#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/06/2200662.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200662_Fobs loop_ _publ_author_name 'Patra, Goutam Kumar' 'Goldberg, Israel' _publ_section_title ; Tetrakis(4-acetylpyridine)diisothiocyanatocobalt(II) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m483 _journal_page_last m484 _journal_volume 57 _journal_year 2001 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.9180 _cell_length_b 15.9700 _cell_length_c 33.1930 _exptl_crystal_F_000 2728.00 _reflns_d_resolution_high 0.7599 _[local]_cod_data_source_file cv6061Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound ga26-Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 324.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 21515.48 20928.18 731.92 o 4 0 0 25250.48 24410.69 866.15 o 6 0 0 31584.12 30413.97 894.37 o 8 0 0 2243.79 2279.93 205.19 o 10 0 0 232.87 223.08 156.33 o 12 0 0 12670.18 13733.00 730.96 o 14 0 0 0.53 215.88 279.99 o 2 1 0 2089.77 2427.85 92.21 o 4 1 0 532.20 693.50 42.02 o 6 1 0 10230.31 10541.05 234.85 o 8 1 0 2758.85 2455.22 140.84 o 10 1 0 593.57 461.53 116.10 o 12 1 0 1.37 86.21 196.91 o 14 1 0 48.62 209.75 177.70 o 2 2 0 39296.82 38927.23 916.10 o 4 2 0 9874.12 9704.43 232.09 o 6 2 0 1.61 13.21 43.34 o 8 2 0 6554.50 6384.62 254.78 o 10 2 0 8530.38 8994.36 348.31 o 12 2 0 1574.26 1864.02 197.51 o 14 2 0 604.01 307.37 190.78 o 2 3 0 14616.77 15388.11 421.19 o 4 3 0 205.89 111.66 33.74 o 6 3 0 8146.99 8285.86 195.59 o 8 3 0 3948.52 3681.22 185.02 o 10 3 0 72.91 67.48 137.12 o 12 3 0 5166.98 6078.33 437.64 o 14 3 0 2052.27 2349.93 255.26 o 0 4 0 888.06 966.05 58.11 o 2 4 0 7600.98 7492.10 179.98 o 4 4 0 397.60 474.98 37.70 o 6 4 0 4653.27 4707.06 128.35 o 8 4 0 449.89 625.90 98.81 o 10 4 0 889.75 772.26 150.20 o 12 4 0 6.71 -6.00 133.87 o 14 4 0 1502.62 1587.87 347.95 o 2 5 0 4149.96 3894.45 103.74 o 4 5 0 3089.24 2755.75 94.61 o 6 5 0 1319.87 1099.56 64.36 o 8 5 0 1146.71 1034.01 106.98 o 10 5 0 1067.15 1065.46 122.11 o 12 5 0 766.25 482.66 140.12 o 14 5 0 2355.58 2545.27 360.08 o 0 6 0 61930.02 63580.45 2586.22 o 2 6 0 40277.43 41061.40 940.84 o 4 6 0 127.70 201.83 38.42 o 6 6 0 2192.65 2597.98 106.02 o 8 6 0 2930.15 2948.21 173.13 o 10 6 0 4724.53 4537.40 210.12 o 12 6 0 2802.87 3201.79 243.13 o 14 6 0 143.68 -48.99 283.72 o 2 7 0 22533.48 24334.92 572.95 o 4 7 0 45.03 86.21 40.58 o 6 7 0 2938.04 2869.69 126.19 o 8 7 0 1498.72 1436.95 136.63 o 10 7 0 1910.71 1837.25 169.29 o 12 7 0 341.57 224.04 240.61 o 14 7 0 1810.86 1598.92 230.05 o 0 8 0 32136.34 31376.18 969.77 o 2 8 0 8028.50 7691.41 206.63 o 4 8 0 4730.37 4726.15 138.20 o 6 8 0 834.51 805.40 82.61 o 8 8 0 8539.93 8355.38 297.76 o 10 8 0 4757.21 4977.08 254.18 o 12 8 0 2934.65 3252.94 359.72 o 14 8 0 73.70 -97.49 236.77 o 2 9 