#------------------------------------------------------------------------------ #$Date: 2020-09-11 08:26:38 +0300 (Fri, 11 Sep 2020) $ #$Revision: 256342 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/10/86/2108658.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108658 loop_ _publ_author_name 'Mali, Bhupendra P.' 'Dash, Soumya Ranjan' 'Nikam, Shrikant B.' 'Puthuvakkal, Anisha' 'Vanka, Kumar' 'Manoj, Kochunnoonny' 'Gonnade, Rajesh G.' _publ_section_title ; Five concomitant polymorphs of a green fluorescent protein chromophore (GFPc) analogue: understanding variations in photoluminescence with \p-stacking interactions ; _journal_coeditor_code AW5046SUP1 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first ; ; _journal_paper_doi 10.1107/S2052520620010343 _journal_volume 76 _journal_year 2020 _chemical_formula_moiety 'C15 H18 N2 O4' _chemical_formula_sum 'C15 H18 N2 O4' _chemical_formula_weight 290.31 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 98.6000(10) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 12.7410(4) _cell_length_b 7.7542(3) _cell_length_c 29.3961(11) _cell_measurement_reflns_used 4617 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 30.53 _cell_measurement_theta_min 3.08 _cell_volume 2871.57(18) _computing_cell_refinement 'SAINT (Bruker, 2016)' _computing_data_collection 'APEX3 (Bruker, 2016)' _computing_data_reduction 'SAINT (Bruker, 2016)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 100(2) _diffrn_detector 'Photon II CPAD Area Detector' _diffrn_detector_area_resol_mean 7.39 _diffrn_measured_fraction_theta_full 0.992 _diffrn_measured_fraction_theta_max 0.983 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE Kappa Duo PHOTON II CPAD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0441 _diffrn_reflns_av_unetI/netI 0.0524 _diffrn_reflns_Laue_measured_fraction_full 0.992 _diffrn_reflns_Laue_measured_fraction_max 0.983 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 41 _diffrn_reflns_limit_l_min -41 _diffrn_reflns_number 13345 _diffrn_reflns_point_group_measured_fraction_full 0.992 _diffrn_reflns_point_group_measured_fraction_max 0.983 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.543 _diffrn_reflns_theta_min 3.085 _diffrn_source 'micro-focus sealed tube' _diffrn_source_type 'Incoatech I\mS HB' _exptl_absorpt_coefficient_mu 0.098 _exptl_absorpt_correction_T_max 0.993 _exptl_absorpt_correction_T_min 0.988 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Bruker, 2006)' _exptl_crystal_colour YELLOW _exptl_crystal_density_diffrn 1.343 _exptl_crystal_description BLOCK _exptl_crystal_F_000 1232 _exptl_crystal_size_max 0.120 _exptl_crystal_size_mid 0.090 _exptl_crystal_size_min 0.070 _refine_diff_density_max 0.411 _refine_diff_density_min -0.277 _refine_diff_density_rms 0.054 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.087 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 195 _refine_ls_number_reflns 4321 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.087 _refine_ls_R_factor_all 0.0735 _refine_ls_R_factor_gt 0.0559 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0443P)^2^+2.8645P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1191 _refine_ls_wR_factor_ref 0.1267 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3469 _reflns_number_total 4321 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file aw5046sup1.cif _cod_data_source_block Form_I _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was changed to 'multi-scan' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/IUCr/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas ; _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 2108658 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.988 _shelx_estimated_absorpt_t_max 0.993 _shelx_res_file ; PIM.res created by SHELXL-2014/7 TITL PIM_a.res in C2/c CELL 0.71073 12.7410 7.7542 29.3961 90.000 98.600 90.000 ZERR 8.00 0.0004 0.0003 0.0011 0.000 0.001 0.000 LATT 7 SYMM -x, y, -z+1/2 SFAC C H N O UNIT 120 144 16 32 L.S. 30 ACTA BOND $H FMAP 2 PLAN 2 HTAB C14 O4 HTAB C13 O2_$3 HTAB C13 O3_$3 HTAB C12 O1_$2 HTAB C6 O1_$1 HTAB C2 N2 HTAB C14 O4 HTAB C13 O2_$3 HTAB C13 O3_$3 HTAB C12 O1_$2 HTAB C6 O1_$1 HTAB C2 N2 HTAB C14 O4 HTAB C13 O2_$3 HTAB C13 O3_$3 HTAB C12 O1_$2 HTAB C6 O1_$1 HTAB C2 N2 HTAB C14 O4 HTAB C13 O2_$3 HTAB C13 O3_$3 HTAB C12 O1_$2 HTAB C6 O1_$1 HTAB C2 N2 HTAB SIZE 0.12 0.09 0.07 CONF HTAB C2 N2 EQIV $1 -x+1/2, -y+1/2, -z+1 HTAB C6 O1_$1 EQIV $2 -x+1, -y, -z+1 HTAB C12 O1_$2 EQIV $3 -x+1/2, y-1/2, -z+1/2 HTAB C13 O3_$3 HTAB C13 O2_$3 HTAB C14 O4 HTAB C2 N2 HTAB C6 O1_$1 HTAB C12 O1_$2 HTAB C13 O3_$3 HTAB C13 O2_$3 HTAB C14 O4 HTAB C2 N2 HTAB C6 O1_$1 HTAB C12 O1_$2 HTAB C13 O3_$3 HTAB C13 O2_$3 HTAB C14 O4 HTAB C2 N2 HTAB C6 O1_$1 HTAB C12 O1_$2 HTAB C13 O3_$3 HTAB C13 O2_$3 HTAB C14 O4 TEMP -173.090 WGHT 0.044300 2.864500 FVAR 0.54528 O1 4 0.352018 0.042781 0.478363 11.00000 0.02503 0.02313 = 0.01640 0.00459 0.00425 0.00258 O2 4 0.222673 0.733532 0.284956 11.00000 0.02857 0.01631 = 0.01220 0.00038 0.00842 0.00252 O3 4 0.145054 0.979697 0.332809 11.00000 0.02171 0.01387 = 0.01923 0.00322 0.00561 0.00080 O4 4 0.111659 0.929603 0.419654 11.00000 0.02491 0.01840 = 0.01363 -0.00090 0.00657 0.00551 N1 3 0.418567 -0.025979 0.411356 11.00000 0.01648 0.01492 = 0.01768 0.00095 0.00199 0.00102 N2 3 0.365242 0.202495 0.366022 11.00000 0.01541 0.01608 = 0.01557 0.00040 0.00340 -0.00032 C1 1 0.236869 0.513707 0.397268 11.00000 0.01156 0.01681 = 0.01365 0.00030 0.00076 -0.00042 C2 1 0.250979 0.541407 0.351286 11.00000 0.01396 0.01619 = 0.01465 -0.00102 0.00332 0.00170 AFIX 43 H2 2 0.283714 0.455753 0.335047 11.00000 -1.20000 AFIX 0 C3 1 0.216604 0.695118 0.329871 11.00000 0.01357 0.01615 = 0.01272 -0.00013 0.00436 -0.00205 C4 1 0.171296 0.824665 0.353899 11.00000 0.01369 0.01391 = 0.01563 0.00157 0.00344 -0.00022 C5 1 0.156751 0.795842 0.399520 11.00000 0.01351 0.01611 = 0.01498 -0.00198 0.00377 -0.00092 C6 1 0.187597 0.640244 0.420886 11.00000 0.01425 0.01879 = 0.01114 0.00045 0.00229 0.00080 AFIX 43 H6 2 0.175321 0.619514 0.451505 11.00000 -1.20000 AFIX 0 C7 1 0.273090 0.357439 0.422377 11.00000 0.01561 0.01844 = 0.01232 0.00118 0.00131 -0.00074 AFIX 43 H7 2 0.254556 0.347629 0.452394 11.00000 -1.20000 AFIX 0 C8 1 0.329273 0.225195 0.408729 11.00000 0.01436 0.01616 = 0.01429 0.00136 0.00077 -0.00074 C9 1 0.364363 0.075146 0.438760 11.00000 0.01443 0.01713 = 0.01601 0.00094 0.00146 -0.00082 C10 1 0.415195 0.056066 0.369073 11.00000 0.01278 0.01694 = 0.01518 0.00019 0.00128 -0.00352 C11 1 0.463377 -0.023405 0.331250 11.00000 0.01938 0.01971 = 0.02016 -0.00267 0.00547 0.00104 AFIX 137 H11A 2 0.459717 0.057955 0.305550 11.00000 -1.50000 H11B 2 0.424524 -0.128772 0.320880 11.00000 -1.50000 H11C 2 0.537747 -0.051940 