#------------------------------------------------------------------------------ #$Date: 2019-07-20 06:59:05 +0300 (Sat, 20 Jul 2019) $ #$Revision: 217185 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/10/84/2108447.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108447 loop_ _publ_author_name 'Bodart, Laurie' 'Tumanov, Nikolay' 'Wouters, Johan' _publ_section_title ; Structural variety of clofaziminium salts: effect of the counter-ion on clofaziminium conformation and crystal packing ; _journal_coeditor_code AW5025 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first ; ; _journal_paper_doi 10.1107/S2052520619007649 _journal_volume 75 _journal_year 2019 _chemical_formula_moiety ; C27 H23 Cl2 N4 + , 0.5C8 H4 O4 2- , 0.5C8 H6 O4 ; _chemical_formula_sum 'C35 H28 Cl2 N4 O4' _chemical_formula_weight 639.51 _chemical_name_common ; bis-clofaziminium terephthalate terephthalic acid ; _chemical_name_systematic ; N-[(2E)-10-(4-chlorophenyl)-3-[(4-chlorophenyl)amino] -2,10-dihydrophenazin-2-ylidene]propan-2-aminium benzene-1,4-dicarboxylic acid benzene-1,4-dicarboxylate ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary dual _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 71.183(3) _cell_angle_beta 73.984(3) _cell_angle_gamma 76.148(2) _cell_formula_units_Z 2 _cell_length_a 10.4028(3) _cell_length_b 10.8454(3) _cell_length_c 15.4229(5) _cell_measurement_reflns_used 5839 _cell_measurement_temperature 295(2) _cell_measurement_theta_max 32.3580 _cell_measurement_theta_min 2.4810 _cell_volume 1561.33(9) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 295(2) _diffrn_detector_area_resol_mean 10.3712 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur Ruby Gemini ultra' _diffrn_measurement_method \w _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0179 _diffrn_reflns_av_unetI/netI 0.0255 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 13059 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.349 _diffrn_reflns_theta_min 2.475 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.254 _exptl_absorpt_correction_T_max 0.921 _exptl_absorpt_correction_T_min 0.886 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R. C. Clark & J. S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'Metallic dark red' _exptl_crystal_density_diffrn 1.360 _exptl_crystal_description Prism _exptl_crystal_F_000 664 _exptl_crystal_size_max 0.717 _exptl_crystal_size_mid 0.483 _exptl_crystal_size_min 0.413 _refine_diff_density_max 0.228 _refine_diff_density_min -0.268 _refine_diff_density_rms 0.034 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.025 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 420 _refine_ls_number_reflns 5704 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.025 _refine_ls_R_factor_all 0.0521 _refine_ls_R_factor_gt 0.0395 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0540P)^2^+0.2490P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1008 _refine_ls_wR_factor_ref 0.1092 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4554 _reflns_number_total 5704 _reflns_threshold_expression I>2\s(I) _cod_data_source_file aw5025sup1.cif _cod_data_source_block lb0329_CLZ-TRPTA_reMo _cod_database_code 2108447 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _oxdiff_exptl_absorpt_empirical_full_min 0.869 _oxdiff_exptl_absorpt_empirical_full_max 1.156 _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _shelx_res_file ; TITL lb0329_clz-trpta_remo_a.res in P-1 lb0329_CLZ-TRPTA_reMo.res created by SHELXL-2016/6 at 18:17:06 on 13-Jul-2018 REM Old TITL lb0329_CLZ-TRPTA_reMo in P-1 REM SHELXT solution in P-1 REM R1 0.208, Rweak 0.013, Alpha 0.035, Orientation as input REM Formula found by SHELXT: C36 N3 O4 Cl2 CELL 0.71073 10.4028 10.8454 15.4229 71.183 73.984 76.148 ZERR 2 0.0003 0.0003 0.0005 0.003 0.003 0.002 LATT 1 SFAC C H N O Cl UNIT 70 56 8 8 4 L.S. 10 PLAN 20 BOND $H list 4 fmap 2 ACTA CONF SHEL 99 0.83 TEMP 22 EQIV $1 -x+1, -y+1, -z+1 HTAB C14 O1_$1 HTAB C20 O2 HTAB C26 O2B HTAB N4 O1 HTAB N3 O2 HTAB N3 O1 HTAB O1B O2 WGHT 0.054000 0.249000 FVAR 6.36451 CL2 5 0.397534 -0.167029 0.958731 11.00000 0.08403 0.04292 = 0.07182 0.00116 -0.02328 -0.00425 CL1 5 0.235038 1.154095 0.164788 11.00000 0.09860 0.04294 = 0.08063 -0.00806 -0.00122 -0.01271 O2 4 0.283920 0.542954 0.835618 11.00000 0.07710 0.05885 = 0.07272 -0.03609 -0.05066 0.01587 O1B 4 0.116140 0.696069 0.930734 11.00000 0.08539 0.04787 = 0.06088 -0.02046 -0.02726 0.00565 O1 4 0.497867 0.519052 0.759517 11.00000 0.08931 0.07131 = 0.04942 -0.02779 -0.03778 0.01360 N1 3 0.175275 0.599338 0.365296 11.00000 0.05169 0.04090 = 0.03166 -0.00964 -0.01774 -0.00469 O2B 4 0.141465 0.860025 0.799148 11.00000 0.10053 0.06783 = 0.04798 -0.02344 -0.01764 0.00300 N4 3 0.379324 0.625059 0.600283 11.00000 0.06025 0.04572 = 0.03727 -0.01210 -0.02218 -0.00844 N2 3 0.134698 0.343763 0.471244 11.00000 0.05668 0.04379 = 0.03795 -0.01193 -0.01872 -0.00817 N3 3 0.331461 0.375317 0.706766 11.00000 0.10225 0.04361 = 0.04495 -0.00334 -0.04289 -0.01738 C29 1 0.455479 0.512974 0.919563 11.00000 0.06690 0.03501 = 0.04706 -0.01630 -0.03348 0.00713 C11 1 0.219624 0.545351 0.447160 11.00000 0.04745 0.04131 = 0.03077 -0.01019 -0.01446 -0.00357 C5 1 0.095630 0.399713 0.387341 11.00000 0.04757 0.04708 = 0.03720 -0.01663 -0.01514 -0.00399 C13 1 0.188563 0.735436 0.314284 11.00000 0.05143 0.04099 = 0.03187 -0.00691 -0.01895 -0.00549 C12 1 0.114516 0.527968 0.332356 11.00000 0.04532 0.04822 = 0.03650 -0.01713 -0.01494 -0.00244 C6 1 0.195076 0.412995 0.499770 11.00000 0.04888 0.04049 = 0.03326 -0.01178 -0.01412 -0.00545 C29B 1 0.048610 0.913077 0.944257 11.00000 0.04725 0.04661 = 0.04350 -0.01390 -0.01929 -0.00003 C9 1 0.321552 0.558366 0.566976 11.00000 0.05028 0.04231 = 0.03532 -0.01364 -0.01582 -0.00468 C28B 1 0.106380 0.821792 0.883637 11.00000 0.05383 0.05239 = 0.05088 -0.01748 -0.02469 0.00218 C15 1 0.309674 0.891539 0.193412 11.00000 0.05086 0.05111 = 0.04387 -0.01013 -0.00599 -0.00924 AFIX 43 H15 2 0.381476 0.911439 0.142524 11.00000 -1.20000 AFIX 0 C14 1 0.296398 0.761870 0.239819 11.00000 0.04837 0.04391 = 0.04212 -0.01396 -0.01281 0.00123 AFIX 43 H14 2 0.359316 0.693379 0.221090 11.00000 -1.20000 AFIX 0 C7 1 0.235818 0.358147 0.586440 11.00000 0.06441 0.03939 = 0.03642 -0.00537 -0.02088 -0.00975 AFIX 43 H7 2 0.221092 0.272984 0.620853 11.00000 -1.20000 AFIX 0 C28 1 0.409256 0.527170 0.831926 11.00000 0.08084 0.03347 = 0.05629 -0.02004 -0.04366 0.01194 C10 1 0.283062 0.613176 0.480200 11.00000 0.05801 0.03881 = 0.03447 -0.00708 -0.01812 -0.00980 AFIX 43 H10 2 0.300778 0.696942 0.444351 11.00000 -1.20000 AFIX 0 C31 1 0.369192 0.485836 1.006771 11.00000 0.06080 0.04764 = 0.05715 -0.01589 -0.03365 0.00062 AFIX 43 H31 2 0.280803 0.475950 1.011888 11.00000 -1.20000 AFIX 0 C8 1 0.295610 0.424316 0.621800 11.00000 0.06169 0.04147 = 0.03480 -0.00915 -0.02208 -0.00525 C21 1 0.329373 0.098014 0.920054 11.00000 0.06383 0.05157 = 0.03979 -0.00622 -0.01664 -0.00474 AFIX 43 H21 2 0.310044 0.085678 0.984567 11.00000 -1.20000 AFIX 0 C18 1 0.093382 0.834887 0.343308 11.00000 0.05055 0.05109 = 0.03896 -0.01297 -0.00695 -0.00419 AFIX 43 H18 2 0.020818 0.814795 0.393556 11.00000 -1.20000 AFIX 0 C16 1 0.215981 0.991667 0.222787 11.00000 0.05696 0.04006 = 0.04735 -0.00866 -0.01519 -0.00442 C25 1 0.400355 0.762382 0.555647 11.00000 0.06115 0.04907 = 0.03870 -0.01294 -0.01163 -0.01625 AFIX 13 H25 2 0.441020 0.772207 0.488906 11.00000 -1.20000 AFIX 0 C20 1 0.312430 0.223825 0.860260 11.00000 0.06897 0.04348 = 0.04528 -0.01223 -0.02351 -0.00183 AFIX 43 H20 2 0.281686 0.295948 0.884987 11.00000 -1.20000 AFIX 0 C17 1 0.107149 0.964581 0.296866 11.00000 0.05711 0.04642 = 0.05119 -0.01633 -0.01016 0.00310 AFIX 43 H17 2 0.043752 1.033019 0.315293 11.00000 -1.20000 AFIX 0 C22 1 0.374848 -0.008800 0.883951 11.00000 0.05362 0.04056 = 0.05087 -0.00535 -0.01900 -0.00540 C4 1 0.032022 0.326858 0.355516 11.00000 0.06047 0.05015 = 0.05011 -0.01885 -0.01990 -0.00934 AFIX 43 H4A 2 0.018621 0.241819 0.391230 11.00000 -1.20000 AFIX 0 C19 1 0.340552 0.244222 0.763962 11.00000 0.06273 0.04551 = 0.04242 -0.00635 -0.02709 -0.00981 C1 1 0.070907 0.580940 0.247440 11.00000 0.06383 0.05501 = 0.03967 -0.01092 -0.02374 -0.00773 AFIX 43 H1 2 0.083759 0.665665 0.210633 11.00000 -1.20000 AFIX 0 C30 1 0.586949 0.526796 0.913320 11.00000 0.06643 0.04919 = 0.04470 -0.01486 -0.02518 0.00159 AFIX 43 H30 2 0.646204 0.544698 0.855025 11.00000 -1.20000 AFIX 0 C3 1 -0.010210 0.379585 0.272849 11.00000 0.06176 0.06495 = 0.05315 -0.02716 -0.02518 -0.00813 AFIX 43 H3A 2 -0.051925 0.330510 0.252429 11.00000 -1.20000 AFIX 0 C2 1 0.009245 0.506699 0.219280 11.00000 0.06723 0.06750 = 0.04393 -0.01799 -0.02878 -0.00442 AFIX 43 H2 2 -0.020192 0.542051 0.163199 11.00000 -1.20000 AFIX 0 C30B 1 0.022049 1.046919 0.904004 11.00000 0.08027 0.05216 = 0.03650 -0.00950 -0.01908 -0.00233 AFIX 43 H34 2 0.036702 1.079580 0.839052 11.00000 -1.20000 AFIX 0 C32 1 -0.026194 1.133260 0.959185 11.00000 0.08032 0.04123 = 0.04622 -0.00996 -0.02408 0.00182 AFIX 43 H35 2 -0.043774 1.223561 0.931024 11.00000 -1.20000 AFIX 0 C23 1 0.402658 0.008803 0.788635 11.00000 0.06924 0.04850 = 0.05596 -0.01875 -0.02222 -0.00376 AFIX 43 H23 2 0.432384 -0.063843 0.764443 11.00000 -1.20000 AFIX 0 C24 1 0.386248 0.134758 0.729066 11.00000 0.07517 0.05723 = 0.04008 -0.01285 -0.02200 -0.00950 AFIX 43 H24 2 0.406099 0.146447 0.664611 11.00000 -1.20000 AFIX 0 C26 1 0.268018 0.858607 0.564158 11.00000 0.07545 0.04829 = 0.07616 -0.01689 -0.02101 -0.00848 AFIX 137 H26A 2 0.206996 0.838045 0.536099 11.00000 -1.50000 H26B 2 0.285334 0.946984 0.532543 11.00000 -1.50000 H26C 2 0.227995 0.851673 0.629217 11.00000 -1.50000 AFIX 0 C27 1 0.498459 0.792721 0.599839 11.00000 0.08304 0.06981 = 0.07975 -0.02204 -0.03311 -0.02564 AFIX 137 H27A 2 0.457964 0.788221 0.664522 11.00000 -1.50000 H27B 2 0.519009 0.879794 0.567179 11.00000 -1.50000 H27C 2 0.580454 0.729337 0.595766 11.00000 -1.50000 AFIX 0 H4 2 0.410693 0.587895 0.650420 11.00000 0.05997 H3 2 0.337211 0.429457 0.733976 11.00000 0.08476 H3B 2 0.169304 0.641448 0.892447 11.00000 0.11719 HKLF 4 REM lb0329_clz-trpta_remo_a.res in P-1 REM R1 = 0.0395 for 4554 Fo > 4sig(Fo) and 0.0521 for all 5704 data REM 420 parameters refined using 0 restraints END WGHT 0.0540 0.2490 REM Highest difference peak 0.228, deepest hole -0.268, 1-sigma level 0.034 Q1 1 0.4173 -0.1746 0.8965 11.00000 0.05 0.23 Q2 1 0.2536 1.1543 0.2207 11.00000 0.05 0.22 Q3 1 0.4269 0.3577 0.6763 11.00000 0.05 0.16 Q4 1 0.3980 0.1964 0.7426 11.00000 0.05 0.15 Q5 1 0.0023 1.1187 1.0020 11.00000 0.05 0.14 Q6 1 0.3432 -0.0108 0.8494 11.00000 0.05 0.14 Q7 1 0.2721 0.5012 0.6024 11.00000 0.05 0.13 Q8 1 0.0661 0.4813 0.3750 11.00000 0.05 0.13 Q9 1 0.2649 0.7336 