0 2598.27 2223.98 85.01 o 4 9 0 20.02 178.90 51.87 o 6 9 0 49.96 109.50 66.04 o 8 9 0 13709.93 14901.96 507.64 o 10 9 0 1584.30 1498.06 163.65 o 12 9 0 309.74 108.06 172.89 o 14 9 0 202.77 117.66 171.33 o 0 10 0 309.67 352.75 80.68 o 2 10 0 9768.24 9718.12 252.74 o 4 10 0 2271.81 2482.72 107.10 o 6 10 0 4.33 58.59 63.63 o 8 10 0 195.63 181.66 101.82 o 10 10 0 8075.73 8085.23 380.13 o 12 10 0 39.93 427.91 176.38 o 2 11 0 341.14 224.04 54.99 o 4 11 0 7193.33 7510.11 234.25 o 6 11 0 1346.69 1338.85 106.50 o 8 11 0 3082.92 3421.03 198.59 o 10 11 0 1006.79 817.17 160.41 o 12 11 0 1332.70 1455.44 214.20 o 0 12 0 36676.70 37464.60 1086.47 o 2 12 0 19.68 100.98 57.75 o 4 12 0 1372.96 1259.01 105.78 o 6 12 0 10.78 46.59 89.93 o 8 12 0 57.93 4.80 105.30 o 10 12 0 657.48 673.57 170.85 o 12 12 0 4.93 -234.67 156.45 o 2 13 0 6490.86 6072.92 199.79 o 4 13 0 4888.40 5085.26 207.59 o 6 13 0 9177.05 9649.92 367.64 o 8 13 0 72.39 219.96 126.43 o 10 13 0 0.17 32.30 130.75 o 12 13 0 416.23 208.79 294.40 o 0 14 0 7936.37 8185.24 407.50 o 2 14 0 5938.13 6056.72 275.07 o 4 14 0 208.95 63.51 99.41 o 6 14 0 8.97 39.74 114.06 o 8 14 0 1821.66 2060.45 191.87 o 2 15 0 297.61 133.15 122.35 o 4 15 0 386.78 481.10 124.63 o 6 15 0 1206.32 1511.51 142.76 o 8 15 0 3844.47 4338.94 346.99 o 0 16 0 4060.58 4435.35 313.85 o 2 16 0 2018.22 1792.94 167.25 o 4 16 0 382.73 294.16 123.67 o 6 16 0 478.39 756.89 253.58 o 8 16 0 1679.04 2111.12 324.78 o 10 16 0 322.81 80.56 290.44 o 2 17 0 739.84 646.91 125.11 o 4 17 0 51.87 0.00 12.01 o 6 17 0 3045.74 2669.18 336.54 o 0 18 0 2687.56 2541.79 282.99 o 2 18 0 1271.64 1912.17 227.28 o 4 18 0 1.02 -83.09 188.86 o 6 18 0 213.61 329.70 267.99 o 8 18 0 700.44 423.59 340.87 o 2 19 0 2884.48 2723.09 271.23 o 4 19 0 4952.92 5320.11 520.61 o 6 19 0 1343.54 1146.03 323.82 o 2 1 1 31220.34 30935.90 560.71 o 3 1 1 15383.87 15577.81 285.40 o 4 1 1 11982.78 11538.32 200.99 o 5 1 1 9552.09 10477.06 177.34 o 6 1 1 8649.74 8662.26 154.76 o 7 1 1 366.27 391.41 41.18 o 8 1 1 3259.73 3081.37 126.91 o 9 1 1 24.05 69.76 61.35 o 10 1 1 1700.59 1787.06 114.30 o 11 1 1 2248.13 2583.93 130.39 o 12 1 1 166.24 137.96 90.41 o 13 1 1 313.86 341.11 120.31 o 14 1 1 78.95 1.20 112.98 o 15 1 1 14.17 205.79 134.23 o 1 2 1 18.56 32.30 7.08 o 2 2 1 14101.85 14557.13 259.22 o 3 2 1 2990.09 3193.99 66.64 o 4 2 1 381.19 422.15 27.01 o 5 2 1 15139.35 15474.19 258.62 o 6 2 1 35.01 48.99 26.17 o 7 2 1 359.62 337.26 39.50 o 8 2 1 37.49 26.29 42.98 o 9 2 1 2112.23 1988.77 105.06 o 10 2 1 6432.21 6613.70 197.27 o 11 2 1 339.84 261.86 73.96 o 12 2 1 441.49 527.81 100.25 o 13 2 1 773.95 697.10 104.34 o 14 2 1 480.09 566.71 130.27 o 15 2 1 172.52 98.21 153.20 o 1 3 1 17857.06 18131.13 354.55 o 2 3 1 17528.90 17852.21 314.81 o 3 3 1 803.30 809.24 29.54 o 4 3 1 250.26 295.36 26.17 o 5 3 