.71 5 -4 13 7.09 0.72 -5 3 17 5.80 0.59 -5 3 16 8.71 0.76 5 -3 -16 8.33 0.81 5 -3 -15 1.41 0.42 5 -3 -15 1.49 0.44 5 -3 -14 56.18 2.48 5 -3 -14 56.92 2.42 5 -3 -13 104.51 3.59 5 -3 -13 106.42 3.47 5 -3 -12 7.07 0.98 5 -3 -12 6.14 0.83 5 -3 -11 1.38 0.45 5 -3 -11 0.71 0.31 -5 3 11 2.23 1.11 5 -3 -10 0.55 0.41 5 -3 -10 0.40 0.38 5 -3 -10 0.27 0.22 5 -3 -10 0.08 0.34 -5 3 10 -0.20 0.58 5 -3 -9 143.69 3.61 5 -3 -9 147.08 3.77 5 -3 -9 144.87 4.01 -5 3 9 158.85 8.00 5 -3 -9 148.96 3.79 5 -3 -9 148.38 3.78 5 -3 -8 71.76 2.43 5 -3 -8 75.03 2.59 5 -3 -8 71.93 2.65 5 -3 -8 79.05 2.66 5 -3 -8 75.30 2.50 5 -3 -7 271.91 4.44 5 -3 -7 276.80 4.78 5 -3 -7 271.21 4.85 -5 3 7 286.36 9.15 5 -3 -7 264.13 4.41 5 -3 -7 279.96 4.82 5 -3 -6 383.60 8.95 5 -3 -6 360.46 4.83 5 -3 -6 378.73 5.38 5 -3 -6 364.65 5.30 -5 3 6 385.66 9.50 5 -3 -6 364.62 5.27 5 -3 -5 19.71 1.19 5 -3 -5 19.00 1.17 5 -3 -5 18.41 1.95 -5 3 5 18.85 1.92 5 -3 -5 19.31 1.16 5 -3 -4 11.16 1.46 5 -3 -3 132.08 5.01 5 -3 -2 1091.40 14.51 5 -3 -1 849.06 12.99 5 -3 0 10.06 1.55 5 -3 1 0.39 0.41 5 -3 1 0.81 0.26 5 -3 2 94.24 4.92 5 -3 2 89.29 2.47 5 -3 2 96.87 2.46 5 -3 2 90.63 2.46 5 -3 3 44.90 3.62 5 -3 3 49.01 1.94 5 -3 3 52.43 1.95 5 -3 3 47.44 1.74 5 -3 4 8.39 1.67 5 -3 4 9.84 0.92 5 -3 4 9.11 0.87 5 -3 4 8.97 0.86 5 -3 4 9.36 0.79 5 -3 5 55.88 4.51 -5 3 -5 58.51 2.06 5 -3 5 56.62 2.23 5 -3 5 57.89 2.20 5 -3 5 57.61 2.30 5 -3 5 55.77 2.04 5 -3 6 29.03 3.41 -5 3 -6 31.88 1.62 5 -3 6 30.19 1.71 5 -3 6 30.26 1.70 5 -3 6 31.78 1.78 5 -3 6 30.85 1.62 -5 3 -7 19.77 1.35 5 -3 7 21.00 1.55 5 -3 7 20.50 1.48 5 -3 7 21.78 1.62 5 -3 7 21.01 1.42 -5 3 -8 152.31 3.78 5 -3 8 156.06 3.71 5 -3 8 152.88 4.26 5 -3 8 152.31 3.96 -5 3 -9 32.66 1.79 5 -3 9 34.65 1.77 5 -3 9 32.49 1.92 5 -3 9 32.08 1.83 -5 3 -10 5.59 0.76 5 -3 10 4.37 0.69 -5 3 -11 7.30 0.83 5 -3 11 7.87 0.87 -5 3 -12 0.59 0.32 5 -3 12 -0.02 0.24 -5 3 -13 0.24 0.18 5 -3 13 0.18 0.26 -5 2 17 1.63 0.36 5 -2 -16 2.49 0.50 -5 2 16 2.34 0.44 5 -2 -16 2.64 0.51 -5 2 15 72.87 2.51 5 -2 -15 76.31 2.67 5 -2 -15 76.66 2.74 5 -2 -14 2.50 0.58 5 -2 -14 2.50 0.53 5 -2 -14 1.92 0.51 5 -2 -13 62.53 2.60 5 -2 -13 55.71 2.54 5 -2 -13 55.95 2.65 5 -2 -12 19.77 1.56 5 -2 -12 21.34 1.70 5 -2 -11 3.25 0.74 5 -2 -11 2.61 0.64 5 -2 -10 10.30 1.11 5 -2 -10 9.28 1.09 -5 2 10 11.22 2.29 5 -2 -9 72.93 4.80 5 -2 -9 63.66 2.33 5 -2 -9 65.01 2.55 5 -2 -9 67.33 2.50 -5 2 9 66.96 5.17 5 -2 -9 63.58 2.52 5 -2 -8 0.10 0.24 5 -2 -8 -0.40 0.45 5 -2 -8 0.25 0.21 5 -2 -8 0.05 0.21 5 -2 -8 0.19 0.26 -5 2 8 0.62 0.58 5 -2 -7 113.09 5.44 5 -2 -7 112.67 2.77 5 -2 -7 116.50 3.04 -5 2 7 118.56 5.87 5 -2 -7 118.40 3.08 5 -2 -7 115.94 2.98 5 -2 -6 13.66 1.85 5 -2 -6 15.09 1.09 5 -2 -6 15.87 1.08 -5 2 6 13.89 1.83 5 -2 -6 13.98 1.03 5 -2 -5 0.00 0.41 5 -2 -5 0.00 0.19 -5 2 5 0.17 0.41 5 -2 -4 115.86 5.02 -5 2 4 126.14 4.57 5 -2 -3 49.02 3.26 5 -2 -2 254.20 7.42 5 -2 -1 3.71 0.98 5 -2 0 10.55 1.66 5 -2 1 44.48 3.48 5 -2 1 41.46 1.60 5 -2 1 43.87 1.66 5 -2 2 426.51 5.38 5 -2 2 413.10 5.29 5 -2 2 414.97 5.34 5 -2 3 75.39 4.80 5 -2 3 73.81 2.39 5 -2 3 82.40 2.40 5 -2 3 75.23 2.38 5 -2 3 71.83 2.09 5 -2 4 1.13 0.31 5 -2 4 0.86 0.70 5 -2 4 1.21 0.40 5 -2 4 0.62 0.32 5 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62.33 2.47 6 -7 7 58.43 2.44 6 -7 7 59.49 2.46 6 -7 7 67.42 2.88 6 -7 8 1.00 0.39 6 -7 8 1.40 0.50 6 -7 9 1.32 0.45 6 -7 10 5.28 0.75 6 -7 11 3.66 0.58 6 -7 12 -0.05 0.20 6 -7 12 -0.11 0.25 6 -6 -15 1.89 0.39 6 -6 -14 3.42 0.57 6 -6 -13 4.05 0.72 6 -6 -12 11.29 1.23 6 -6 -11 0.50 0.41 6 -6 -11 -0.36 0.54 6 -6 -11 0.16 0.43 6 -6 -10 3.41 0.68 6 -6 -10 3.63 0.78 6 -6 -10 3.59 0.77 6 -6 -9 47.30 2.28 6 -6 -9 47.33 2.53 6 -6 -9 46.71 2.32 6 -6 -8 5.67 0.79 6 -6 -8 5.06 0.77 6 -6 -8 6.27 0.92 6 -6 -7 47.41 2.27 6 -6 -7 45.69 2.11 6 -6 -7 50.39 2.41 6 -6 -6 25.15 1.53 6 -6 -6 24.72 1.64 6 -6 -5 29.31 1.59 6 -6 -5 30.67 1.76 6 -6 -4 1.43 0.35 6 -6 -4 1.02 0.36 6 -6 -3 44.85 2.01 6 -6 -3 43.80 1.83 6 -6 -2 19.65 1.31 6 -6 -2 15.74 1.07 6 -6 -1 3.70 0.58 6 -6 -1 3.98 0.54 6 -6 0 3.21 0.57 6 -6 0 2.22 0.40 6 -6 1 108.94 2.74 6 -6 1 104.57 2.95 6 -6 2 42.68 1.75 6 -6 2 42.43 1.90 6 -6 2 42.85 1.90 6 -6 3 2.60 0.55 6 -6 3 4.68 0.69 6 -6 3 2.70 0.55 6 -6 3 2.76 0.49 6 -6 3 3.04 0.54 6 -6 4 39.60 