0.4610 11.00000 0.05 0.13 Q10 1 0.3649 0.2380 0.8114 11.00000 0.05 0.13 Q11 1 0.5114 0.5115 0.7275 11.00000 0.05 0.12 Q12 1 0.4865 0.4924 0.7127 11.00000 0.05 0.12 Q13 1 0.1963 0.4738 0.4811 11.00000 0.05 0.12 Q14 1 0.2283 0.5616 0.4003 11.00000 0.05 0.12 Q15 1 0.2682 0.5983 0.5366 11.00000 0.05 0.12 Q16 1 0.2836 0.5656 0.4435 11.00000 0.05 0.12 Q17 1 0.1832 0.6939 0.3326 11.00000 0.05 0.12 Q18 1 0.1379 0.9801 0.2316 11.00000 0.05 0.12 Q19 1 0.3386 0.5568 0.5139 11.00000 0.05 0.12 Q20 1 0.1561 0.4374 0.3527 11.00000 0.05 0.12 ; _shelx_res_checksum 38194 _shelx_hkl_file ; 0 0 2 20107.7 264.194 5 0 0 2 19830.3 216.451 2 0 0 3 30862.3 404.243 5 0 0 3 30385.6 331.289 2 0 0 -4 116.956 37.9367 5 0 0 4 103.562 35.8916 5 0 0 -4 134.918 33.4627 2 0 0 4 65.4557 28.0329 2 0 0 5 25502.7 390.755 2 0 0 5 25121.5 468.805 5 0 0 -5 26612.2 485.676 5 0 0 -5 26250.7 385.551 2 0 0 -6 25244.5 521.972 5 0 0 6 24770.2 514.448 5 0 0 -6 25009.0 564.121 6 0 0 6 23940.2 414.023 2 0 0 -6 24532.6 406.121 2 0 0 -7 25248.4 443.759 2 0 0 7 25192.9 458.977 2 0 0 -7 25520.6 622.911 6 0 0 7 24766.5 563.888 5 0 0 -7 25653.1 572.572 5 0 0 -8 4325.26 254.076 5 0 0 -8 3994.15 190.102 2 0 0 -8 4134.64 274.831 6 0 0 8 3953.50 247.721 5 0 0 -9 5403.83 332.996 6 0 0 -9 5172.29 230.612 2 0 0 -10 4172.19 314.290 6 0 0 -10 4210.36 222.435 2 0 0 -11 388.924 119.173 6 0 0 -11 448.158 89.9892 2 0 0 -12 301.934 116.570 6 0 0 -13 1433.95 235.926 6 0 0 -14 248.203 134.644 6 0 0 -15 2932.84 351.497 6 0 0 -16 254.445 146.960 6 0 0 -17 63.2012 159.986 6 0 0 -18-147.100 164.309 6 0 0 -19-213.204 122.165 6 0 0 -20 84.9274 192.984 6 0 1 -19 569.395 228.258 6 0 1 -18 265.914 170.537 6 0 1 -17 1187.92 276.474 6 0 1 -16 569.750 195.544 6 0 1 -15 211.038 123.721 6 0 1 -14 926.077 203.693 6 0 1 -13 8035.76 521.058 6 0 1 -12 5340.66 405.886 6 0 -1 12 4967.24 357.217 5 0 1 -11 3191.21 300.653 6 0 -1 11 2994.55 224.885 2 0 -1 11 3004.89 274.403 5 0 -1 10 2078.47 181.442 2 0 -1 10 1914.23 208.312 5 0 1 -9 163.397 60.6420 2 0 -1 9 132.178 75.8550 5 0 -1 9 69.2993 42.4818 2 0 -1 8 1688.24 147.080 2 0 1 -8 1571.22 139.893 2 0 -1 8 1464.28 164.574 5 0 -1 7 17753.7 439.686 2 0 -1 7 17397.6 503.858 5 0 1 -7 17048.4 421.544 2 0 -1 6 18099.6 416.103 2 0 1 -6 17605.5 401.017 2 0 -1 6 17063.5 459.170 5 0 1 -6 18608.9 487.869 5 0 1 -5 1574.92 115.219 2 0 -1 5 1509.76 113.462 2 0 1 -5 1507.36 130.089 5 0 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245.202 6 0 -1 -17 2179.01 333.183 6 0 -1 -18 115.623 172.204 6 0 -1 -19 108.737 126.209 6 0 -1 -20-158.507 186.503 6 0 2 -19 223.289 203.207 6 0 2 -18-38.6878 130.196 6 0 2 -17 116.839 125.679 6 0 2 -16 2840.12 382.930 6 0 2 -15 2439.69 330.509 6 0 2 -14 2560.39 333.882 6 0 -2 14 2144.45 278.099 5 0 -2 13 29.7264 84.8040 5 0 2 -13 86.2267 121.276 6 0 -2 12 262.813 114.711 5 0 -2 11 7176.45 431.807 5 0 -2 10 19218.4 662.768 5 0 -2 9 10432.3 464.863 5 0 -2 9 11414.2 430.610 2 0 -2 8 11982.5 426.554 2 0 -2 8 11916.7 470.536 5 0 2 -7 5845.35 282.012 2 0 -2 7 6293.38 295.702 2 0 -2 7 6091.11 317.891 5 0 -2 6 396.249 76.2839 2 0 2 -6 505.745 92.8301 2 0 2 -6 452.050 91.2755 5 0 -2 6 477.108 91.7068 5 0 2 -5 135.671 54.9626 5 0 -2 5 117.574 53.5434 2 0 2 -5 157.999 57.5459 2 0 -2 5 86.1922 41.4388 5 0 2 -4 7836.99 300.225 5 0 2 -4 7643.85 131.757 1 0 2 -4 7711.00 272.229 2 0 -2 4 7282.88 288.452 5 0 -2 4 7477.75 270.443 2 0 -2 3 5846.69 221.867 2 0 2 -3 6058.07 227.140 2 0 -2 3 5824.85 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409.518 4 3 -4 -9 1423.30 190.897 6 3 -4 -8 28514.6 785.535 6 3 -4 -7 7903.28 402.129 6 -3 4 6 29420.7 571.826 4 3 -4 -6 29583.5 739.251 6 3 -4 -5 6894.68 234.317 2 3 -4 -5 7275.78 354.548 6 -3 4 5 7383.04 286.952 4 -3 4 5 7347.95 356.718 6 3 -4 -4 14.3856 29.9446 2 3 -4 -4 0.12380 53.1897 6 -3 4 4 7.20987 41.3433 6 -3 4 4 42.7437 32.7321 4 3 -4 -3 10961.5 343.703 5 3 -4 -3 11093.1 413.066 6 3 -4 -3 10637.1 335.742 2 -3 4 3 10417.3 359.796 4 -3 4 3 11095.0 325.029 2 -3 4 3 11467.7 409.245 6 3 -4 -2 14403.9 412.654 2 -3 4 2 14562.2 397.781 2 3 -4 -2 14834.8 417.169 5 3 -4 -2 14672.7 463.866 6 -3 4 2 14836.6 463.825 6 3 -4 -1 1327.46 146.524 6 3 -4 -1 1240.99 134.186 2 3 -4 -1 1298.67 135.177 5 -3 4 1 1318.25 129.467 2 -3 4 1 1450.02 145.029 6 -3 4 0 6524.10 298.091 2 3 -4 0 6316.80 306.643 2 3 -4 0 6790.58 312.554 5 3 -4 0 5804.79 298.927 6 -3 4 0 6441.29 304.678 6 -3 4 0 6252.44 234.877 3 -3 4 -1 10381.1 393.316 6 -3 4 -1 10400.2 271.040 3 -3 4 -1 10432.4 391.285 2 3 -4 1 10224.1 396.467 5 3 -4 1 10925.3 416.649 2 3 -4 1 10246.6 399.259 6 -3 4 -2 23826.6 614.954 2 -3 4 -2 23654.0 329.241 3 3 -4 2 24831.0 656.198 2 3 -4 2 23981.1 568.710 1 -3 4 -2 23365.1 608.542 6 -3 4 -2 23035.3 606.443 5 3 -4 2 23930.7 635.261 5 3 -4 3 67699.3 941.494 1 3 -4 3 68287.2 1114.88 5 -3 4 -3 68201.7 1081.89 2 -3 4 -3 71000.6 1102.27 6 3 -4 4 16803.5 575.724 5 3 -4 4 17070.5 468.089 1 -3 4 -5 14631.8 542.394 2 3 -4 5 15071.8 570.894 5 3 -4 6 33645.1 878.425 5 -3 4 -6 33207.0 842.418 2 -3 4 -7 39182.5 945.230 2 3 -4 7 40740.9 1011.36 5 -3 4 -8 2454.31 253.053 2 3 -4 8 2342.24 257.726 5 3 -4 9 4381.22 362.766 5 -3 4 -9 4182.38 338.859 2 -3 4 -10 62.4394 104.295 2 3 -4 10-21.9616 81.1414 5 3 -4 11 211.161 98.8033 5 -3 4 -11 114.502 108.458 2 -3 4 -12 1949.85 265.005 2 3 -4 12 1465.31 243.830 5 -3 4 -13 2139.69 285.820 2 3 -4 13 2633.78 338.860 5 -3 4 -14 26.1251 90.6127 2 3 -4 14-58.1442 105.952 5 -3 4 -15 2784.90 330.782 2 3 -4 15 3019.83 382.643 5 3 -4 16-75.8839 142.666 5 -3 4 -17 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29445.8 675.441 6 3 -3 4 29805.3 720.473 2 -3 3 -4 30437.7 719.281 5 3 -3 4 29287.7 702.099 5 3 -3 4 28838.9 582.027 1 3 -3 5 12157.9 476.082 5 3 -3 6 1545.89 183.519 5 -3 3 -6 1384.28 169.779 2 -3 3 -7 17738.0 601.409 2 -3 3 -7 17779.3 463.321 1 3 -3 7 18005.0 635.952 5 -3 3 -8 9758.59 353.098 1 3 -3 8 10107.6 499.517 5 -3 3 -8 9381.72 452.220 2 3 -3 9 6062.39 128.042 3 -3 3 -9 7269.47 417.391 2 3 -3 9 7281.20 448.221 5 -3 3 -9 6846.00 300.195 1 3 -3 10 15878.8 679.683 5 -3 3 -10 15880.4 623.233 2 -3 3 -10 15036.3 454.596 1 3 -3 10 14857.4 269.119 3 -3 3 -11 614.858 106.560 1 3 -3 11 657.905 164.496 5 3 -3 11 597.775 74.6860 3 -3 3 -11 326.374 103.758 2 -3 3 -12 636.856 146.467 2 3 -3 12 615.852 155.474 5 -3 3 -13 986.809 197.023 2 3 -3 13 1172.04 225.944 5 3 -3 14 55.0142 92.9287 5 -3 3 -14 49.0910 104.893 2 -3 3 -15 1354.33 231.378 2 3 -3 15 1942.01 292.092 5 -3 3 -16 57.6753 114.541 2 -3 3 -16-159.541 130.878 6 -3 3 -17-28.4087 148.527 6 -3 3 -17 241.732 135.729 2 -3 3 -18 468.769 175.770 6 -3 3 -19-123.891 191.087 6 3 -2 -19 570.560 210.275 6 3 -2 -18 285.779 167.941 6 3 -2 -17 65.2406 115.978 6 3 -2 -16 778.915 211.410 6 3 -2 -16 951.683 186.173 4 3 -2 -15 465.401 134.263 4 3 -2 -15 460.113 160.020 6 3 -2 -14 1393.48 252.388 6 3 -2 -14 1354.58 198.982 4 3 -2 -13 344.224 125.710 6 3 -2 -13-62.1608 92.5619 4 3 -2 -12 9119.40 540.741 6 3 -2 -12 9253.53 447.722 4 3 -2 -11 178.425 75.5180 5 3 -2 -11 59.4435 80.1437 4 3 -2 -11 147.463 120.866 6 3 -2 -10 20040.8 501.743 5 3 -2 -10 21279.3 726.969 6 3 -2 -10 20427.0 607.020 4 3 -2 -9 267.246 76.4937 4 3 -2 -9 340.139 70.0452 5 3 -2 -9 449.889 130.532 6 3 -2 -8 6176.34 304.600 4 3 -2 -8 5431.73 333.543 6 3 -2 -8 5718.82 230.429 5 3 -2 -7 5060.76 305.916 6 3 -2 -7 4931.82 265.525 4 3 -2 -7 5006.35 195.839 5 3 -2 -6 4372.31 262.691 6 3 -2 -6 4357.10 164.362 5 3 -2 -6 4789.46 249.107 4 -3 2 6 4397.84 260.770 6 -3 2 5 4422.66 94.8705 2 -3 2 5 4616.93 251.067 6 -3 2 5 4810.13 233.201 4 3 -2 -5 4619.30 230.722 4 3 -2 -5 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1363.64 159.419 2 7 -4 -3 1297.17 121.858 5 7 -4 -3 1686.28 240.979 1 7 -4 -3 1248.23 169.097 6 7 -4 -2 96.5629 82.1047 6 7 -4 -2 188.952 111.390 1 7 -4 -2 169.041 63.2227 5 -7 4 2 154.470 79.6725 2 7 -4 -1 38.5306 55.9059 6 7 -4 -1 103.159 93.3728 1 7 -4 -1-10.6892 50.4138 5 -7 4 1 182.543 88.5467 2 7 -4 0 255.297 88.3562 6 7 -4 0 274.124 83.3114 5 7 -4 0 178.623 93.5060 1 -7 4 0 293.035 113.188 2 -7 4 -1 5.04295 60.2277 2 7 -4 1 166.923 93.4844 1 7 -4 1 48.4518 64.2414 5 7 -4 2 8792.23 492.032 1 -7 4 -2 8370.35 451.666 2 7 -4 2 9123.64 443.456 5 7 -4 3 926.358 161.386 5 7 -4 3 941.414 180.655 1 -7 4 -3 1251.92 187.226 2 -7 4 -3 852.792 110.841 3 -7 4 -4 4358.37 348.122 2 7 -4 4 3999.94 323.275 5 -7 4 -4 4464.64 207.564 3 7 -4 4 3947.94 321.909 1 7 -4 5-101.647 92.8657 5 -7 4 -5 41.6121 30.8415 3 -7 4 -5 112.064 109.651 2 7 -4 6 20.3621 86.2316 5 -7 4 -6 14.8626 90.2522 2 7 -4 7 1768.81 255.990 5 -7 4 -7 1572.55 238.973 2 7 -4 8 211.449 150.524 5 -7 4 -8-132.638 106.157 2 7 -4 9 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325.341 1 7 -2 3 22511.5 632.720 5 -7 2 -3 22059.5 696.236 2 -7 2 -3 21778.5 556.243 3 7 -2 3 22076.8 719.745 1 -7 2 -3 19897.6 469.353 6 -7 2 -4 52.2269 36.6798 6 -7 2 -4 87.7790 66.6382 2 7 -2 4 32.2654 59.8767 5 -7 2 -4 72.1297 56.9195 3 7 -2 5 5456.50 350.778 5 -7 2 -5 5243.58 363.196 2 -7 2 -5 5049.09 235.910 3 -7 2 -6 775.659 114.022 6 -7 2 -6 778.844 95.1898 3 -7 2 -6 869.616 164.047 2 7 -2 6 891.225 157.684 5 -7 2 -7 240.305 91.5389 2 -7 2 -7 104.567 40.6660 3 7 -2 7 78.3693 94.8752 5 7 -2 8 5835.38 411.942 5 -7 2 -8 5803.07 416.560 2 -7 2 -8 5926.85 191.027 3 -7 2 -9 744.799 162.900 2 7 -2 9 908.945 190.294 5 -7 2 -10 1829.14 255.702 2 7 -2 10 1626.81 234.212 5 -7 2 -11 1334.80 231.261 2 7 -2 11 988.635 198.936 5 -7 2 -12 79.1622 115.093 2 -7 2 -13 80.7888 100.324 2 -7 2 -14 55.9046 119.780 2 -7 2 -15 1225.60 248.670 2 -7 2 -15 1510.48 254.083 6 -7 2 -16 305.425 147.169 6 -7 2 -16 70.0553 118.646 2 -7 2 -17 83.7126 109.678 2 -7 2 -17-0.35715 106.866 6 -7 2 -18 1966.60 320.813 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1816.52 319.671 5 -8 7 -9 1416.05 287.714 2 8 -7 10-90.0479 131.377 5 -8 7 -10 207.465 174.186 2 8 -7 11 847.080 282.835 5 -8 7 -11 796.049 219.521 2 8 -7 12 86.0428 179.928 5 8 -6 -14-205.049 167.364 6 8 -6 -13 173.114 161.616 6 8 -6 -12 183.006 128.382 6 8 -6 -11-81.1894 97.8245 6 8 -6 -10-87.0211 129.099 6 8 -6 -9 910.177 202.926 6 8 -6 -8 224.323 132.096 6 8 -6 -7 3.28161 103.907 6 8 -6 -6 336.878 117.024 6 8 -6 -6 102.153 122.352 1 8 -6 -5-23.0999 80.8756 6 -8 6 5 149.314 82.5516 2 8 -6 -5-36.9000 127.094 1 8 -6 -4 303.475 129.859 6 -8 6 4 140.183 86.4021 2 8 -6 -4 60.4601 116.541 1 8 -6 -3 254.023 107.506 6 8 -6 -3 163.936 74.3222 5 -8 6 3 207.181 102.954 2 8 -6 -3 110.764 145.501 1 8 -6 -2 450.924 136.414 6 8 -6 -2 531.072 164.660 1 8 -6 -2 261.929 97.8998 5 -8 6 2 459.969 132.037 2 8 -6 -1 242.077 112.004 5 -8 6 1 177.586 103.708 2 8 -6 -1 400.900 151.452 1 8 -6 0 12270.5 678.425 1 -8 6 0 11033.3 557.023 2 8 -6 0 12688.7 566.531 5 8 -6 1 7892.04 543.427 1 -8 6 -1 7734.04 484.713 2 8 -6 1 8388.28 485.523 5 8 -6 2 278.700 