1 6163.25 6395.78 116.34 o 6 3 1 15867.12 16597.29 249.98 o 7 3 1 66.44 -15.61 38.30 o 8 3 1 1989.81 1867.02 89.81 o 9 3 1 297.46 167.97 63.75 o 10 3 1 901.68 805.40 94.37 o 11 3 1 4.74 67.48 73.36 o 12 3 1 7.17 60.27 107.10 o 13 3 1 517.16 605.25 168.81 o 14 3 1 560.89 542.22 138.80 o 15 3 1 120.48 128.35 149.96 o 0 4 1 16819.69 17028.68 497.43 o 1 4 1 222.58 246.37 15.25 o 2 4 1 1958.35 2136.69 48.03 o 3 4 1 124.69 68.56 20.65 o 4 4 1 71.80 46.59 21.73 o 5 4 1 25059.39 25827.34 423.23 o 6 4 1 4646.63 4579.55 103.14 o 7 4 1 8881.50 8533.79 172.89 o 8 4 1 18909.51 18553.52 415.31 o 9 4 1 373.86 337.26 64.96 o 10 4 1 191.07 277.83 80.80 o 11 4 1 1186.69 1333.81 101.22 o 12 4 1 6541.95 7130.70 280.95 o 13 4 1 3453.16 3344.55 168.33 o 14 4 1 1.66 60.27 154.88 o 15 4 1 501.70 902.53 166.53 o 1 5 1 1857.02 2123.84 47.91 o 2 5 1 1149.20 1186.25 35.78 o 3 5 1 22380.63 23488.34 371.72 o 4 5 1 127.25 152.12 26.53 o 5 5 1 4985.62 4952.71 97.49 o 6 5 1 3463.67 3514.92 90.41 o 7 5 1 480.96 519.88 58.47 o 8 5 1 129.82 129.91 61.59 o 9 5 1 1892.06 1879.03 108.18 o 10 5 1 5014.18 5386.03 198.35 o 11 5 1 1316.90 1711.66 123.31 o 12 5 1 120.85 105.90 101.22 o 13 5 1 302.11 693.50 180.70 o 14 5 1 885.20 827.13 161.49 o 15 5 1 314.10 367.16 159.33 o 0 6 1 1537.96 1688.84 68.32 o 1 6 1 1336.07 1372.11 35.90 o 2 6 1 5046.49 5110.00 103.98 o 3 6 1 49092.34 50462.79 825.09 o 4 6 1 503.54 474.98 33.26 o 5 6 1 3121.96 3031.54 76.36 o 6 6 1 649.39 689.90 47.31 o 7 6 1 36.67 30.02 40.94 o 8 6 1 5023.16 5144.70 149.12 o 9 6 1 2343.81 2644.21 135.43 o 10 6 1 2364.04 2566.29 126.43 o 11 6 1 1858.20 1688.84 113.94 o 12 6 1 512.17 726.76 130.75 o 13 6 1 86.34 105.90 97.73 o 14 6 1 223.42 231.37 144.44 o 15 6 1 4.26 16.69 221.64 o 1 7 1 26073.90 27663.15 438.00 o 2 7 1 550.11 573.31 29.90 o 3 7 1 2276.34 2256.76 52.71 o 4 7 1 2703.10 2207.65 55.35 o 5 7 1 670.97 645.11 45.75 o 6 7 1 1254.59 1392.64 62.07 o 7 7 1 3198.39 3453.57 109.98 o 8 7 1 16229.07 16215.60 379.53 o 9 7 1 1852.07 1541.28 111.54 o 10 7 1 136.58 67.48 84.29 o 11 7 1 5005.06 4812.23 192.35 o 12 7 1 3491.33 3320.54 183.70 o 13 7 1 61.55 -102.42 117.78 o 14 7 1 299.63 386.01 205.55 o 0 8 1 5201.32 5519.06 133.87 o 1 8 1 1215.64 1364.43 46.11 o 2 8 1 8140.77 8591.42 147.80 o 3 8 1 27.77 52.95 28.70 o 4 8 1 292.70 309.89 34.10 o 5 8 1 342.65 245.29 48.87 o 6 8 1 3058.79 3396.78 105.06 o 7 8 1 63.00 111.66 50.55 o 8 8 1 4792.36 4726.15 142.88 o 9 8 1 313.30 153.92 74.80 o 10 8 1 854.56 770.34 100.01 o 11 8 1 1.14 -34.70 111.42 o 12 8 1 54.64 -53.91 124.75 o 13 8 1 279.55 275.43 126.55 o 14 8 1 3.29 -43.34 117.66 o 1 9 1 319.49 219.96 28.82 o 2 9 1 10004.82 10223.24 175.18 o 3 9 1 1966.61 1810.59 58.95 o 4 9 1 10289.40 10885.28 188.02 o 5 9 1 4845.93 4769.01 114.90 o 6 9 1 10881.87 11037.64 225.72 o 7 9 1 1329.18 