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24.92 1.48 9 -3 1 12.86 1.16 9 -3 1 12.19 1.15 9 -3 1 12.92 1.05 -9 3 -2 18.27 1.19 9 -3 2 20.51 1.35 9 -3 2 21.10 1.43 9 -3 2 19.36 1.42 9 -3 2 21.94 1.31 -9 3 -3 1.13 0.37 9 -3 3 1.39 0.43 9 -3 3 1.73 0.54 9 -3 3 2.20 0.65 -9 3 -4 20.56 1.20 9 -3 4 21.93 1.47 -9 3 -5 9.94 0.78 9 -3 5 11.12 0.90 9 -3 6 7.77 0.76 -9 2 14 1.32 0.34 -9 2 13 1.81 0.41 -9 2 12 7.22 0.79 -9 2 11 0.21 0.28 -9 2 10 5.71 0.76 -9 2 9 3.86 0.66 -9 2 8 27.55 1.60 -9 2 7 4.35 0.65 9 -2 -7 3.47 0.59 9 -2 -6 0.63 0.30 9 -2 -6 0.04 0.36 9 -2 -5 132.51 3.71 9 -2 -5 127.35 3.42 9 -2 -4 1.23 0.42 9 -2 -4 1.93 0.54 9 -2 -3 32.56 1.83 9 -2 -3 31.97 1.74 9 -2 -2 28.29 1.70 9 -2 -2 26.98 1.60 9 -2 -1 0.16 0.33 9 -2 -1 0.79 0.35 -9 2 1 0.72 0.29 9 -2 0 -0.34 0.32 9 -2 0 -0.13 0.31 9 -2 0 0.11 0.32 9 -2 1 14.25 1.18 9 -2 1 12.54 1.14 9 -2 1 13.08 0.96 9 -2 2 2.35 0.51 9 -2 2 2.61 0.61 9 -2 2 1.05 0.40 -9 2 -3 6.40 0.73 9 -2 3 5.76 0.70 9 -2 3 6.37 0.80 -9 2 -4 9.52 0.83 9 -2 4 10.38 1.01 9 -2 4 9.32 0.84 -9 2 -5 0.70 0.27 9 -2 5 0.67 0.26 9 -2 5 1.13 0.38 9 -2 6 3.15 0.45 -9 1 14 0.05 0.15 -9 1 13 3.43 0.52 -9 1 12 0.36 0.29 -9 1 11 0.03 0.28 -9 1 10 0.21 0.27 -9 1 9 2.15 0.53 -9 1 8 33.67 1.74 -9 1 7 10.84 0.98 9 -1 -6 5.65 0.78 9 -1 -5 4.40 0.69 9 -1 -4 1.52 0.46 9 -1 -3 8.08 0.92 9 -1 -2 39.07 1.92 9 -1 -2 36.08 1.76 -9 1 2 35.59 1.70 9 -1 -1 23.01 1.47 9 -1 -1 22.21 1.41 -9 1 1 24.28 1.35 9 -1 -1 22.35 1.27 9 -1 0 0.62 0.42 9 -1 0 0.35 0.30 9 -1 1 7.91 0.86 9 -1 1 6.55 0.81 9 -1 2 13.40 1.10 -9 1 -3 0.14 0.19 9 -1 3 0.05 0.24 9 -1 3 -0.19 0.38 -9 1 -4 12.06 0.87 -9 1 -4 15.60 1.02 9 -1 4 16.69 1.17 9 -1 4 13.13 0.93 -9 1 -5 0.02 0.17 9 -1 5 0.28 0.22 -9 0 13 1.90 0.39 -9 0 12 5.48 0.66 -9 0 11 0.23 0.25 -9 0 10 0.39 0.31 -9 0 9 1.70 0.46 -9 0 8 0.54 0.34 -9 0 7 6.57 0.74 9 0 -7 6.16 0.79 9 0 -6 0.11 0.33 9 0 -5 0.64 0.38 9 0 -4 32.15 1.73 9 0 -3 2.45 0.54 -9 0 3 2.81 0.54 9 0 -2 4.85 0.69 -9 0 2 5.39 0.70 9 0 -1 12.87 1.08 -9 0 1 12.72 0.99 9 0 0 0.35 0.32 -9 0 0 -0.02 0.21 9 0 1 13.47 1.07 -9 0 -2 3.24 0.55 9 0 2 2.53 0.49 -9 0 -3 9.82 0.83 -9 0 -3 10.12 0.85 9 0 3 10.59 0.90 -9 0 -4 4.88 0.55 -9 -1 13 0.01 0.17 -9 -1 12 0.24 0.27 -9 -1 11 1.53 0.37 -9 -1 10 0.70 0.33 9 1 -10 0.24 0.25 -9 -1 9 0.94 0.35 9 1 -9 0.70 0.33 -9 -1 8 3.85 0.59 9 1 -8 4.48 0.64 -9 -1 7 0.44 0.26 9 1 -7 -0.08 0.26 9 1 -6 0.27 0.28 9 1 -5 2.21 0.48 9 1 -4 32.21 1.62 -9 -1 4 32.66 1.68 9 1 -3 17.05 1.18 -9 -1 3 17.70 1.22 9 1 -2 2.23 0.46 -9 -1 2 1.30 0.42 9 1 -1 2.56 0.49 -9 -1 1 2.24 0.44 9 1 0 1.57 0.37 -9 -1 0 1.42 0.37 -9 -1 -1 12.52 1.05 9 1 1 9.77 0.87 -9 -1 -2 0.32 0.27 -9 -1 -2 0.24 0.23 9 1 2 0.27 0.26 -9 -1 -3 1.06 0.30 -9 -2 12 0.77 0.28 -9 -2 11 1.38 0.39 9 2 -11 1.39 0.33 -9 -2 10 12.67 0.96 9 2 -10 11.66 0.87 -9 -2 9 1.21 0.39 9 2 -9 0.75 0.30 -9 -2 8 9.04 0.82 9 2 -8 7.55 0.73 -9 -2 7 1.51 0.37 9 2 -7 1.54 0.36 -9 -2 7 1.69 0.44 9 2 -6 3.31 0.50 -9 -2 6 3.83 0.64 9 2 -5 0.93 0.34 -9 -2 5 0.97 0.36 9 2 -4 4.45 0.57 -9 -2 4 4.94 0.66 9 2 -3 23.68 1.22 -9 -2 3 23.42 1.33 -9 -2 2 0.54 0.25 -9 -2 1 8.05 0.88 -9 -2 1 8.30 0.76 -9 -2 0 5.89 0.67 -9 -2 -1 4.46 0.57 -9 -2 -1 4.75 0.57 -9 -3 11 0.23 0.19 -9 -3 10 3.10 0.46 -9 -3 10 2.64 0.43 -9 -3 9 0.10 0.22 -9 -3 9 -0.17 0.27 -9 -3 8 6.09 0.63 -9 -3 8 6.07 0.68 -9 -3 7 0.34 0.21 -9 -3 7 0.51 0.30 -9 -3 6 2.85 0.44 -9 -3 6 4.12 0.57 -9 -3 5 1.45 0.41 -9 -3 5 1.66 0.40 -9 -3 4 0.69 0.29 -9 -3 4 0.54 0.26 -9 -3 3 2.79 0.49 -9 -3 3 2.34 0.47 -9 -3 2 1.78 0.39 -9 -3 1 0.24 0.22 -9 -3 0 2.41 0.40 -9 -3 0 2.38 0.38 -9 -4 8 11.51 0.81 -9 -4 7 0.38 0.23 -9 -4 6 0.03 0.22 -9 -4 5 0.82 0.26 -9 -4 4 2.27 0.40 10 -10 -6 0.76 0.28 10 -10 -5 4.43 0.58 10 -10 -4 18.90 1.15 10 -10 -3 0.07 0.24 10 -10 -3 -0.29 0.22 10 -10 -2 2.69 0.48 10 -10 -2 3.94 0.52 10 -10 -1 1.68 0.40 10 -10 -1 2.71 0.47 10 -10 0 -0.59 0.34 10 -10 0 -0.09 0.23 10 -10 1 1.96 0.39 10 -10 1 1.66 0.37 10 -10 2 -0.11 0.22 10 -9 -8 3.23 0.49 10 -9 -7 0.57 0.28 10 -9 -6 2.00 0.46 10 -9 -5 6.79 0.77 10 -9 -5 6.46 0.64 10 -9 -4 9.68 0.91 10 -9 -4 10.34 0.83 10 -9 -3 7.83 0.84 10 -9 -3 9.43 0.82 10 -9 -2 4.73 0.67 10 -9 -2 5.65 0.66 10 -9 -1 0.01 0.28 10 -9 -1 0.01 0.23 10 -9 0 1.82 0.44 10 -9 0 3.22 0.53 10 -9 1 0.77 0.32 10 -9 1 1.48 0.39 10 -9 2 -0.12 0.26 10 -9 2 0.49 0.31 10 -9 3 0.99 0.36 10 -9 3 0.11 0.30 10 -8 -9 3.24 0.52 10 -8 -8 0.05 0.35 10 -8 -7 0.47 0.21 10 -8 -7 0.88 0.34 10 -8 -6 1.05 0.32 10 -8 -6 0.85 0.34 10 -8 -5 0.31 0.25 10 -8 -5 0.47 0.29 10 -8 -4 0.80 0.33 10 -8 -4 0.82 0.34 10 -8 -3 16.11 1.23 10 -8 -3 17.54 1.18 10 -8 -2 10.54 0.99 10 -8 -2 12.99 1.01 10 -8 -1 0.75 0.33 10 -8 -1 0.93 0.39 10 -8 0 9.77 0.95 10 -8 0 10.14 0.92 10 -8 1 -0.33 0.37 10 -8 1 0.16 0.31 10 -8 2 0.31 0.32 10 -8 2 0.48 0.30 10 -8 3 3.07 0.56 10 -8 3 3.01 0.53 10 -8 4 3.47 0.54 10 -7 -10 0.08 0.28 10 -7 -9 3.76 0.64 10 -7 -8 1.34 0.40 10 -7 -7 -0.03 0.29 10 -7 -7 -0.29 0.23 10 -7 -6 0.38 0.27 10 -7 -6 0.54 0.27 10 -7 -5 14.24 1.01 10 -7 -5 13.38 1.15 10 -7 -4 1.39 0.42 10 -7 -4 1.48 0.46 10 -7 -4 1.52 0.40 10 -7 -3 3.93 0.61 10 -7 -3 4.47 0.71 10 -7 -3 3.97 0.55 10 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4 36.05 1.53 10 -5 -11 0.37 0.24 10 -5 -10 0.23 0.26 10 -5 -10 -0.09 0.28 10 -5 -9 54.32 2.07 10 -5 -9 51.79 2.10 10 -5 -8 21.79 1.35 10 -5 -8 21.29 1.38 10 -5 -7 0.77 0.36 10 -5 -7 0.33 0.29 10 -5 -6 11.07 0.99 10 -5 -6 10.17 1.01 10 -5 -5 0.50 0.33 10 -5 -5 0.60 0.31 10 -5 -4 0.42 0.33 10 -5 -4 0.34 0.28 10 -5 -3 -0.13 0.30 10 -5 -3 0.02 0.31 10 -5 -2 -0.07 0.33 10 -5 -2 -0.06 0.28 10 -5 -2 0.43 0.33 10 -5 -1 0.21 0.24 10 -5 -1 0.09 0.27 10 -5 0 21.75 1.36 10 -5 0 22.12 1.41 10 -5 0 22.01 1.31 10 -5 1 4.78 0.63 10 -5 1 4.45 0.64 10 -5 1 4.15 0.66 10 -5 2 7.91 0.83 10 -5 2 9.32 0.93 10 -5 2 9.10 0.84 10 -5 3 20.77 1.27 10 -5 3 21.57 1.32 10 -5 3 20.98 1.17 10 -5 4 79.65 2.31 -10 4 11 7.56 0.70 -10 4 10 20.74 1.20 10 -4 -10 22.43 1.38 10 -4 -10 20.07 1.16 10 -4 -9 66.40 2.40 10 -4 -9 61.35 2.17 10 -4 -8 95.53 2.91 10 -4 -8 89.93 2.71 10 -4 -7 79.15 2.66 10 -4 -7 73.85 2.52 10 -4 -6 0.41 0.29 10 -4 -6 -0.08 0.27 10 -4 -5 -0.06 0.24 10 -4 -5 0.39 0.30 10 -4 -4 5.33 0.71 10 -4 -4 5.46 0.76 10 -4 -3 0.47 0.34 10 -4 -3 0.31 0.31 10 -4 -2 0.55 0.34 10 -4 -2 0.30 0.28 10 -4 -2 0.53 0.31 10 -4 -1 0.49 0.28 10 -4 -1 0.29 0.31 10 -4 -1 0.80 0.35 10 -4 0 0.07 0.23 10 -4 0 -0.16 0.29 10 -4 0 -0.05 0.30 10 -4 1 0.87 0.39 10 -4 1 1.20 0.39 10 -4 1 1.47 0.38 10 -4 2 4.88 0.66 10 -4 2 5.39 0.73 10 -4 2 4.93 0.59 10 -4 3 2.64 0.52 10 -4 4 5.22 0.62 -10 3 11 0.29 0.21 -10 3 10 14.72 1.01 10 -3 -10 16.54 1.20 10 -3 -9 60.47 2.31 10 -3 -8 92.82 2.88 10 -3 -7 53.85 2.20 10 -3 -7 52.29 1.98 10 -3 -6 7.74 0.87 10 -3 -6 8.25 0.84 10 -3 -5 0.20 0.35 10 -3 -5 -0.27 0.31 10 -3 -4 3.35 0.57 10 -3 -4 4.38 0.68 10 -3 -3 0.71 0.36 10 -3 -3 0.89 0.36 10 -3 -2 1.52 0.40 10 -3 -2 0.83 0.37 10 -3 -2 1.71 0.44 10 -3 -1 -0.04 0.26 10 -3 -1 0.01 0.30 10 -3 -1 -0.22 0.33 10 -3 0 9.22 0.88 10 -3 0 8.76 0.89 10 -3 0 9.50 0.77 10 -3 1 0.05 0.24 10 -3 1 0.82 0.38 10 -3 2 40.14 1.74 10 -3 3 8.80 0.82 10 -2 -12 2.76 0.45 -10 2 11 0.26 0.21 10 -2 -11 0.20 0.26 -10 2 10 0.31 0.25 10 -2 -10 0.58 0.29 10 -2 -9 -0.15 0.31 10 -2 -8 5.37 0.71 10 -2 -7 14.05 1.12 10 -2 -6 -0.17 0.29 10 -2 -5 4.23 0.65 10 -2 -4 15.18 1.15 10 -2 -3 4.67 0.65 -10 2 3 5.26 0.60 10 -2 -2 0.05 0.20 10 -2 -2 0.70 0.33 10 -2 -2 -0.10 0.28 10 -2 -1 1.21 0.38 10 -2 -1 1.31 0.38 10 -2 0 0.38 0.28 10 -2 0 0.19 0.26 -10 2 -1 4.67 0.54 10 -2 1 5.50 0.67 10 -2 2 6.87 0.72 10 -1 -11 -0.16 0.27 -10 1 10 14.67 0.94 10 -1 -10 14.61 1.04 10 -1 -9 -0.01 0.26 10 -1 -8 13.06 1.03 10 -1 -7 1.25 0.36 10 -1 -6 2.94 0.52 10 -1 -5 9.10 0.88 10 -1 -4 11.67 0.97 -10 1 4 9.54 0.83 10 -1 -3 15.34 1.09 -10 1 3 15.83 1.02 10 -1 -2 52.81 1.97 10 -1 -1 5.86 0.68 10 -1 0 -0.15 0.24 -10 1 -1 22.92 1.12 10 -1 1 23.10 1.23 10 0 -10 4.12 0.52 10 0 -9 28.44 1.37 10 0 -8 -0.24 0.26 10 0 -7 0.83 0.30 10 0 -6 2.48 0.46 -10 0 6 4.10 0.57 10 0 -5 8.33 0.77 -10 0 5 7.72 0.76 10 0 -4 0.37 0.26 -10 0 4 0.53 0.28 10 0 -3 1.29 0.34 -10 0 3 1.31 0.33 10 0 -2 1.55 0.36 -10 0 2 0.57 0.24 10 0 -1 1.12 0.30 -10 0 0 8.86 0.77 -10 0 0 8.64 0.70 -10 -1 9 1.03 0.31 -10 -1 8 0.36 0.22 10 1 -7 0.27 0.20 -10 -1 7 0.20 0.23 -10 -1 6 0.32 0.19 10 1 -6 0.18 0.20 -10 -1 6 0.04 0.22 -10 -1 5 10.42 0.84 10 1 -5 10.24 0.76 -10 -1 5 11.87 0.87 -10 -1 4 4.10 0.58 -10 -1 4 4.50 0.53 -10 -1 3 0.90 0.33 -10 -1 3 0.05 0.18 -10 -1 2 0.68 0.28 11 -8 -5 0.22 0.23 11 -8 -4 1.85 0.36 11 -8 -4 1.60 0.36 11 -8 -3 1.60 0.34 