0.342312 11.00000 -1.50000 AFIX 0 C12 1 0.470346 -0.188110 0.426239 11.00000 0.02236 0.01513 = 0.02494 0.00416 0.00272 0.00381 AFIX 137 H12A 2 0.505421 -0.177083 0.458127 11.00000 -1.50000 H12B 2 0.523260 -0.216111 0.406375 11.00000 -1.50000 H12C 2 0.417200 -0.280240 0.424233 11.00000 -1.50000 AFIX 0 C13 1 0.256459 0.598993 0.257301 11.00000 0.02633 0.02488 = 0.01402 -0.00264 0.00446 0.00749 AFIX 137 H13A 2 0.330548 0.569548 0.268655 11.00000 -1.50000 H13B 2 0.250323 0.638004 0.225303 11.00000 -1.50000 H13C 2 0.211690 0.497096 0.258967 11.00000 -1.50000 AFIX 0 C14 1 0.034794 0.995748 0.316211 11.00000 0.02474 0.02362 = 0.02624 0.00812 0.00160 0.00391 AFIX 137 H14A 2 0.012339 0.901246 0.294821 11.00000 -1.50000 H14B 2 0.021395 1.106288 0.300237 11.00000 -1.50000 H14C 2 -0.005341 0.990771 0.342138 11.00000 -1.50000 AFIX 0 C15 1 0.099170 0.907520 0.466754 11.00000 0.02559 0.02367 = 0.01557 -0.00113 0.00852 0.00559 AFIX 137 H15A 2 0.049186 0.813250 0.469362 11.00000 -1.50000 H15B 2 0.071713 1.014347 0.478350 11.00000 -1.50000 H15C 2 0.168039 0.879802 0.484889 11.00000 -1.50000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM PIM_a.res in C2/c REM R1 = 0.0559 for 3469 Fo > 4sig(Fo) and 0.0735 for all 4321 data REM 195 parameters refined using 0 restraints END WGHT 0.0443 2.8645 REM Instructions for potential hydrogen bonds HTAB C2 N2 HTAB C6 O1_$1 HTAB C12 O1_$2 HTAB C13 O3_$3 HTAB C13 O2_$3 HTAB C14 O4 REM Highest difference peak 0.411, deepest hole -0.277, 1-sigma level 0.054 Q1 1 0.2541 0.5323 0.3773 11.00000 0.05 0.41 Q2 1 0.1727 0.8184 0.3798 11.00000 0.05 0.37 ; _shelx_res_checksum 59436 _shelx_hkl_file ; 2 0 -2 767.42 30.60 -2 0 2 830.92 30.10 -2 0 2 699.13 29.50 2 0 -2 797.52 29.90 2 0 -2 815.22 29.70 -4 0 4 35.30 5.60 4 0 -4 28.60 5.00 4 0 -4 38.00 5.70 4 0 -4 27.30 4.50 -4 0 4 34.30 5.40 -6 0 6 602.74 27.10 6 0 -6 623.34 26.40 -6 0 6 646.54 28.00 6 0 -6 541.05 26.60 6 0 -6 573.24 27.20 8 0 -8 90.19 8.60 -8 0 8 85.39 9.00 -8 0 8 92.09 11.10 8 0 -8 94.09 9.80 8 0 -8 81.89 9.00 10 0 -10 98.29 9.90 -10 0 10 76.39 11.50 10 0 -10 92.59 11.70 12 0 -12 52.69 10.10 12 0 -12 66.29 10.50 14 0 -14 68.29 11.60 -3 1 3 2126.79 80.99 -3 1 3 2226.68 81.39 3 -1 -3 2193.98 81.69 3 -1 -3 2187.88 81.19 3 -1 -3 2194.48 81.19 -3 -1 3 2137.39 78.69 -5 1 5 192.38 12.10 5 1 -5 186.58 8.80 5 1 -5 175.38 9.10 -5 1 5 184.58 12.10 5 -1 -5 178.48 12.00 -5 -1 5 182.98 11.00 5 -1 -5 155.88 11.90 5 -1 -5 168.98 11.60 -5 -1 5 185.28 10.20 7 1 -7 51.49 5.20 -7 1 7 49.60 8.30 -7 1 7 42.30 7.90 7 1 -7 49.99 5.50 -7 -1 7 59.59 7.80 -7 -1 7 58.39 8.20 7 -1 -7 61.89 9.00 7 -1 -7 53.49 8.90 7 -1 -7 49.00 8.20 9 1 -9 11.80 4.30 -9 1 9 22.80 6.80 9 1 -9 14.30 4.00 9 -1 -9 18.30 6.20 -9 -1 9 11.50 5.60 -9 -1 9 19.90 5.90 9 -1 -9 11.70 6.10 9 -1 -9 12.10 6.40 11 1 -11 3.90 3.60 11 -1 -11 3.60 6.20 11 -1 -11 12.40 6.40 11 -1 -11 0.00 5.90 13 1 -13 38.50 4.70 13 1 -13 37.30 4.60 13 -1 -13 45.20 10.00 15 -1 -15 450.65 26.90 17 -1 -17 -7.10 8.70 -2 2 2 2238.18 81.99 2 -2 -2 2128.69 81.79 2 -2 -2 2235.68 82.09 -2 -2 2 2167.28 78.89 -4 2 4 1506.55 60.49 -4 2 4 1552.24 60.69 -4 -2 4 1525.15 56.59 4 -2 -4 1567.34 61.89 4 -2 -4 1533.05 60.79 4 -2 -4 1554.64 60.99 -6 2 6 2372.06 89.29 -6 2 6 2409.16 89.79 6 -2 -6 2287.97 90.49 -6 -2 6 2296.47 86.99 6 -2 -6 2234.48 89.19 -6 -2 6 2257.17 90.19 6 -2 -6 2151.78 88.89 -8 2 8 21.00 6.60 8 -2 -8 12.20 6.40 -8 -2 8 22.30 5.30 8 -2 -8 28.10 8.30 8 -2 -8 17.70 7.10 10 -2 -10 196.28 17.20 10 -2 -10 251.97 18.90 12 -2 -12 205.68 17.70 12 -2 -12 208.68 19.00 14 -2 -14 31.20 9.80 16 -2 -16 32.80 10.50 -1 3 1 255.97 13.30 1 -3 -1 258.97 14.10 1 -3 -1 267.47 14.60 -1 -3 1 245.88 12.80 -3 3 3 717.93 31.20 3 -3 -3 695.23 31.30 3 -3 -3 731.53 31.70 -3 -3 3 672.73 27.50 3 -3 -3 702.63 32.50 -5 3 5 74.39 9.80 5 -3 -5 75.59 11.20 5 -3 -5 64.79 9.40 -5 -3 5 77.39 5.50 5 -3 -5 81.09 10.90 -7 3 7 454.85 25.00 -7 3 7 430.16 24.70 7 -3 -7 411.06 24.80 7 -3 -7 515.15 26.60 -7 -3 7 415.76 20.00 7 -3 -7 445.86 26.50 -7 -3 7 460.05 22.60 9 -3 -9 185.38 16.60 -9 -3 9 193.38 12.80 9 -3 -9 200.88 17.20 -9 -3 9 167.98 13.90 11 -3 -11 147.69 16.40 11 -3 -11 178.48 17.40 -11 -3 11 149.88 13.00 13 -3 -13 39.40 11.20 13 -3 -13 26.80 11.00 15 -3 -15 -10.00 7.50 15 -3 -15 1.40 8.90 0 -4 0 4449.65 164.88 0 -4 0 4549.04 165.88 -2 4 2 470.55 21.80 2 -4 -2 420.86 22.00 2 -4 -2 401.06 22.70 2 -4 -2 420.66 22.00 -4 4 4 53.59 8.60 4 -4 -4 52.89 8.70 -4 -4 4 65.19 5.80 4 -4 -4 45.70 9.20 4 -4 -4 59.09 9.30 -6 4 6 12.50 6.10 -6 -4 6 13.00 3.90 6 -4 -6 11.00 6.20 6 -4 -6 13.50 6.80 6 -4 -6 10.80 6.60 8 -4 -8 72.29 13.00 8 -4 -8 75.59 12.90 -8 -4 8 71.09 7.10 -8 -4 8 73.89 9.70 -10 -4 10 33.90 7.10 10 -4 -10 33.20 10.40 10 -4 -10 31.90 10.60 12 -4 -12 6.70 7.80 12 -4 -12 15.00 8.50 14 -4 -14 24.00 11.90 14 -4 -14 2.10 8.20 16 -4 -16 19.90 9.50 16 -4 -16 26.60 11.20 1 -5 -1 136.89 11.50 -1 -5 1 130.49 11.30 -1 -5 1 167.48 11.30 1 -5 -1 153.38 12.80 -3 5 3 20.90 5.80 3 -5 -3 26.20 7.70 -3 -5 3 27.20 5.90 3 -5 -3 20.10 6.70 3 -5 -3 28.40 7.10 -5 5 5 33.70 7.90 5 -5 -5 9.80 7.00 5 -5 -5 13.20 6.50 -5 -5 5 18.90 4.60 7 -5 -7 806.92 40.80 -7 -5 7 777.32 33.00 7 -5 -7 782.22 41.30 -9 -5 9 50.79 7.40 9 -5 -9 57.99 12.70 9 -5 -9 33.90 11.00 11 -5 -11 4.00 8.10 11 -5 -11 7.30 8.80 -11 -5 11 12.60 5.30 13 -5 -13 -9.40 6.20 13 -5 -13 12.30 10.00 15 -5 -15 32.20 10.90 15 -5 -15 47.20 13.20 0 -6 0 172.68 13.70 2 -6 -2 654.83 31.90 -2 -6 2 625.64 30.60 -2 -6 2 600.04 28.80 2 -6 -2 550.84 32.30 2 -6 -2 577.74 31.00 -4 6 4 15.40 6.10 4 -6 -4 14.70 7.10 -4 -6 4 14.30 5.30 4 -6 -4 5.30 6.50 -6 -6 6 321.27 17.60 6 -6 -6 323.67 23.40 6 -6 -6 352.66 24.70 8 -6 -8 119.19 17.30 8 -6 -8 123.39 18.70 -8 -6 8 124.09 9.90 10 -6 -10 -0.40 6.80 10 -6 -10 -6.90 6.90 -10 -6 10 11.30 4.90 12 -6 -12 -1.30 6.50 12 -6 -12 -7.30 7.30 14 -6 -14 92.89 17.90 14 -6 -14 82.39 17.40 -1 -7 1 145.29 14.30 -1 -7 1 100.59 11.30 1 -7 -1 145.79 17.00 3 -7 -3 144.59 17.70 3 -7 -3 172.58 16.30 -3 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12.50 8.60 11 -5 -15 31.90 10.80 11 -5 -15 71.09 15.50 -11 -5 15 72.09 9.70 13 -5 -17 7.50 9.90 13 -5 -17 30.20 11.60 15 -5 -19 102.49 19.20 12 -6 -8 57.69 14.10 12 -6 -8 26.70 11.30 -10 -6 6 133.29 12.70 10 -6 -6 149.19 21.30 10 -6 -6 162.38 17.80 8 -6 -4 115.69 16.60 8 -6 -4 130.09 18.90 6 -6 -2 124.79 17.30 6 -6 -2 124.29 13.70 -6 -6 2 123.59 11.60 4 -6 0 383.96 24.00 -4 -6 0 361.66 21.60 4 -6 0 356.56 22.30 -2 -6 -2 32.20 8.00 2 -6 2 35.00 8.00 2 -6 2 45.40 9.30 2 -6 2 25.20 7.40 0 -6 4 1158.38 47.70 0 -6 -4 1110.49 49.50 0 -6 4 1103.29 48.60 0 -6 -4 1062.59 51.09 -2 -6 6 64.49 8.10 2 -6 -6 41.10 9.30 -2 -6 6 41.50 7.30 -4 -6 8 280.37 14.80 4 -6 -8 287.47 21.30 4 -6 -8 271.37 20.80 -4 -6 8 292.17 15.80 -6 -6 10 369.16 17.80 6 -6 -10 354.36 25.60 6 -6 -10 404.66 27.10 -8 -6 12 32.00 4.50 -8 -6 12 25.50 6.40 8 -6 -12 18.80 8.60 8 -6 -12 37.20 11.80 -10 -6 14 110.09 9.20 10 -6 -14 106.19 18.60 10 -6 -14 116.19 18.70 12 -6 -16 367.26 30.40 12 -6 -16 329.17 28.60 14 -6 -18 37.10 12.70 14 -6 -18 -2.20 8.30 13 -7 -9 161.18 24.60 11 -7 -7 12.70 10.50 11 -7 -7 38.10 11.60 9 -7 -5 1.60 7.70 9 -7 -5 11.50 9.40 7 -7 -3 0.10 8.10 7 -7 -3 -4.10 7.30 -7 -7 3 0.40 4.90 5 -7 -1 116.69 16.90 -5 -7 1 96.59 13.40 5 -7 -1 95.19 14.50 3 -7 1 150.28 14.80 -3 -7 -1 120.29 12.60 3 -7 1 130.39 12.90 -3 -7 -1 130.59 13.90 1 -7 3 291.57 18.80 -1 -7 -3 294.67 20.20 1 -7 3 237.58 17.80 1 -7 -5 1029.80 49.50 -1 -7 5 992.00 45.50 -1 -7 5 1106.69 48.40 -3 -7 7 1181.08 52.49 3 -7 -7 1226.18 57.59 -3 -7 7 1234.28 50.69 3 -7 -7 1246.48 57.59 5 -7 -9 5.00 7.20 -5 -7 9 2.00 3.60 5 -7 -9 2.80 7.00 -5 -7 9 4.90 4.30 7 -7 -11 14.90 9.80 -7 -7 11 13.40 4.00 7 -7 -11 9.10 9.10 9 -7 -13 106.79 19.10 9 -7 -13 145.29 21.40 11 -7 -15 44.60 14.00 11 -7 -15 31.60 11.90 13 -7 -17 178.38 24.80 12 -8 -8 10.50 10.50 12 -8 -8 4.20 8.60 10 -8 -6 4.60 8.50 10 -8 -6 19.50 11.90 8 -8 -4 26.60 12.20 8 -8 -4 28.10 11.10 6 -8 -2 8.80 8.60 -6 -8 2 16.10 7.00 6 -8 -2 28.80 10.60 -4 -8 0 548.55 29.90 4 -8 0 530.95 32.90 4 -8 0 476.75 30.10 2 -8 2 17.20 8.40 -2 -8 -2 17.70 8.60 2 -8 2 21.20 7.80 0 -8 -4 185.38 18.00 0 -8 4 197.38 16.30 0 -8 4 181.68 15.50 2 -8 -6 456.15 29.70 -2 -8 6 465.15 25.50 2 -8 -6 433.36 29.40 -4 -8 8 -2.60 4.30 4 -8 -8 2.70 7.60 -4 -8 8 -3.50 4.80 4 -8 -8 0.80 6.90 -6 -8 10 8.20 5.60 6 -8 -10 4.30 8.70 -6 -8 10 13.50 4.90 6 -8 -10 18.70 11.20 8 -8 -12 19.50 9.40 8 -8 -12 21.90 10.30 -8 -8 12 17.40 5.10 10 -8 -14 116.49 21.00 10 -8 -14 103.79 18.30 9 -9 -5 51.79 15.40 -9 -9 5 94.49 13.20 9 -9 -5 59.39 14.20 -7 -9 3 11.70 6.90 7 -9 -3 0.00 7.50 7 -9 -3 9.80 9.80 -5 -9 1 63.19 11.90 5 -9 -1 54.69 14.50 5 -9 -1 48.20 13.40 3 -9 1 7.40 7.50 -3 -9 -1 10.90 7.50 3 -9 1 25.50 10.20 -1 -9 -3 4.50 6.10 1 -9 3 11.40 7.20 1 -9 3 17.30 8.30 1 -9 -5 9.30 8.00 -1 -9 5 7.60 5.50 -1 -9 5 10.80 6.30 -3 -9 7 16.20 7.30 3 -9 -7 35.30 11.30 3 -9 -7 26.30 10.20 5 -9 -9 -10.10 6.90 -5 -9 9 9.90 5.60 5 -9 -9 -3.20 7.20 7 -9 -11 -9.40 7.90 7 -9 -11 7.30 10.20 9 -9 -13 72.09 17.70 9 -9 -13 78.09 16.90 6 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2.90 4 0 -9 -3.00 3.20 4 0 -9 2.20 2.80 -4 0 9 -1.40 2.80 -4 0 9 3.00 3.60 -6 0 11 -0.30 3.00 6 0 -11 0.10 3.10 -6 0 11 4.90 3.90 6 0 -11 1.50 3.60 -6 0 11 -0.60 4.40 8 0 -13 0.20 3.30 -8 0 13 10.20 5.30 -8 0 13 3.70 3.90 8 0 -13 -4.20 3.10 10 0 -15 -8.00 4.60 10 0 -15 3.00 4.10 10 0 -15 12.20 4.70 12 0 -17 11.00 5.20 14 0 -19 -0.70 4.00 14 0 -19 6.80 7.20 17 -1 -12 4.30 9.10 15 1 -10 -1.60 5.40 15 1 -10 40.50 7.30 15 -1 -10 -2.70 6.90 13 1 -8 16.20 6.20 13 1 -8 21.90 6.40 13 -1 -8 4.40 7.50 11 1 -6 26.10 7.20 11 1 -6 51.29 8.40 11 -1 -6 43.90 9.80 11 -1 -6 33.90 9.70 -9 1 4 482.15 27.20 9 1 -4 503.55 24.20 9 1 -4 491.75 24.70 -9 -1 4 495.35 26.70 9 -1 -4 515.45 27.10 9 -1 -4 546.85 31.00 -9 -1 4 510.15 29.00 -7 1 2 2342.77 93.59 -7 1 2 2355.16 93.89 7 1 -2 2504.75 91.29 7 -1 -2 2466.45 93.89 -7 -1 2 2365.56 92.39 -7 -1 2 2481.45 93.29 7 -1 -2 2402.46 93.59 5 1 0 27.50 5.10 -5 1 0 22.30 5.20 -5 1 0 21.80 5.60 -5 -1 0 21.40 5.00 5 -1 0 16.20 4.90 5 -1 0 17.90 5.30 -1 1 -4 1783.02 61.99 -1 1 -4 1581.14 62.69 1 1 4 1671.63 63.99 1 -1 4 1861.31 63.49 -1 -1 -4 1659.13 63.79 -1 1 6 36.30 6.20 -1 1 6 31.10 5.00 1 -1 -6 34.20 5.80 -1 -1 6 22.00 2.20 -1 -1 6 22.20 2.20 1 -1 -6 30.70 4.80 3 1 -8 123.09 7.40 -3 1 8 121.29 8.90 -3 1 8 137.09 10.50 -3 -1 8 112.09 6.40 3 -1 -8 128.39 9.20 -3 -1 8 137.09 7.60 -3 -1 8 134.79 6.90 3 -1 -8 125.29 9.70 3 -1 -8 123.79 8.70 -5 1 10 197.68 13.90 -5 1 10 173.88 12.00 -5 1 10 193.48 12.70 5 1 -10 175.88 11.00 5 -1 -10 194.38 12.20 -5 -1 10 167.18 11.00 -5 -1 10 203.68 11.70 5 -1 -10 166.88 12.30 -5 -1 10 165.48 10.10 5 -1 -10 207.28 13.50 -7 1 12 198.68 14.90 -7 1 12 248.48 16.90 -7 1 12 227.68 15.10 7 -1 -12 209.98 14.80 -7 -1 12 220.48 14.50 7 -1 -12 234.28 15.60 -7 -1 12 264.17 15.10 7 -1 -12 212.38 14.30 -7 -1 12 193.78 12.80 9 -1 -14 46.10 8.70 9 -1 -14 34.20 8.70 9 -1 -14 51.19 9.90 -9 -1 14 33.20 7.00 -9 -1 14 44.40 8.60 11 -1 -16 16.60 7.20 11 -1 -16 16.20 8.10 13 -1 -18 260.87 21.60 13 -1 -18 293.77 19.30 13 -1 -18 246.88 19.80 15 -1 -20 31.40 7.60 16 -2 -11 64.19 13.50 14 -2 -9 1.80 6.90 12 2 -7 49.00 5.60 12 2 -7 66.59 5.80 12 -2 -7 66.99 12.70 10 2 -5 257.27 14.00 10 2 -5 257.37 13.60 10 -2 -5 279.07 20.10 10 -2 -5 254.77 19.20 -10 -2 5 228.98 16.40 -8 2 3 28.90 7.40 8 2 -3 23.40 4.50 -8 2 3 10.10 4.80 8 2 -3 17.50 4.30 8 -2 -3 21.60 7.20 -8 -2 3 19.30 5.80 8 -2 -3 9.00 5.10 -8 -2 3 14.20 4.90 -6 2 1 1967.00 76.39 -6 2 1 2005.00 76.19 6 2 -1 1931.71 71.99 6 -2 -1 1897.31 75.59 6 -2 -1 1846.12 76.49 -6 -2 1 1889.21 73.59 -4 2 -1 786.52 33.70 -4 2 -1 805.12 33.30 4 2 1 768.12 31.50 4 -2 1 762.82 34.00 4 -2 1 790.92 33.20 2 2 3 8.50 3.70 -2 2 -3 10.70 3.90 -2 2 -3 4.60 2.80 2 -2 3 9.40 3.20 2 -2 3 8.10 3.80 -2 -2 -3 4.60 4.00 0 2 5 57.19 7.50 0 -2 -5 48.50 5.30 0 -2 5 54.59 6.50 0 -2 5 42.40 3.30 -2 2 7 994.40 42.50 -2 2 7 988.60 41.00 2 -2 -7 1033.80 41.40 2 -2 -7 994.20 42.20 -4 2 9 106.99 10.90 -4 2 9 109.69 9.70 -4 -2 9 110.89 4.60 -4 -2 9 115.49 7.40 4 -2 -9 98.49 9.30 4 -2 -9 122.69 10.40 4 -2 -9 98.49 10.20 -4 -2 9 112.79 4.60 -6 2 11 507.25 27.50 -6 2 11 569.54 26.90 -6 -2 11 424.76 21.10 6 -2 -11 523.35 26.30 -6 -2 11 545.15 22.60 -6 -2 11 482.05 23.40 6 -2 -11 515.65 26.70 6 -2 -11 511.35 27.30 8 -2 -13 250.67 17.50 8 -2 -13 266.67 18.60 8 -2 -13 252.27 18.40 -8 -2 13 258.97 16.00 -8 -2 13 227.88 14.00 10 -2 -15 47.40 10.60 10 -2 -15 46.90 10.40 12 -2 -17 319.07 22.00 12 -2 -17 284.67 23.40 14 -2 -19 67.69 13.90 14 -2 -19 102.69 14.70 16 -2 -21 62.69 12.50 17 -3 -12 17.90 10.70 15 -3 -10 40.00 12.40 13 -3 -8 35.60 11.50 13 -3 -8 50.29 14.50 11 -3 -6 156.78 16.30 11 -3 -6 145.29 18.00 -11 -3 6 121.19 15.50 9 -3 -4 577.84 31.50 9 -3 -4 564.04 32.00 -9 -3 4 599.74 28.80 -7 3 2 1.20 4.70 -7 3 2 9.10 5.30 -7 -3 2 10.20 4.20 7 -3 -2 7.70 5.90 7 -3 -2 9.00 5.30 -5 3 0 363.76 19.40 -5 3 0 332.17 18.60 5 3 0 334.47 14.90 5 -3 0 339.17 18.80 5 -3 0 342.37 20.00 -5 -3 0 319.67 16.90 3 3 2 3339.37 127.29 -3 3 -2 3435.16 128.49 -3 3 -2 3532.65 128.79 3 -3 2 3540.85 129.89 3 -3 2 3426.76 128.49 -3 -3 -2 3610.64 128.79 1 3 4 3.40 4.20 -1 3 -4 -0.70 2.30 1 -3 4 -1.80 2.90 1 -3 4 1.10 2.50 -1 -3 -4 5.00 4.10 -1 3 6 3195.38 120.19 1 -3 -6 3202.58 120.59 1 -3 -6 3108.59 119.19 -1 -3 6 3233.68 114.59 -3 3 8 126.49 10.80 -3 3 8 150.88 12.60 3 -3 -8 123.29 10.90 3 -3 -8 127.59 11.90 3 -3 -8 116.79 10.70 -5 3 10 226.68 16.70 5 -3 -10 214.08 16.50 -5 -3 10 207.88 11.60 5 -3 -10 201.68 15.20 7 -3 -12 1.40 5.60 -7 -3 12 25.90 5.70 -7 -3 12 13.40 3.30 7 -3 -12 9.00 6.40 7 -3 -12 14.50 