1366.95 79.48 o 8 9 1 7.06 -104.10 69.40 o 9 9 1 510.14 598.41 88.13 o 10 9 1 285.54 51.39 87.53 o 11 9 1 2017.14 1775.41 169.41 o 12 9 1 284.87 430.80 113.58 o 13 9 1 388.44 307.37 153.08 o 14 9 1 583.67 179.86 173.74 o 0 10 1 7343.02 7072.23 198.11 o 1 10 1 411.56 415.07 36.74 o 2 10 1 76.44 53.91 32.54 o 3 10 1 38.84 44.30 37.34 o 4 10 1 781.85 855.23 54.75 o 5 10 1 2622.68 2612.15 77.92 o 6 10 1 8324.74 8675.11 180.70 o 7 10 1 1298.28 1395.28 85.37 o 8 10 1 821.21 855.23 91.25 o 9 10 1 2505.83 2583.94 116.22 o 10 10 1 41.95 -17.89 105.18 o 11 10 1 44.94 104.46 92.81 o 12 10 1 165.62 58.59 80.08 o 13 10 1 154.52 139.64 174.46 o 1 11 1 3081.33 3073.68 88.37 o 2 11 1 12.54 67.48 35.90 o 3 11 1 991.71 927.63 50.67 o 4 11 1 1055.06 1212.66 60.39 o 5 11 1 948.15 1049.61 62.91 o 6 11 1 1651.26 1626.77 83.81 o 7 11 1 103.50 142.04 71.08 o 8 11 1 2819.81 2933.21 131.35 o 9 11 1 2.87 -103.02 87.29 o 10 11 1 528.81 499.47 108.42 o 11 11 1 5.95 -53.91 122.23 o 12 11 1 103.10 130.75 100.62 o 13 11 1 0.31 80.56 290.44 o 0 12 1 10069.70 10279.43 267.03 o 1 12 1 158.02 124.51 41.78 o 2 12 1 259.03 287.08 45.75 o 3 12 1 6444.55 6772.43 148.28 o 4 12 1 3927.88 3851.35 111.78 o 5 12 1 4759.96 4673.80 132.67 o 6 12 1 95.25 27.74 67.48 o 7 12 1 953.02 902.53 95.81 o 8 12 1 1370.60 1452.80 110.94 o 9 12 1 300.14 267.51 97.49 o 10 12 1 3111.50 3523.21 185.14 o 11 12 1 960.67 946.72 191.87 o 12 12 1 1000.13 936.15 178.06 o 1 13 1 996.77 1045.17 62.67 o 2 13 1 2719.85 2597.98 84.77 o 3 13 1 763.80 825.09 57.75 o 4 13 1 91.21 176.14 56.07 o 5 13 1 1299.15 1263.93 91.13 o 6 13 1 1625.79 1688.84 105.42 o 7 13 1 452.84 485.67 96.17 o 8 13 1 172.37 223.08 84.89 o 9 13 1 181.82 171.57 129.79 o 10 13 1 305.87 280.11 124.15 o 11 13 1 163.63 405.34 192.59 o 12 13 1 187.07 93.41 148.76 o 0 14 1 271.19 277.83 88.97 o 1 14 1 171.62 35.90 61.11 o 2 14 1 770.70 865.43 69.28 o 3 14 1 1915.08 1982.53 92.57 o 4 14 1 250.61 201.83 76.84 o 5 14 1 4212.72 4453.84 175.78 o 6 14 1 144.42 244.21 92.09 o 7 14 1 88.63 -62.43 87.65 o 8 14 1 742.03 625.90 103.98 o 9 14 1 19.57 214.80 149.36 o 10 14 1 2888.72 3328.46 427.79 o 11 14 1 34.62 186.34 198.71 o 1 15 1 7756.05 7715.66 206.99 o 2 15 1 508.62 346.27 65.80 o 3 15 1 872.54 890.05 82.73 o 4 15 1 5108.11 5700.72 193.55 o 5 15 1 1121.36 1088.16 102.90 o 6 15 1 341.04 386.01 91.25 o 7 15 1 165.88 319.74 92.93 o 8 15 1 929.06 1143.75 175.78 o 9 15 1 298.84 268.59 258.98 o 10 15 1 67.03 -248.54 296.08 o 0 16 1 786.82 678.97 130.03 o 1 16 1 1977.13 1924.41 109.50 o 2 16 1 2097.59 2146.29 125.23 o 3 16 1 33.77 172.41 80.08 o 4 16 1 33.06 28.82 85.25 o 5 16 1 770.82 873.60 94.25 o 6 16 1 1782.83 1772.41 145.88 o 7 16 1 153.32 302.57 176.02 o 8 16 1 85.15 -119.95 136.63 o 9 16 1 311.45 284.80 162.57 o 10 16 1 146.72 272.07 229.81 o 1 17 