11 -8 -3 1.81 0.39 11 -8 -2 -0.07 0.26 11 -8 -2 0.16 0.20 11 -7 -6 1.40 0.32 11 -7 -6 0.79 0.31 11 -7 -5 0.53 0.26 11 -7 -5 0.39 0.27 11 -7 -4 11.24 0.89 11 -7 -4 10.19 0.79 11 -7 -3 0.04 0.19 11 -7 -3 -0.35 0.27 11 -7 -2 1.91 0.37 11 -7 -2 1.13 0.36 11 -7 -1 0.28 0.30 11 -7 -1 0.36 0.23 11 -6 -7 0.11 0.18 11 -6 -6 2.90 0.43 11 -6 -6 2.56 0.45 11 -6 -6 2.45 0.41 11 -6 -5 10.64 0.79 11 -6 -5 10.58 0.87 11 -6 -5 10.24 0.81 11 -6 -4 9.64 0.77 11 -6 -4 10.09 0.85 11 -6 -4 9.96 0.81 11 -6 -3 -0.12 0.23 11 -6 -3 -0.36 0.33 11 -6 -3 -0.31 0.24 11 -6 -2 0.18 0.21 11 -6 -2 -0.11 0.27 11 -6 -2 0.33 0.22 11 -6 -1 0.26 0.22 11 -6 -1 -0.09 0.18 11 -6 -1 0.34 0.26 11 -5 -7 0.90 0.30 11 -5 -6 1.11 0.33 11 -5 -6 1.15 0.34 11 -5 -5 20.38 1.14 11 -5 -5 18.74 1.10 11 -5 -5 21.62 1.18 11 -5 -4 2.10 0.39 11 -5 -4 1.67 0.40 11 -5 -4 1.61 0.36 11 -5 -3 0.02 0.19 11 -5 -3 0.38 0.26 11 -5 -3 -0.23 0.21 11 -5 -2 -0.03 0.18 11 -5 -2 0.13 0.24 11 -5 -2 0.09 0.22 11 -5 -1 0.11 0.21 11 -5 -1 0.32 0.26 11 -5 -1 0.52 0.23 11 -4 -8 11.80 0.87 11 -4 -7 22.49 1.20 11 -4 -6 0.63 0.30 11 -4 -5 17.70 1.07 11 -4 -5 17.17 1.03 11 -4 -4 0.92 0.25 11 -4 -4 1.23 0.32 11 -4 -3 0.10 0.16 11 -4 -3 -0.20 0.24 11 -4 -2 0.93 0.29 11 -4 -1 0.59 0.28 11 -3 -8 0.47 0.25 11 -3 -7 8.03 0.72 11 -3 -6 0.72 0.28 11 -3 -5 0.54 0.23 11 -3 -5 0.64 0.31 11 -3 -4 6.41 0.64 11 -3 -3 2.17 0.38 11 -3 -2 4.89 0.55 11 -2 -6 5.44 0.57 11 -2 -5 0.13 0.19 11 -2 -4 4.21 0.51 0 0 0 0.00 0.00 TITL lb0214_CLZ-24DHBA in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 9.486085 12.532195 15.364076 98.4154 103.3788 110.4501 ZERR 2.00 0.000367 0.000491 0.000473 0.0029 0.0030 0.0036 LATT 1 SFAC C H N O Cl UNIT 70.00 64.00 8.00 10.00 4.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 20432 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.92778(7) 0.64690(5) 1.08028(3) 0.08218(18) Uani 1 1 d . . . . . Cl2 Cl 0.42975(7) 0.25241(5) -0.01186(3) 0.08626(19) Uani 1 1 d . . . . . N1 N 0.80881(14) 0.52714(10) 0.37170(8) 0.0405(3) Uani 1 1 d . . . . . N2 N 1.00055(14) 0.65504(10) 0.55080(8) 0.0445(3) Uani 1 1 d . . . . . N4 N 0.43568(14) 0.29295(10) 0.50511(9) 0.0459(3) Uani 1 1 d . . . . . N3 N 0.62938(16) 0.42285(11) 0.68051(8) 0.0489(3) Uani 1 1 d . . . . . C6 C 0.86292(16) 0.56847(11) 0.53666(9) 0.0399(3) Uani 1 1 d . . . . . C11 C 0.75643(16) 0.50049(11) 0.44487(9) 0.0387(3) Uani 1 1 d . . . . . C9 C 0.56945(16) 0.38265(11) 0.51290(9) 0.0407(3) Uani 1 1 d . . . . . C8 C 0.67605(16) 0.45195(11) 0.60654(9) 0.0408(3) Uani 1 1 d . . . . . C13 C 0.71374(16) 0.45841(12) 0.27813(9) 0.0422(3) Uani 1 1 d . . . . . C7 C 0.81622(17) 0.53962(12) 0.61393(9) 0.0429(3) Uani 1 1 d . . . . . H7 H 0.884238 0.582415 0.672638 0.052 Uiso 1 1 calc R U . . . C12 C 0.95332(16) 0.61812(12) 0.38469(9) 0.0408(3) Uani 1 1 d . . . . . C14 C 0.64032(17) 0.50957(13) 0.21917(10) 0.0469(3) Uani 1 1 d . . . . . H14 H 0.648524 0.585737 0.239635 0.056 Uiso 1 1 calc R U . . . C19 C 0.71067(17) 0.48042(13) 0.77468(10) 0.0458(3) Uani 1 1 d . . . . . C5 C 1.04507(17) 0.68274(12) 0.47617(10) 0.0428(3) Uani 1 1 d . . . . . C10 C 0.61242(16) 0.41237(12) 0.43546(9) 0.0422(3) Uani 1 1 d . . . . . H10 H 0.542748 0.372060 0.376658 0.051 Uiso 1 1 calc R U . . . C1 C 1.01126(18) 0.64547(14) 0.31100(10) 0.0484(3) Uani 1 1 d . . . . . H1 H 0.953983 0.600969 0.250864 0.058 Uiso 1 1 calc R U . . . C24 C 0.78060(19) 0.60214(13) 0.80789(10) 0.0509(4) Uani 1 1 d . . . . . H24 H 0.781350 0.649648 0.766675 0.061 Uiso 1 1 calc R U . . . C18 C 0.7033(2) 0.34564(14) 0.24968(11) 0.0524(4) Uani 1 1 d . . . . . H18 H 0.754710 0.313048 0.290148 0.063 Uiso 1 1 calc R U . . . C20 C 0.7081(2) 0.41092(14) 0.83753(11) 0.0530(4) Uani 1 1 d . . . . . H20 H 0.660565 0.329458 0.816225 0.064 Uiso 1 1 calc R U . . . C15 C 0.55427(18) 0.44575(15) 0.12910(11) 0.0537(4) Uani 1 1 d . . . . . H15 H 0.505144 0.479035 0.088101 0.064 Uiso 1 1 calc R U . . . C4 C 1.18961(18) 0.77851(14) 0.49095(11) 0.0521(4) Uani 1 1 d . . . . . H4 H 1.249615 0.823192 0.550681 0.063 Uiso 1 1 calc R U . . . C2 C 1.15274(19) 0.73815(14) 0.32829(11) 0.0528(4) Uani 1 1 d . . . . . H2 H 1.190395 0.756419 0.279274 0.063 Uiso 1 1 calc R U . . . C16 C 0.54218(19) 0.33319(15) 0.10096(11) 0.0558(4) Uani 1 1 d . . . . . C3 