6.70 9 -3 -14 0.40 6.00 -9 -3 14 3.20 3.50 -9 -3 14 1.90 4.30 9 -3 -14 -0.80 5.60 11 -3 -16 11.80 8.00 -11 -3 16 18.10 5.70 11 -3 -16 9.90 8.80 13 -3 -18 163.08 24.20 13 -3 -18 155.88 21.20 15 -3 -20 17.70 9.60 15 -3 -20 1.20 8.70 16 -4 -11 49.99 14.30 14 -4 -9 72.99 16.00 14 -4 -9 35.60 11.90 12 -4 -7 37.90 11.90 12 -4 -7 73.49 14.30 10 -4 -5 283.77 22.40 -10 -4 5 228.98 16.50 10 -4 -5 234.38 19.90 8 -4 -3 581.54 31.90 8 -4 -3 631.34 34.00 -8 -4 3 574.14 27.90 -6 4 1 67.29 10.20 -6 4 1 76.99 10.50 6 -4 -1 66.39 11.60 -6 -4 1 80.19 7.90 6 -4 -1 74.79 11.70 -4 4 -1 503.25 24.30 -4 -4 -1 496.35 23.50 4 -4 1 446.36 25.00 4 -4 1 472.05 24.10 -2 4 -3 394.76 19.50 2 4 3 405.96 19.80 2 -4 3 437.56 20.50 2 -4 3 405.76 21.00 -2 -4 -3 430.26 22.00 0 4 5 379.46 20.00 0 -4 -5 363.06 20.70 0 -4 5 364.56 17.20 0 -4 -5 319.17 18.90 -2 4 7 941.01 42.80 -2 4 7 947.21 42.00 2 -4 -7 983.80 42.80 2 -4 -7 970.30 44.20 -4 4 9 427.46 24.10 4 -4 -9 448.36 26.30 4 -4 -9 463.35 25.30 4 -4 -9 433.76 24.70 -6 -4 11 244.58 10.00 -6 -4 11 236.68 13.70 6 -4 -11 235.48 18.30 6 -4 -11 253.07 18.80 8 -4 -13 167.68 19.80 8 -4 -13 134.19 15.00 -8 -4 13 152.48 11.70 -8 -4 13 144.19 9.00 10 -4 -15 114.89 17.40 -10 -4 15 94.19 8.90 10 -4 -15 72.69 14.60 12 -4 -17 95.19 16.40 12 -4 -17 90.29 15.90 -12 -4 17 103.69 10.70 14 -4 -19 234.98 22.90 14 -4 -19 189.98 20.00 15 -5 -10 23.30 13.70 13 -5 -8 52.19 14.10 13 -5 -8 40.10 12.20 11 -5 -6 32.20 11.90 11 -5 -6 20.60 10.10 9 -5 -4 598.64 35.80 9 -5 -4 581.04 33.90 7 -5 -2 1990.20 84.39 -7 -5 2 1942.61 77.99 7 -5 -2 2017.00 82.89 -5 5 0 4.10 4.90 5 -5 0 1.60 4.40 -5 -5 0 12.60 4.60 5 -5 0 2.60 6.20 -3 5 -2 523.55 25.60 -3 -5 -2 527.35 27.20 3 -5 2 547.65 26.80 3 -5 2 537.25 27.60 -1 -5 -4 6.90 5.00 1 -5 4 8.00 4.30 1 -5 4 3.10 3.80 -1 -5 -4 6.20 5.00 1 -5 -6 1666.53 73.79 1 -5 -6 1778.32 72.99 -1 -5 6 1707.63 65.99 -3 5 8 183.48 14.30 -3 -5 8 185.98 9.60 3 -5 -8 172.78 14.80 3 -5 -8 168.18 14.90 3 -5 -8 161.18 15.30 5 -5 -10 280.07 20.70 -5 -5 10 304.27 13.00 5 -5 -10 298.37 21.10 7 -5 -12 88.09 14.40 -7 -5 12 83.49 5.50 7 -5 -12 103.79 15.60 -7 -5 12 78.49 9.50 -9 -5 14 11.40 3.20 -9 -5 14 -0.80 4.10 9 -5 -14 6.90 8.10 9 -5 -14 9.80 7.60 11 -5 -16 -2.70 7.70 -11 -5 16 9.80 4.90 11 -5 -16 7.00 8.70 13 -5 -18 26.90 9.20 13 -5 -18 6.90 8.70 14 -6 -9 -1.20 8.50 12 -6 -7 163.28 22.00 12 -6 -7 150.28 22.90 10 -6 -5 16.00 8.50 10 -6 -5 8.30 9.40 -8 -6 3 405.26 23.10 8 -6 -3 406.06 29.10 8 -6 -3 473.95 28.60 6 -6 -1 9.30 7.30 6 -6 -1 17.70 7.20 -6 -6 1 10.80 5.50 -4 6 -1 273.07 18.00 4 -6 1 318.57 19.70 -4 -6 -1 273.37 18.60 4 -6 1 264.17 19.80 2 -6 3 522.15 26.00 2 -6 3 435.96 26.60 -2 -6 -3 491.35 27.60 2 -6 3 501.85 26.70 0 -6 5 80.99 10.20 0 -6 -5 60.49 10.60 0 -6 -5 79.49 13.00 0 -6 5 81.59 10.60 -2 -6 7 391.46 20.60 -2 -6 7 430.16 20.40 2 -6 -7 359.96 24.10 -4 -6 9 831.52 34.10 4 -6 -9 857.11 42.80 -4 -6 9 831.82 35.10 4 -6 -9 821.12 42.40 6 -6 -11 102.19 16.00 6 -6 -11 89.49 15.60 -6 -6 11 95.69 7.70 -8 -6 13 1.10 4.80 8 -6 -13 8.40 8.30 -8 -6 13 6.10 2.50 10 -6 -15 655.03 40.30 10 -6 -15 640.24 39.70 -10 -6 15 611.14 27.70 12 -6 -17 15.40 9.70 12 -6 -17 15.10 9.70 14 -6 -19 100.59 19.50 13 -7 -8 177.08 25.40 11 -7 -6 46.40 12.70 11 -7 -6 29.80 12.40 9 -7 -4 245.78 22.10 9 -7 -4 268.17 24.80 -7 -7 2 9.50 6.90 7 -7 -2 5.60 7.10 -5 -7 0 94.99 13.10 5 -7 0 123.99 17.20 5 -7 0 137.59 16.90 3 -7 2 -3.70 4.40 -3 -7 -2 -6.10 4.90 3 -7 2 -1.30 5.90 1 -7 4 2143.89 85.79 -1 -7 -4 2086.69 87.19 1 -7 -6 30.30 9.50 -1 -7 6 20.90 6.80 -1 -7 6 16.60 8.20 3 -7 -8 6.00 7.20 -3 -7 8 8.80 5.10 -3 -7 8 13.40 5.20 3 -7 -8 18.10 7.90 -5 -7 10 89.99 7.80 5 -7 -10 92.59 16.00 -5 -7 10 81.39 8.30 5 -7 -10 72.69 14.40 -7 -7 12 2.50 3.10 7 -7 -12 -4.80 7.30 7 -7 -12 -3.80 7.10 9 -7 -14 7.20 9.00 9 -7 -14 -10.10 6.10 11 -7 -16 56.09 13.90 11 -7 -16 76.59 16.70 12 -8 -7 109.09 19.70 10 -8 -5 12.50 9.30 10 -8 -5 3.40 8.60 8 -8 -3 28.60 11.00 8 -8 -3 16.70 9.10 -6 -8 1 14.80 7.70 6 -8 -1 17.90 8.30 6 -8 -1 17.20 10.40 4 -8 1 14.60 8.00 -4 -8 -1 5.10 6.40 4 -8 1 8.50 8.30 -2 -8 -3 194.18 17.40 2 -8 3 195.48 16.50 2 -8 3 182.68 16.70 0 -8 -5 53.59 12.40 0 -8 5 42.60 9.30 0 -8 5 42.60 9.40 -2 -8 7 346.27 21.70 2 -8 -7 391.96 28.00 2 -8 -7 363.36 26.60 -2 -8 7 415.36 25.40 4 -8 -9 67.59 14.70 -4 -8 9 79.89 9.00 -4 -8 9 75.09 12.50 6 -8 -11 316.07 26.10 6 -8 -11 271.77 24.90 -6 -8 11 293.37 18.20 -6 -8 11 279.77 16.40 8 -8 -13 18.40 10.30 8 -8 -13 1.90 9.50 -8 -8 13 30.00 5.40 10 -8 -15 -0.30 14.10 10 -8 -15 20.50 10.90 9 -9 -4 181.08 18.80 9 -9 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-4 -4 62.99 8.90 2 4 6 7.30 5.40 -2 -4 -6 12.90 5.00 2 -4 6 18.80 5.60 2 -4 6 11.20 4.00 0 4 8 10.20 5.30 0 -4 8 3.60 2.40 0 -4 -8 2.90 5.30 0 -4 8 1.60 2.90 0 -4 -8 6.10 5.00 -2 4 10 19.80 8.10 2 -4 -10 35.90 8.00 -2 -4 10 35.50 4.00 2 -4 -10 28.80 9.70 -4 4 12 753.42 39.00 -4 4 12 709.03 36.60 4 -4 -12 743.93 37.30 -4 -4 12 756.52 30.20 4 -4 -12 774.72 37.50 4 -4 -12 849.32 39.90 -6 4 14 279.47 21.30 6 -4 -14 272.67 20.20 -6 -4 14 259.67 14.10 6 -4 -14 252.27 19.30 8 -4 -16 14.40 8.60 -8 -4 16 13.60 4.70 8 -4 -16 7.80 7.50 -8 -4 16 14.10 4.00 -10 -4 18 30.70 6.10 10 -4 -18 22.60 10.10 12 -4 -20 205.18 21.50 12 -4 -20 235.88 21.80 14 -4 -22 15.40 8.80 14 -4 -22 14.30 9.20 15 -5 -7 18.80 11.60 13 -5 -5 4.40 8.50 13 -5 -5 14.60 9.80 11 -5 -3 12.70 9.20 -9 -5 1 232.58 16.30 9 -5 -1 171.98 19.00 9 -5 -1 216.58 18.50 7 -5 1 1030.40 47.00 -7 -5 -1 990.70 47.30 7 -5 1 1001.80 49.10 5 5 3 590.54 24.00 -5 -5 -3 547.65 28.20 5 -5 3 528.05 28.00 5 -5 3 518.95 29.70 -3 5 -5 20.10 5.40 3 5 5 25.30 6.20 3 -5 5 22.20 6.10 3 -5 5 27.80 7.70 -3 -5 -5 19.60 6.30 1 5 7 737.23 35.50 1 -5 7 779.72 32.30 1 -5 7 755.92 33.80 -1 -5 -7 758.32 37.40 -1 5 9 64.29 11.10 -1 -5 9 53.89 5.50 -1 -5 9 59.79 6.10 1 -5 -9 53.19 10.60 1 -5 -9 50.19 9.60 -3 5 11 383.36 24.60 3 -5 -11 359.36 23.60 -3 -5 11 397.56 16.30 5 -5 -13 270.77 20.70 5 -5 -13 275.57 21.20 -5 -5 13 307.07 14.70 -7 -5 15 67.29 3.90 7 -5 -15 59.89 13.10 7 -5 -15 85.59 14.30 -7 -5 15 73.39 7.50 9 -5 -17 13.10 9.00 9 -5 -17 13.60 9.30 -9 -5 17 21.90 6.10 -9 -5 17 23.90 4.10 11 -5 -19 121.39 19.20 11 -5 -19 112.99 18.60 13 -5 -21 39.20 11.80 13 -5 -21 52.89 12.80 14 -6 -6 65.09 15.00 12 -6 -4 16.90 10.40 12 -6 -4 15.20 10.30 10 -6 -2 61.09 14.30 10 -6 -2 47.00 13.70 8 -6 0 175.28 16.70 8 -6 0 175.38 18.60 -6 -6 -2 108.49 13.70 6 -6 2 94.39 15.20 6 -6 2 91.29 12.80 -4 6 -4 542.65 26.90 -4 -6 -4 507.65 28.90 4 -6 4 558.64 30.30 -2 -6 -6 107.29 12.20 2 -6 6 116.09 11.50 -2 -6 -6 147.99 14.70 2 -6 6 123.69 10.70 0 -6 8 80.79 7.90 0 -6 -8 88.99 13.60 0 -6 8 80.99 10.30 -2 -6 10 65.69 7.70 2 -6 -10 57.49 11.40 -4 -6 12 26.50 4.10 4 -6 -12 35.40 10.40 4 -6 -12 35.90 9.50 -6 -6 14 21.30 3.10 -6 -6 14 27.10 5.10 6 -6 -14 60.59 13.20 6 -6 -14 13.20 8.60 8 -6 -16 189.88 20.20 -8 -6 16 174.28 8.70 8 -6 -16 179.18 23.30 -8 -6 16 196.88 13.10 10 -6 -18 -1.40 7.10 10 -6 -18 10.70 8.30 12 -6 -20 208.18 23.30 12 -6 -20 275.27 25.80 13 -7 -5 166.78 25.90 13 -7 -5 193.18 21.00 11 -7 -3 5.60 8.50 11 -7 -3 -4.70 9.50 9 -7 -1 37.70 12.60 7 -7 1 1.90 5.90 -5 7 -3 5.50 5.60 5 -7 3 8.10 7.70 5 -7 3 3.40 6.30 -3 -7 -5 153.38 14.70 3 -7 5 143.39 14.40 3 -7 5 111.29 12.00 1 -7 7 65.09 10.80 -1 -7 -7 42.70 10.60 1 -7 7 67.89 9.90 1 -7 -9 -1.50 5.70 -1 -7 9 4.80 4.40 -1 -7 9 1.90 4.70 3 -7 -11 473.45 31.00 3 -7 -11 536.25 32.50 -3 -7 11 484.35 24.90 -3 -7 11 509.95 23.90 5 -7 -13 165.58 18.10 -5 -7 13 141.09 10.20 -5 -7 13 148.29 9.40 5 -7 -13 202.08 26.00 7 -7 -15 210.08 22.10 -7 -7 15 244.28 14.60 7 -7 -15 237.88 22.90 -7 -7 15 218.18 11.00 9 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2.20 1 -1 -10 8.40 4.20 1 -1 -10 2.00 4.00 -1 -1 10 8.30 3.00 3 1 -12 2001.30 76.69 -3 1 12 2189.98 82.09 -3 1 12 2123.79 80.09 3 -1 -12 2141.29 80.19 3 -1 -12 2052.99 79.29 -3 -1 12 2154.08 77.59 -3 -1 12 2040.70 76.99 3 -1 -12 1948.41 79.39 -5 1 14 2340.77 91.89 5 1 -14 2268.27 89.09 -5 1 14 2256.97 93.89 -5 -1 14 2478.95 89.09 5 -1 -14 2448.16 91.09 5 -1 -14 2377.16 91.79 5 -1 -14 2494.15 92.39 -5 -1 14 2375.06 90.39 -5 -1 14 2339.37 89.69 7 1 -16 58.69 8.20 -7 1 16 34.50 9.40 -7 1 16 70.29 9.80 -7 -1 16 57.59 8.10 -7 -1 16 50.99 8.30 7 -1 -16 63.29 9.70 -7 -1 16 59.89 9.70 7 -1 -16 81.99 10.30 7 -1 -16 55.29 9.50 9 1 -18 2496.55 93.69 -9 1 18 2532.15 99.09 -9 -1 18 2375.86 92.89 9 -1 -18 2161.58 95.29 -9 -1 18 2309.97 97.19 9 -1 -18 2309.47 95.39 11 -1 -20 194.58 18.20 11 -1 -20 182.68 15.50 11 -1 -20 191.18 15.00 13 -1 -22 35.80 10.60 13 -1 -22 46.70 8.80 13 -1 -22 29.00 7.20 16 -2 -7 47.80 12.70 14 2 -5 18.70 5.90 14 2 -5 18.20 6.60 14 -2 -5 11.80 10.30 12 2 -3 6.40 5.30 12 2 -3 8.30 5.30 12 -2 -3 10.70 7.60 10 2 -1 -5.30 4.30 10 -2 -1 -1.30 6.10 -10 -2 1 -7.00 4.80 -8 2 -1 525.55 27.80 -8 2 -1 580.44 29.10 8 2 1 512.85 25.40 8 -2 1 537.25 29.10 -8 -2 -1 521.55 27.10 -6 2 -3 1288.27 53.69 -6 2 -3 1257.77 52.59 6 2 3 1310.77 51.79 -6 -2 -3 1329.47 52.69 6 -2 3 1212.18 53.89 6 -2 3 1275.07 52.49 4 2 5 104.29 9.10 -4 2 -5 114.69 8.60 -4 2 -5 115.39 9.50 4 -2 5 109.49 10.00 4 -2 5 113.09 8.50 -4 -2 -5 120.59 9.50 -2 2 -7 624.94 27.00 2 2 7 615.84 29.00 -2 2 -7 685.93 25.90 2 -2 7 643.94 28.00 -2 -2 -7 633.84 28.70 0 2 -9 2184.78 77.49 0 2 9 2081.89 83.79 0 -2 -9 2045.10 82.59 0 -2 9 2390.86 80.09 0 -2 -9 2080.49 82.99 -2 2 11 2375.06 93.39 -2 2 11 2406.46 95.39 2 -2 -11 2530.15 94.69 -2 -2 11 2449.16 88.19 2 -2 -11 2428.06 93.29 -2 -2 11 2459.05 88.29 -4 2 13 1159.28 50.39 -4 2 13 1196.38 53.09 -4 -2 13 1207.08 44.80 -4 -2 13 1234.18 45.10 4 -2 -13 1217.28 51.59 4 -2 -13 1179.38 49.99 4 -2 -13 1201.08 50.69 -4 -2 13 1166.38 45.80 -6 2 15 403.06 23.80 -6 2 15 442.46 26.60 6 -2 -15 434.86 24.50 6 -2 -15 397.86 24.20 -6 -2 15 456.25 21.20 -6 -2 15 444.16 19.60 -6 -2 15 442.46 20.90 -8 2 17 -4.30 6.50 8 -2 -17 -3.50 4.80 -8 -2 17 -1.00 3.60 8 -2 -17 -3.10 4.50 -8 -2 17 2.80 4.20 8 -2 -17 13.30 7.10 -8 -2 17 -0.50 3.60 -10 -2 19 207.78 15.00 10 -2 -19 179.28 17.60 10 -2 -19 208.58 17.30 12 -2 -21 10.90 7.60 12 -2 -21 14.60 8.30 14 -2 -23 -6.40 6.40 14 -2 -23 5.40 7.80 17 -3 -8 165.48 21.80 15 -3 -6 44.50 12.40 13 -3 -4 34.00 11.90 11 3 -2 10.90 4.00 11 3 -2 -0.30 3.10 11 -3 -2 0.00 6.70 11 -3 -2 10.30 7.80 9 3 0 67.49 8.30 -9 -3 0 68.49 10.40 9 -3 0 65.29 10.70 9 -3 0 60.69 12.30 -7 3 -2 1.80 4.70 7 3 2 4.20 3.70 -7 3 -2 0.00 4.00 -7 -3 -2 -1.30 3.10 7 -3 2 -2.50 5.10 -5 3 -4 156.08 11.20 5 3 4 153.28 11.50 -5 3 -4 160.88 12.10 5 -3 4 155.18 11.20 5 -3 4 132.59 12.30 -5 -3 -4 152.08 11.50 3 3 6 1267.87 52.49 -3 3 -6 1274.77 49.80 -3 3 -6 1308.37 50.79 3 -3 6 1252.37 51.99 3 -3 6 1287.87 49.80 -3 -3 -6 1253.17 52.39 1 3 8 542.15 26.60 -1 3 -8 508.55 21.20 -1 -3 -8 497.95 25.80 1 -3 8 519.55 23.30 1 -3 8 541.25 21.10 -1 3 10 1534.25 66.69 1 -3 -10 1557.64 66.19 -1 -3 10 1711.33 60.09 1 -3 -10 1658.03 65.49 -3 3 12 1519.15 61.79 -3 3 12 1437.46 63.49 -3 -3 12 1554.54 54.19 3 -3 -12 1436.96 62.39 3 -3 -12 1430.46 61.09 -5 3 14 160.98 15.90 -5 3 14 197.88 15.00 -5 -3 14 189.08 8.30 -5 -3 14 195.48 10.70 5 -3 -14 175.78 15.50 5 -3 -14 182.38 14.70 5 -3 -14 204.58 15.70 -5 -3 14 187.38 8.40 -7 3 16 473.05 30.50 7 -3 -16 540.25 29.30 -7 -3 16 517.75 22.80 -7 -3 16 486.85 22.90 7 -3 -16 504.65 29.30 -7 -3 16 509.15 24.40 9 -3 -18 10.00 7.80 -9 -3 18 22.10 5.50 9 -3 -18 14.40 8.10 -9 -3 18 17.10 6.30 11 -3 -20 22.50 9.00 11 -3 -20 16.30 8.90 -11 -3 20 10.60 5.70 13 -3 -22 7.00 9.50 15 -3 -24 37.40 12.50 15 -3 -24 22.00 10.70 16 -4 -7 36.60 12.50 14 -4 -5 78.39 15.70 12 -4 -3 2.50 8.10 12 -4 -3 15.40 10.60 10 -4 -1 1130.69 53.59 10 -4 -1 1137.39 55.69 8 4 1 139.69 8.70 8 -4 1 139.89 13.60 -8 -4 -1 144.49 12.30 8 -4 1 137.89 15.30 -6 4 -3 22.60 6.00 6 4 3 24.50 5.40 -6 4 -3 27.00 7.10 6 -4 3 36.10 7.30 6 -4 3 25.40 7.90 -6 -4 -3 32.20 7.50 4 4 5 666.03 29.80 -4 4 -5 612.94 29.10 4 -4 5 612.44 28.70 4 -4 5 619.14 31.00 -4 -4 -5 655.73 30.70 2 4 7 169.98 13.30 2 -4 7 200.88 12.90 -2 -4 -7 159.88 13.40 2 -4 7 170.48 10.30 0 4 9 1860.91 77.79 0 -4 9 1915.21 70.39 0 -4 9 2022.50 72.69 0 -4 -9 1886.71 77.99 0 -4 -9 1875.91 76.89 -2 4 11 4.70 5.90 2 -4 -11 12.90 6.20 2 -4 -11 5.80 5.80 -4 4 13 59.09 10.10 -4 4 13 49.90 11.20 4 -4 -13 57.89 10.60 4 -4 -13 43.70 9.70 -4 -4 13 41.90 4.00 4 -4 -13 49.99 9.90 -6 4 15 -1.20 6.60 6 -4 -15 23.70 8.00 -6 -4 15 10.30 1.60 -6 -4 15 8.30 3.20 -6 -4 15 13.00 1.60 6 -4 -15 10.70 6.70 -8 -4 17 173.18 12.50 8 -4 -17 157.48 16.40 -8 -4 17 158.08 10.20 8 -4 -17 167.88 17.40 -8 -4 17 178.78 9.80 -10 -4 19 43.30 6.70 10 -4 -19 17.90 9.70 10 -4 -19 28.30 10.00 -10 -4 19 22.30 7.80 12 -4 -21 107.19 17.10 12 -4 -21 100.29 17.50 14 -4 -23 71.19 15.30 15 -5 -6 53.49 15.40 13 -5 -4 27.40 10.50 13 -5 -4 13.50 10.40 11 -5 -2 1.30 8.30 11 -5 -2 10.70 9.50 9 -5 0 882.51 44.00 9 -5 0 877.81 46.90 -7 -5 -2 836.52 39.80 7 -5 2 890.01 44.30 7 -5 2 872.11 41.50 -5 5 -4 37.90 7.80 5 5 4 39.00 6.30 5 -5 4 35.20 7.60 5 -5 4 35.30 9.30 3 5 6 99.89 9.90 -3 5 -6 98.39 8.80 3 -5 6 114.29 11.40 3 -5 6 107.99 9.40 1 5 8 8.20 5.70 1 -5 8 7.20 3.50 -1 -5 -8 10.20 6.40 -1 -5 -8 18.50 6.90 1 -5 8 8.20 4.80 -1 5 10 0.40 5.50 -1 -5 10 3.70 2.30 1 -5 -10 1.70 5.80 1 -5 -10 2.10 5.10 -1 -5 10 -1.40 2.60 -3 5 12 731.93 37.30 -3 -5 12 648.14 26.80 3 -5 -12 709.23 36.10 -5 5 14 151.88 19.10 5 -5 -14 150.28 15.10 5 -5 -14 107.79 15.60 -5 -5 14 126.59 8.10 -7 -5 16 267.87 10.70 -7 -5 16 255.67 14.60 7 -5 -16 278.47 22.40 7 -5 -16 275.37 22.20 -7 -5 16 259.77 11.00 -9 -5 18 264.77 13.80 9 -5 -18 323.57 25.40 9 -5 -18 324.87 25.10 11 -5 -20 104.09 18.10 11 -5 -20 74.79 15.90 13 -5 -22 144.79 21.10 13 -5 -22 125.99 