#------------------------------------------------------------------------------ #$Date: 2020-09-25 08:56:24 +0300 (Fri, 25 Sep 2020) $ #$Revision: 256761 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/86/2108663.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108663 _cell_angle_alpha 78.551 _cell_angle_beta 80.825 _cell_angle_gamma 72.163 _cell_length_a 8.0548 _cell_length_b 10.7806 _cell_length_c 13.7195 _exptl_crystal_F_000 756.00 _reflns_d_resolution_high 0.6157 _cod_data_source_file rm5038Isup2.hkl _cod_data_source_block I _shelx_title ' RS_RuLi_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 470.47 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 22501.94 22811.66 173.08 o 2 0 0 1083.99 1131.03 7.80 o 3 0 0 6917.88 7175.06 39.72 o 4 0 0 37579.79 37917.13 200.56 o 5 0 0 6411.94 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1141.84 1171.29 52.50 o -7 8 0 1144.29 1271.98 31.88 o -6 8 0 3445.59 3426.01 44.70 o -5 8 0 4065.33 4064.58 39.28 o -4 8 0 112.72 138.07 11.32 o -3 8 0 1241.83 1254.08 19.24 o -2 8 0 296.02 290.89 11.64 o -1 8 0 7363.78 7528.07 54.08 o 0 8 0 24.76 33.57 4.82 o 1 8 0 865.15 866.17 14.45 o 2 8 0 2834.52 2754.98 23.95 o 3 8 0 3262.95 3402.49 27.99 o 4 8 0 276.38 258.09 16.30 o 5 8 0 59.77 64.74 7.14 o 6 8 0 4651.21 5161.68 43.27 o 7 8 0 12889.53 12958.77 90.79 o 8 8 0 84.10 100.62 12.53 o 9 8 0 1786.35 1774.30 36.21 o 10 8 0 7221.08 7544.25 74.57 o 11 8 0 4875.41 4798.29 73.21 o 12 8 0 367.19 443.68 35.22 o -8 9 0 60.12 73.20 24.89 o -7 9 0 97.84 129.64 26.74 o -6 9 0 230.44 200.68 17.76 o -5 9 0 272.58 372.62 22.34 o -4 9 0 325.54 338.55 15.82 o -3 9 0 14.07 25.69 9.17 o -2 9 0 30.84 17.23 9.46 o -1 9 0 2751.01 2722.67 32.26 o 0 9 0 145.97 153.11 9.53 o 1 9 0 197.68 213.13 9.62 o 2 9 0 289.23 255.02 9.71 o 3 9 0 460.81 445.48 12.69 o 4 9 0 95.53 97.08 9.33 o 5 9 0 1153.59 1051.78 19.78 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