C 1.24169(19) 0.80584(14) 0.41809(12) 0.0552(4) Uani 1 1 d . . . . . H3 H 1.336321 0.869475 0.428220 0.066 Uiso 1 1 calc R U . . . C25 C 0.32132(18) 0.20930(13) 0.41840(11) 0.0510(3) Uani 1 1 d . . . . . H25 H 0.292871 0.253720 0.374869 0.061 Uiso 1 1 calc R U . . . C21 C 0.7753(2) 0.46162(16) 0.93132(11) 0.0591(4) Uani 1 1 d . . . . . H21 H 0.773179 0.414730 0.973056 0.071 Uiso 1 1 calc R U . . . C22 C 0.8452(2) 0.58181(16) 0.96217(10) 0.0559(4) Uani 1 1 d . . . . . C17 C 0.6151(2) 0.28162(15) 0.16008(11) 0.0597(4) Uani 1 1 d . . . . . H17 H 0.604941 0.204881 0.139826 0.072 Uiso 1 1 calc R U . . . C23 C 0.8489(2) 0.65304(14) 0.90151(11) 0.0556(4) Uani 1 1 d . . . . . H23 H 0.896850 0.734418 0.923422 0.067 Uiso 1 1 calc R U . . . C27 C 0.1743(2) 0.13729(16) 0.44088(14) 0.0672(5) Uani 1 1 d . . . . . H27A H 0.198898 0.088269 0.479234 0.101 Uiso 1 1 calc R U . . . H27B H 0.092802 0.088933 0.384642 0.101 Uiso 1 1 calc R U . . . H27C H 0.138323 0.189207 0.472965 0.101 Uiso 1 1 calc R U . . . C26 C 0.3899(2) 0.13041(16) 0.37480(15) 0.0704(5) Uani 1 1 d . . . . . H26A H 0.480622 0.177625 0.359681 0.106 Uiso 1 1 calc R U . . . H26B H 0.311824 0.075790 0.319589 0.106 Uiso 1 1 calc R U . . . H26C H 0.420588 0.087949 0.417556 0.106 Uiso 1 1 calc R U . . . C28A C 0.3578(11) 0.1478(10) 0.6875(7) 0.070(4) Uani 0.632(6) 1 d D . P A 1 O1A O 0.3539(18) 0.2399(9) 0.6657(7) 0.067(2) Uani 0.632(6) 1 d D . P A 1 O2A O 0.4533(14) 0.1034(10) 0.6683(10) 0.085(2) Uani 0.632(6) 1 d D . P A 1 C34A C 0.1363(13) 0.1257(8) 0.7532(8) 0.048(2) Uani 0.632(6) 1 d D . P A 1 H34A H 0.135193 0.193619 0.736008 0.057 Uiso 0.632(6) 1 calc R U P A 1 C29A C 0.2461(14) 0.0839(9) 0.7342(10) 0.043(3) Uani 0.632(6) 1 d D . P A 1 C30A C 0.2368(17) -0.0234(9) 0.7544(11) 0.053(2) Uani 0.632(6) 1 d D . P A 1 O3A O 0.3403(13) -0.0703(9) 0.7363(8) 0.0704(15) Uani 0.632(6) 1 d D . P A 1 H3OA H 0.410(5) -0.019(3) 0.704(5) 0.106 Uiso 0.632(6) 1 calc DR U P A 1 C33A C 0.0282(11) 0.0715(7) 0.7964(6) 0.0518(16) Uani 0.632(6) 1 d D . P A 1 H33A H -0.037936 0.105349 0.812741 0.062 Uiso 0.632(6) 1 calc R U P A 1 C31A C 0.1240(11) -0.0823(8) 0.7933(8) 0.062(2) Uani 0.632(6) 1 d D . P A 1 H31A H 0.117285 -0.154325 0.805059 0.074 Uiso 0.632(6) 1 calc R U P A 1 C32A C 0.0217(14) -0.0348(8) 0.8147(8) 0.0604(18) Uani 0.632(6) 1 d D . P A 1 O4A O -0.0945(9) -0.1010(8) 0.8473(6) 0.0910(18) Uani 0.632(6) 1 d D . P A 1 H4OA H -0.136155 -0.059926 0.867831 0.098(15) Uiso 0.632(6) 1 calc R . P A 1 C35A C 0.302(2) 0.9240(15) 0.0614(13) 0.187(7) Uani 0.632(6) 1 d D U P A 1 H35A H 0.225923 0.847255 0.056713 0.224 Uiso 0.632(6) 1 calc R U P A 1 H35B H 0.403930 0.921390 0.068755 0.224 Uiso 0.632(6) 1 calc R U P A 1 H35C H 0.271236 0.948527 0.006253 0.224 Uiso 0.632(6) 1 calc R U P A 1 O5A O 0.3087(4) 1.0002(3) 0.1342(3) 0.1140(15) Uani 0.632(6) 1 d D U P A 1 H5OA H 0.398751 1.029525 0.170189 0.171 Uiso 0.632(6) 1 calc R U P A 1 C28B C 0.3707(16) 0.1417(11) 0.6888(9) 0.048(4) Uani 0.368(6) 1 d D . P A 2 O1B O 0.364(3) 0.2324(14) 0.6664(14) 0.071(4) Uani 0.368(6) 1 d D . P A 2 O2B O 0.474(2) 0.1010(16) 0.6845(18) 0.096(6) Uani 0.368(6) 1 d D . P A 2 C34B C 0.154(2) 0.1260(13) 0.7577(16) 0.065(6) Uani 0.368(6) 1 d D . P A 2 H34B H 0.158153 0.197994 0.746758 0.078 Uiso 0.368(6) 1 calc R U P A 2 C29B C 0.256(3) 0.0801(18) 0.735(2) 0.056(6) Uani 0.368(6) 1 d D . P A 2 C30B C 0.266(3) -0.0172(18) 0.765(2) 0.059(5) Uani 0.368(6) 1 d D . P A 2 O3B O 0.376(2) -0.0558(19) 0.7494(16) 0.094(6) Uani 0.368(6) 1 d D . P A 2 H3OB H 0.445(12) -0.001(8) 0.719(9) 0.141 Uiso 0.368(6) 1 calc DR U P A 2 C33B C 0.045(3) 0.0648(17) 0.7968(16) 0.083(6) Uani 0.368(6) 1 d D . P A 2 H33B H -0.034319 0.089174 0.804819 0.099 Uiso 0.368(6) 1 calc R U P A 2 C31B C 0.165(2) -0.0732(16) 0.8099(15) 0.076(5) Uani 0.368(6) 1 d D . P A 2 H31B H 0.172229 -0.137879 0.830571 0.091 Uiso 0.368(6) 1 calc R U P A 2 C32B C 0.054(3) -0.0329(17) 0.8241(17) 0.088(7) Uani 0.368(6) 1 d D . P A 2 O4B O -0.0386(18) -0.0842(15) 0.8755(12) 0.117(5) Uani 0.368(6) 1 d D . P A 2 H4OB H 0.010197 -0.056396 0.930586 0.30(11) Uiso 0.368(6) 1 calc R . P A 2 C35B C 0.291(2) 0.9229(19) 0.0590(17) 0.123(6) Uani 0.368(6) 1 d D U P A 2 H35D H 0.248996 0.851786 0.010883 0.148 