23.60 14 -6 -5 24.10 10.50 12 -6 -3 62.89 14.30 12 -6 -3 61.69 15.80 10 -6 -1 60.29 14.50 10 -6 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-10 161.88 17.00 -1 -7 10 184.18 12.20 -1 -7 10 187.68 13.60 3 -7 -12 144.09 19.30 -3 -7 12 131.69 10.00 3 -7 -12 125.09 17.70 5 -7 -14 -2.90 7.90 -5 -7 14 10.00 3.20 -5 -7 14 9.50 3.40 -5 -7 14 7.80 3.00 5 -7 -14 16.60 9.60 -7 -7 16 38.00 6.00 7 -7 -16 25.00 11.00 7 -7 -16 25.70 11.10 -7 -7 16 26.50 3.60 -7 -7 16 27.80 3.60 9 -7 -18 8.30 9.50 9 -7 -18 25.60 10.90 11 -7 -20 155.78 23.20 11 -7 -20 116.69 20.10 12 -8 -3 4.30 7.40 12 -8 -3 20.40 12.10 10 -8 -1 28.10 12.30 10 -8 -1 18.50 10.50 8 -8 1 55.09 11.80 8 -8 1 25.90 11.90 6 -8 3 39.70 10.00 -6 -8 -3 46.20 11.30 6 -8 3 48.40 14.20 -4 -8 -5 1162.98 55.69 4 -8 5 1170.38 52.99 4 -8 5 1184.88 57.19 2 -8 7 200.18 15.60 -2 -8 -7 239.68 20.00 2 -8 7 214.58 18.40 0 -8 9 135.79 11.80 0 -8 9 146.79 13.90 0 -8 -9 140.19 19.60 -2 -8 11 50.19 7.60 -2 -8 11 55.69 9.70 2 -8 -11 35.70 11.00 4 -8 -13 42.90 12.60 -4 -8 13 53.59 9.10 -4 -8 13 48.30 7.70 4 -8 -13 65.59 14.20 6 -8 -15 104.49 18.50 -6 -8 15 87.59 7.50 6 -8 -15 90.39 17.30 8 -8 -17 -1.40 8.70 8 -8 -17 -2.30 8.90 10 -8 -19 -2.40 8.10 10 -8 -19 -5.30 7.50 9 -9 0 13.70 10.40 9 -9 0 8.80 8.90 7 -9 2 102.79 18.10 -7 -9 -2 64.59 14.90 7 -9 2 55.39 12.50 5 -9 4 17.60 10.40 -5 -9 -4 19.00 9.10 5 -9 4 11.70 7.60 3 -9 6 2.80 6.30 -3 -9 -6 9.50 7.60 3 -9 6 4.30 7.90 1 -9 8 7.90 7.10 1 -9 8 3.00 6.20 -1 -9 -8 18.00 9.30 1 -9 -10 72.59 15.50 -1 -9 10 72.49 12.30 3 -9 -12 58.69 13.90 -3 -9 12 61.39 8.50 -3 -9 12 59.59 9.50 3 -9 -12 72.29 15.60 -5 -9 14 2.10 4.90 5 -9 -14 12.40 8.90 -5 -9 14 10.00 5.30 5 -9 -14 7.50 8.80 7 -9 -16 7.50 9.20 -6 -10 -3 287.07 24.00 6 -10 3 315.77 26.90 6 -10 3 292.57 23.70 -4 -10 -5 0.00 7.30 4 -10 5 8.10 6.90 4 -10 5 -0.70 6.60 2 -10 7 143.99 19.90 -2 -10 -7 167.08 18.60 2 -10 7 147.09 14.90 0 -10 9 -6.30 5.10 0 -10 -9 4.30 7.30 2 -10 -11 101.19 17.50 2 -10 -11 79.39 17.00 -2 -10 11 71.29 14.70 -2 -10 11 107.79 14.20 4 -10 -13 38.30 15.70 4 -10 -13 64.99 15.00 18 0 -8 -7.90 10.40 16 0 -6 168.98 16.50 14 0 -4 326.97 22.50 12 0 -2 5.80 6.20 10 0 0 1571.44 65.79 -8 0 -2 27.20 6.90 -8 0 -2 16.20 5.60 8 0 2 8.00 5.30 6 0 4 1004.00 43.20 -6 0 -4 1027.20 43.70 -4 0 -6 746.33 32.60 4 0 6 755.32 32.60 -2 0 -8 1822.52 65.99 2 0 8 1620.04 65.79 0 0 10 76.19 7.10 0 0 -10 73.79 6.50 -2 0 12 928.11 38.00 2 0 -12 951.00 37.10 2 0 -12 917.41 36.90 -2 0 12 923.61 38.60 4 0 -14 163.88 10.20 -4 0 14 204.38 11.80 4 0 -14 166.68 11.40 -4 0 14 166.98 12.50 4 0 -14 192.48 10.90 6 0 -16 58.99 8.30 -6 0 16 60.19 10.00 6 0 -16 46.20 6.40 6 0 -16 59.39 8.10 -6 0 16 57.09 8.40 8 0 -18 46.10 8.60 -8 0 18 44.60 8.80 8 0 -18 51.89 6.80 -8 0 18 52.29 11.00 -8 0 18 42.90 8.90 8 0 -18 52.69 6.90 -10 0 20 249.68 19.80 10 0 -20 246.08 18.50 10 0 -20 244.48 13.70 12 0 -22 114.19 15.90 17 1 -7 84.19 11.10 17 -1 -7 64.79 14.00 15 1 -5 28.00 8.70 15 1 -5 36.50 11.10 15 -1 -5 24.30 9.90 13 1 -3 77.09 12.00 13 1 -3 62.59 10.60 13 -1 -3 61.79 12.60 11 1 -1 2.20 5.90 11 -1 -1 -3.50 5.10 9 1 1 426.66 23.20 9 -1 1 445.86 25.30 -9 -1 -1 438.76 24.60 -7 1 -3 828.92 36.20 -7 1 -3 770.02 36.50 7 1 3 792.12 35.30 7 -1 3 763.72 36.50 -7 -1 -3 770.32 35.80 5 1 5 414.46 21.70 -5 1 -5 448.56 21.40 -5 1 -5 480.75 23.20 -5 -1 -5 447.66 22.20 5 -1 5 429.06 22.70 -3 1 -7 1427.46 56.89 3 1 7 1438.46 57.39 3 -1 7 1491.95 57.49 -3 -1 -7 1462.05 57.29 -1 1 -9 426.66 18.70 1 1 9 396.96 20.00 -1 -1 -9 408.86 19.90 1 -1 9 421.96 19.20 1 1 -11 372.66 15.60 1 1 -11 351.96 15.50 -1 1 11 371.46 19.70 1 -1 -11 387.06 18.60 1 -1 -11 391.36 19.00 -1 -1 11 378.26 16.90 -3 1 13 39.00 7.00 -3 1 13 48.90 8.60 3 1 -13 50.29 4.90 3 -1 -13 52.79 7.80 3 -1 -13 52.29 7.40 3 -1 -13 39.30 6.80 -3 -1 13 50.79 5.90 -3 -1 13 44.30 5.90 -5 1 15 885.71 44.20 5 1 -15 894.31 39.40 -5 1 15 1061.99 43.00 -5 -1 15 978.70 41.30 5 -1 -15 1007.60 42.80 -5 -1 15 963.20 39.70 5 -1 -15 987.50 41.60 5 -1 -15 986.00 42.20 -5 -1 15 1020.80 40.50 -7 1 17 367.56 20.60 -7 1 17 297.67 21.40 7 1 -17 302.57 17.40 7 -1 -17 266.37 18.70 7 -1 -17 280.47 18.00 7 -1 -17 313.07 18.20 -7 -1 17 285.07 17.60 -7 -1 17 287.37 16.80 -7 -1 17 325.07 19.40 -9 1 19 1084.09 52.39 9 1 -19 1092.89 47.60 9 -1 -19 1126.59 50.69 -9 -1 19 1069.09 53.69 9 -1 -19 1098.19 48.00 -9 -1 19 1020.00 47.10 11 -1 -21 331.57 21.00 11 -1 -21 344.27 24.20 11 -1 -21 376.96 21.50 13 -1 -23 149.29 19.80 13 -1 -23 145.89 13.80 16 2 -6 113.09 10.20 16 -2 -6 113.09 17.20 14 2 -4 9.80 6.90 14 2 -4 5.50 5.30 12 2 -2 7.60 5.90 12 2 -2 12.90 6.40 12 -2 -2 5.30 7.30 10 2 0 280.27 17.50 10 -2 0 303.47 21.40 8 2 2 831.72 36.90 -8 2 -2 837.22 39.80 -8 2 -2 807.22 38.60 -8 -2 -2 856.91 41.70 8 -2 2 831.32 39.90 -6 2 -4 9795.52 354.06 -6 2 -4 9735.53 355.16 6 2 4 9999.00 353.46 -6 -2 -4 9959.40 354.16 6 -2 4 9515.15 355.66 4 2 6 2524.85 94.99 -4 2 -6 2490.65 94.89 -4 2 -6 2486.75 93.49 -4 -2 -6 2528.95 95.09 4 -2 6 2440.56 95.49 2 2 8 953.70 41.40 -2 2 -8 1010.90 40.60 -2 2 -8 977.50 37.50 -2 -2 -8 980.10 41.10 2 -2 8 951.20 39.90 0 2 -10 477.45 17.90 0 2 -10 484.85 19.80 0 2 10 469.45 23.80 0 -2 -10 440.06 22.80 0 -2 10 444.86 20.00 0 -2 -10 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492.55 32.20 -11 -3 21 449.86 25.10 13 -3 -23 -2.90 8.60 13 -3 -23 7.60 8.60 15 -3 -25 68.99 14.90 15 -3 -25 44.70 12.60 16 -4 -6 3.40 8.80 14 -4 -4 44.60 12.90 12 -4 -2 1188.08 63.29 12 -4 -2 1178.78 59.39 10 -4 0 685.93 36.70 10 -4 0 666.43 38.60 8 4 2 17.50 4.50 -8 -4 -2 17.70 6.10 8 -4 2 13.00 8.20 8 -4 2 15.00 6.80 6 4 4 121.09 10.50 -6 4 -4 163.58 12.90 -6 4 -4 129.59 11.60 6 -4 4 119.99 15.10 6 -4 4 145.49 12.20 -6 -4 -4 108.49 10.70 4 4 6 44.40 7.90 -4 4 -6 48.50 7.40 -4 4 -6 47.00 7.00 -4 -4 -6 33.10 7.60 4 -4 6 37.60 6.50 4 -4 6 31.80 7.70 2 4 8 148.79 12.60 -2 4 -8 138.29 8.90 2 -4 8 148.39 9.20 -2 -4 -8 131.69 12.00 2 -4 8 135.99 11.00 0 4 10 952.70 45.20 0 -4 -10 1070.19 46.40 0 -4 10 958.60 39.70 0 -4 10 1013.70 37.90 0 -4 -10 952.10 44.40 -2 4 12 1422.26 62.69 -2 -4 12 1454.95 53.09 2 -4 -12 1344.27 61.49 2 -4 -12 1468.05 61.09 -4 4 14 177.68 16.90 -4 -4 14 181.58 8.70 4 -4 -14 170.78 15.40 4 -4 -14 165.98 14.90 -6 4 16 87.09 15.60 -6 -4 16 58.89 6.00 6 -4 -16 78.39 12.80 6 -4 -16 90.49 13.80 -6 -4 16 62.39 3.70 -6 -4 16 57.69 3.80 -8 -4 18 13.80 3.50 -8 -4 18 12.60 3.90 8 -4 -18 -1.10 7.60 8 -4 -18 -0.10 6.30 -8 -4 18 10.20 4.70 10 -4 -20 184.08 19.10 -10 -4 20 177.68 13.90 -10 -4 20 157.78 11.60 10 -4 -20 176.68 19.30 12 -4 -22 66.19 13.90 12 -4 -22 100.49 17.90 14 -4 -24 157.68 21.00 14 -4 -24 86.59 19.70 15 -5 -5 69.09 15.40 13 -5 -3 1.10 8.00 13 -5 -3 -5.10 6.80 11 -5 -1 15.60 9.10 11 -5 -1 12.70 9.20 9 -5 1 21.70 8.40 9 -5 1 28.80 11.20 7 5 3 539.25 23.30 7 -5 3 568.64 29.90 7 -5 3 583.54 33.00 -7 -5 -3 522.05 