1 1937.06 2016.62 112.02 o 2 17 1 6907.62 7277.66 218.76 o 3 17 1 1169.46 1224.79 109.14 o 4 17 1 1283.90 1379.80 141.56 o 5 17 1 524.24 615.58 168.45 o 6 17 1 465.80 548.70 176.98 o 7 17 1 814.56 584.96 162.57 o 8 17 1 55.36 -81.76 153.56 o 9 17 1 37.76 73.24 222.36 o 0 18 1 3816.20 4203.02 224.64 o 1 18 1 85.58 50.43 105.90 o 2 18 1 373.38 375.21 119.47 o 3 18 1 23.06 -96.17 121.63 o 4 18 1 227.21 68.56 158.37 o 5 18 1 481.62 287.08 165.57 o 6 18 1 90.94 74.44 183.58 o 7 18 1 614.23 291.76 168.09 o 8 18 1 642.52 346.27 190.90 o 1 19 1 929.47 605.25 240.37 o 2 19 1 0.98 14.53 151.88 o 3 19 1 384.45 361.88 145.04 o 4 19 1 317.63 85.01 179.50 o 5 19 1 36.62 -127.63 185.50 o 6 19 1 7.33 -126.07 203.03 o 4 20 1 268.85 513.52 257.54 o 2 0 2 12545.93 12604.02 311.21 o 3 0 2 12964.58 12004.41 296.08 o 4 0 2 8415.74 9372.81 214.68 o 5 0 2 31418.27 31943.49 767.94 o 6 0 2 17422.11 17982.12 446.04 o 7 0 2 2878.07 2538.31 104.70 o 8 0 2 2565.25 2356.65 144.68 o 9 0 2 222.58 160.89 73.00 o 10 0 2 33.58 -73.24 115.02 o 11 0 2 45.62 -159.93 151.64 o 12 0 2 1087.20 753.17 150.20 o 13 0 2 8310.78 9172.66 444.72 o 14 0 2 3.83 -129.91 156.45 o 15 0 2 1082.48 770.34 238.45 o 2 1 2 16457.60 16374.80 274.95 o 3 1 2 4613.25 5030.99 98.33 o 4 1 2 5313.14 5294.90 100.86 o 5 1 2 46.57 119.95 25.09 o 6 1 2 5256.76 5021.15 103.14 o 7 1 2 5.19 -45.62 33.74 o 8 1 2 1548.37 1397.81 82.97 o 9 1 2 785.72 843.10 78.52 o 10 1 2 2210.32 2204.41 110.58 o 11 1 2 1855.30 1900.16 123.91 o 12 1 2 0.49 103.02 94.97 o 13 1 2 440.34 127.63 126.07 o 14 1 2 102.42 179.86 123.55 o 15 1 2 884.24 760.74 160.53 o 0 2 2 13960.17 12210.32 344.59 o 1 2 2 7446.94 6681.54 124.63 o 2 2 2 14216.19 12838.51 227.76 o 3 2 2 56114.82 54932.11 909.62 o 4 2 2 4.72 -1.20 20.65 o 5 2 2 35342.18 37009.90 559.99 o 6 2 2 492.91 435.12 34.70 o 7 2 2 276.15 191.14 37.34 o 8 2 2 668.67 657.48 65.80 o 9 2 2 869.71 1003.03 83.45 o 10 2 2 339.95 248.54 76.48 o 11 2 2 732.69 556.86 94.85 o 12 2 2 58.42 140.48 99.41 o 13 2 2 97.13 78.04 133.51 o 14 2 2 246.53 242.05 128.35 o 15 2 2 821.93 381.93 157.05 o 1 3 2 12328.72 12418.04 239.41 o 2 3 2 21527.96 21676.67 346.87 o 3 3 2 1599.05 1723.18 43.10 o 4 3 2 5808.74 5805.90 121.51 o 5 3 2 11211.17 11345.61 184.54 o 6 3 2 441.15 454.09 41.30 o 7 3 2 8607.10 8688.08 193.79 o 8 3 2 1625.60 1755.00 78.40 o 9 3 2 2782.54 2836.43 121.75 o 10 3 2 3138.01 3139.36 124.27 o 11 3 2 1677.62 1772.41 122.59 o 12 3 2 57.58 39.74 94.01 o 13 3 2 8.45 43.34 103.62 o 14 3 2 63.72 -188.26 136.87 o 15 3 2 183.35 386.01 159.33 o 0 4 2 5262.93 5375.94 152.48 o 1 4 2 33995.48 35531.77 626.98 o 2 4 2 605.62 578.24 23.29 o 3 4 2 2289.08 2306.46 53.31 o 4 4 2 58.73 61.35 21.73 o 6 4 2 274.73 214.80 38.54 o 7 4 2 678.27 760.74 55.47 o 8 4 2 62.35 52.95 52.95 o 9 4 2 1706.75 1988.77 114.30 o 10 