Uiso 0.368(6) 1 calc R U P A 2 H35E H 0.312159 0.904921 0.118059 0.148 Uiso 0.368(6) 1 calc R U P A 2 H35F H 0.387500 0.976280 0.052943 0.148 Uiso 0.368(6) 1 calc R U P A 2 O5B O 0.1889(11) 0.9714(9) 0.0523(6) 0.153(4) Uani 0.368(6) 1 d D U P A 2 H5OB H 0.218144 1.025765 0.098031 0.230 Uiso 0.368(6) 1 calc R U P A 2 H4N H 0.417(2) 0.2781(15) 0.5548(13) 0.051(4) Uiso 1 1 d . . . . . H3N H 0.549(3) 0.355(2) 0.6725(15) 0.074(6) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0994(4) 0.1009(4) 0.0376(2) 0.0095(2) 0.0120(2) 0.0387(3) Cl2 0.0885(4) 0.0909(4) 0.0471(2) -0.0049(2) -0.0042(2) 0.0230(3) N1 0.0442(6) 0.0417(6) 0.0360(6) 0.0121(5) 0.0130(5) 0.0160(5) N2 0.0438(6) 0.0457(6) 0.0397(6) 0.0102(5) 0.0136(5) 0.0126(5) N4 0.0466(7) 0.0423(6) 0.0434(7) 0.0113(5) 0.0153(5) 0.0102(5) N3 0.0546(7) 0.0456(6) 0.0405(6) 0.0118(5) 0.0194(5) 0.0095(6) C6 0.0424(7) 0.0401(7) 0.0374(7) 0.0105(5) 0.0131(5) 0.0158(6) C11 0.0434(7) 0.0396(6) 0.0357(7) 0.0120(5) 0.0130(5) 0.0179(6) C9 0.0431(7) 0.0372(6) 0.0418(7) 0.0102(5) 0.0139(6) 0.0153(6) C8 0.0476(7) 0.0401(7) 0.0379(7) 0.0123(5) 0.0168(6) 0.0179(6) C13 0.0437(7) 0.0466(7) 0.0353(7) 0.0112(6) 0.0134(6) 0.0157(6) C7 0.0456(7) 0.0442(7) 0.0350(7) 0.0090(5) 0.0119(6) 0.0138(6) C12 0.0427(7) 0.0429(7) 0.0423(7) 0.0163(6) 0.0154(6) 0.0197(6) C14 0.0472(8) 0.0498(8) 0.0451(8) 0.0150(6) 0.0132(6) 0.0200(6) C19 0.0512(8) 0.0494(8) 0.0391(7) 0.0139(6) 0.0209(6) 0.0171(6) C5 0.0439(7) 0.0443(7) 0.0428(7) 0.0141(6) 0.0158(6) 0.0177(6) C10 0.0438(7) 0.0413(7) 0.0366(7) 0.0090(5) 0.0101(5) 0.0131(6) C1 0.0515(8) 0.0587(8) 0.0425(7) 0.0212(6) 0.0183(6) 0.0249(7) C24 0.0619(9) 0.0487(8) 0.0413(8) 0.0157(6) 0.0210(7) 0.0162(7) C18 0.0651(9) 0.0506(8) 0.0432(8) 0.0132(6) 0.0131(7) 0.0266(7) C20 0.0669(10) 0.0505(8) 0.0489(8) 0.0183(7) 0.0259(7) 0.0241(7) C15 0.0514(8) 0.0649(9) 0.0435(8) 0.0181(7) 0.0094(6) 0.0233(7) C4 0.0468(8) 0.0503(8) 0.0520(8) 0.0125(7) 0.0149(7) 0.0112(6) C2 0.0541(8) 0.0616(9) 0.0563(9) 0.0302(7) 0.0279(7) 0.0253(7) C16 0.0530(9) 0.0637(9) 0.0395(8) 0.0054(7) 0.0082(6) 0.0169(7) C3 0.0477(8) 0.0536(8) 0.0651(10) 0.0239(7) 0.0227(7) 0.0139(7) C25 0.0458(8) 0.0459(8) 0.0516(8) 0.0083(6) 0.0091(6) 0.0123(6) C21 0.0770(11) 0.0691(10) 0.0460(8) 0.0270(8) 0.0264(8) 0.0362(9) C22 0.0610(9) 0.0697(10) 0.0379(8) 0.0123(7) 0.0159(7) 0.0269(8) C17 0.0726(11) 0.0513(8) 0.0493(9) 0.0053(7) 0.0138(8) 0.0239(8) C23 0.0620(9) 0.0529(8) 0.0454(8) 0.0092(7) 0.0200(7) 0.0140(7) C27 0.0489(9) 0.0612(10) 0.0745(12) 0.0076(9) 0.0160(8) 0.0075(7) C26 0.0597(10) 0.0553(9) 0.0778(12) -0.0062(8) 0.0173(9) 0.0129(8) C28A 0.056(4) 0.068(5) 0.071(5) -0.008(3) 0.014(3) 0.018(3) O1A 0.078(4) 0.052(3) 0.065(4) 0.014(2) 0.038(3) 0.009(3) O2A 0.080(4) 0.092(4) 0.105(3) 0.030(2) 0.059(4) 0.039(3) C34A 0.050(3) 0.043(4) 0.056(4) 0.012(3) 0.023(2) 0.020(3) C29A 0.054(5) 0.032(4) 0.043(4) 0.010(3) 0.017(4) 0.013(4) C30A 0.059(5) 0.052(3) 0.048(3) 0.0072(19) 0.011(4) 0.028(3) O3A 0.078(4) 0.068(2) 0.084(3) 0.023(2) 0.029(4) 0.047(3) C33A 0.062(3) 0.038(3) 0.062(3) 0.018(2) 0.034(2) 0.017(2) C31A 0.078(4) 0.047(2) 0.069(4) 0.031(2) 0.024(3) 0.025(2) C32A 0.072(3) 0.053(3) 0.066(3) 0.022(2) 0.036(2) 0.023(2) O4A 0.101(4) 0.076(3) 0.122(5) 0.054(3) 0.071(3) 0.030(3) C35A 0.147(11) 0.181(13) 0.154(12) -0.040(9) 0.027(8) 0.019(9) O5A 0.081(2) 0.146(3) 0.102(3) 0.001(2) 0.0326(18) 0.0398(19) C28B 0.052(6) 0.034(5) 0.053(6) 0.017(4) 0.035(5) -0.001(4) O1B 0.079(7) 0.043(5) 0.097(9) 0.034(5) 0.044(5) 0.013(5) O2B 0.061(4) 0.072(5) 0.159(15) 0.031(6) 0.053(6) 0.019(4) C34B 0.076(10) 0.032(7) 0.071(8) 0.024(5) 0.019(6) 0.002(5) C29B 0.039(7) 0.062(13) 0.055(10) 0.005(8) 0.014(6) 0.009(7) C30B 0.057(8) 0.058(6) 0.056(7) 0.024(6) 0.008(6) 0.017(4) O3B 0.076(8) 0.102(8) 0.109(8) 0.028(6) 0.015(5) 0.048(6) C33B 0.077(7) 0.082(10) 0.102(10) 0.010(7) 0.048(7) 0.037(6) C31B 0.105(11) 0.079(7) 0.068(8) 0.038(6) 0.035(9) 0.053(8) C32B 0.122(14) 0.067(7) 0.095(10) 0.052(7) 0.068(11) 0.026(7) O4B 0.149(11) 0.102(6) 0.129(10) 0.065(7) 0.098(10) 0.034(8) C35B 0.092(9) 0.153(15) 0.130(14) 0.029(11) 0.061(10) 0.041(9) O5B 0.172(8) 0.206(9) 0.147(7) 0.075(6) 0.093(7) 0.111(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C11 N1 C12 121.36(11) C11 N1 