28.40 -5 5 -5 16.70 5.90 5 5 5 14.90 5.40 5 -5 5 23.30 6.40 -5 -5 -5 29.00 7.70 5 -5 5 23.20 8.10 3 5 7 27.50 7.00 -3 5 -7 22.80 5.10 -3 -5 -7 25.20 6.80 3 -5 7 18.10 6.70 3 -5 7 20.90 5.10 1 5 9 9.00 5.60 -1 -5 -9 0.00 5.10 1 -5 9 4.00 2.90 -1 -5 -9 -0.10 4.90 1 -5 9 2.20 3.80 -1 5 11 119.69 15.50 1 -5 -11 98.69 13.70 -1 -5 11 113.69 8.40 -1 -5 11 126.59 7.00 -3 5 13 294.27 22.30 -3 -5 13 315.17 12.90 -3 -5 13 295.77 13.30 3 -5 -13 293.47 21.10 -5 5 15 15.50 8.90 5 -5 -15 11.90 8.20 -5 -5 15 14.80 3.30 5 -5 -15 12.40 7.60 7 -5 -17 1436.06 67.89 7 -5 -17 1437.96 67.59 -7 -5 17 1516.55 53.79 -7 -5 17 1436.66 54.09 -7 -5 17 1552.54 58.29 9 -5 -19 0.50 6.50 -9 -5 19 5.20 2.50 9 -5 -19 8.10 8.70 -9 -5 19 5.10 5.00 11 -5 -21 204.38 21.70 11 -5 -21 170.28 22.90 13 -5 -23 114.49 18.80 14 -6 -4 46.50 17.70 14 -6 -4 76.89 15.60 12 -6 -2 176.18 19.40 12 -6 -2 189.68 25.90 10 -6 0 223.38 19.60 10 -6 0 178.78 24.10 8 -6 2 165.68 16.30 8 -6 2 166.28 18.60 -6 6 -4 49.99 10.40 6 -6 4 34.00 11.10 6 -6 4 45.30 9.10 -4 6 -6 74.69 9.40 4 6 6 45.00 8.00 4 -6 6 45.90 10.50 4 -6 6 68.79 10.00 2 6 8 43.60 9.90 -2 -6 -8 75.69 12.10 2 -6 8 53.59 9.40 2 -6 8 41.00 7.10 0 6 10 4.90 5.60 0 -6 10 1.20 3.10 0 -6 10 6.30 4.70 0 -6 -10 8.30 6.90 -2 6 12 45.10 11.00 -2 -6 12 39.40 6.00 2 -6 -12 47.50 10.90 -2 -6 12 49.80 5.50 4 -6 -14 318.57 24.00 -4 -6 14 335.47 15.00 4 -6 -14 329.47 24.40 -4 -6 14 334.07 14.90 -6 -6 16 1.60 1.10 6 -6 -16 3.60 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21.50 9.70 -6 -4 -32 43.10 12.90 4 4 34 18.10 11.60 -4 -4 -34 -3.80 8.00 4 -4 34 5.10 9.50 2 4 36 -3.10 9.60 2 -4 36 20.60 8.20 0 4 38 15.50 13.90 0 -4 38 27.60 10.60 0 -4 -38 28.00 13.30 7 5 31 231.58 31.30 7 -5 31 254.67 25.30 5 5 33 12.40 11.70 5 -5 33 17.20 12.50 -5 -5 -33 26.60 11.90 3 5 35 137.79 25.50 3 -5 35 157.78 22.70 -3 -5 -35 159.58 23.50 12 0 27 14.10 11.10 10 0 29 3.90 8.20 8 0 31 12.30 11.80 6 0 33 9.20 9.70 -4 0 -35 11.60 10.20 4 0 35 10.70 11.20 -2 0 -37 14.40 9.60 2 0 37 15.20 10.00 0 0 39 1.30 8.90 0 0 -39 17.30 8.20 2 0 -41 -10.50 8.70 11 1 28 133.39 22.60 11 -1 28 160.38 25.20 9 1 30 92.49 18.80 9 -1 30 115.09 21.70 7 1 32 43.70 15.40 7 -1 32 39.70 13.70 5 1 34 51.99 15.50 -5 1 -34 55.89 12.80 5 -1 34 33.60 12.10 -5 -1 -34 52.69 13.70 3 1 36 119.39 22.00 -3 1 -36 160.48 16.00 3 -1 36 147.59 22.00 -3 -1 -36 131.59 20.40 -1 1 -38 121.19 13.60 1 1 38 126.19 22.90 -1 -1 -38 151.88 20.20 1 -1 38 115.89 21.00 -1 -1 40 25.60 10.80 1 -1 -40 20.80 8.00 10 2 29 11.70 10.20 10 -2 29 16.80 10.50 8 2 31 110.49 21.40 6 2 33 30.00 15.90 6 -2 33 49.99 14.10 -4 2 -35 28.90 9.70 4 2 35 42.80 14.50 4 -2 35 43.00 15.10 -4 -2 -35 49.20 12.70 -2 2 -37 9.30 7.10 2 -2 37 10.90 7.90 -2 -2 -37 9.90 8.30 0 2 39 27.60 14.70 0 -2 -39 3.90 8.90 0 -2 39 -6.60 6.90 -2 2 41 71.89 19.40 2 -2 -41 65.59 13.30 2 -2 -41 46.80 14.00 -2 -2 41 77.99 15.80 9 3 30 6.90 11.10 9 -3 30 24.30 12.30 7 3 32 18.70 11.50 5 3 34 54.09 16.30 -5 3 -34 73.79 13.40 5 -3 34 87.49 17.60 -5 -3 -34 55.49 14.80 3 3 36 97.09 20.00 -3 -3 -36 84.29 16.90 3 -3 36 73.69 17.60 1 3 38 259.87 28.20 1 -3 38 252.87 24.10 -1 3 40 28.00 14.30 1 -3 -40 18.40 10.20 -1 -3 40 -0.20 7.70 8 4 31 108.99 22.40 8 -4 31 109.79 20.60 6 4 33 144.69 24.60 -6 4 -33 172.08 17.00 -6 -4 -33 160.48 23.80 4 4 35 97.99 21.30 4 -4 35 130.69 20.80 -4 -4 -35 125.69 21.20 2 4 37 91.49 20.50 2 -4 37 73.09 16.70 -2 -4 -37 89.79 17.60 10 0 30 252.97 27.10 8 0 32 6.30 10.20 6 0 34 29.90 13.00 -4 0 -36 100.39 16.30 4 0 36 60.69 17.80 -2 0 -38 17.10 9.30 2 0 38 2.20 9.10 0 0 -40 48.80 11.10 0 0 -40 9.80 9.90 11 1 29 50.39 14.60 9 1 31 28.70 12.40 9 -1 31 16.80 10.60 7 1 33 263.27 27.50 -5 1 -35 7.20 9.70 5 -1 35 -10.10 7.30 -5 -1 -35 -0.80 8.30 3 1 37 27.00 14.20 3 -1 37 32.20 11.70 -3 -1 -37 48.70 12.20 -1 1 -39 62.49 11.80 -1 -1 -39 54.69 12.20 1 -1 39 111.19 20.20 -1 1 41 427.46 35.90 1 -1 -41 395.46 28.30 -1 -1 41 315.27 34.90 1 -1 -41 357.56 26.20 10 2 30 50.09 15.60 10 -2 30 52.89 14.80 8 2 32 19.30 12.50 8 -2 32 12.40 9.50 6 2 34 53.39 17.90 -6 -2 -34 45.70 14.10 4 2 36 372.16 33.80 -4 -2 -36 356.66 29.50 4 -2 36 330.57 29.40 2 2 38 -6.40 9.00 -2 2 -38 29.80 7.40 2 -2 38 22.80 9.90 -2 -2 -38 29.60 9.70 0 2 40 11.80 12.80 0 -2 -40 12.80 9.40 0 -2 40 9.00 8.50 9 3 31 35.70 13.50 9 -3 31 13.60 9.90 7 3 33 72.09 18.60 5 3 35 1.80 9.80 -5 3 -35 10.70 9.20 5 -3 35 23.20 10.90 -5 -3 -35 25.30 12.20 3 3 37 74.79 19.20 -3 -3 -37 62.29 16.70 3 -3 37 76.59 15.90 1 3 39 95.29 20.70 1 -3 39 99.29 18.60 -1 -3 -39 75.09 16.30 6 4 34 65.89 17.70 -6 -4 -34 53.39 14.70 6 -4 34 54.49 16.00 4 4 36 3.90 10.40 -4 -4 -36 26.10 10.10 8 0 33 12.30 10.80 -6 0 -35 6.50 8.40 6 0 35 15.80 10.70 -4 0 -37 -13.20 8.20 4 0 37 5.60 10.90 2 0 39 -2.50 10.20 -2 0 -39 -8.80 8.30 0 0 41 13.00 9.90 0 0 -41 -2.60 9.10 0 0 -41 -16.20 9.30 9 1 32 6.00 11.60 9 -1 32 17.00 9.70 7 1 34 8.00 10.10 7 -1 34 -3.50 9.10 5 1 36 14.80 11.10 -5 1 -36 7.20 9.10 -5 -1 -36 10.30 8.70 3 1 38 174.78 26.50 -3 -1 -38 112.99 18.40 1 1 40 -7.60 8.30 -1 1 -40 -3.60 8.80 -1 -1 -40 0.00 9.10 8 2 33 18.10 14.10 8 -2 33 53.99 13.90 6 2 35 68.89 18.40 -6 2 -35 98.29 16.30 6 -2 35 75.79 17.80 4 2 37 280.07 29.70 -4 2 -37 271.57 21.80 -4 -2 -37 314.67 26.40 2 2 39 -0.40 10.30 -2 -2 -39 10.10 9.90 7 3 34 58.59 18.00 -7 -3 -34 61.59 16.40 7 -3 34 64.89 16.70 5 3 36 26.10 16.30 -5 3 -36 15.40 9.80 -5 -3 -36 21.30 11.80 5 -3 36 9.40 8.20 3 3 38 12.00 13.90 -3 -3 -38 7.70 10.20 8 0 34 13.60 11.00 -6 0 -36 35.50 11.50 6 0 36 3.40 10.00 -4 0 -38 34.60 11.50 4 0 38 0.50 8.50 2 0 40 28.90 14.50 -2 0 -40 50.59 12.70 7 1 35 35.40 13.90 7 -1 35 31.70 13.60 5 1 37 5.80 10.70 -5 1 -37 -1.10 9.30 -5 -1 -37 16.00 10.20 5 -1 37 4.40 9.00 -3 1 -39 22.90 10.00 3 1 39 68.09 17.30 -3 -1 -39 7.30 8.60 3 -1 39 23.80 13.80 -6 2 -36 43.60 14.10 6 2 36 26.50 15.40 -6 -2 -36 24.20 10.20 6 -2 36 8.90 9.60 4 2 38 40.10 15.50 4 -2 38 47.60 15.90 6 0 37 12.60 10.60 -6 0 -37 21.10 10.20 4 0 39 12.60 10.10 -4 0 -39 20.40 9.70 5 -1 38 2.50 9.