4 2 4738.79 5050.69 182.26 o 11 4 2 93.74 256.22 84.29 o 12 4 2 21.07 76.84 110.58 o 13 4 2 23.05 235.57 122.35 o 14 4 2 13.07 -111.66 144.32 o 15 4 2 127.39 57.63 134.59 o 1 5 2 8259.87 7576.27 144.80 o 2 5 2 313.93 300.16 21.61 o 3 5 2 1878.01 2407.44 54.39 o 4 5 2 33.22 19.09 23.89 o 5 5 2 415.10 392.86 33.02 o 6 5 2 1.02 40.70 33.62 o 7 5 2 11429.85 11419.57 229.57 o 8 5 2 1265.50 1354.10 76.48 o 9 5 2 4563.36 4884.63 159.81 o 10 5 2 1285.25 1356.74 94.49 o 11 5 2 18268.36 19268.15 500.19 o 12 5 2 71.78 124.51 89.69 o 13 5 2 1208.86 1338.85 169.89 o 14 5 2 182.05 147.92 155.97 o 15 5 2 11.30 62.43 153.80 o 0 6 2 1701.40 1697.37 62.79 o 1 6 2 3986.89 4118.13 84.53 o 2 6 2 2422.59 2500.01 55.47 o 3 6 2 1008.99 835.18 38.06 o 4 6 2 847.57 781.87 36.86 o 5 6 2 13088.55 12980.19 205.31 o 6 6 2 5790.40 6002.93 123.55 o 7 6 2 9088.75 9541.38 209.87 o 8 6 2 348.01 518.20 63.15 o 9 6 2 4392.56 4481.57 153.08 o 10 6 2 4022.40 4051.74 145.52 o 11 6 2 953.93 931.95 99.41 o 12 6 2 90.09 119.11 99.89 o 13 6 2 1814.28 2370.10 226.08 o 14 6 2 26.49 -156.45 134.35 o 15 6 2 497.27 276.63 244.33 o 1 7 2 7224.46 7043.18 139.64 o 2 7 2 33.64 16.69 21.49 o 3 7 2 3978.90 4626.61 94.25 o 4 7 2 1287.31 1439.59 49.95 o 5 7 2 740.69 931.95 57.15 o 6 7 2 5.71 67.48 42.14 o 7 7 2 12605.99 12650.73 272.79 o 8 7 2 0.40 219.96 63.75 o 9 7 2 15.78 90.17 68.44 o 10 7 2 4256.82 4467.65 176.02 o 11 7 2 4049.29 3770.06 170.25 o 12 7 2 282.23 193.07 122.35 o 13 7 2 279.28 236.65 155.61 o 14 7 2 838.20 540.54 196.55 o 0 8 2 1.26 -21.61 38.30 o 1 8 2 6310.63 6373.57 110.70 o 2 8 2 3707.26 4012.12 92.21 o 3 8 2 8648.13 8824.23 156.21 o 4 8 2 304.62 357.92 32.78 o 5 8 2 23333.73 23786.70 416.87 o 6 8 2 432.10 355.27 52.23 o 7 8 2 12418.89 13011.88 252.98 o 8 8 2 17.53 16.69 67.12 o 9 8 2 3021.04 2832.71 136.51 o 10 8 2 263.13 350.11 84.29 o 11 8 2 113.64 238.81 88.85 o 12 8 2 546.62 550.26 107.34 o 13 8 2 1614.09 1273.78 210.24 o 14 8 2 122.23 111.66 111.30 o 1 9 2 687.13 598.41 35.66 o 2 9 2 806.30 900.49 41.54 o 3 9 2 2346.40 2383.66 64.24 o 4 9 2 2612.26 2748.54 72.64 o 5 9 2 748.05 678.97 54.15 o 6 9 2 569.09 440.88 52.35 o 7 9 2 699.03 783.91 64.00 o 8 9 2 17.68 97.49 80.80 o 9 9 2 2954.47 2644.21 135.43 o 10 9 2 410.61 203.75 85.13 o 11 9 2 2007.50 1870.02 149.84 o 12 9 2 196.01 300.16 129.67 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725.20 o 2 5 11 9592.82 9179.27 212.52 o 3 5 11 3181.75 2963.22 64.12 o 4 5 11 578.82 675.37 34.22 o 5 5 11 3868.95 4118.13 97.85 o 6 5 11 460.53 608.61 46.11 o 7 5 11 516.92 399.70 62.31 o 8 5 11 2087.45 2250.27 108.54 o 9 5 11 2128.93 2246.91 105.18 o 10 5 11 188.76 -20.29 105.18 o 11 5 11 341.96 135.55 88.73 o 12 5 11 225.63 276.63 119.83 o 13 5 11 1097.77 1143.75 145.28 o 14 5 11 89.05 129.91 143.00 o 0 6 11 661.33 620.74 32.78 