#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/06/2200669.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200669_Fobs loop_ _publ_author_name 'Wendt, Ola F.' _publ_section_title ; Chloro(methyl)(\h^5^-pentamethylcyclopentadienyl)(trimethylphosphine)rhodium(III) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m517 _journal_page_last m518 _journal_volume 57 _journal_year 2001 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.9295 _cell_length_b 14.7915 _cell_length_c 25.8117 _exptl_crystal_F_000 1504.00 _reflns_d_resolution_high 0.6721 _[local]_cod_data_source_file cv6068Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 512.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 287.54 321.44 27.14 o 4 0 0 69660.43 66127.16 1697.68 o 6 0 0 4.01 -14.62 38.17 o 8 0 0 19519.70 18102.95 320.06 o 10 0 0 241.83 432.71 174.48 o 12 0 0 774.70 565.31 237.29 o 2 1 0 1807.96 1421.16 33.53 o 4 1 0 824.42 1010.63 47.54 o 6 1 0 1573.65 1742.34 98.51 o 8 1 0 545.53 666.25 65.47 o 10 1 0 1.56 -6.72 94.11 o 12 1 0 13.22 96.15 172.90 o 0 2 0 237540.06 232651.53 2806.14 o 2 2 0 92.72 147.06 13.68 o 4 2 0 71454.89 65541.63 382.78 o 6 2 0 70.66 100.67 29.53 o 8 2 0 8241.83 8028.38 154.87 o 10 2 0 17.23 135.97 90.48 o 12 2 0 863.83 777.03 190.93 o 2 3 0 30907.84 26697.54 132.21 o 4 3 0 2374.47 1786.99 52.41 o 6 3 0 8631.01 7766.48 129.79 o 8 3 0 1603.82 1555.74 91.55 o 10 3 0 528.07 405.30 94.65 o 12 3 0 113.13 157.13 174.72 o 0 4 0 14887.57 15742.36 545.12 o 2 4 0 9909.92 8903.25 144.25 o 4 4 0 47779.08 42413.50 455.63 o 6 4 0 1919.29 1687.46 76.92 o 8 4 0 2610.30 2443.01 129.72 o 10 4 0 3.13 -23.09 95.17 o 12 4 0 526.04 511.42 171.88 o 2 5 0 71706.30 56500.68 405.57 o 4 5 0 1950.66 1753.79 54.36 o 6 5 0 9042.68 8727.49 111.14 o 8 5 0 576.68 510.83 79.59 o 10 5 0 2314.18 2316.08 156.38 o 12 5 0 177.43 195.29 417.01 o 0 6 0 641.69 1144.02 50.11 o 2 6 0 212.48 268.45 21.49 o 4 6 0 95.33 13.07 36.69 o 6 6 0 132.82 139.02 52.14 o 8 6 0 1028.02 1034.95 93.93 o 10 6 0 0.01 -103.37 103.37 o 12 6 0 9.28 97.45 148.74 o 2 7 0 64743.70 58073.48 570.40 o 4 7 0 221.94 203.41 42.52 o 6 7 0 12770.02 12435.57 325.40 o 8 7 0 146.87 184.83 77.34 o 10 7 0 2585.02 2501.71 193.36 o 12 7 0 69.98 -13.96 244.27 o 0 8 0 33.66 48.16 29.17 o 2 8 0 14.28 43.23 21.21 o 4 8 0 10620.17 10448.35 162.85 o 6 8 0 573.37 532.04 74.33 o 8 8 0 2.29 55.24 78.75 o 10 8 0 49.25 91.32 101.57 o 12 8 0 96.71 150.05 261.72 o 2 9 0 30743.13 27886.02 196.89 o 4 9 0 153.80 117.39 41.21 o 6 9 0 13517.60 13536.61 313.79 o 8 9 0 33.66 -45.52 73.67 o 10 9 0 1243.48 1094.07 135.42 o 0 10 0 15162.66 15192.67 196.70 o 2 10 0 1195.68 1274.67 53.20 o 4 10 0 2976.71 2976.08 133.12 o 6 10 0 127.09 233.78 62.74 o 8 10 0 2336.56 2158.50 124.74 o 10 10 0 310.46 475.06 127.07 o 2 11 0 8735.78 8270.02 123.03 o 4 11 0 1.83 41.58 47.99 o 6 11 0 4504.01 4426.23 142.42 o 8 11 0 2.22 -3.67 84.72 o 10 11 0 419.24 515.78 136.60 o 0 12 0 19773.30 18778.98 254.61 o 2 12 0 889.04 966.24 58.94 o 4 12 0 6220.62 6143.46 148.49 o 6 12 0 273.67 294.39 70.74 o 8 12 0 2994.35 3172.60 151.70 o 10 12 0 210.62 174.19 139.84 o 2 13 0 968.37 932.73 67.88 o 4 13 0 27.63 -20.12 60.21 o 6 13 