109.292 5 -8 6 -2 402.617 129.248 2 8 -6 2 487.072 173.970 1 -8 6 -3 2380.44 290.062 2 8 -6 3 2338.06 276.795 5 8 -6 3 2297.44 309.927 1 8 -6 4 77.2918 114.238 1 8 -6 4 53.9122 94.2361 5 -8 6 -4 240.140 127.740 2 8 -6 5 652.851 181.722 5 -8 6 -5 822.386 199.824 2 -8 6 -6 2489.59 322.341 2 8 -6 6 2909.39 350.749 5 8 -6 7 376.032 165.451 5 -8 6 -7 612.771 193.927 2 8 -6 8 581.162 189.668 5 -8 6 -8 413.445 179.236 2 8 -6 9 936.290 235.030 5 -8 6 -9 565.900 186.988 2 8 -6 10 124.326 124.768 5 -8 6 -10 59.7201 119.867 2 8 -6 11 1254.13 267.896 5 -8 6 -11 947.842 249.247 2 8 -6 12 77.6502 116.540 5 -8 6 -12 254.849 161.735 2 8 -6 13 519.804 211.993 5 -8 6 -13 259.594 171.866 2 8 -5 -14 285.929 144.328 6 8 -5 -13 23.3883 109.250 6 8 -5 -12-29.4972 112.769 6 8 -5 -11-61.7427 119.830 6 8 -5 -10 320.110 146.833 6 8 -5 -9 587.445 170.123 6 8 -5 -8 1311.65 214.724 6 8 -5 -7 3613.48 338.027 6 8 -5 -6 2713.86 350.846 1 8 -5 -6 2244.80 255.228 6 8 -5 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1146.23 232.576 2 -8 5 -8 8480.14 573.663 2 8 -5 8 8092.25 570.228 5 8 -5 9 358.529 155.006 5 -8 5 -9 180.842 108.590 2 -8 5 -10 2856.11 365.131 2 8 -5 10 2704.74 353.646 5 8 -5 11 100.758 138.660 5 -8 5 -11-71.8619 140.305 2 -8 5 -12 3089.50 397.129 2 8 -5 12 2758.16 384.180 5 8 -5 13 1034.36 286.865 5 -8 5 -13 534.714 186.270 2 8 -5 14 27.4742 128.119 5 -8 5 -14-171.148 164.126 2 -8 5 -15-51.5905 137.235 2 8 -4 -15 464.057 215.279 1 8 -4 -14-84.4599 149.089 6 8 -4 -13 130.790 116.302 6 8 -4 -12 396.478 138.466 6 8 -4 -11 303.178 125.874 6 8 -4 -10-74.6884 118.946 6 8 -4 -9 88.1740 104.796 6 8 -4 -8 1552.52 231.148 6 8 -4 -8 1402.61 257.106 1 8 -4 -7 3054.72 365.037 1 8 -4 -7 3405.44 312.801 6 -8 4 6 4321.19 235.844 2 8 -4 -6 5003.75 445.198 1 8 -4 -6 4115.18 330.243 6 8 -4 -5 147.130 77.6421 6 8 -4 -5-49.7611 106.620 1 -8 4 5 46.8524 57.4694 2 8 -4 -4 1007.71 224.925 1 8 -4 -4 809.813 143.514 6 -8 4 4 1037.96 147.425 2 8 -4 -3 36.4555 56.1009 6 8 -4 -3 169.113 110.198 1 -8 4 3 30.8689 75.3179 2 8 -4 -2 582.663 156.746 1 8 -4 -2 586.623 112.202 6 8 -4 -2 543.972 92.3102 5 -8 4 2 769.787 144.748 2 8 -4 -1 4671.54 310.560 6 8 -4 -1 5304.40 421.513 1 -8 4 1 4395.03 320.193 2 8 -4 -1 4840.24 274.532 5 8 -4 0 1105.61 148.821 5 8 -4 0 1186.12 214.819 1 -8 4 0 1271.71 183.051 2 8 -4 1-21.1977 100.813 1 8 -4 1 65.6852 60.2711 5 -8 4 -1-17.7850 89.8000 2 -8 4 -2 754.777 157.653 2 8 -4 2 849.200 152.909 5 8 -4 2 625.514 165.241 1 -8 4 -3 237.086 94.0597 2 8 -4 3 182.737 96.0813 5 8 -4 3 137.911 110.574 1 -8 4 -3 92.6273 50.3441 3 8 -4 4-66.6483 96.3490 5 -8 4 -4-3.68383 45.5082 3 -8 4 -4 22.7982 94.2407 2 8 -4 5 63.4593 70.0045 5 -8 4 -5 37.2317 42.9241 3 -8 4 -5 110.397 100.790 2 8 -4 6-129.890 93.3051 5 -8 4 -6-110.041 92.7585 2 8 -4 7 825.829 191.754 5 -8 4 -7 785.204 187.167 2 8 -4 8 404.197 148.444 5 -8 4 -8 318.914 146.833 2 -8 4 -9 3127.22 356.081 2 8 -4 9 3302.77 366.417 5 8 -4 10 181.397 114.644 5 -8 4 -10 36.3533 126.014 2 -8 4 -11 126.917 117.410 2 8 -4 11 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640.136 174.202 2 8 -3 9 420.770 140.677 5 -8 3 -10 260.360 139.098 2 8 -3 10 347.427 142.118 5 -8 3 -11 7129.20 538.257 2 8 -3 11 7129.22 542.752 5 -8 3 -12 7.91436 123.770 2 -8 3 -13 376.746 170.389 2 -8 3 -14-5.39859 145.103 2 -8 3 -15-11.6181 118.837 2 -8 3 -16 927.157 235.627 6 -8 3 -16 576.361 199.770 2 -8 3 -17-52.1166 165.816 2 -8 3 -17 122.022 145.383 6 -8 3 -18 98.2295 140.499 6 8 -2 -15 235.618 160.594 6 8 -2 -14-201.120 177.500 1 8 -2 -14 79.8010 121.813 6 8 -2 -13-290.679 136.367 1 8 -2 -13-221.067 154.120 4 8 -2 -13 141.240 118.615 6 8 -2 -12-48.5633 125.790 4 8 -2 -12 99.3973 122.797 1 8 -2 -12 119.734 105.707 6 8 -2 -11 218.466 153.194 1 8 -2 -11-7.15808 141.115 4 8 -2 -11 128.380 97.1352 6 8 -2 -10 40.3412 93.1202 4 8 -2 -10-58.6578 84.5140 6 8 -2 -9 2326.15 317.947 1 8 -2 -9 2194.85 260.088 6 8 -2 -8 3929.23 388.493 1 8 -2 -8 3316.51 298.857 6 8 -2 -7-77.9096 111.003 1 8 -2 -7 44.3349 70.8811 6 8 -2 -6-14.1702 72.5882 6 -8 2 6 202.702 67.8659 2 8 -2 -6-36.7042 108.427 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295.114 163.281 3 8 5 -9 422.231 158.893 6 8 5 -9 260.767 158.661 4 -8 -5 9 223.007 176.561 3 8 5 -8-68.7941 95.7089 6 8 5 -8 162.232 158.739 4 -8 -5 8 112.899 143.849 3 8 5 -7 960.619 191.974 6 8 5 -7 761.780 209.761 4 -8 -5 7 1238.67 247.583 3 -8 -5 6 1579.20 164.431 5 8 5 -6 1744.98 233.275 6 8 5 -6 1641.11 289.242 4 -8 -5 6 1839.81 292.023 3 -8 -5 5 388.694 97.8442 5 8 5 -5 239.097 86.1715 6 8 5 -5 225.269 138.107 4 -8 -5 5 323.041 162.714 3 -8 -5 4 464.413 99.1282 5 8 5 -4 407.678 141.887 4 -8 -5 4 531.799 180.364 3 -8 -5 3 2003.14 179.239 5 -8 -5 3 1801.57 271.142 3 8 5 -3 1924.36 282.229 4 8 5 -2 1615.54 166.083 6 -8 -5 2 1898.48 177.916 5 -8 -5 2 2104.33 279.203 3 8 5 -2 1896.74 278.229 4 8 5 -1 2100.39 174.625 6 -8 -5 1 2516.36 296.723 3 8 5 -1 2384.03 294.800 4 -8 -5 0 2953.86 311.077 3 8 5 0 3373.85 339.750 4 8 5 0 2693.95 176.052 6 -8 -5 -1 3639.77 339.135 3 8 5 1 3960.15 357.042 4 8 5 1 3544.39 182.006 6 -8 -5 -2-72.2082 84.7826 3 8 5 2-14.0988 31.0609 6 -8 -5 -3 1702.68 233.666 3 8 5 3 2095.10 259.440 4 8 5 3 1259.28 88.6707 6 8 5 4 2818.78 293.210 4 8 5 4 2322.81 112.843 6 -8 -5 -5 729.171 162.629 3 8 5 5 686.888 66.8630 6 8 5 5 887.044 170.613 4 -8 -5 -6 3744.38 171.942 6 -8 -5 -6 4045.55 324.258 3 8 5 6 3368.28 157.531 6 -8 -5 -7 2394.61 256.853 3 -8 -5 -7 2173.44 143.563 6 -8 -5 -8 480.100 79.4613 6 -8 -5 -8 534.234 136.626 3 -8 -5 -9 4134.24 332.756 3 -8 -5 -9 4258.74 238.669 6 -8 -5 -10 1145.70 136.463 6 -8 -5 -10 1069.91 182.401 3 -8 -5 -11 1085.00 201.096 3 -8 -5 -11 1097.07 150.326 6 -8 -5 -12 875.226 176.162 3 -8 -5 -12 885.857 144.167 6 -8 -5 -13 1266.74 209.611 3 -8 -5 -13 1193.51 172.111 6 -8 -5 -14 1562.34 238.420 3 -8 -5 -14 1808.47 225.324 6 -8 -5 -15 5651.24 399.014 6 -8 -5 -15 5262.99 415.112 3 -8 -5 -16 457.085 145.713 3 -8 -5 -16 356.016 127.470 6 -8 -5 -17 15.9535 120.422 2 -8 -5 -17-73.5377 113.783 6 -8 -5 -18 56.6872 124.307 2 -8 -5 -18 42.7403 105.835 6 -8 -5 -19-22.5941 115.506 2 -8 -5 -19 82.0140 105.108 6 -8 -5 -20 1123.75 231.163 2 -8 -5 -20 1747.70 309.969 6 -8 -5 -21 1860.34 293.137 2 -8 -5 -21 1382.44 281.113 6 -8 -5 -22 645.591 199.610 6 8 6 -12-44.8499 132.304 6 -8 -6 12 255.524 166.762 3 8 6 -11-253.063 200.714 4 8 6 -11-344.691 203.178 6 -8 -6 11-222.343 190.064 3 8 6 -10 142.864 143.145 6 -8 -6 10 64.7887 126.792 3 8 6 -9-163.656 136.279 6 8 6 -9 210.805 150.584 4 -8 -6 9 115.620 136.304 3 8 6 -8 0.28057 98.7994 6 8 6 -8 0.82862 127.980 4 -8 -6 8-70.7364 113.789 3 8 6 -7 2354.06 287.163 6 8 6 -7 1546.89 295.814 4 -8 -6 7 1859.33 292.185 3 -8 -6 6 1050.92 161.312 5 8 6 -6 1064.79 241.475 4 -8 -6 6 857.101 203.085 3 -8 -6 5 40.4537 64.2856 5 8 6 -5 72.1526 114.384 4 -8 -6 5 123.347 131.069 3 -8 -6 4 94.0157 68.6901 5 8 6 -4 235.374 120.958 4 -8 -6 4 130.178 129.976 3 -8 -6 3 2357.98 215.699 5 8 6 -3 1962.22 291.454 4 -8 -6 3 2004.62 271.388 3 -8 -6 2 1701.69 188.497 5 8 6 -2 1643.09 269.737 4 -8 -6 2 1874.16 272.843 3 -8 -6 1 3572.68 366.443 3 8 6 -1 3597.72 368.708 4 -8 -6 0 30252.6 973.197 3 8 6 0 28787.3 999.464 4 8 6 1 631.041 101.188 6 -8 -6 -1 612.706 156.936 3 -8 -6 -2 9788.54 541.833 3 8 6 2 9394.40 549.840 4 8 6 2 7978.04 309.682 6 -8 -6 -3 2806.24 292.618 3 8 6 3 2876.99 312.012 4 8 6 3 2396.87 163.143 6 -8 -6 -4 503.263 151.146 3 8 6 4 391.677 117.715 4 8 6 4 269.075 60.0887 6 -8 -6 -5-14.0981 82.1802 3 8 6 5 8.27480 43.0306 6 8 6 5-23.3824 85.7788 4 -8 -6 -6 952.986 112.878 6 -8 -6 -6 1237.04 195.387 3 8 6 6 766.784 96.5192 6 8 6 6 1117.10 186.701 4 -8 -6 -7 3040.75 192.987 6 -8 -6 -7 2777.50 286.883 3 8 6 7 2570.74 176.981 6 -8 -6 -8 815.950 170.153 3 8 6 8 651.941 98.1242 6 -8 -6 -8 898.056 119.070 6 -8 -6 -9-78.6108 55.0130 6 -8 -6 -9-52.0746 110.569 3 8 6 9 46.1694 63.8561 6 -8 -6 -10 1719.52 250.785 3 -8 -6 -10 1839.29 182.228 6 -8 -6 -11 3272.11 318.965 3 -8 -6 -11 3045.31 247.666 6 -8 -6 -12 429.376 141.316 3 -8 -6 -12 245.516 100.035 6 -8 -6 -13 377.841 132.334 3 -8 -6 -13 443.928 121.338 6 -8 -6 -14 2051.22 283.595 3 -8 -6 -14 2001.78 242.484 6 -8 -6 -15 261.353 120.682 3 -8 -6 -15 321.479 132.503 6 -8 -6 -16 407.263 171.635 3 -8 -6 -16 322.653 127.655 6 -8 -6 -17 1139.17 219.524 3 -8 -6 -17 804.792 185.078 6 -8 -6 -18 177.897 138.218 2 -8 -6 -18 314.082 143.356 6 -8 -6 -19 562.809 194.215 2 -8 -6 -19 484.044 167.039 6 -8 -6 -20 20.0761 124.451 2 -8 -6 -20 258.319 131.404 6 -8 -6 -21 708.099 206.764 2 -8 -6 -21 695.808 212.632 6 -8 -6 -22 283.328 148.095 6 8 7 -11-26.5899 153.773 6 -8 -7 11-170.798 124.462 3 8 7 -10 82.4643 125.571 6 8 7 -10 104.267 162.816 4 -8 -7 10 15.9475 129.844 3 8 7 -9 281.247 143.341 6 8 7 -9 107.702 158.096 4 -8 -7 9 311.827 159.067 3 8 7 -8 122.110 143.011 4 -8 -7 8-199.402 161.911 3 8 7 -7 600.224 214.167 4 -8 -7 7 385.830 158.957 3 -8 -7 6 164.798 97.0017 5 8 7 -6 218.804 143.730 4 -8 -7 6 215.280 155.610 3 -8 -7 5-18.8872 106.298 3 -8 -7 5 34.1821 78.5363 5 8 7 -5 94.7326 142.657 4 -8 -7 4 208.638 99.7971 5 8 7 -4 139.006 137.369 4 -8 -7 4 172.988 128.949 3 -8 -7 3-222.186 125.615 3 -8 -7 3 129.723 92.0138 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301.020 3 8 8 -2 1984.63 302.561 4 -8 -8 1-3.57119 70.9829 5 -8 -8 1 20.6208 97.0113 3 8 8 -1 74.2868 96.3083 4 -8 -8 0 2052.29 288.498 3 8 8 0 2012.96 296.608 4 -8 -8 -1 4617.18 411.949 3 8 8 1 3955.55 399.893 4 -8 -8 -2 1599.86 260.334 3 8 8 2 1062.81 198.093 4 -8 -8 -3 1015.93 214.433 3 8 8 3 515.887 153.385 4 -8 -8 -4 2495.56 299.554 3 8 8 4 1720.10 258.018 4 -8 -8 -5 1169.50 229.299 3 8 8 5 1189.11 210.919 4 -8 -8 -6 1429.76 171.877 6 -8 -8 -6 1128.33 203.214 3 8 8 6 1128.68 198.056 4 -8 -8 -7 132.755 66.4327 6 -8 -8 -7 194.910 107.960 3 8 8 7 81.3209 83.7291 4 -8 -8 -8 315.792 103.671 6 -8 -8 -8 499.464 164.507 3 -8 -8 -9 140.640 77.6650 6 -8 -8 -9 340.397 162.798 3 -8 -8 -10-2.72425 68.3732 6 -8 -8 -10 135.086 129.562 3 -8 -8 -11 1888.81 267.795 3 -8 -8 -11 2046.50 231.215 6 -8 -8 -12 148.247 99.2831 6 -8 -8 -12 102.406 143.726 3 -8 -8 -13 3299.06 369.954 3 -8 -8 -13 3702.69 326.195 6 -8 -8 -14 671.589 157.177 6 -8 -8 -14 805.106 193.800 3 -8 -8 -15 987.490 197.420 6 -8 -8 -15 1354.56 273.898 3 -8 -8 -16 2032.37 312.415 3 -8 -8 -16 2295.88 294.900 6 -8 -8 -17 2590.84 345.051 3 -8 -8 -17 2877.68 341.254 6 -8 -8 -18 1451.44 263.099 6 -8 -8 -19-64.8389 105.713 6 -8 -8 -20 172.338 117.620 2 -8 -8 -20-248.395 181.398 6 -8 -8 -21 672.237 208.107 6 -8 -8 -22 80.0003 174.877 6 -8 -9 9 170.380 194.389 3 8 9 -8 338.677 216.532 4 -8 -9 8 1125.61 280.910 3 8 9 -7 40.6486 139.367 4 -8 -9 7 622.645 207.615 3 8 9 -6 313.268 199.102 4 -8 -9 6 198.943 154.557 3 -8 -9 5 155.063 102.332 5 -8 -9 5 128.400 135.667 3 8 9 -5-155.539 178.889 4 -8 -9 4-10.0782 