o 1 6 11 485.83 482.66 31.94 o 2 6 11 420.65 455.65 39.98 o 3 6 11 3974.59 3950.88 100.13 o 4 6 11 126.46 84.29 24.13 o 5 6 11 6098.63 5848.16 137.84 o 6 6 11 3199.63 3280.68 103.26 o 7 6 11 2681.43 2548.76 108.42 o 8 6 11 509.90 497.91 66.52 o 9 6 11 16.97 115.38 86.33 o 10 6 11 3325.80 3256.90 193.79 o 11 6 11 112.63 56.55 120.43 o 12 6 11 262.92 244.21 108.30 o 13 6 11 1993.32 1982.53 154.28 o 14 6 11 9.47 129.91 235.45 o 1 7 11 4976.67 4730.83 104.82 o 2 7 11 447.49 392.86 37.10 o 3 7 11 9512.58 9869.04 192.83 o 4 7 11 6218.55 6301.89 137.48 o 5 7 11 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27 191.39 256.22 200.75 o 1 15 27 238.92 330.90 220.68 o 2 15 27 29.32 -216.84 175.54 o 3 15 27 611.16 766.50 264.74 o 4 15 27 1.54 208.79 181.30 o 5 15 27 0.15 -73.24 202.79 o 0 16 27 654.63 304.97 271.11 o 1 16 27 46.94 278.91 234.97 o 2 16 27 0.63 -338.59 244.81 o 3 16 27 156.81 219.96 261.02 o 0 0 28 75.15 46.59 122.11 o 1 0 28 1393.31 1522.31 137.96 o 2 0 28 955.53 772.26 138.68 o 3 0 28 247.50 165.21 103.38 o 4 0 28 64.45 -42.02 104.58 o 6 0 28 1746.31 1568.54 137.24 o 7 0 28 10235.61 12042.47 517.12 o 8 0 28 543.69 617.26 168.69 o 9 0 28 1645.79 1490.02 206.03 o 10 0 28 124.67 78.04 142.64 o 11 0 28 91.97 1.20 306.17 o 12 0 28 796.36 700.82 187.18 o 1 1 28 898.94 787.75 83.69 o 2 1 28 505.81 632.87 78.40 o 3 1 28 430.05 323.46 73.48 o 4 1 28 931.98 865.43 89.69 o 5 1 28 2476.85 2836.43 162.45 o 6 1 28 1450.92 1377.15 113.10 o 7 1 28 691.66 728.56 110.34 o 8 1 28 0.16 44.30 94.49 o 9 1 28 150.91 150.44 105.42 o 10 1 28 22.58 6.00 130.27 o 11 1 28 502.82 312.29 138.44 o 12 1 28 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174.94 o 3 11 28 867.79 915.02 171.93 o 4 11 28 1239.12 1303.67 205.19 o 5 11 28 311.30 618.94 210.36 o 6 11 28 5.77 4.80 187.78 o 7 11 28 44.33 -130.75 200.51 o 8 11 28 790.49 1219.99 251.78 o 0 12 28 619.50 291.76 282.99 o 1 12 28 69.78 303.77 142.52 o 2 12 28 170.91 45.62 155.00 o 3 12 28 181.72 318.41 200.39 o 4 12 28 5.48 -126.07 182.86 o 5 12 28 142.02 272.07 193.19 o 6 12 28 20.93 44.30 137.84 o 7 12 28 182.45 306.17 173.37 o 8 12 28 302.31 529.37 346.03 o 1 13 28 439.95 470.54 159.33 o 2 13 28 3.05 -148.76 205.43 o 3 13 28 8.91 192.11 168.09 o 4 13 28 202.88 579.92 183.58 o 5 13 28 190.07 561.79 239.77 o 6 13 28 189.94 289.48 207.47 o 7 13 28 753.38 618.94 196.55 o 0 14 28 26.25 -234.61 380.01 o 1 14 28 159.45 662.76 215.88 o 2 14 28 112.20 -74.44 217.08 o 3 14 28 182.38 -142.88 248.54 o 4 14 28 302.10 367.16 245.65 o 5 14 28 42.80 230.29 196.67 o 1 15 28 445.24 394.18 211.92 o 2 15 28 0.76 -61.35 224.64 o 3 15 28 123.82 54.99 215.88 o 4 15 28 9.76 30.02 260.30 o 0 16 28 882.47 805.40 352.03 o 1 16 28 13.03 70.84 260.78 o 1 1 29 221.77 140.48 64.84 o 2 1 29 2467.41 2326.51 127.03 o 3 1 29 3319.07 