C13 119.95(11) C12 N1 C13 118.68(11) C6 N2 C5 118.51(12) C9 N4 C25 126.25(13) C9 N4 H4N 117.7(12) C25 N4 H4N 115.8(12) C8 N3 C19 126.69(13) C8 N3 H3N 119.7(14) C19 N3 H3N 112.9(14) N2 C6 C7 118.67(12) N2 C6 C11 123.14(12) C7 C6 C11 118.19(12) N1 C11 C10 123.55(12) N1 C11 C6 116.59(12) C10 C11 C6 119.84(12) N4 C9 C10 122.11(13) N4 C9 C8 118.62(12) C10 C9 C8 119.27(12) C7 C8 N3 123.81(13) C7 C8 C9 118.22(12) N3 C8 C9 117.96(12) C18 C13 C14 121.71(13) C18 C13 N1 119.37(12) C14 C13 N1 118.89(12) C8 C7 C6 123.11(13) C8 C7 H7 118.4 C6 C7 H7 118.4 N1 C12 C1 122.45(13) N1 C12 C5 117.86(12) C1 C12 C5 119.67(13) C13 C14 C15 119.00(14) C13 C14 H14 120.5 C15 C14 H14 120.5 C20 C19 C24 118.84(14) C20 C19 N3 117.54(13) C24 C19 N3 123.38(13) N2 C5 C12 122.38(12) N2 C5 C4 118.69(13) C12 C5 C4 118.92(13) C11 C10 C9 121.27(13) C11 C10 H10 119.4 C9 C10 H10 119.4 C2 C1 C12 119.53(14) C2 C1 H1 120.2 C12 C1 H1 120.2 C23 C24 C19 120.58(14) C23 C24 H24 119.7 C19 C24 H24 119.7 C13 C18 C17 119.05(14) C13 C18 H18 120.5 C17 C18 H18 120.5 C21 C20 C19 120.71(15) C21 C20 H20 119.6 C19 C20 H20 119.6 C16 C15 C14 119.40(14) C16 C15 H15 120.3 C14 C15 H15 120.3 C3 C4 C5 120.43(15) C3 C4 H4 119.8 C5 C4 H4 119.8 C1 C2 C3 121.35(14) C1 C2 H2 119.3 C3 C2 H2 119.3 C15 C16 C17 121.66(14) C15 C16 Cl2 119.02(12) C17 C16 Cl2 119.31(13) C4 C3 C2 119.99(14) C4 C3 H3 120.0 C2 C3 H3 120.0 N4 C25 C26 111.55(13) N4 C25 C27 107.63(14) C26 C25 C27 111.05(14) N4 C25 H25 108.8 C26 C25 H25 108.8 C27 C25 H25 108.8 C22 C21 C20 119.29(14) C22 C21 H21 120.4 C20 C21 H21 120.4 C21 C22 C23 121.32(15) C21 C22 Cl1 119.77(12) C23 C22 Cl1 118.90(13) C18 C17 C16 119.16(15) C18 C17 H17 120.4 C16 C17 H17 120.4 C22 C23 C24 119.26(15) C22 C23 H23 120.4 C24 C23 H23 120.4 C25 C27 H27A 109.5 C25 C27 H27B 109.5 H27A C27 H27B 109.5 C25 C27 H27C 109.5 H27A C27 H27C 109.5 H27B C27 H27C 109.5 C25 C26 H26A 109.5 C25 C26 H26B 109.5 H26A C26 H26B 109.5 C25 C26 H26C 109.5 H26A C26 H26C 109.5 H26B C26 H26C 109.5 O1A C28A O2A 122.2(10) O1A C28A C29A 120.3(9) O2A C28A C29A 117.4(8) C33A C34A C29A 123.3(7) C33A C34A H34A 118.4 C29A C34A H34A 118.4 C34A C29A C30A 117.0(6) C34A C29A C28A 119.7(7) C30A C29A C28A 123.2(7) O3A C30A C31A 119.5(7) O3A C30A C29A 119.9(7) C31A C30A C29A 120.5(6) C30A O3A H3OA 109.5 C32A C33A C34A 117.9(8) C32A C33A H33A 121.0 C34A C33A H33A 121.0 C32A C31A C30A 120.4(6) C32A C31A H31A 119.8 C30A C31A H31A 119.8 O4A C32A C31A 117.7(7) O4A C32A C33A 121.5(7) C31A C32A C33A 120.7(7) C32A O4A H4OA 109.5 O5A C35A H35A 109.5 O5A C35A H35B 109.5 H35A C35A H35B 109.5 O5A C35A H35C 109.5 H35A C35A H35C 109.5 H35B C35A H35C 109.5 C35A O5A H5OA 109.5 O1B C28B O2B 127.0(14) O1B C28B C29B 118.1(13) O2B C28B C29B 114.5(11) C33B C34B C29B 119.5(12) C33B C34B H34B 120.3 C29B C34B H34B 120.3 C34B C29B C30B 119.5(11) C34B C29B C28B 120.7(11) C30B C29B C28B 119.3(11) O3B C30B C31B 120.2(14) O3B C30B C29B 119.4(13) C31B C30B C29B 120.4(12) C30B O3B H3OB 109.5 C34B C33B C32B 119.3(13) C34B C33B H33B 120.4 C32B C33B H33B 120.4 C32B C31B C30B 119.0(13) C32B C31B H31B 120.5 C30B C31B H31B 120.5 C31B C32B O4B 118.5(13) C31B C32B C33B 121.6(12) O4B C32B C33B 119.6(14) C32B O4B H4OB 109.5 O5B C35B H35D 109.5 O5B C35B H35E 109.5 H35D C35B H35E 109.5 O5B C35B H35F 109.5 H35D C35B H35F 109.5 H35E C35B H35F 109.5 C35B O5B H5OB 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Cl1 C22 1.7419(16) Cl2 C16 1.7446(16) N1 C11 1.3692(17) N1 C12 1.3905(18) N1 C13 1.4549(17) N2 C6 1.3185(18) N2 C5 1.3607(18) N4 C9 1.3349(18) N4 C25 1.4759(19) N4 H4N 0.853(19) N3 C8 1.3645(18) N3 C19 1.4135(19) N3 H3N 0.89(2) C6 C7 1.4119(19) C6 C11 1.4569(19) C11 C10 1.3836(19) C9 C10 1.4031(19) C9 C8 1.4812(19) C8 C7 1.364(2) C13 C18 1.378(2) C13 C14 1.381(2) C7 H7 0.9300 C12 C1 1.404(2) C12 C5 1.413(2) C14 C15 1.385(2) C14 H14 0.9300 C19 C20 1.391(2) C19 C24 1.391(2) C5 C4 1.414(2) C10 H10 0.9300 C1 C2 1.370(2) C1 H1 0.9300 C24 C23 1.381(2) C24 H24 0.9300 C18 C17 1.383(2) C18 H18 0.9300 C20 C21 1.382(2) C20 H20 0.9300 C15 C16 1.369(2) C15 H15 0.9300 C4 C3 1.365(2) C4 H4 0.9300 C2 C3 1.398(2) C2 H2 0.9300 C16 C17 1.384(2) C3 H3 0.9300 C25 C26 1.519(2) C25 C27 1.521(2) C25 H25 0.9800 C21 C22 1.371(3) C21 H21 0.9300 C22 C23 1.380(2) C17 H17 0.9300 C23 H23 