112.357 5 -8 -9 4 146.423 115.340 3 8 9 -4-182.536 169.967 4 -8 -9 3 56.7333 101.179 5 -8 -9 3 56.1940 125.715 3 8 9 -3 265.831 184.277 4 -8 -9 2 113.663 89.5378 5 -8 -9 2 269.774 144.610 3 8 9 -2 166.032 121.117 4 -8 -9 1 249.774 130.112 5 -8 -9 1 138.487 138.331 3 8 9 -1 379.408 154.303 4 -8 -9 0 3.56852 116.429 3 8 9 0 103.682 124.688 4 -8 -9 -1 2173.96 296.539 3 8 9 1 1522.90 254.441 4 -8 -9 -2 444.709 162.630 3 8 9 2 178.714 123.154 4 -8 -9 -3 150.139 122.045 3 8 9 3 76.9434 96.5729 4 -8 -9 -4 189.205 129.036 3 8 9 4 164.695 122.912 4 -8 -9 -5-89.3585 107.838 3 8 9 5 73.0250 82.3505 4 -8 -9 -6-105.856 99.5353 3 8 9 6 34.4823 87.7733 4 -8 -9 -7 82.8367 73.8747 6 -8 -9 -7 45.7680 103.455 3 8 9 7 38.4488 93.1106 4 -8 -9 -8 1082.14 178.015 6 -8 -9 -8 1279.97 237.289 3 8 9 8 1235.50 205.295 4 -8 -9 -9 1016.50 170.022 6 -8 -9 -9 1059.22 235.163 3 -8 -9 -10 1302.20 193.864 6 -8 -9 -10 1020.43 229.838 3 -8 -9 -11 98.4642 71.0984 6 -8 -9 -11 39.1381 129.503 3 -8 -9 -12-17.0523 79.7688 6 -8 -9 -12-159.685 126.927 3 -8 -9 -13 122.288 94.7740 6 -8 -9 -13 127.390 154.118 3 -8 -9 -14 403.081 148.949 6 -8 -9 -14-3.94292 126.598 3 -8 -9 -15 209.605 91.8225 6 -8 -9 -15 292.336 199.505 3 -8 -9 -16 119.240 125.439 6 -8 -9 -16-151.125 166.978 3 -8 -9 -17 2258.50 335.463 3 -8 -9 -17 2791.33 338.294 6 -8 -9 -18 776.953 195.694 6 -8 -9 -18 576.926 218.690 3 -8 -9 -19 1722.17 301.696 6 -8 -9 -20 255.769 136.345 6 -8 -9 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239.516 2 9 -9 5 581.320 205.207 5 -9 9 -6 201.986 154.941 2 9 -9 6 376.364 175.667 5 9 -9 7-108.234 159.818 5 9 -8 -8-206.837 180.959 1 9 -8 -7 165.436 159.877 1 9 -8 -6-1.28854 173.251 1 9 -8 -5 9.18879 186.402 1 9 -8 -4 145.467 124.884 6 9 -8 -4 123.137 128.320 1 9 -8 -3 4.77856 140.025 1 -9 8 2-27.1734 100.289 2 9 -8 -2 172.930 163.372 1 9 -8 -1 19.9428 133.295 1 -9 8 1-125.295 133.565 2 9 -8 0-15.4807 163.447 1 -9 8 0 118.949 111.148 2 9 -8 1 6436.65 563.791 1 -9 8 -1 5412.04 471.019 2 9 -8 1 5399.44 451.420 5 9 -8 2 567.279 177.442 5 -9 8 -2 26.3759 157.879 2 9 -8 2 230.930 150.410 1 9 -8 3 1404.36 266.523 5 9 -8 3 1495.42 288.688 1 -9 8 -3 797.880 217.112 2 9 -8 4 262.468 150.628 5 -9 8 -4 801.577 224.700 2 9 -8 5 467.618 189.929 5 -9 8 -5 873.354 227.622 2 9 -8 6-218.793 170.848 5 -9 8 -6 105.551 151.787 2 9 -8 7 738.415 213.614 5 -9 8 -7 1000.89 220.798 2 9 -8 8 457.002 213.621 5 -9 8 -8 327.793 165.055 2 9 -8 9-90.8602 157.655 5 9 -7 -10-311.741 196.468 1 9 -7 -9 188.705 171.072 1 9 -7 -8-212.564 224.130 1 9 -7 -7-64.3344 162.927 1 9 -7 -6 746.836 252.666 1 9 -7 -6 890.806 208.523 6 9 -7 -5 239.708 122.781 6 9 -7 -5 658.048 236.770 1 9 -7 -4-61.2137 84.8024 6 9 -7 -4-237.491 194.768 1 9 -7 -3-177.861 126.533 6 -9 7 3-244.042 129.327 2 9 -7 -3-183.330 161.526 1 -9 7 2 105.603 101.574 2 9 -7 -2 113.796 126.544 1 9 -7 -1 458.934 184.518 1 -9 7 1 220.291 114.468 2 9 -7 0 16.6338 122.915 1 -9 7 0 288.861 106.591 2 9 -7 1 364.402 126.136 5 -9 7 -1 314.212 140.808 2 9 -7 1 284.851 135.207 1 9 -7 2 1439.03 238.584 5 -9 7 -2 1176.21 236.990 2 9 -7 2 1617.94 283.168 1 9 -7 3 107.175 120.860 5 9 -7 3 195.362 141.553 1 -9 7 -3 178.711 133.409 2 9 -7 4 292.141 133.299 5 -9 7 -4 339.773 185.207 2 9 -7 5-20.1933 123.288 5 -9 7 -5 97.2608 111.107 2 9 -7 6 12.7901 132.970 5 -9 7 -6-100.655 123.723 2 9 -7 7 48.5096 112.709 5 -9 7 -7-141.101 149.077 2 9 -7 8 376.939 173.746 5 -9 7 -8 170.965 168.650 2 9 -7 9 1118.20 275.744 5 -9 7 -9 770.771 231.346 2 9 -7 10 45.5305 141.192 5 -9 7 -10 174.470 169.823 2 9 -7 11-377.776 214.619 5 9 -6 -11-10.5126 142.136 1 9 -6 -10 226.008 188.537 1 9 -6 -9-159.328 167.772 1 9 -6 -8 381.735 192.125 1 9 -6 -7 435.762 167.314 6 9 -6 -7 185.129 184.672 1 9 -6 -6 134.238 106.006 6 9 -6 -6-29.3963 134.439 1 9 -6 -5-29.5722 90.6238 6 9 -6 -5 140.752 149.924 1 9 -6 -4 40.3790 96.8354 6 9 -6 -4-124.059 138.971 1 -9 6 4 23.3153 77.7444 2 9 -6 -3-95.8221 76.7525 6 -9 6 3 94.8510 76.1931 2 9 -6 -3 111.685 164.961 1 9 -6 -2 172.043 117.403 6 9 -6 -2 236.573 149.234 1 9 -6 -1-169.450 157.702 1 -9 6 1-63.5802 106.244 2 9 -6 0 77.3370 147.440 1 9 -6 0 181.894 101.771 5 -9 6 0 139.501 109.613 2 9 -6 1 756.601 165.219 5 -9 6 -1 500.340 142.138 2 9 -6 1 731.261 215.066 1 9 -6 2 4.13096 82.0250 5 9 -6 2 87.8744 126.537 1 -9 6 -2 148.782 127.477 2 9 -6 3 142.797 87.1323 5 9 -6 3 248.014 120.357 1 -9 6 -3 207.830 116.787 2 9 -6 4 708.326 170.611 5 -9 6 -4 595.000 178.276 2 9 -6 5 2037.86 291.431 5 -9 6 -5 1881.16 287.538 2 9 -6 6 1512.78 258.099 5 -9 6 -6 1088.54 237.037 2 -9 6 -7 2469.29 345.065 2 9 -6 7 2085.14 314.382 5 9 -6 8 590.664 176.687 5 -9 6 -8 938.839 210.703 2 9 -6 9 131.593 117.647 5 -9 6 -9 454.369 163.305 2 9 -6 10-47.8147 122.220 5 -9 6 -10 104.828 181.616 2 9 -6 11 310.338 163.326 5 -9 6 -11-240.665 181.467 2 9 -6 12 309.605 179.061 5 -9 6 -12 465.882 208.979 2 9 -5 -13 284.454 186.059 1 9 -5 -12 154.347 161.764 1 9 -5 -11 136.943 144.120 1 9 -5 -10 92.0842 167.459 1 9 -5 -9-290.209 169.093 1 9 -5 -8 36.1603 99.9768 6 9 -5 -8-56.9285 147.235 1 9 -5 -7 3415.64 421.597 1 9 -5 -7 2422.66 283.043 6 9 -5 -6 2425.62 351.901 1 9 -5 -6 2106.51 251.835 6 9 -5 -5-52.9841 91.0800 6 9 -5 -5-157.271 151.554 1 9 -5 -4 320.513 159.853 1 9 -5 -4 216.996 103.875 6 -9 5 4 109.521 80.9941 2 9 -5 -3 59.7317 84.1569 6 -9 5 3 18.3300 77.4533 2 9 -5 -3 54.3763 103.624 1 9 -5 -2 33.6869 62.5379 6 9 -5 -2-109.579 136.548 1 -9 5 2-101.774 84.3798 2 9 -5 -1 428.102 171.574 1 -9 5 1 359.493 112.387 2 9 -5 0 626.579 197.812 1 9 -5 0 275.475 85.8606 5 -9 5 0 315.743 135.819 2 9 -5 1 513.972 133.823 5 -9 5 -1 476.160 161.223 2 9 -5 1 602.155 195.603 1 -9 5 -2 7908.61 502.595 2 9 -5 2 8714.39 490.859 5 -9 5 -2 7449.02 391.146 3 9 -5 2 8689.62 576.416 1 9 -5 3-92.9619 145.405 1 9 -5 3-114.633 92.2353 5 -9 5 -3-49.2369 98.6289 2 -9 5 -3 60.1439 69.8103 3 9 -5 4 1994.99 262.556 5 -9 5 -4 1771.04 259.163 2 9 -5 5 405.626 149.506 5 -9 5 -5 214.901 134.751 2 9 -5 6 1172.78 228.468 5 -9 5 -6 655.652 182.498 2 9 -5 7 1961.54 283.294 5 -9 5 -7 2018.50 301.888 2 9 -5 8 64.4239 122.133 5 -9 5 -8 56.9641 127.411 2 9 -5 9 831.563 209.128 5 -9 5 -9 535.898 199.206 2 9 -5 10 249.666 115.677 5 -9 5 -10 255.060 157.748 2 9 -5 11 139.593 130.660 5 -9 5 -11 77.4557 154.874 2 9 -5 12 35.5652 151.247 5 -9 5 -12-41.6252 120.178 2 9 -5 13-221.384 193.426 5 -9 5 -13-88.1674 141.812 2 9 -4 -14-74.4078 163.724 1 9 -4 -13-341.469 225.130 1 9 -4 -12 139.033 153.023 1 9 -4 -11-93.4973 173.689 1 9 -4 -10 220.243 152.619 1 9 -4 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249.652 167.140 3 9 13 5 264.566 181.771 4 -9 -13 -6 10.6936 126.056 3 9 13 6-69.3418 112.804 4 -9 -13 -7-203.986 167.402 3 9 13 7 6.40377 125.070 4 -9 -13 -8 449.292 183.868 3 -9 -13 -9 622.553 232.724 3 -9 -13 -10 97.6099 120.472 6 -9 -13 -10-12.8550 188.643 3 -9 -13 -11 9.85328 100.168 6 -9 -13 -11 105.194 176.962 3 -9 -13 -12 331.825 155.338 6 -9 -13 -12-311.323 204.853 3 -9 -13 -13 86.8691 114.604 6 -9 -13 -13-136.652 168.424 3 -9 -13 -14 141.165 139.035 6 -9 -13 -14 390.450 211.368 3 -9 -13 -15 124.698 156.851 6 -9 -14 -1-28.0873 140.165 5 -9 -14 -2-49.6582 137.935 5 -9 -14 -2 65.8510 166.675 3 9 14 2 278.486 147.559 4 -9 -14 -3-243.885 178.319 3 9 14 3-295.509 220.927 4 -9 -14 -4 240.444 181.841 3 9 14 4-130.715 174.085 4 -9 -14 -5 351.013 190.698 3 9 14 5-107.997 120.818 4 -9 -14 -6 139.873 168.426 3 -9 -14 -7-182.986 178.452 3 -9 -14 -8-167.033 144.249 3 -9 -14 -9-196.769 156.501 3 -9 -14 -10 170.005 182.664 3 -9 -14 -11 38.5414 197.594 3 10 -9 0 284.719 177.077 1 10 -9 1 149.758 202.987 1 -10 9 -2 146.527 153.509 2 10 -9 2-148.319 163.887 1 -10 9 -3 389.410 150.541 2 10 -8 -4-101.086 182.863 1 10 -8 -3 0.44021 139.222 1 10 -8 -2 275.668 194.905 1 10 -8 -1-5.93678 153.312 1 -10 8 1-62.8546 118.664 2 -10 8 0-80.0384 130.981 2 10 -8 0 99.1140 166.750 1 -10 8 -1 673.865 206.676 2 10 -8 1 546.493 247.753 1 10 -8 2-24.9368 143.479 1 -10 8 -2 326.627 132.661 2 -10 8 -3 117.262 150.700 2 -10 8 -4 604.486 225.526 2 10 -8 5 518.653 204.732 5 -10 8 -5 392.938 175.342 2 10 -8 6 261.110 132.723 5 -10 8 -6 185.938 137.109 2 10 -8 7 401.358 178.942 5 10 -8 8-25.4067 193.162 5 10 -7 -7-176.363 168.124 1 10 -7 -6-2.22708 162.448 1 10 -7 -5-168.498 212.292 1 10 -7 -4 67.8832 140.326 1 10 -7 -3-190.905 184.476 1 10 -7 -2-220.027 168.089 1 -10 7 2 267.712 128.077 2 10 -7 -1 270.140 155.035 1 -10 7 1 250.553 111.174 2 -10 7 0 165.479 114.873 2 10 -7 0-173.282 144.148 1 -10 7 -1 68.7426 127.331 2 10 -7 1 332.848 212.322 1 10 -7 2 978.329 237.417 1 -10 7 -2 542.717 184.740 2 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120.902 2 10 -6 7-101.412 171.306 5 -10 6 -7-18.7172 112.942 2 10 -6 8 298.600 158.448 5 -10 6 -8-214.501 148.778 2 10 -6 9-9.26534 129.607 5 -10 6 -9-53.6012 155.746 2 10 -6 10-67.7144 152.568 5 -10 6 -10 625.120 222.688 2 10 -6 11-60.7850 158.496 5 10 -5 -10 561.434 218.942 1 10 -5 -9 429.263 227.885 1 10 -5 -8 825.562 233.467 1 10 -5 -7 488.843 231.054 1 10 -5 -6 547.603 231.283 1 10 -5 -5-159.168 163.197 1 10 -5 -4 1427.85 294.491 1 10 -5 -3 233.710 155.836 1 -10 5 3 381.755 123.468 2 10 -5 -2 552.300 195.830 1 -10 5 2 202.652 109.939 2 10 -5 -1 621.572 195.935 1 -10 5 1 678.178 158.388 2 -10 5 0 230.782 107.813 2 10 -5 0 533.147 223.213 1 -10 5 -1 1292.68 210.482 3 10 -5 1 1884.72 304.876 1 -10 5 -1 1807.49 253.206 2 10 -5 2 83.8557 137.105 1 10 -5 2 395.008 132.823 5 -10 5 -2-89.4501 130.652 2 10 -5 3 163.221 103.886 5 -10 5 -3-44.3563 96.8571 2 10 -5 4 1852.69 257.385 5 -10 5 -4 1396.15 254.767 2 10 -5 5 1495.20 249.456 5 -10 5 -5 1499.18 274.180 2 10 -5 6 912.154 206.303 5 -10 5 -6 1047.55 242.567 2 10 -5 7 709.151 186.827 5 -10 5 -7 384.811 150.402 2 10 -5 8-182.819 119.550 5 -10 5 -8 244.096 156.081 2 10 -5 9 80.7914 126.333 5 -10 5 -9-113.361 152.948 2 10 -5 10 387.402 170.931 5 -10 5 -10 287.692 135.303 2 -10 5 -11 1169.30 263.944 2 -10 5 -12-100.994 135.187 2 10 -4 -12 218.735 232.385 1 10 -4 -11-252.797 180.284 1 10 -4 -10 326.044 227.736 1 10 -4 -9 362.803 180.318 1 10 -4 -8 456.732 188.547 1 10 -4 -7-276.057 218.532 1 10 -4 -6 58.9394 121.529 1 10 -4 -5 281.321 159.936 1 10 -4 -4 573.546 203.257 1 10 -4 -3-160.249 123.451 1 -10 4 3 47.0010 66.9767 2 10 -4 -2-226.962 166.408 1 -10 4 2 224.654 120.076 2 10 -4 -1-51.5727 142.993 1 -10 4 1-32.8180 82.3305 2 10 -4 0 583.784 159.195 1 -10 4 0 556.853 143.940 2 10 -4 1 1975.28 307.902 1 -10 4 -1 1961.41 243.919 3 -10 4 -1 1482.11 221.197 2 10 -4 2 621.025 199.858 1 -10 4 -2 460.398 143.401 3 -10 4 -2 272.925 111.480 2 -10 4 -3 1066.62 171.524 3 -10 4 -3 964.777 201.247 2 -10 4 -4 487.033 176.717 2 -10 4 -5 486.994 172.211 2 -10 4 -6 515.676 170.935 2 -10 4 -7 307.054 137.550 2 -10 4 -8 218.167 152.741 2 -10 4 -9 3275.85 401.302 2 -10 4 -10-14.3271 130.640 