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 14438 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.35202(9) 0.04278(14) 0.47836(4) 0.0214(2) Uani 1 1 d . . . . . O2 O 0.22267(9) 0.73353(13) 0.28496(3) 0.0185(2) Uani 1 1 d . . . . . O3 O 0.14505(9) 0.97970(13) 0.33281(3) 0.0180(2) Uani 1 1 d . . . . . O4 O 0.11166(9) 0.92960(13) 0.41965(3) 0.0186(2) Uani 1 1 d . . . . . N1 N 0.41857(10) -0.02598(15) 0.41136(4) 0.0164(2) Uani 1 1 d . . . . . N2 N 0.36524(10) 0.20249(15) 0.36602(4) 0.0156(2) Uani 1 1 d . . . . . C1 C 0.23687(11) 0.51371(18) 0.39727(5) 0.0141(3) Uani 1 1 d . . . . . C2 C 0.25098(11) 0.54141(18) 0.35129(5) 0.0148(3) Uani 1 1 d . . . . . H2 H 0.2837 0.4558 0.3350 0.018 Uiso 1 1 calc R U . . . C3 C 0.21660(11) 0.69512(18) 0.32987(4) 0.0139(3) Uani 1 1 d . . . . . C4 C 0.17130(11) 0.82467(18) 0.35390(5) 0.0143(3) Uani 1 1 d . . . . . C5 C 0.15675(11) 0.79584(18) 0.39952(5) 0.0147(3) Uani 1 1 d . . . . . C6 C 0.18760(11) 0.64024(18) 0.42089(4) 0.0147(3) Uani 1 1 d . . . . . H6 H 0.1753 0.6195 0.4515 0.018 Uiso 1 1 calc R U . . . C7 C 0.27309(12) 0.35744(18) 0.42238(5) 0.0155(3) Uani 1 1 d . . . . . H7 H 0.2546 0.3476 0.4524 0.019 Uiso 1 1 calc R U . . . C8 C 0.32927(11) 0.22519(18) 0.40873(5) 0.0151(3) Uani 1 1 d . . . . . C9 C 0.36436(11) 0.07515(19) 0.43876(5) 0.0159(3) Uani 1 1 d . . . . . C10 C 0.41519(11) 0.05607(18) 0.36907(5) 0.0151(3) Uani 1 1 d . . . . . C11 C 0.46338(12) -0.02340(19) 0.33125(5) 0.0195(3) Uani 1 1 d . . . . . H11A H 0.4597 0.0580 0.3055 0.029 Uiso 1 1 calc R U . . . H11B H 0.4245 -0.1288 0.3209 0.029 Uiso 1 1 calc R U . . . H11C H 0.5377 -0.0519 0.3423 0.029 Uiso 1 1 calc R U . . . C12 C 0.47035(13) -0.18811(19) 0.42624(5) 0.0209(3) Uani 1 1 d . . . . . H12A H 0.5054 -0.1771 0.4581 0.031 Uiso 1 1 calc R U . . . H12B H 0.5233 -0.2161 0.4064 0.031 Uiso 1 1 calc R U . . . H12C H 0.4172 -0.2802 0.4242 0.031 Uiso 1 1 calc R U . . . C13 C 0.25646(13) 0.5990(2) 0.25730(5) 0.0216(3) Uani 1 1 d . . . . . H13A H 0.3305 0.5695 0.2687 0.032 Uiso 1 1 calc R U . . . H13B H 0.2503 0.6380 0.2253 0.032 Uiso 1 1 calc R U . . . H13C H 0.2117 0.4971 0.2590 0.032 Uiso 1 1 calc R U . . . C14 C 0.03479(13) 0.9957(2) 0.31621(6) 0.0251(3) Uani 1 1 d . . . . . H14A H 0.0123 0.9012 0.2948 0.038 Uiso 1 1 calc R U . . . H14B H 0.0214 1.1063 0.3002 0.038 Uiso 1 1 calc R U . . . H14C H -0.0053 0.9908 0.3421 0.038 Uiso 1 1 calc R U . . . C15 C 0.09917(13) 0.9075(2) 0.46675(5) 0.0211(3) Uani 1 1 d . . . . . H15A H 0.0492 0.8133 0.4694 0.032 Uiso 1 1 calc R U . . . H15B H 0.0717 1.0143 0.4783 0.032 Uiso 1 1 calc R U . . . H15C H 0.1680 0.8798 0.4849 0.032 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0250(6) 0.0231(5) 0.0164(5) 0.0046(4) 0.0043(4) 0.0026(4) O2 0.0286(6) 0.0163(5) 0.0122(4) 0.0004(4) 0.0084(4) 0.0025(4) O3 0.0217(6) 0.0139(5) 0.0192(5) 0.0032(4) 0.0056(4) 0.0008(4) O4 0.0249(6) 0.0184(5) 0.0136(4) -0.0009(4) 0.0066(4) 0.0055(4) N1 0.0165(6) 0.0149(6) 0.0177(6) 0.0010(4) 0.0020(5) 0.0010(5) N2 0.0154(6) 0.0161(5) 0.0156(5) 0.0004(4) 0.0034(4) -0.0003(5) C1 0.0116(6) 0.0168(6) 0.0136(6) 0.0003(5) 0.0008(5) -0.0004(5) C2 0.0140(7) 0.0162(6) 0.0147(6) -0.0010(5) 0.0033(5) 0.0017(5) C3 0.0136(6) 0.0162(6) 0.0127(6) -0.0001(5) 0.0044(5) -0.0020(5) C4 0.0137(6) 0.0139(6) 0.0156(6) 0.0016(5) 0.0034(5) -0.0002(5) C5 0.0135(6) 0.0161(6) 0.0150(6) -0.0020(5) 0.0038(5) -0.0009(5) C6 0.0143(7) 0.0188(7) 0.0111(6) 0.0005(5) 0.0023(5) 0.0008(5) C7 0.0156(7) 0.0184(7) 0.0123(6) 0.0012(5) 0.0013(5) -0.0007(5) C8 0.0144(7) 0.0162(6) 0.0143(6) 0.0014(5) 0.0008(5) -0.0007(5) C9 0.0144(7) 0.0171(6) 0.0160(6) 0.0009(5) 0.0015(5) -0.0008(5) C10 0.0128(6) 0.0169(6) 0.0152(6) 0.0002(5) 0.0013(5) -0.0035(5) C11 0.0194(7) 0.0197(7) 0.0202(7) -0.0027(5) 0.0055(6) 0.0010(6) C12 0.0224(8) 0.0151(7) 0.0249(7) 0.0042(5) 0.0027(6) 0.0038(6) C13 0.0263(8) 0.0249(7) 0.0140(6) -0.0026(5) 0.0045(6) 0.0075(6) C14 0.0247(8) 0.0236(8) 0.0262(8) 0.0081(6) 0.0016(6) 0.0039(7) C15 0.0256(8) 0.0237(7) 0.0156(6) -0.0011(5) 0.0085(6) 0.0056(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C3 O2 C13 117.13(11) . . ? C4 O3 C14 113.18(11) . . ? C5 O4 C15 116.44(11) . . ? C9 N1 C10 108.07(12) . . ? C9 N1 C12 123.95(12) . . ? C10 N1 C12 127.97(12) . . ? C10 N2 C8 105.60(11) . . ? C6 C1 C2 119.98(13) . . ? C6 C1 C7 117.51(12) . . ? C2 C1 C7 122.50(12) . . ? C3 C2 C1 119.34(12) . . ? C3 C2 H2 120.3 . . ? C1 C2 H2 120.3 . . ? O2 C3 C2 124.45(12) . . ? O2 C3 C4 114.69(12) . . ? C2 C3 C4 120.86(12) . . ? O3 C4 C5 121.02(12) . . ? O3 C4 C3 119.45(12) . . ? C5 C4 C3 119.49(12) . . ? O4 C5 C6 125.00(12) . . ? O4 C5 C4 114.81(12) . . ? C6 C5 C4 120.20(12) . . ? C5 C6 C1 120.05(12) . . ? C5 C6 H6 120.0 . . ? C1 C6 H6 120.0 . . ? C8 C7 C1 128.67(12) . . ? C8 C7 H7 115.7 . . ? C1 C7 H7 115.7 . . ? C7 C8 N2 128.22(13) . . ? C7 C8 C9 123.02(12) . . ? N2 C8 C9 108.76(12) . . ? O1 C9 N1 125.81(13) . . ? O1 C9 C8 130.89(13) . . ? N1 C9 C8 103.30(11) . . ? N2 C10 N1 114.27(12) . . ? N2 C10 C11 124.44(13) . . ? N1 C10 C11 121.27(13) . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N1 C12 H12A 109.5 . . ? N1 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? N1 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? O2 C13 H13A 109.5 . . ? O2 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? O2 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? O3 C14 H14A 109.5 . . ? O3 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? O3 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? O4 C15 H15A 109.5 . . ? O4 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? O4 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C9 1.2239(16) . ? O2 C3 1.3669(15) . ? O2 C13 1.4280(17) . ? O3 C4 1.3709(16) . ? O3 C14 1.422(2) . ? O4 C5 1.3630(16) . ? O4 C15 1.4274(16) . ? N1 C9 1.3810(18) . ? N1 C10 1.3912(17) . ? N1 C12 1.4563(19) . ? N2 C10 1.2982(18) . ? N2 C8 1.4104(17) . ? C1 C6 1.4033(19) . ? C1 C2 1.4065(18) . ? C1 C7 1.4575(19) . ? C2 C3 1.3879(19) . ? C2 H2 0.9500 . ? C3 C4 1.4011(19) . ? C4 C5 1.3990(18) . ? C5 C6 1.3896(19) . ? C6 H6 0.9500 . ? C7 C8 1.346(2) . ? C7 H7 0.9500 . ? C8 C9 1.4882(19) . ? C10 C11 1.4822(19) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C6 C1 C2 C3 0.6(2) . . . . ? C7 C1 C2 C3 -178.53(13) . . . . ? C13 O2 C3 C2 6.8(2) . . . . ? C13 O2 C3 C4 -172.82(13) . . . . ? C1 C2 C3 O2 -177.55(13) . . . . ? C1 C2 C3 C4 2.1(2) . . . . ? C14 O3 C4 C5 -80.83(17) . . . . ? C14 O3 C4 C3 101.28(15) . . . . ? O2 C3 C4 O3 -4.97(19) . . . . ? C2 C3 C4 O3 175.39(13) . . . . ? O2 C3 C4 C5 177.11(13) . . . . ? C2 C3 C4 C5 -2.5(2) . . . . ? C15 O4 C5 C6 2.2(2) . . . . ? C15 O4 C5 C4 -177.74(13) . . . . ? O3 C4 C5 O4 2.4(2) . . . . ? C3 C4 C5 O4 -179.71(13) . . . . ? O3 C4 C5 C6 -177.52(13) . . . . ? C3 C4 C5 C6 0.4(2) . . . . ? O4 C5 C6 C1 -177.69(13) . . . . ? C4 C5 C6 C1 2.2(2) . . . . ? C2 C1 C6 C5 -2.7(2) . . . . ? C7 C1 C6 C5 176.44(13) . . . . ? C6 C1 C7 C8 -174.24(15) . . . . ? C2 C1 C7 C8 4.9(2) . . . . ? C1 C7 C8 N2 -1.7(3) . . . . ? C1 C7 C8 C9 177.82(14) . . . . ? C10 N2 C8 C7 -179.81(15) . . . . ? C10 N2 C8 C9 0.62(16) . . . . ? C10 N1 C9 O1 -179.55(14) . . . . ? C12 N1 C9 O1 -0.5(2) . . . . ? C10 N1 C9 C8 -0.34(15) . . . . ? C12 N1 C9 C8 178.74(13) . . . . ? C7 C8 C9 O1 -0.6(3) . . . . ? N2 C8 C9 O1 179.00(15) . . . . ? C7 C8 C9 N1 -179.76(14) . . . . ? N2 C8 C9 N1 -0.16(15) . . . . ? C8 N2 C10 N1 -0.89(16) . . . . ? C8 N2 C10 C11 177.71(13) . . . . ? C9 N1 C10 N2 0.81(17) . . . . ? C12 N1 C10 N2 -178.22(14) . . . . ? C9 N1 C10 C11 -177.84(13) . . . . ? C12 N1 C10 C11 3.1(2) . . . . ? _cod_database_fobs_code 2108658