0.9300 C27 H27A 0.9600 C27 H27B 0.9600 C27 H27C 0.9600 C26 H26A 0.9600 C26 H26B 0.9600 C26 H26C 0.9600 C28A O1A 1.259(8) C28A O2A 1.282(9) C28A C29A 1.486(8) C34A C33A 1.384(7) C34A C29A 1.387(8) C34A H34A 0.9300 C29A C30A 1.401(7) C30A O3A 1.366(7) C30A C31A 1.385(8) O3A H3OA 1.02(4) C33A C32A 1.383(7) C33A H33A 0.9300 C31A C32A 1.378(8) C31A H31A 0.9300 C32A O4A 1.377(8) O4A H4OA 0.8200 C35A O5A 1.334(13) C35A H35A 0.9600 C35A H35B 0.9600 C35A H35C 0.9600 O5A H5OA 0.8200 C28B O1B 1.251(12) C28B O2B 1.264(12) C28B C29B 1.483(11) C34B C33B 1.373(13) C34B C29B 1.376(12) C34B H34B 0.9300 C29B C30B 1.390(12) C30B O3B 1.343(12) C30B C31B 1.366(12) O3B H3OB 1.02(4) C33B C32B 1.375(13) C33B H33B 0.9300 C31B C32B 1.363(13) C31B H31B 0.9300 C32B O4B 1.374(12) O4B H4OB 0.8200 C35B O5B 1.306(15) C35B H35D 0.9600 C35B H35E 0.9600 C35B H35F 0.9600 O5B H5OB 0.8200 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C14 H14 O1A 0.93 2.45 3.346(11) 161.4 2_666 C14 H14 O1B 0.93 2.57 3.467(19) 162.1 2_666 C23 H23 O4A 0.93 2.50 3.207(8) 132.8 1_665 C23 H23 O4B 0.93 2.41 3.204(16) 143.3 1_665 O3A H3OA O2A 1.02 1.66 2.556(15) 144.5 . O4A H4OA O5A 0.82 2.02 2.786(10) 155.2 2_566 O5A H5OA O3A 0.82 2.39 3.192(12) 166.6 2_666 O3B H3OB O2B 1.02 1.42 2.33(3) 146.4 . O4B H4OB O5B 0.82 2.10 2.86(2) 154.5 1_546 O5B H5OB O4B 0.82 2.17 2.64(2) 116.1 2_566 N4 H4N O1A 0.853(19) 2.00(2) 2.852(10) 174.9(17) . N4 H4N O1B 0.853(19) 2.00(3) 2.854(18) 176.2(18) . N3 H3N O1A 0.89(2) 1.88(3) 2.743(13) 164(2) . N3 H3N O1B 0.89(2) 1.86(3) 2.73(2) 169(2) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C5 N2 C6 C7 -179.89(12) C5 N2 C6 C11 0.4(2) C12 N1 C11 C10 178.75(12) C13 N1 C11 C10 -2.25(19) C12 N1 C11 C6 -2.82(18) C13 N1 C11 C6 176.18(11) N2 C6 C11 N1 2.78(19) C7 C6 C11 N1 -176.97(12) N2 C6 C11 C10 -178.73(13) C7 C6 C11 C10 1.53(19) C25 N4 C9 C10 4.1(2) C25 N4 C9 C8 -175.31(12) C19 N3 C8 C7 3.7(2) C19 N3 C8 C9 -177.49(13) N4 C9 C8 C7 176.72(13) C10 C9 C8 C7 -2.73(19) N4 C9 C8 N3 -2.12(19) C10 C9 C8 N3 178.43(13) C11 N1 C13 C18 -72.77(17) C12 N1 C13 C18 106.25(15) C11 N1 C13 C14 109.26(15) C12 N1 C13 C14 -71.71(17) N3 C8 C7 C6 179.85(13) C9 C8 C7 C6 1.1(2) N2 C6 C7 C8 179.75(13) C11 C6 C7 C8 -0.5(2) C11 N1 C12 C1 178.53(12) C13 N1 C12 C1 -0.48(19) C11 N1 C12 C5 -0.05(18) C13 N1 C12 C5 -179.06(11) C18 C13 C14 C15 -0.1(2) N1 C13 C14 C15 177.78(13) C8 N3 C19 C20 -142.18(15) C8 N3 C19 C24 43.5(2) C6 N2 C5 C12 -3.5(2) C6 N2 C5 C4 177.50(13) N1 C12 C5 N2 3.4(2) C1 C12 C5 N2 -175.19(13) N1 C12 C5 C4 -177.61(12) C1 C12 C5 C4 3.8(2) N1 C11 C10 C9 175.10(12) C6 C11 C10 C9 -3.3(2) N4 C9 C10 C11 -175.55(13) C8 C9 C10 C11 3.9(2) N1 C12 C1 C2 178.35(13) C5 C12 C1 C2 -3.1(2) C20 C19 C24 C23 1.2(2) N3 C19 C24 C23 175.50(15) C14 C13 C18 C17 -0.9(2) N1 C13 C18 C17 -178.79(14) C24 C19 C20 C21 -0.8(2) N3 C19 C20 C21 -175.36(15) C13 C14 C15 C16 0.9(2) N2 C5 C4 C3 177.12(14) C12 C5 C4 C3 -1.9(2) C12 C1 C2 C3 0.5(2) C14 C15 C16 C17 -0.6(3) C14 C15 C16 Cl2 178.54(12) C5 C4 C3 C2 -0.7(2) C1 C2 C3 C4 1.4(2) C9 N4 C25 C26 68.3(2) C9 N4 C25 C27 -169.69(14) C19 C20 C21 C22 0.0(3) C20 C21 C22 C23 0.4(3) C20 C21 C22 Cl1 179.05(13) C13 C18 C17 C16 1.1(3) C15 C16 C17 C18 -0.4(3) Cl2 C16 C17 C18 -179.56(14) C21 C22 C23 C24 0.1(3) Cl1 C22 C23 C24 -178.59(13) C19 C24 C23 C22 -0.9(2) C33A C34A C29A C30A 5(2) C33A C34A C29A C28A 180.0(11) O1A C28A C29A C34A 0(2) O2A C28A C29A C34A -177.5(13) O1A C28A C29A C30A 175.4(15) O2A C28A C29A C30A -3(2) C34A C29A C30A O3A 179.2(13) C28A C29A C30A O3A 4(2) C34A C29A C30A C31A -1(2) C28A C29A C30A C31A -176.2(13) C29A C34A C33A C32A -5.4(18) O3A C30A C31A C32A 178.0(13) C29A C30A C31A C32A -2(2) C30A C31A C32A O4A 175.7(12) C30A C31A C32A C33A 1(2) C34A C33A C32A O4A -172.2(11) C34A C33A C32A C31A 2.4(18) C33B C34B C29B C30B -10(4) C33B C34B C29B C28B 177(2) O1B C28B C29B C34B -4(4) O2B C28B C29B C34B 169(2) O1B C28B C29B C30B -177(3) O2B C28B C29B C30B -3(4) C34B C29B C30B O3B -174(3) C28B C29B C30B O3B -2(4) C34B C29B C30B C31B 6(5) C28B C29B C30B C31B 178(2) C29B C34B C33B C32B 9(4) O3B C30B C31B C32B -179(3) C29B C30B C31B C32B 1(4) C30B C31B C32B O4B -175(2) C30B C31B C32B C33B -2(4) C34B C33B C32B C31B -3(4) C34B C33B C32B O4B 170(2) _cod_database_fobs_code 2108445