2 -10 4 -11 769.587 232.444 2 -10 4 -12 159.051 152.221 2 -10 4 -13 309.299 179.727 2 10 -3 -12 205.002 138.084 1 10 -3 -11-24.1392 132.651 1 10 -3 -10 329.373 177.997 1 10 -3 -9-228.460 196.283 1 10 -3 -8 85.7724 135.807 1 10 -3 -7 80.7139 112.725 1 10 -3 -6 370.873 192.160 1 10 -3 -5-198.107 140.069 1 10 -3 -4 24.6678 117.091 1 -10 3 4 71.1382 78.9552 2 -10 3 3-40.2957 73.8777 2 10 -3 -3-127.869 128.118 1 -10 3 2 116.697 86.6333 2 10 -3 -2 141.508 111.943 1 -10 3 1 26.8854 83.7065 2 10 -3 -1 247.484 127.853 1 -10 3 0 557.274 148.855 2 10 -3 0 1016.46 219.401 1 -10 3 -1 117.115 81.3219 3 -10 3 -1 213.581 107.158 2 -10 3 -2 109.070 106.284 2 -10 3 -2 7.37009 82.3808 3 -10 3 -3 524.722 155.549 2 -10 3 -3 525.040 135.916 3 -10 3 -4 48.9383 89.9656 2 -10 3 -4-11.7714 88.5176 3 -10 3 -5 369.078 143.247 2 -10 3 -5 176.497 81.1307 3 -10 3 -6 642.678 199.516 2 -10 3 -7 63.4657 128.047 2 -10 3 -8 1255.32 249.490 2 -10 3 -9 1439.70 281.842 2 -10 3 -10 892.684 209.761 2 -10 3 -11-409.508 176.464 2 -10 3 -12 399.158 173.071 2 -10 3 -13 2331.04 362.256 2 -10 3 -14 960.287 258.318 2 -10 3 -15 243.374 158.119 2 10 -2 -12 5.74152 155.766 1 10 -2 -11-219.984 179.490 1 10 -2 -10 266.013 162.355 1 10 -2 -9 346.149 163.373 1 10 -2 -8 327.784 187.622 1 10 -2 -7-226.460 156.249 1 10 -2 -6 165.830 133.869 1 10 -2 -5-65.4873 130.190 1 10 -2 -4 283.927 171.809 1 -10 2 4 56.7307 68.8368 2 -10 2 3 1449.94 187.928 2 10 -2 -3 2000.39 300.184 1 -10 2 2 319.096 108.067 2 10 -2 -2 302.515 171.336 1 -10 2 1 2088.59 243.258 2 10 -2 -1 2780.20 337.563 1 -10 2 0-110.571 123.590 3 -10 2 0 65.0541 83.4336 2 10 -2 0-64.4195 106.128 1 -10 2 -1 3410.98 327.925 2 -10 2 -1 3586.32 322.198 3 10 -2 1 4348.48 399.941 1 -10 2 -2 1151.33 206.923 2 -10 2 -2 1163.03 184.574 3 -10 2 -3 70.0755 96.6297 2 -10 2 -3 168.855 105.150 3 -10 2 -4 205.220 116.393 2 -10 2 -4 324.388 122.427 3 -10 2 -5 666.616 164.126 2 -10 2 -5 636.824 123.239 3 -10 2 -6 271.906 165.699 2 -10 2 -6 224.862 82.6626 3 -10 2 -7 126.545 105.819 2 -10 2 -7 149.154 87.7409 3 -10 2 -8 270.846 151.098 2 -10 2 -9 2928.30 358.881 2 -10 2 -10-51.8651 128.454 2 -10 2 -11 1267.45 263.505 2 -10 2 -12 2161.63 327.685 2 -10 2 -13 215.967 131.101 2 -10 2 -14-56.1989 133.383 2 -10 2 -15 561.733 180.940 2 -10 2 -16-58.5386 154.420 2 10 -1 -11-135.794 111.614 1 10 -1 -10 183.517 177.412 1 10 -1 -9 360.673 145.918 1 10 -1 -8-253.032 163.833 1 10 -1 -7 142.519 155.713 1 10 -1 -6-157.557 116.535 1 10 -1 -5-30.1598 129.494 1 -10 1 4 422.186 110.314 2 10 -1 -4 551.727 167.972 1 -10 1 3 539.680 131.803 2 10 -1 -3 824.353 208.925 1 -10 1 2 161.528 95.2110 2 10 -1 -2 45.1865 104.482 1 -10 1 1 1134.40 210.570 3 -10 1 1 798.252 160.543 2 10 -1 -1 1185.91 226.116 1 -10 1 0 295.086 120.879 3 10 -1 0 561.744 179.819 1 -10 1 0 213.787 108.877 2 -10 1 -1 579.830 157.563 2 -10 1 -1 582.694 151.887 3 -10 1 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96.0135 75.0553 6 -10 0 -13 325.987 160.747 2 -10 0 -14 416.858 166.049 2 -10 0 -15 586.170 204.538 2 -10 0 -16 272.617 120.472 2 -10 0 -17 198.548 156.341 2 -10 0 -18 1576.70 326.825 2 10 1 -13-164.613 171.522 4 10 1 -12-249.176 189.834 4 10 1 -11-1.79836 136.734 4 10 1 -10 166.545 190.280 4 10 1 -9 100.572 121.639 1 10 1 -9 367.832 186.941 4 10 1 -8 351.414 131.097 1 10 1 -8 456.688 175.696 4 10 1 -7 25.7454 111.292 1 10 1 -7 36.0023 114.606 4 10 1 -6 238.349 136.242 1 10 1 -6 93.1412 133.032 4 10 1 -5 662.074 200.052 4 10 1 -4 212.803 131.829 4 -10 -1 3 863.982 210.004 3 -10 -1 2-95.5451 122.643 3 -10 -1 1 1284.29 225.932 3 -10 -1 0 3394.56 346.853 3 -10 -1 -1 1420.18 223.854 3 -10 -1 -2 118.043 109.873 3 -10 -1 -3-132.806 114.140 3 -10 -1 -4 826.902 156.602 3 -10 -1 -5 3802.62 316.498 3 -10 -1 -6 1049.16 168.523 3 -10 -1 -7 2477.09 239.381 3 -10 -1 -7 2718.55 310.472 2 -10 -1 -8 10792.9 496.699 3 -10 -1 -8 10646.3 608.569 2 -10 -1 -9 278.994 104.929 3 -10 -1 -9 334.025 150.235 2 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6-112.510 147.009 3 10 3 -6 322.792 167.039 4 -10 -3 5 225.258 131.604 3 10 3 -5 63.8088 103.984 4 -10 -3 4 645.620 200.615 3 10 3 -4 369.506 161.492 4 10 3 -3 317.467 143.883 4 -10 -3 3 416.810 173.998 3 10 3 -2 1019.23 221.775 4 -10 -3 2 1616.39 263.516 3 10 3 -1 636.074 193.959 4 -10 -3 1 711.415 189.011 3 -10 -3 0 705.454 180.009 3 10 3 0 976.163 222.665 4 -10 -3 -1 130.642 103.061 3 -10 -3 -2 282.193 132.333 3 -10 -3 -3 105.298 111.835 3 -10 -3 -4 679.464 157.199 3 -10 -3 -5 2095.11 255.385 3 -10 -3 -6 561.736 153.667 3 -10 -3 -7 5018.76 373.605 3 -10 -3 -8 856.141 179.545 3 -10 -3 -9 67.3873 95.4682 3 -10 -3 -10 225.101 108.951 3 -10 -3 -11 411.707 128.474 3 -10 -3 -11 181.983 70.0168 6 -10 -3 -12 160.562 94.4214 3 -10 -3 -12 141.233 63.5095 6 -10 -3 -13 322.687 136.114 3 -10 -3 -13 388.710 138.244 2 -10 -3 -13 539.212 113.943 6 -10 -3 -14 1574.24 229.610 3 -10 -3 -14 1670.15 287.015 2 -10 -3 -14 1265.10 188.746 6 -10 -3 -15 674.511 162.602 3 -10 -3 -15 656.279 191.382 2 -10 -3 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172.771 4 -10 -7 -6-196.608 143.490 3 -10 -7 -7 1230.66 237.543 3 -10 -7 -8 3902.57 383.474 3 -10 -7 -9 10.0820 119.242 3 -10 -7 -10-38.7845 125.889 3 -10 -7 -11 1275.39 235.569 3 -10 -7 -12 356.909 152.829 3 -10 -7 -13 333.548 174.944 3 -10 -7 -14 697.684 202.069 3 -10 -7 -15 91.3496 138.433 3 -10 -7 -16 7093.52 555.484 3 -10 -7 -17 218.581 148.762 3 -10 -7 -18-47.3505 162.092 3 -10 -7 -19 331.163 177.257 2 -10 -7 -20 740.882 229.533 2 -10 -7 -21 612.961 225.968 2 10 8 -7-367.413 206.258 4 -10 -8 7 103.584 167.654 3 -10 -8 6-119.175 171.640 3 10 8 -6 112.853 144.600 4 -10 -8 5 127.538 128.041 3 10 8 -5 100.415 147.489 4 -10 -8 4 73.1402 128.147 3 10 8 -4 425.434 233.689 4 -10 -8 3 189.127 135.951 3 10 8 -3 103.904 178.082 4 -10 -8 2 307.120 145.416 3 10 8 -2 17.1432 141.387 4 -10 -8 1 334.994 122.758 5 -10 -8 1 135.372 150.846 3 -10 -8 0 129.259 130.320 3 10 8 0 271.177 145.694 4 -10 -8 -1 66.5916 113.160 3 10 8 1 75.6710 132.573 4 -10 -8 -2 2316.11 332.372 3 10 8 2 1775.88 297.885 4 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577.280 201.806 3 10 9 0 286.129 166.760 4 -10 -9 -1 265.955 154.381 3 10 9 1 62.6756 111.596 4 -10 -9 -2 184.290 149.482 3 10 9 2 64.9118 114.308 4 -10 -9 -3 414.751 181.257 3 10 9 3 186.339 154.931 4 -10 -9 -4 75.5217 109.492 3 10 9 4 75.1723 159.791 4 -10 -9 -5 716.875 211.374 3 10 9 5 445.198 151.996 4 -10 -9 -6 15.2377 120.868 3 10 9 6 132.780 106.861 4 -10 -9 -7-137.695 143.416 3 10 9 7 43.1922 123.809 4 -10 -9 -8 337.412 170.620 3 -10 -9 -9 182.689 133.039 3 -10 -9 -10 176.086 145.813 3 -10 -9 -11 493.279 192.222 3 -10 -9 -12 496.312 196.615 3 -10 -9 -13 7.55389 139.162 3 -10 -9 -14 1.07177 149.651 3 -10 -9 -15 415.466 187.324 3 -10 -9 -16 4009.32 463.334 3 -10 -9 -17 260.570 188.313 3 -10 -9 -18-249.802 168.464 3 -10 -9 -19 223.029 148.922 3 -10 -10 5 1.28496 127.211 3 -10 -10 4 25.9124 144.945 3 10 10 -4-11.2488 164.051 4 -10 -10 3 203.409 167.057 3 10 10 -3 191.615 169.973 4 -10 -10 2-80.7600 138.233 3 10 10 -2 22.3042 145.260 4 -10 -10 1 869.176 203.771 5 -10 -10 1 493.965 190.064 3 10 10 -1 695.517 219.817 4 -10 -10 0 43.9019 94.6536 5 -10 -10 0 283.858 161.544 3 10 10 0 261.137 187.358 4 -10 -10 -1-242.565 183.028 3 10 10 1 64.9182 138.034 4 -10 -10 -2-134.457 122.782 3 10 10 2 4.70821 124.427 4 -10 -10 -3 64.2206 145.609 3 10 10 3 100.278 141.522 4 -10 -10 -4-154.386 146.953 3 10 10 4 117.836 126.257 4 -10 -10 -5 586.270 209.263 3 10 10 5 465.577 161.811 4 -10 -10 -6 31.3441 123.450 3 10 10 6 49.5558 122.905 4 -10 -10 -7-137.261 121.582 3 10 10 7-118.768 111.417 4 -10 -10 -8 862.281 219.089 3 -10 -10 -9 110.863 164.126 3 -10 -10 -10 276.757 144.268 3 -10 -10 -11 419.391 199.916 3 -10 -10 -12 138.299 132.884 3 -10 -10 -13 327.389 181.707 3 -10 -10 -14-189.600 145.385 3 -10 -10 -15 79.6887 139.044 3 -10 -10 -16 803.624 260.690 3 -10 -10 -17-194.149 167.668 3 -10 -10 -18-167.191 178.914 3 -10 -10 -19-435.472 205.584 3 -10 -11 3 339.590 219.009 3 -10 -11 2 385.915 199.296 3 10 11 -2 184.716 151.032 4 -10 -11 1 336.695 187.386 3 10 11 -1 152.026 184.420 4 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126.675 3 10 13 6-227.150 166.666 4 -10 -13 -7 298.306 202.592 3 10 13 7 486.154 191.541 4 -10 -13 -8 237.938 179.336 3 -10 -13 -9-301.634 191.925 3 -10 -13 -10 406.465 194.845 3 -10 -13 -11-31.2441 147.130 3 -10 -13 -12-14.0537 156.136 3 -10 -13 -13-43.2826 158.986 3 -10 -14 -3-64.5988 131.759 5 10 14 3 54.2254 155.389 4 10 14 4 28.0983 161.934 4 10 14 5-178.517 188.951 4 -11 8 -1 735.331 197.246 2 -11 8 -2-94.0639 145.235 2 -11 8 -3-12.9650 130.565 2 11 -7 -2 16.6474 145.029 1 11 -7 -1 234.648 182.777 1 -11 7 0-70.7452 121.987 2 11 -7 0-94.8241 148.919 1 11 -7 1-59.2054 170.576 1 -11 7 -1 193.899 123.652 2 -11 7 -2-241.434 171.681 2 -11 7 -3-293.450 152.537 2 -11 7 -4 3.26800 156.580 2 -11 7 -5 305.320 173.643 2 -11 7 -6 212.747 156.821 2 11 -7 8 147.449 144.982 5 11 -6 -5 116.004 177.126 1 11 -6 -4 467.400 224.307 1 11 -6 -3-426.102 221.139 1 11 -6 -2-202.550 173.532 1 -11 6 1-223.111 124.986 2 11 -6 -1-130.949 201.973 1 11 -6 0 90.1015 137.697 1 -11 6 0-72.8570 100.068 2 11 -6 1 1432.50 313.429 1 -11 6 -1 1182.70 233.656 2 -11 6 -2 1158.85 232.225 2 -11 6 -3-49.7707 106.871 2 -11 6 -4 43.5278 115.310 2 -11 6 -5-81.6522 118.104 2 -11 6 -6 39.9855 119.938 2 -11 6 -7 207.171 139.823 2 -11 6 -8 228.162 126.612 2 11 -5 -7 662.601 259.583 1 11 -5 -6-45.5920 164.991 1 11 -5 -5-79.7632 174.225 1 11 -5 -4 423.464 192.013 1 11 -5 -3 205.075 144.571 1 11 -5 -2-261.889 200.870 1 11 -5 -1-155.193 153.874 1 -11 5 1-45.5917 99.1754 2 11 -5 0 231.591 160.499 1 -11 5 0 264.131 127.438 2 11 -5 1 432.279 197.431 1 -11 5 -1 180.833 120.919 2 -11 5 -2 1211.28 238.834 2 -11 5 -3-12.0639 127.801 2 -11 5 -4 438.322 180.038 2 -11 5 -5 187.170 144.825 2 -11 5 -6 123.385 142.324 2 -11 5 -7 53.4367 116.593 2 -11 5 -8 138.838 126.598 2 -11 5 -9 71.5228 149.048 2 -11 5 -10-53.5744 154.347 2 11 -4 -9 422.990 224.250 1 11 -4 -8 189.056 180.867 1 11 -4 -7-13.7554 153.193 1 11 -4 -6 261.524 198.258 1 11 -4 -5 191.652 169.950 1 11 -4 -4 245.007 173.687 1 11 -4 -3 234.108 154.617 1 11 -4 -2 49.6225 161.106 1 -11 4 2-121.499 83.0725 2 -11 4 1 2272.60 275.073 2 11 -4 -1 3282.17 411.100 1 -11 4 0-144.708 107.205 3 11 -4 0-33.2505 167.212 1 -11 4 0 71.4714 108.883 2 11 -4 1 754.327 250.705 1 -11 4 -1 680.695 177.549 2 -11 4 -1 412.587 130.992 3 -11 4 -2 534.971 136.980 3 -11 4 -2 728.889 176.013 2 -11 4 -3 966.969 212.474 2 -11 4 -4 129.060 108.557 2 -11 4 -5 218.641 153.912 2 -11 4 -6 720.826 193.502 2 -11 4 -7 399.172 194.154 2 -11 4 -8 970.092 236.586 2 -11 4 -9 120.040 152.604 2 -11 4 -10-261.964 181.109 2 -11 4 -11-18.0411 141.849 2 -11 4 -12 190.994 188.342 2 11 -3 -10 280.235 190.252 1 11 -3 -9-453.132 213.338 1 11 -3 -8 58.0745 170.914 1 11 -3 -7-231.014 171.981 1 11 -3 -6-28.8736 184.644 1 11 -3 -5-96.0882 172.983 1 11 -3 -4 294.328 156.253 1 11 -3 -3 232.091 167.282 1 -11 3 2 416.678 138.485 2 11 -3 -2 143.013 139.879 1 -11 3 1-78.4264 87.7017 2 -11 3 1-76.9073 90.0988 3 11 -3 -1-229.473 161.094 1 -11 3 0 323.483 129.255 3 -11 3 0 568.226 164.019 2 11 -3 0 430.499 194.523 1 -11 3 -1 178.836 118.607 2 -11 3 -1-85.1910 99.8794 3 -11 3 -2 476.854 161.110 2 -11 3 -2 112.259 91.9411 3 -11 3 -3 65.4805 95.9828 2 -11 3 -3-64.4498 103.445 3 -11 3 -4 19.8483 100.244 2 -11 3 -4 92.4454 95.6063 3 -11 3 -5 95.5540 97.3978 2 -11 3 -6 706.534 209.297 2 -11 3 -7-184.894 142.118 2 -11 3 -8-34.1904 117.258 2 -11 3 -9 2211.73 326.999 2 -11 3 -10-162.892 159.029 2 -11 3 -11-35.3185 132.640 2 -11 3 -12 75.6726 135.258 2 -11 3 -13-20.8896 133.960 2 11 -2 -11-565.321 239.045 1 11 -2 -10-125.212 146.762 1 11 -2 -9 123.739 129.495 1 11 -2 -8 819.331 265.254 1 11 -2 -7 484.522 201.416 1 11 -2 -6 412.892 198.834 1 11 -2 -5 33.8890 129.668 1 11 -2 -4 402.327 168.667 1 -11 2 3-90.2180 93.3739 2 11 -2 -3 21.5600 142.778 1 -11 2 2-123.172 87.3166 2 11 -2 -2 195.214 144.454 1 -11 2 1-30.5289 108.988 3 -11 2 1 38.3575 80.2732 2 11 -2 -1 28.0497 108.018 1 -11 2 0 30.7164 98.1397 3 -11 2 0-73.7688 105.409 2 -11 2 -1 78.2806 87.8490 2 -11 2 -1 314.597 128.393 3 -11 2 -2 236.881 122.122 2 -11 2 -2 261.912 109.152 3 -11 2 -3 614.325 174.174 2 -11 2 -3 268.555 101.748 3 -11 2 -4 561.996 168.985 2 -11 2 -4 597.647 153.408 3 -11 2 -5 205.379 132.904 2 -11 2 -5 185.936 83.1254 3 -11 2 -6 165.874 131.484 2 -11 2 -7-73.1866 111.343 2 -11 2 -8 1193.72 239.399 2 -11 2 -9 106.697 127.536 2 -11 2 -10-187.670 161.652 2 -11 2 -11 142.052 131.383 2 -11 2 -12 351.732 156.136 2 -11 2 -13 297.055 163.736 2 -11 2 -14 1686.56 328.259 2 11 -1 -10 346.640 198.589 1 11 -1 -9-12.2721 130.532 1 11 -1 -8-176.040 161.568 1 11 -1 -7 717.997 215.568 1 11 -1 -6-39.6907 127.910 1 11 -1 -5 377.048 150.439 1 11 -1 -4-297.909 169.537 1 -11 1 3 12.5414 74.0582 2 11 -1 -3 115.357 123.238 1 -11 1 2 192.545 132.766 3 -11 1 2 351.962 121.054 2 11 -1 -2 178.190 124.934 1 -11 1 1 784.975 193.131 3 -11 1 1 448.481 142.103 2 -11 1 0 2679.14 293.765 2 -11 1 0 3091.31 343.057 3 -11 1 -1 3032.77 320.633 2 -11 1 -1 2691.64 303.270 3 -11 1 -2 30.0861 119.016 2 -11 1 -2 217.448 112.622 3 -11 1 -3-10.3657 87.5546 2 -11 1 -3 53.5575 102.341 3 -11 1 -4 1610.15 255.740 2 -11 1 -4 1275.25 202.197 3 -11 1 -5 1251.58 221.073 2 -11 1 -5 1166.85 192.988 3 -11 1 -6 749.181 193.405 2 -11 1 -6 792.769 162.803 3 -11 1 -7 24.9208 106.788 2 -11 1 -7 146.243 105.162 3 -11 1 -8-46.4079 103.769 2 -11 1 -9 256.881 139.960 2 -11 1 -10 320.658 176.304 2 -11 1 -11 2353.79 340.154 2 -11 1 -12 448.102 179.716 2 -11 1 -13 349.126 154.802 2 -11 1 -14 542.664 201.838 2 -11 1 -15 577.297 207.622 2 11 0 -9 81.5966 132.239 1 11 0 -8 278.870 162.737 1 11 0 -7 86.7236 120.960 1 11 0 -6 12.5019 105.222 1 11 0 -5-23.2582 134.634 1 -11 0 4 306.513 150.552 3 -11 0 3-276.111 177.797 3 -11 0 3 251.423 112.114 2 -11 0 2 784.321 206.737 3 -11 0 2 603.677 149.093 2 -11 0 1 123.904 100.957 3 -11 0 1 90.5863 99.9873 2 -11 0 0 532.131 172.834 2 -11 0 0 454.103 154.287 3 -11 0 -1 478.138 145.805 2 -11 0 -1 283.069 114.414 3 -11 0 -2 431.513 138.808 2 -11 0 -2 140.791 121.518 3 -11 0 -3 3569.29 362.779 2 -11 0 -3 3295.89 328.633 3 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0 -3 197.093 132.400 2 -13 0 -3 70.2415 102.733 3 -13 0 -4 488.865 194.440 2 -13 0 -4 9.96230 123.165 3 -13 0 -5 4324.09 390.021 3 -13 0 -5 4085.25 444.287 2 -13 0 -6 1749.87 302.379 2 -13 0 -6 1436.15 236.584 3 -13 0 -7 687.561 213.361 2 -13 0 -8 44.6420 121.576 2 -13 0 -9 111.368 144.616 2 -13 0 -10 404.994 182.625 2 -13 0 -11 58.0986 151.091 2 -13 0 -12 81.1085 180.096 2 -13 -1 5 151.254 147.228 3 -13 -1 4-204.861 195.052 3 -13 -1 3-196.653 181.740 3 -13 -1 2 83.3158 138.891 3 -13 -1 1 1.12250 118.598 2 -13 -1 1 155.104 112.867 3 -13 -1 0 209.281 135.568 2 -13 -1 0-63.3088 118.335 3 -13 -1 -1 47.5489 100.751 2 -13 -1 -1 84.1721 123.767 3 -13 -1 -2-0.31595 103.396 2 -13 -1 -2 71.7373 102.696 3 -13 -1 -3 70.2525 112.089 2 -13 -1 -3 92.6134 135.339 3 -13 -1 -4-73.0334 143.740 2 -13 -1 -4-8.89817 110.686 3 -13 -1 -5 523.100 188.253 2 -13 -1 -5 648.620 182.218 3 -13 -1 -6 4160.41 401.479 3 -13 -1 -6 4253.93 459.284 2 -13 -1 -7 1590.27 299.591 2 -13 -1 -7 1762.33 255.107 3 -13 -1 -8 292.484 175.725 2 -13 -1 -8-26.3889 119.397 3 -13 -1 -9 3.11544 108.428 2 -13 -1 -10-41.7914 123.815 2 -13 -1 -11-71.3283 133.315 2 -13 -1 -12-41.9639 139.214 2 -13 -1 -13 1590.03 348.950 2 -13 -2 5-30.7766 197.295 3 -13 -2 4 222.344 182.589 3 -13 -2 3 63.3534 160.083 3 -13 -2 2 163.200 133.513 3 -13 -2 1-52.7968 151.554 3 -13 -2 0 418.745 179.672 3 -13 -2 -1 34.2171 122.894 3 -13 -2 -2 109.591 106.065 3 -13 -2 -3 130.291 101.816 3 -13 -2 -4 151.660 109.901 3 -13 -2 -5 120.505 104.360 3 -13 -2 -6 252.221 159.404 3 -13 -2 -6 469.087 205.163 2 -13 -2 -7-80.6934 128.684 3 -13 -2 -7 146.006 181.402 2 -13 -2 -8-157.423 115.455 3 -13 -2 -8 72.0325 145.882 2 -13 -2 -9 137.527 89.4731 3 -13 -2 -9 169.846 134.549 2 -13 -2 -10 478.729 142.219 3 -13 -2 -10 233.880 158.187 2 -13 -2 -11-167.020 170.368 2 -13 -2 -12 20.9257 170.978 2 -13 -2 -13-61.1556 135.258 2 -13 -2 -14 1332.06 291.808 2 -13 -3 4 89.3758 166.404 3 -13 -3 3 259.150 164.631 3 -13 -3 2 347.830 164.994 3 -13 -3 1 122.238 144.287 3 -13 -3 0-83.1703 166.056 3 -13 -3 -1-112.812 124.411 3 -13 -3 -2-230.874 150.620 3 -13 -3 -3 111.974 116.046 3 -13 -3 -4 256.495 133.585 3 -13 -3 -5 517.480 172.455 3 -13 -3 -6-4.88756 112.935 3 -13 -3 -7 496.344 169.541 3 -13 -3 -8 90.3513 122.083 3 -13 -3 -9 357.024 160.641 3 -13 -3 -10 169.566 113.718 3 -13 -3 -10 230.029 169.729 2 -13 -3 -11 22.6959 132.364 3 -13 -3 -11 71.8878 136.045 2 -13 -3 -12-103.477 138.906 2 -13 -3 -13 39.0902 142.007 2 -13 -3 -14 237.395 166.892 2 -13 -3 -15-297.650 192.328 2 -13 -4 4 620.919 232.913 3 13 4 -4 563.085 249.713 4 -13 -4 3 364.625 181.236 3 -13 -4 2 526.024 275.369 3 -13 -4 1 503.515 206.648 3 -13 -4 0 301.758 194.613 3 -13 -4 -1-36.0318 129.025 3 -13 -4 -2 37.6618 114.435 3 -13 -4 -3 794.786 215.865 3 -13 -4 -4 44.5983 138.997 3 -13 -4 -5 363.929 182.146 3 -13 -4 -6 1744.22 286.986 3 -13 -4 -7 28.2456 121.282 3 -13 -4 -8 140.924 146.531 3 -13 -4 -9 100.014 104.741 3 -13 -4 -10 34.2450 101.373 3 -13 -4 -11-92.9108 136.827 3 -13 -4 -12 355.532 167.935 3 -13 -4 -13-199.956 117.631 3 -13 -4 -13-21.5575 138.681 2 -13 -4 -14 388.681 193.238 2 -13 -4 -15 117.284 153.875 2 -13 -5 3 180.636 162.232 3 13 5 -3-116.837 169.360 4 -13 -5 2 412.954 201.355 3 13 5 -2 28.7283 187.815 4 -13 -5 1 330.638 176.760 3 13 5 -1 581.478 230.295 4 -13 -5 0-11.1543 132.895 3 -13 -5 -1 8.08466 120.392 3 -13 -5 -2 594.536 200.475 3 -13 -5 -3 32.9601 126.047 3 -13 -5 -4 645.726 191.207 3 -13 -5 -5 1357.20 273.742 3 -13 -5 -6-126.537 152.463 3 -13 -5 -7 582.957 180.301 3 -13 -5 -8 159.192 144.362 3 -13 -5 -9 193.362 146.029 3 -13 -5 -10 202.809 132.358 3 -13 -5 -11-18.6919 107.366 3 -13 -5 -12 269.837 152.581 3 -13 -5 -13 215.709 177.333 3 -13 -5 -14 168.203 145.765 3 -13 -5 -15-65.4779 185.049 2 -13 -6 2 223.397 191.373 3 13 6 -2 131.519 149.094 4 -13 -6 1 56.3896 141.270 3 13 6 -1-173.478 139.868 4 -13 -6 0-253.508 163.451 3 13 6 0 227.452 162.563 4 -13 -6 -1 172.089 165.482 3 -13 -6 -2 315.815 193.712 3 -13 -6 -3 282.426 150.086 3 -13 -6 -4 450.270 202.631 3 -13 -6 -5 1049.60 245.122 3 -13 -6 -6 772.369 219.292 3 -13 -6 -7 405.537 200.212 3 -13 -6 -8 33.5228 131.062 3 -13 -6 -9-71.4061 160.578 3 -13 -6 -10 218.523 146.892 3 -13 -6 -11 403.140 156.598 3 -13 -6 -12 462.315 203.588 3 -13 -6 -13-6.62671 117.487 3 -13 -6 -14 232.877 161.368 3 -13 -6 -15 64.3112 153.840 3 -13 -7 1 385.002 220.111 3 13 7 -1 119.922 152.259 4 -13 -7 0-570.664 219.833 3 13 7 0 212.907 152.256 4 -13 -7 -1-66.0780 171.817 3 13 7 1-21.0060 149.115 4 -13 -7 -2-14.2837 174.167 3 13 7 2-139.556 167.858 4 -13 -7 -3-121.237 132.261 3 -13 -7 -4 137.612 175.327 3 -13 -7 -5 487.070 210.578 3 -13 -7 -6 215.248 156.431 3 -13 -7 -7 423.163 202.348 3 -13 -7 -8 11.4825 156.880 3 -13 -7 -9 105.731 133.279 3 -13 -7 -10 138.832 164.256 3 -13 -7 -11 622.077 181.883 3 -13 -7 -12 279.731 143.248 3 -13 -7 -13-304.623 202.554 3 -13 -7 -14 354.523 172.993 3 -13 -7 -15-174.382 150.832 3 -13 -7 -16-88.9281 144.412 3 -13 -7 -17-76.6635 154.280 3 -13 -8 0 297.459 244.264 3 13 8 0 490.500 204.208 4 -13 -8 -1-156.502 185.626 3 13 8 1 411.360 229.236 4 -13 -8 -2 104.844 131.165 3 13 8 2 69.2443 148.317 4 -13 -8 -3 212.762 183.520 3 13 8 3-242.811 151.433 4 -13 -8 -4 542.567 201.319 3 -13 -8 -5-62.5982 138.124 3 -13 -8 -6 190.722 137.633 3 -13 -8 -7 336.634 168.318 3 -13 -8 -8 469.464 200.445 3 -13 -8 -9 263.301 176.956 3 -13 -8 -10 159.446 145.128 3 -13 -8 -11-107.535 144.397 3 -13 -8 -12-8.96923 129.429 3 -13 -8 -13 664.618 234.320 3 -13 -8 -14 398.217 185.324 3 -13 -8 -15 270.777 147.096 3 -13 -8 -16 28.6801 159.309 3 -13 -8 -17-51.6343 207.122 3 13 9 1-336.108 202.335 4 -13 -9 -2 305.914 192.270 3 13 9 2-59.8408 142.046 4 -13 -9 -3-368.405 231.052 3 13 9 3 107.353 124.834 4 -13 -9 -4-39.8991 149.835 3 13 9 4 32.9274 144.959 4 -13 -9 -5 245.238 132.167 3 -13 -9 -6 48.4104 159.391 3 -13 -9 -7 306.197 199.246 3 -13 -9 -8 228.629 167.929 3 -13 -9 -9-230.844 202.164 3 -13 -9 -10-121.085 140.395 3 -13 -9 -11 176.211 179.829 3 -13 -9 -12 198.310 156.569 3 -13 -9 -13 247.114 148.284 3 -13 -9 -14 553.565 205.092 3 -13 -9 -15 107.556 165.484 3 -13 -9 -16 983.755 258.949 3 13 10 3-11.1150 149.482 4 13 10 4 163.606 177.119 4 -13 -10 -5-266.709 204.489 3 -13 -10 -6-352.581 206.259 3 -13 -10 -7 314.934 237.936 3 -13 -10 -8 223.673 195.139 3 -13 -10 -9-98.6954 156.330 3 -13 -10 -10-190.515 148.216 3 -13 -10 -11 119.283 217.869 3 -13 -10 -12 513.621 207.871 3 -13 -10 -13 1269.52 311.253 3 13 11 5-15.9928 151.617 4 -14 3 -3 27.1261 116.538 2 -14 3 -4 263.273 160.711 2 -14 3 -5 98.4167 112.990 2 -14 2 2-261.063 166.323 3 -14 2 1-12.3416 107.513 3 -14 2 0-52.8959 131.094 3 -14 2 -2-20.3721 178.008 2 -14 2 -3-132.996 153.276 2 -14 2 -4 35.2168 121.780 2 -14 2 -5 103.624 133.138 2 -14 2 -6-196.507 185.696 2 -14 2 -7-175.862 203.187 2 -14 1 2-325.910 189.363 3 -14 1 1-141.238 150.390 3 -14 1 0-379.715 207.710 3 -14 1 -1-5.41166 114.947 3 -14 1 -2 34.5063 122.468 2 -14 1 -2-191.819 147.572 3 -14 1 -3 278.899 164.344 2 -14 1 -4 259.734 165.891 2 -14 1 -5 50.4885 133.789 2 -14 1 -6 67.6200 150.556 2 -14 1 -7-330.327 221.618 2 -14 1 -8 54.1503 172.179 2 -14 0 2-184.707 165.602 3 -14 0 1 425.655 176.501 3 -14 0 0 326.989 168.778 3 -14 0 -1 31.0390 102.236 2 -14 0 -1-173.584 201.057 3 -14 0 -2-258.014 133.784 2 -14 0 -2-44.2433 125.189 3 -14 0 -3-187.453 