3433.28 142.16 o 4 1 29 5787.64 6186.87 201.71 o 5 1 29 2221.94 2353.29 134.47 o 6 1 29 345.53 386.01 88.49 o 7 1 29 190.25 145.40 95.21 o 8 1 29 2939.27 3412.99 166.05 o 9 1 29 20.88 -10.81 110.70 o 10 1 29 2.85 -38.42 128.47 o 11 1 29 695.37 283.60 187.90 o 0 2 29 1022.27 900.49 122.71 o 1 2 29 430.00 298.96 64.72 o 2 2 29 347.80 278.91 63.63 o 3 2 29 935.78 1263.93 91.13 o 4 2 29 787.51 787.75 101.10 o 5 2 29 156.07 99.53 89.93 o 6 2 29 1590.84 1657.63 126.91 o 7 2 29 0.95 -16.69 73.12 o 8 2 29 523.75 686.18 150.68 o 9 2 29 306.92 237.73 128.23 o 10 2 29 1261.63 1364.43 158.73 o 11 2 29 37.92 165.21 163.89 o 1 3 29 497.70 348.79 62.07 o 2 3 29 247.02 258.50 61.23 o 3 3 29 598.79 515.08 83.33 o 4 3 29 19.84 -51.39 95.93 o 5 3 29 1452.71 1452.80 103.02 o 6 3 29 1066.34 1005.19 101.10 o 7 3 29 195.57 159.93 120.07 o 8 3 29 6.78 156.45 139.52 o 9 3 29 345.35 413.75 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8 30 353.47 307.37 154.28 o 8 8 30 483.06 538.98 170.49 o 9 8 30 14.11 12.01 169.29 o 1 9 30 232.28 14.53 171.21 o 2 9 30 1631.20 1683.20 218.88 o 3 9 30 20.54 58.59 159.21 o 4 9 30 1030.29 1167.28 222.60 o 5 9 30 14.42 108.06 194.51 o 6 9 30 706.67 643.31 282.99 o 7 9 30 6.48 -97.49 150.56 o 8 9 30 4.85 230.29 156.69 o 9 9 30 6.46 240.97 185.02 o 0 10 30 607.79 743.69 306.17 o 1 10 30 157.55 139.64 180.10 o 2 10 30 1639.69 1697.37 239.89 o 3 10 30 110.04 298.96 182.14 o 4 10 30 399.85 523.01 193.31 o 5 10 30 31.40 137.96 181.54 o 6 10 30 233.73 -33.50 204.95 o 7 10 30 20.94 40.70 208.55 o 8 10 30 13.73 128.35 227.76 o 1 11 30 1212.91 1541.28 236.65 o 2 11 30 29.62 119.95 303.53 o 3 11 30 81.93 3.60 207.35 o 4 11 30 1603.02 1503.46 214.92 o 5 11 30 80.52 34.70 195.59 o 6 11 30 865.19 1088.16 235.45 o 7 11 30 489.74 388.77 210.48 o 0 12 30 1876.74 5001.58 1877.11 o 1 12 30 134.75 278.91 202.55 o 2 12 30 8.15 211.80 224.88 o 3 12 30 79.30 -66.28 197.51 o 4 12 30 9.71 142.04 210.60 o 5 12 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116.76 67.48 203.15 o 3 6 41 3.61 -87.53 266.43 o 1 7 41 4.72 -238.81 261.26 o 3 0 42 274.38 220.92 269.91 o 4 0 42 5.68 26.29 57.63 o 1 1 42 1.94 94.85 296.20 o 2 1 42 43.91 -261.86 234.37 o 3 1 42 84.91 44.30 297.40 o 4 1 42 2.10 246.37 313.25 o 0 2 42 162.83 -10.81 276.51 o 1 2 42 57.35 142.04 199.91 o 2 2 42 443.22 697.10 334.86 o 3 2 42 2.10 -214.80 314.93 o 4 2 42 112.28 290.68 300.04 o 1 3 42 13.83 26.29 203.63 o 2 3 42 90.02 -43.34 211.68 o 3 3 42 7.51 88.85 233.17 o 0 4 42 59.30 268.59 331.62 o 1 4 42 4.03 -143.72 214.32 o 2 4 42 185.18 -103.02 208.91 o 3 4 42 113.83 13.21 205.43 o 1 5 42 18.81 111.66 247.58 o 2 5 42 433.93 135.55 150.08 o 2 1 43 16.79 -87.53 300.16 o 0 2 43 473.39 303.77 306.77 o 1 2 43 2.40 -584.24 389.49 o 2 2 43 131.01 -109.50 345.91 o 1 3 43 15.08 -135.55 189.58 o