151.814 2 -14 0 -3 276.109 172.740 3 -14 0 -4 295.073 170.683 2 -14 0 -4 566.631 177.307 3 -14 0 -5 68.4576 125.370 2 -14 0 -6 187.966 151.666 2 -14 0 -7-198.105 177.192 2 -14 0 -8 460.231 216.796 2 -14 0 -9-73.6960 160.154 2 -14 0 -10 144.864 153.034 2 -14 -1 2-191.629 184.156 3 -14 -1 1-28.8484 137.593 3 -14 -1 0 61.5444 141.552 3 -14 -1 -1 155.314 118.258 2 -14 -1 -1 113.799 146.982 3 -14 -1 -2-122.398 133.042 2 -14 -1 -2-258.163 175.688 3 -14 -1 -3 442.971 168.293 2 -14 -1 -3-47.7159 140.948 3 -14 -1 -4 180.657 132.259 2 -14 -1 -4-66.8478 134.142 3 -14 -1 -5 86.4989 158.975 2 -14 -1 -5-21.1590 138.656 3 -14 -1 -6-123.102 142.004 2 -14 -1 -6-63.9184 130.296 3 -14 -1 -7 968.477 251.055 2 -14 -1 -8 233.437 163.918 2 -14 -1 -9 641.545 212.683 2 -14 -1 -10 596.351 215.080 2 -14 -1 -11 122.276 190.365 2 -14 -2 2-278.148 182.459 3 -14 -2 1 381.896 186.329 3 -14 -2 0-75.5874 134.357 2 -14 -2 0 321.909 159.202 3 -14 -2 -1-55.5252 135.308 2 -14 -2 -1 145.806 153.156 3 -14 -2 -2-24.0038 103.152 2 -14 -2 -2 160.374 119.960 3 -14 -2 -3-251.484 172.386 2 -14 -2 -3-18.1567 127.386 3 -14 -2 -4 142.220 107.571 2 -14 -2 -4 88.3479 116.737 3 -14 -2 -5 340.591 169.236 3 -14 -2 -5 254.219 147.974 2 -14 -2 -6 92.2453 138.212 3 -14 -2 -6-236.775 168.785 2 -14 -2 -7-110.332 133.738 3 -14 -2 -7 158.021 144.499 2 -14 -2 -8 185.761 118.316 3 -14 -2 -8 6.64612 141.616 2 -14 -2 -9 523.835 221.013 2 -14 -2 -10 123.019 143.571 2 -14 -2 -11-104.192 152.090 2 -14 -3 2 258.342 169.538 3 -14 -3 1 107.924 137.843 3 -14 -3 0 209.026 181.197 3 -14 -3 -1-152.635 178.387 3 -14 -3 -2 124.189 133.262 3 -14 -3 -3 44.5330 133.639 3 -14 -3 -4-168.872 182.635 3 -14 -3 -5 208.902 145.766 3 -14 -3 -6-189.632 163.565 3 -14 -3 -7 81.0686 110.416 3 -14 -3 -8-293.941 176.801 3 -14 -3 -8 182.144 192.018 2 -14 -3 -9-125.459 141.186 3 -14 -3 -9 274.434 152.347 2 -14 -3 -10 176.348 122.508 3 -14 -3 -10 455.367 211.418 2 -14 -3 -11-65.3849 181.164 2 -14 -3 -12 333.858 189.990 2 -14 -4 1 149.655 165.263 3 -14 -4 0 253.849 168.086 3 -14 -4 -1-174.582 148.412 3 -14 -4 -2 30.1830 136.886 3 -14 -4 -3-208.170 147.892 3 -14 -4 -4-60.5830 173.468 3 -14 -4 -5-66.0306 162.017 3 -14 -4 -6 191.025 141.453 3 -14 -4 -7-237.829 148.041 3 -14 -4 -8-166.086 154.957 3 -14 -4 -9 85.8045 139.385 3 -14 -4 -10 357.409 172.619 3 -14 -4 -11-141.150 130.254 3 -14 -4 -11 316.466 170.088 2 -14 -4 -12 22.4919 133.028 2 -14 -5 0 81.4118 156.247 3 -14 -5 -1 330.747 187.640 3 -14 -5 -2-166.256 172.555 3 -14 -5 -3 191.691 146.982 3 -14 -5 -4 434.598 180.925 3 -14 -5 -5 32.4533 132.355 3 -14 -5 -6 378.115 188.073 3 -14 -5 -7 289.432 163.758 3 -14 -5 -8-195.332 203.625 3 -14 -5 -9 164.524 145.296 3 -14 -5 -10-74.2284 134.346 3 -14 -5 -11 118.799 160.957 3 -14 -5 -12 777.865 205.145 3 -14 -5 -13 421.935 179.116 3 -14 -6 -1 29.4284 171.888 3 -14 -6 -2 189.622 142.026 3 -14 -6 -3 97.4153 132.703 3 -14 -6 -4-40.5865 164.458 3 -14 -6 -5-26.0075 157.520 3 -14 -6 -6-213.519 173.556 3 -14 -6 -7-138.796 149.146 3 -14 -6 -8 604.838 191.111 3 -14 -6 -9 188.029 126.545 3 -14 -6 -10 151.337 149.807 3 -14 -6 -11 107.830 109.007 3 -14 -6 -12-237.505 174.623 3 -14 -6 -13 1182.84 259.440 3 -14 -6 -14-504.582 212.502 3 -14 -7 -2-55.8821 176.769 3 -14 -7 -3-53.8213 144.818 3 -14 -7 -4-9.68977 146.394 3 -14 -7 -5 103.725 148.057 3 -14 -7 -6 52.3937 139.743 3 -14 -7 -7-15.9519 148.621 3 -14 -7 -8 446.954 203.379 3 -14 -7 -9 311.161 149.314 3 -14 -7 -10 27.8958 159.011 3 -14 -7 -11 241.306 165.208 3 -14 -7 -12-67.2003 145.046 3 -14 -7 -13-155.786 152.005 3 -14 -7 -14 88.3354 168.622 3 -14 -7 -15 173.127 159.906 3 -14 -8 -4 197.043 185.477 3 -14 -8 -5 207.018 159.561 3 -14 -8 -6-403.076 177.161 3 -14 -8 -7 227.892 159.513 3 -14 -8 -8 455.446 158.226 3 -14 -8 -9 192.355 146.324 3 -14 -8 -10 368.392 180.599 3 -14 -8 -11 90.3097 134.224 3 -14 -8 -12-90.3748 157.313 3 -14 -8 -13 242.612 191.465 3 -14 -8 -14 82.0935 178.028 3 -14 -8 -15-131.631 186.484 3 -14 -9 -8 105.949 178.873 3 -14 -9 -9 431.134 196.595 3 -14 -9 -10 126.968 143.883 3 -14 -9 -11 305.960 201.276 3 -15 1 -4 140.015 152.507 2 -15 0 -1-151.766 157.719 3 -15 0 -2 49.2545 114.972 3 -15 0 -3 231.163 152.572 2 -15 0 -4 6.39099 164.477 2 -15 0 -5 403.831 179.798 2 -15 -1 -1-110.625 133.127 3 -15 -1 -2-139.115 156.531 2 -15 -1 -2 296.055 132.725 3 -15 -1 -3 182.923 147.128 2 -15 -1 -3 346.793 169.288 3 -15 -1 -4-58.9930 147.292 2 -15 -1 -4-58.4216 163.612 3 -15 -1 -5 360.209 144.020 2 -15 -1 -6 5.94208 119.269 2 -15 -1 -7-140.186 159.182 2 -15 -2 -1 113.406 118.660 3 -15 -2 -2-48.4269 129.210 2 -15 -2 -2 39.0476 122.796 3 -15 -2 -3 238.473 149.017 2 -15 -2 -3-68.3212 161.057 3 -15 -2 -4 167.462 135.607 2 -15 -2 -4-83.2507 164.123 3 -15 -2 -5-146.854 169.565 2 -15 -2 -5 70.6745 143.132 3 -15 -2 -6 79.5248 160.511 2 -15 -2 -6 403.020 198.450 3 -15 -2 -7 47.6852 127.339 2 -15 -3 -2 149.513 135.718 3 -15 -3 -2-24.1275 134.920 2 -15 -3 -3 276.967 173.190 3 -15 -3 -3-47.2910 141.674 2 -15 -3 -4 259.454 153.797 3 -15 -3 -4 158.669 141.933 2 -15 -3 -5-28.0051 157.091 3 -15 -3 -5 273.300 153.643 2 -15 -3 -6-19.2248 129.741 3 -15 -3 -6-189.450 152.377 2 -15 -3 -7-186.363 171.588 3 -15 -3 -7 50.0410 162.165 2 -15 -3 -8 114.863 172.007 3 -15 -3 -8-193.331 183.043 2 -15 -4 -3-38.0907 143.500 3 -15 -4 -4 290.785 173.855 3 -15 -4 -5-18.3718 111.578 3 -15 -4 -6-0.77228 121.047 3 -15 -4 -7-64.1279 137.182 3 -15 -4 -8-520.574 242.580 3 -15 -4 -9-76.1985 127.836 3 -15 -5 -4 325.413 195.641 3 -15 -5 -5 196.010 159.516 3 -15 -5 -6 298.403 160.552 3 -15 -5 -7-4.31449 113.832 3 -15 -5 -8-53.2901 156.905 3 -15 -5 -9-388.682 188.847 3 -15 -5 -10-112.032 158.333 3 -15 -5 -11 239.118 154.379 3 -15 -6 -6-110.892 149.848 3 -15 -6 -7 66.3303 154.254 3 -15 -6 -8 4.84653 150.344 3 -15 -6 -9 33.1896 142.010 3 -15 -6 -10-40.3104 134.150 3 -15 -6 -11-379.300 209.724 3 -15 -6 -12 321.995 168.853 3 -15 -7 -9 186.583 143.778 3 -15 -7 -10-112.752 181.974 3 -15 -7 -11-15.0687 140.956 3 0 0 0 0.00 0.00 0 TITL lb0329_CLZ-TRPTA_reMo in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 10.402793 10.845366 15.422948 71.1834 73.9843 76.1485 ZERR 2.00 0.000282 0.000330 0.000493 0.0028 0.0026 0.0025 LATT 1 SFAC C H N O Cl UNIT 70.00 56.00 8.00 8.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 22498 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Cl2 Cl 0.39753(6) -0.16703(5) 0.95873(4) 0.07025(18) Uani 1 1 d . . Cl1 Cl 0.23504(6) 1.15410(5) 0.16479(4) 0.0799(2) Uani 1 1 d . . O2 O 0.28392(14) 0.54295(13) 0.83562(10) 0.0627(4) Uani 1 1 d . . O1B O 0.11614(15) 0.69607(14) 0.93073(10) 0.0639(4) Uani 1 1 d . . O1 O 0.49787(15) 0.51905(14) 0.75952(10) 0.0673(4) Uani 1 1 d . . N1 N 0.17527(13) 0.59934(13) 0.36530(9) 0.0402(3) Uani 1 1 d . . O2B O 0.14146(16) 0.86002(15) 0.79915(10) 0.0730(4) Uani 1 1 d . . N4 N 0.37932(15) 0.62506(15) 0.60028(10) 0.0452(3) Uani 1 1 d . . N2 N 0.13470(14) 0.34376(14) 0.47124(9) 0.0442(3) Uani 1 1 d . . N3 N 0.33146(19) 0.37532(16) 0.70677(11) 0.0592(5) Uani 1 1 d . . C29 C 0.45548(18) 0.51297(16) 0.91956(12) 0.0468(4) Uani 1 1 d . . C11 C 0.21962(16) 0.54535(16) 0.44716(11) 0.0392(4) Uani 1 1 d . . C5 C 0.09563(16) 0.39971(17) 0.38734(11) 0.0421(4) Uani 1 1 d . . C13 C 0.18856(16) 0.73544(16) 0.31428(11) 0.0405(4) Uani 1 1 d . . C12 C 0.11452(16) 0.52797(17) 0.33236(11) 0.0417(4) Uani 1 1 d . . C6 C 0.19508(16) 0.41300(16) 0.49977(11) 0.0397(4) Uani 1 1 d . . C29B C 0.04861(16) 0.91308(17) 0.94426(12) 0.0448(4) Uani 1 1 d . . C9 C 0.32155(16) 0.55837(16) 0.56698(11) 0.0411(4) Uani 1 1 d . . C28B C 0.10638(18) 0.82179(19) 0.88364(14) 0.0507(4) Uani 1 1 d . . C15 C 0.30967(18) 0.89154(18) 0.19341(12) 0.0501(4) Uani 1 1 d . . H15 H 0.381476 0.911439 0.142524 0.060 Uiso 1 1 calc R U C14 C 0.29640(17) 0.76187(17) 0.23982(12) 0.0452(4) Uani 1 1 d . . H14 H 0.359316 0.693379 0.221090 0.054 Uiso 1 1 calc R U C7 C 0.23582(17) 0.35815(17) 0.58644(11) 0.0457(4) Uani 1 1 d . . H7 H 0.221092 0.272984 0.620853 0.055 Uiso 1 1 calc R U C28 C 0.4093(2) 0.52717(16) 0.83193(14) 0.0528(5) Uani 1 1 d . . C10 C 0.28306(17) 0.61318(16) 0.48020(11) 0.0425(4) Uani 1 1 d . . H10 H 0.300778 0.696942 0.444351 0.051 Uiso 1 1 calc R U C31 C 0.36919(19) 0.48584(18) 1.00677(13) 0.0522(5) Uani 1 1 d . . H31 H 0.280803 0.475950 1.011888 0.063 Uiso 1 1 calc R U C8 C 0.29561(17) 0.42432(17) 0.62180(11) 0.0445(4) Uani 1 1 d . . C21 C 0.32937(18) 0.09801(18) 0.92005(13) 0.0530(5) Uani 1 1 d . . H21 H 0.310044 0.085678 0.984567 0.064 Uiso 1 1 calc R U C18 C 0.09338(17) 0.83489(18) 0.34331(12) 0.0481(4) Uani 1 1 d . . H18 H 0.020818 0.814795 0.393556 0.058 Uiso 1 1 calc R U C16 C 0.21598(18) 0.99167(17) 0.22279(12) 0.0488(4) Uani 1 1 d . . C25 C 0.40036(18) 0.76238(17) 0.55565(12) 0.0480(4) Uani 1 1 d . . H25 H 0.441020 0.772207 0.488906 0.058 Uiso 1 1 calc R U C20 C 0.31243(19) 0.22383(18) 0.86026(12) 0.0516(4) Uani 1 1 d . . H20 H 0.281686 0.295948 0.884987 0.062 Uiso 1 1 calc R U C17 C 0.10715(18) 0.96458(18) 0.29687(13) 0.0533(5) Uani 1 1 d . . H17 H 0.043752 1.033019 0.315293 0.064 Uiso 1 1 calc R U C22 C 0.37485(17) -0.00880(17) 0.88395(13) 0.0490(4) Uani 1 1 d . . C4 C 0.03202(18) 0.32686(19) 0.35552(13) 0.0506(4) Uani 1 1 d . . H4A H 0.018621 0.241819 0.391230 0.061 Uiso 1 1 calc R U C19 C 0.34055(18) 0.24422(17) 0.76396(12) 0.0482(4) Uani 1 1 d . . C1 C 0.07091(18) 0.58094(19) 0.24744(12) 0.0511(4) Uani 1 1 d . . H1 H 0.083759 0.665665 0.210633 0.061 Uiso 1 1 calc R U C30 C 0.58695(19) 0.52680(18) 0.91332(13) 0.0522(5) Uani 1 1 d . . H30 H 0.646204 0.544698 0.855025 0.063 Uiso 1 1 calc R U C3 C -0.01021(19) 0.3796(2) 0.27285(13) 0.0550(5) Uani 1 1 d . . H3A H -0.051925 0.330510 0.252429 0.066 Uiso 1 1 calc R U C2 C 0.00924(19) 0.5067(2) 0.21928(13) 0.0566(5) Uani 1 1 d . . H2 H -0.020192 0.542051 0.163199 0.068 Uiso 1 1 calc R U C30B C 0.0220(2) 1.04692(19) 0.90400(13) 0.0572(5) Uani 1 1 d . . H34 H 0.036702 1.079580 0.839052 0.069 Uiso 1 1 calc R U C32 C -0.0262(2) 1.13326(19) 0.95919(13) 0.0564(5) Uani 1 1 d . . H35 H -0.043774 1.223561 0.931024 0.068 Uiso 1 1 calc R U C23 C 0.4027(2) 0.00880(19) 0.78864(14) 0.0561(5) Uani 1 1 d . . H23 H 0.432384 -0.063843 0.764443 0.067 Uiso 1 1 calc R U C24 C 0.3862(2) 0.13476(19) 0.72907(13) 0.0559(5) Uani 1 1 d . . H24 H 0.406099 0.146447 0.664611 0.067 Uiso 1 1 calc R U C26 C 0.2680(2) 0.85861(19) 0.56416(16) 0.0660(5) Uani 1 1 d . . H26A H 0.206996 0.838045 0.536099 0.099 Uiso 1 1 calc R U H26B H 0.285334 0.946984 0.532543 0.099 Uiso 1 1 calc R U H26C H 0.227995 0.851673 0.629217 0.099 Uiso 1 1 calc R U C27 C 0.4985(2) 0.7927(2) 0.59984(17) 0.0716(6) Uani 1 1 d . . H27A H 0.457964 0.788221 0.664522 0.107 Uiso 1 1 calc R U H27B H 0.519009 0.879794 0.567179 0.107 Uiso 1 1 calc R U H27C H 0.580454 0.729337 0.595766 0.107 Uiso 1 1 calc R U H4 H 0.4107(18) 0.5879(19) 0.6504(14) 0.060(6) Uiso 1 1 d . . H3 H 0.337(2) 0.429(2) 0.7340(17) 0.085(8) Uiso 1 1 d . . H3B H 0.169(3) 0.641(3) 0.892(2) 0.117(10) Uiso 1 1 d . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl2 0.0840(4) 0.0429(3) 0.0718(4) 0.0012(2) -0.0233(3) -0.0043(2) Cl1 0.0986(4) 0.0429(3) 0.0806(4) -0.0081(3) -0.0012(3) -0.0127(3) O2 0.0771(9) 0.0589(8) 0.0727(9) -0.0361(7) -0.0507(7) 0.0159(7) O1B 0.0854(10) 0.0479(8) 0.0609(9) -0.0205(7) -0.0273(7) 0.0057(7) O1 0.0893(10) 0.0713(10) 0.0494(8) -0.0278(7) -0.0378(8) 0.0136(7) N1 0.0517(8) 0.0409(8) 0.0317(7) -0.0096(6) -0.0177(6) -0.0047(6) O2B 0.1005(11) 0.0678(10) 0.0480(9) -0.0234(7) -0.0176(7) 0.0030(8) N4 0.0603(9) 0.0457(8) 0.0373(8) -0.0121(7) -0.0222(7) -0.0084(7) N2 0.0567(8) 0.0438(8) 0.0379(8) -0.0119(6) -0.0187(6) -0.0082(6) N3 0.1023(13) 0.0436(9) 0.0449(9) -0.0033(7) -0.0429(9) -0.0174(8) C29 0.0669(11) 0.0350(9) 0.0471(10) -0.0163(8) -0.0335(9) 0.0071(8) C11 0.0475(9) 0.0413(9) 0.0308(8) -0.0102(7) -0.0145(7) -0.0036(7) C5 0.0476(9) 0.0471(10) 0.0372(9) -0.0166(8) -0.0151(7) -0.0040(7) C13 0.0514(9) 0.0410(9) 0.0319(8) -0.0069(7) -0.0189(7) -0.0055(7) C12 0.0453(9) 0.0482(10) 0.0365(9) -0.0171(8) -0.0149(7) -0.0024(7) C6 0.0489(9) 0.0405(9) 0.0333(8) -0.0118(7) -0.0141(7) -0.0054(7) C29B 0.0473(9) 0.0466(10) 0.0435(10) -0.0139(8) -0.0193(7) 0.0000(7) C9 0.0503(9) 0.0423(9) 0.0353(9) -0.0136(7) -0.0158(7) -0.0047(7) C28B 0.0538(10) 0.0524(11) 0.0509(11) -0.0175(9) -0.0247(8) 0.0022(8) C15 0.0509(10) 0.0511(11) 0.0439(10) -0.0101(8) -0.0060(8) -0.0092(8) C14 0.0484(9) 0.0439(10) 0.0421(9) -0.0140(8) -0.0128(7) 0.0012(7) C7 0.0644(11) 0.0394(9) 0.0364(9) -0.0054(7) -0.0209(8) -0.0097(8) C28 0.0808(14) 0.0335(9) 0.0563(12) -0.0200(8) -0.0437(11) 0.0119(8) C10 0.0580(10) 0.0388(9) 0.0345(9) -0.0071(7) -0.0181(7) -0.0098(7) C31 0.0608(11) 0.0476(10) 0.0571(12) -0.0159(9) -0.0336(9) 0.0006(8) C8 0.0617(10) 0.0415(9) 0.0348(9) -0.0091(7) -0.0221(8) -0.0053(8) C21 0.0638(11) 0.0516(11) 0.0398(10) -0.0062(8) -0.0166(8) -0.0047(9) C18 0.0505(10) 0.0511(11) 0.0390(9) -0.0130(8) -0.0069(7) -0.0042(8) C16 0.0570(10) 0.0401(10) 0.0473(10) -0.0087(8) -0.0152(8) -0.0044(8) C25 0.0612(11) 0.0491(10) 0.0387(9) -0.0129(8) -0.0116(8) -0.0162(8) C20 0.0690(11) 0.0435(10) 0.0453(10) -0.0122(8) -0.0235(9) -0.0018(8) C17 0.0571(11) 0.0464(11) 0.0512(11) -0.0163(9) -0.0102(8) 0.0031(8) C22 0.0536(10) 0.0406(10) 0.0509(11) -0.0053(8) -0.0190(8) -0.0054(8) C4 0.0605(11) 0.0502(11) 0.0501(10) -0.0188(9) -0.0199(8) -0.0093(8) C19 0.0627(11) 0.0455(10) 0.0424(10) -0.0063(8) -0.0271(8) -0.0098(8) C1 0.0638(11) 0.0550(11) 0.0397(10) -0.0109(8) -0.0237(8) -0.0077(9) C30 0.0664(12) 0.0492(11) 0.0447(10) -0.0149(8) -0.0252(9) 0.0016(8) C3 0.0618(11) 0.0649(13) 0.0532(11) -0.0272(10) -0.0252(9) -0.0081(9) C2 0.0672(12) 0.0675(13) 0.0439(10) -0.0180(9) -0.0288(9) -0.0044(9) C30B 0.0803(13) 0.0522(11) 0.0365(10) -0.0095(9) -0.0191(9) -0.0023(9) C32 0.0803(13) 0.0412(10) 0.0462(11) -0.0100(8) -0.0241(9) 0.0018(9) C23 0.0692(12) 0.0485(11) 0.0560(12) -0.0188(9) -0.0222(9) -0.0038(9) C24 0.0752(12) 0.0572(12) 0.0401(10) -0.0129(9) -0.0220(9) -0.0095(9) C26 0.0755(13) 0.0483(12) 0.0762(14) -0.0169(10) -0.0210(11) -0.0085(10) C27 0.0830(14) 0.0698(14) 0.0798(15) -0.0220(12) -0.0331(12) -0.0256(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C28B O1B H3B 111.5(18) . . C11 N1 C12 121.20(14) . . C11 N1 C13 118.73(13) . . C12 N1 C13 120.03(12) . . C9 N4 C25 124.72(14) . . C9 N4 H4 120.9(13) . . C25 N4 H4 114.3(13) . . C6 N2 C5 118.12(14) . . C8 N3 C19 127.90(16) . . C8 N3 H3 118.2(16) . . C19 N3 H3 113.1(16) . . C31 C29 C30 118.90(16) . . C31 C29 C28 121.25(17) . . C30 C29 C28 119.84(18) . . N1 C11 C10 122.27(15) . . N1 C11 C6 117.12(14) . . C10 C11 C6 120.60(14) . . N2 C5 C12 122.53(14) . . N2 C5 C4 118.86(16) . . C12 C5 C4 118.60(15) . . C14 C13 C18 121.84(16) . . C14 C13 N1 119.45(14) . . C18 C13 N1 118.69(15) . . N1 C12 C1 121.95(16) . . N1 C12 C5 117.97(14) . . C1 C12 C5 120.07(15) . . N2 C6 C7 119.41(15) . . N2 C6 C11 123.00(14) . . C7 C6 C11 117.57(14) . . C30B C29B C32 118.75(17) . 2_577 C30B C29B C28B 119.87(16) . . C32 C29B C28B 121.32(16) 2_577 . N4 C9 C10 121.46(16) . . N4 C9 C8 119.93(14) . . C10 C9 C8 118.61(14) . . O2B C28B O1B 123.41(18) . . O2B C28B C29B 122.98(18) . . O1B C28B C29B 113.61(16) . . C14 C15 C16 119.68(16) . . C14 C15 H15 120.2 . . C16 C15 H15 120.2 . . C13 C14 C15 118.88(16) . . C13 C14 H14 120.6 . . C15 C14 H14 120.6 . . C8 C7 C6 122.99(16) . . C8 C7 H7 118.5 . . C6 C7 H7 118.5 . . O1 C28 O2 123.17(16) . . O1 C28 C29 118.01(17) . . O2 C28 C29 118.79(18) . . C11 C10 C9 121.32(15) . . C11 C10 H10 119.3 . . C9 C10 H10 119.3 . . C29 C31 C30 120.61(17) . 2_667 C29 C31 H31 119.7 . . C30 C31 H31 119.7 2_667 . C7 C8 N3 124.07(16) . . C7 C8 C9 118.88(14) . . N3 C8 C9 117.04(14) . . C22 C21 C20 119.77(17) . . C22 C21 H21 120.1 . . C20 C21 H21 120.1 . . C13 C18 C17 119.14(16) . . C13 C18 H18 120.4 . . C17 C18 H18 120.4 . . C15 C16 C17 121.18(17) . . C15 C16 Cl1 119.20(14) . . C17 C16 Cl1 119.61(14) . . N4 C25 C26 111.82(15) . . N4 C25 C27 109.06(15) . . C26 C25 C27 110.44(16) . . N4 C25 H25 108.5 . . C26 C25 H25 108.5 . . C27 C25 H25 108.5 . . C21 C20 C19 120.98(17) . . C21 C20 H20 119.5 . . C19 C20 H20 119.5 . . C18 C17 C16 119.27(16) . . C18 C17 H17 120.4 . . C16 C17 H17 120.4 . . C21 C22 C23 120.36(17) . . C21 C22 Cl2 119.95(14) . . C23 C22 Cl2 119.68(14) . . C3 C4 C5 120.78(18) . . C3 C4 H4A 119.6 . . C5 C4 H4A 119.6 . . C20 C19 C24 118.24(16) . . C20 C19 N3 117.98(16) . . C24 C19 N3 123.57(16) . . C2 C1 C12 119.37(18) . . C2 C1 H1 120.3 . . C12 C1 H1 120.3 . . C31 C30 C29 120.49(18) 2_667 . C31 C30 H30 119.8 2_667 . C29 C30 H30 119.8 . . C4 C3 C2 119.88(17) . . C4 C3 H3A 120.1 . . C2 C3 H3A 120.1 . . C1 C2 C3 121.30(16) . . C1 C2 H2 119.4 . . C3 C2 H2 119.4 . . C29B C30B C32 120.56(17) . . C29B C30B H34 119.7 . . C32 C30B H34 119.7 . . C29B C32 C30B 120.68(17) 2_577 . C29B C32 H35 119.7 2_577 . C30B C32 H35 119.7 . . C22 C23 C24 119.70(17) . . C22 C23 H23 120.2 . . C24 C23 H23 120.2 . . C23 C24 C19 120.95(17) . . C23 C24 H24 119.5 . . C19 C24 H24 119.5 . . C25 C26 H26A 109.5 . . C25 C26 H26B 109.5 . . H26A C26 H26B 109.5 . . C25 C26 H26C 109.5 . . H26A C26 H26C 109.5 . . H26B C26 H26C 109.5 . . C25 C27 H27A 109.5 . . C25 C27 H27B 109.5 . . H27A C27 H27B 109.5 . . C25 C27 H27C 109.5 . . H27A C27 H27C 109.5 . . H27B C27 H27C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Cl2 C22 1.7350(17) . Cl1 C16 1.7308(18) . O2 C28 1.261(2) . O1B C28B 1.316(2) . O1B H3B 0.95(3) . O1 C28 1.249(2) . N1 C11 1.3656(19) . N1 C12 1.386(2) . N1 C13 1.451(2) . O2B C28B 1.210(2) . N4 C9 1.329(2) . N4 C25 1.467(2) . N4 H4 0.86(2) . N2 C6 1.320(2) . N2 C5 1.369(2) . N3 C8 1.365(2) . N3 C19 1.408(2) . N3 H3 0.85(2) . C29 C31 1.381(3) . C29 C30 1.385(3) . C29 C28 1.507(2) . C11 C10 1.377(2) . C11 C6 1.447(2) . C5 C12 1.404(2) . C5 C4 1.408(2) . C13 C14 1.375(2) . C13 C18 1.378(2) . C12 C1 1.403(2) . C6 C7 1.414(2) . C29B C30B 1.375(2) . C29B C32 1.381(2) 2_577 C29B C28B 1.489(2) . C9 C10 1.405(2) . C9 C8 1.473(2) . C15 C14 1.378(2) . C15 C16 1.379(2) . C15 H15 0.9300 . C14 H14 0.9300 . C7 C8 1.361(2) . C7 H7 0.9300 . C10 H10 0.9300 . C31 C30 1.385(2) 2_667 C31 H31 0.9300 . C21 C22 1.373(3) . C21 C20 1.381(2) . C21 H21 0.9300 . C18 C17 1.379(2) . C18 H18 0.9300 . C16 C17 1.379(2) . C25 C26 1.517(3) . C25 C27 1.518(2) . C25 H25 0.9800 . C20 C19 1.386(2) . C20 H20 0.9300 . C17 H17 0.9300 . C22 C23 1.375(3) . C4 C3 1.365(2) . C4 H4A 0.9300 . C19 C24 1.388(3) . C1 C2 1.369(2) . C1 H1 0.9300 . C30 H30 0.9300 . C3 C2 1.389(3) . C3 H3A 0.9300 . C2 H2 0.9300 . C30B C32 1.381(3) . C30B H34 0.9300 . C32 H35 0.9300 . C23 C24 1.380(3) . C23 H23 0.9300 . C24 H24 0.9300 . C26 H26A 0.9600 . C26 H26B 0.9600 . C26 H26C 0.9600 . C27 H27A 0.9600 . C27 H27B 0.9600 . C27 H27C 0.9600 . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C14 H14 O1 0.93 2.40 3.276(2) 156.7 2_666 C20 H20 O2 0.93 2.54 3.307(2) 139.7 . C26 H26C O2B 0.96 2.55 3.502(3) 171.5 . N4 H4 O1 0.86(2) 1.98(2) 2.8363(19) 172.9(18) . N3 H3 O2 0.85(2) 2.17(2) 2.976(2) 159(2) . N3 H3 O1 0.85(2) 2.30(2) 2.996(2) 140(2) . O1B H3B O2 0.95(3) 1.66(3) 2.5936(19) 170(3) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_4 C12 N1 C11 C10 178.47(15) . . C13 N1 C11 C10 -3.6(2) . . C12 N1 C11 C6 -2.6(2) . . C13 N1 C11 C6 175.29(13) . . C6 N2 C5 C12 -1.5(2) . . C6 N2 C5 C4 179.52(15) . . C11 N1 C13 C14 98.18(18) . . C12 N1 C13 C14 -83.88(19) . . C11 N1 C13 C18 -80.62(19) . . C12 N1 C13 C18 97.32(18) . . C11 N1 C12 C1 -178.66(15) . . C13 N1 C12 C1 3.5(2) . . C11 N1 C12 C5 2.1(2) . . C13 N1 C12 C5 -175.76(14) . . N2 C5 C12 N1 0.0(2) . . C4 C5 C12 N1 178.97(15) . . N2 C5 C12 C1 -179.20(16) . . C4 C5 C12 C1 -0.3(2) . . C5 N2 C6 C7 179.60(15) . . C5 N2 C6 C11 1.0(2) . . N1 C11 C6 N2 1.1(2) . . C10 C11 C6 N2 179.99(16) . . N1 C11 C6 C7 -177.58(15) . . C10 C11 C6 C7 1.3(2) . . C25 N4 C9 C10 4.5(3) . . C25 N4 C9 C8 -174.99(15) . . C30B C29B C28B O2B 5.7(3) . . C32 C29B C28B O2B -171.44(19) 2_577 . C30B C29B C28B O1B -174.57(16) . . C32 C29B C28B O1B 8.2(2) 2_577 . C18 C13 C14 C15 0.3(3) . . N1 C13 C14 C15 -178.43(14) . . C16 C15 C14 C13 0.6(3) . . N2 C6 C7 C8 -178.37(16) . . C11 C6 C7 C8 0.3(3) . . C31 C29 C28 O1 -162.65(17) . . C30 C29 C28 O1 17.1(2) . . C31 C29 C28 O2 15.4(2) . . C30 C29 C28 O2 -164.78(16) . . N1 C11 C10 C9 176.65(15) . . C6 C11 C10 C9 -2.2(3) . . N4 C9 C10 C11 -178.07(15) . . C8 C9 C10 C11 1.4(2) . . C30 C29 C31 C30 0.3(3) . 2_667 C28 C29 C31 C30 -179.93(15) . 2_667 C6 C7 C8 N3 177.59(17) . . C6 C7 C8 C9 -1.1(3) . . C19 N3 C8 C7 13.9(3) . . C19 N3 C8 C9 -167.39(17) . . N4 C9 C8 C7 179.73(16) . . C10 C9 C8 C7 0.2(2) . . N4 C9 C8 N3 1.0(2) . . C10 C9 C8 N3 -178.53(16) . . C14 C13 C18 C17 -0.5(3) . . N1 C13 C18 C17 178.27(14) . . C14 C15 C16 C17 -1.3(3) . . C14 C15 C16 Cl1 179.20(13) . . C9 N4 C25 C26 71.4(2) . . C9 N4 C25 C27 -166.14(17) . . C22 C21 C20 C19 0.1(3) . . C13 C18 C17 C16 -0.2(3) . . C15 C16 C17 C18 1.2(3) . . Cl1 C16 C17 C18 -179.38(14) . . C20 C21 C22 C23 -0.5(3) . . C20 C21 C22 Cl2 179.52(13) . . N2 C5 C4 C3 179.11(16) . . C12 C5 C4 C3 0.1(3) . . C21 C20 C19 C24 0.0(3) . . C21 C20 C19 N3 -175.03(16) . . C8 N3 C19 C20 -148.7(2) . . C8 N3 C19 C24 36.6(3) . . N1 C12 C1 C2 -178.79(16) . . C5 C12 C1 C2 0.4(3) . . C31 C29 C30 C31 -0.3(3) . 2_667 C28 C29 C30 C31 179.93(15) . 2_667 C5 C4 C3 C2 -0.1(3) . . C12 C1 C2 C3 -0.4(3) . . C4 C3 C2 C1 0.3(3) . . C32 C29B C30B C32 0.0(3) 2_577 . C28B C29B C30B C32 -177.29(17) . . C29B C30B C32 C29B 0.0(3) . 2_577 C21 C22 C23 C24 0.8(3) . . Cl2 C22 C23 C24 -179.19(14) . . C22 C23 C24 C19 -0.7(3) . . C20 C19 C24 C23 0.3(3) . . N3 C19 C24 C23 175.06(17) . . _cod_database_fobs_code 2108447