0 199.04 214.40 75.76 o 8 13 0 118.99 245.90 115.99 o 0 14 0 4270.71 4829.63 140.82 o 2 14 0 92.04 68.69 52.30 o 4 14 0 7258.08 7550.40 173.88 o 6 14 0 323.85 370.10 85.59 o 8 14 0 1007.85 1110.91 149.98 o 2 15 0 259.44 326.75 65.00 o 4 15 0 81.58 128.64 71.81 o 6 15 0 175.28 137.72 88.27 o 8 15 0 112.79 21.08 132.78 o 0 16 0 2887.36 3360.47 251.25 o 2 16 0 0.54 -63.06 64.13 o 4 16 0 3234.95 3446.96 144.18 o 6 16 0 25.53 -62.36 112.98 o 8 16 0 583.69 987.55 261.72 o 2 17 0 1462.38 1463.89 116.95 o 4 17 0 141.25 254.46 87.39 o 6 17 0 504.01 485.82 126.50 o 0 18 0 1295.76 1671.51 233.80 o 2 18 0 22.18 20.15 109.62 o 4 18 0 156.03 198.76 97.62 o 6 18 0 41.47 103.68 147.05 o 2 19 0 1549.79 1517.71 239.04 o 4 19 0 35.02 151.23 162.97 o 6 19 0 652.01 645.57 261.72 o 0 20 0 42.57 97.71 202.40 o 2 20 0 14.38 134.56 140.58 o 4 20 0 0.05 27.92 254.74 o 2 21 0 894.54 924.74 247.76 o 1 1 1 46409.87 51464.98 458.96 o 2 1 1 14106.92 18563.93 264.41 o 3 1 1 11383.20 14425.62 100.60 o 4 1 1 260.46 263.90 18.19 o 5 1 1 6000.01 5663.57 81.11 o 6 1 1 6619.03 6173.38 87.82 o 7 1 1 3320.51 3271.65 62.43 o 8 1 1 333.63 410.19 36.66 o 9 1 1 1008.45 1065.37 59.36 o 10 1 1 1023.05 971.77 82.41 o 11 1 1 350.69 373.66 100.52 o 12 1 1 55.02 -61.31 116.39 o 13 1 1 118.77 199.70 148.15 o 0 2 1 45311.90 47556.91 720.69 o 1 2 1 22378.40 22741.69 194.14 o 2 2 1 931.62 804.26 18.03 o 3 2 1 1.92 -11.11 11.11 o 4 2 1 854.17 997.92 29.68 o 5 2 1 11.79 0.92 17.14 o 6 2 1 312.92 343.40 26.89 o 7 2 1 1961.03 1963.81 54.61 o 8 2 1 1429.45 1530.32 56.02 o 9 2 1 983.18 942.57 67.56 o 10 2 1 35.72 86.89 62.52 o 11 2 1 11.38 30.68 95.42 o 12 2 1 52.29 20.60 124.86 o 13 2 1 21.89 19.87 216.97 o 1 3 1 10304.76 13006.11 88.70 o 2 3 1 10386.65 13360.86 210.30 o 3 3 1 5888.85 6403.37 88.73 o 4 3 1 36.14 25.58 16.86 o 5 3 1 5189.27 5441.92 61.26 o 6 3 1 2553.30 2589.52 51.05 o 7 3 1 1079.32 1160.75 45.27 o 8 3 1 24.83 78.63 38.36 o 9 3 1 1097.46 1216.40 75.88 o 10 3 1 1050.84 944.70 77.64 o 11 3 1 431.79 510.51 80.63 o 12 3 1 14.50 -122.83 122.83 o 13 3 1 35.32 -296.61 296.61 o 0 4 1 3518.07 3891.09 86.90 o 1 4 1 728.09 670.46 18.44 o 2 4 1 121.30 136.12 13.18 o 3 4 1 4367.04 3684.28 49.67 o 4 4 1 10857.79 10417.74 88.47 o 5 4 1 2649.38 2674.79 46.19 o 6 4 1 82.08 124.57 23.06 o 7 4 1 302.48 268.44 35.22 o 8 4 1 1316.22 1331.20 70.75 o 9 4 1 452.41 351.71 60.47 o 10 4 1 29.47 -40.36 66.52 o 11 4 1 115.79 197.74 81.96 o 12 4 1 294.93 157.67 143.25 o 1 5 1 2131.57 2451.00 29.95 o 2 5 1 276.29 309.43 19.36 o 3 5 1 1119.47 1206.84 36.02 o 4 5 1 515.57 555.14 31.82 o 5 5 1 907.70 848.35 31.49 o 6 5 1 379.44 414.29 29.50 o 7 5 1 344.64 387.51 44.80 o 8 5 1 14.85 39.00 48.80 o 9 5 1 203.11 296.86 61.97 o 10 5 1 268.02 275.70 71.82 o 11 5 1 72.08 13.94 83.11 o 12 5 1 1.66 -0.22 98.86 o 0 6 1 7981.01 9166.00 97.97 o 1 6 1 4215.89 3519.87 38.14 o 2 6 1 941.97 819.97 25.88 o 3 6 1 14796.04 13684.47 186.37 o 4 6 1 16635.67 17040.00 134.73 o 5 6 1 8768.72 8058.19 94.02 o 6 6 1 137.79 106.51 38.05 o 7 6 1 195.29 228.68 47.11 o 8 6 1 1657.13 1686.99 86.61 o 9 6 1 521.26 384.67 63.31 o 10 6 1 38.80 -29.89 73.99 o 11 6 1 301.40 406.88 98.82 o 12 6 1 450.69 485.89 116.55 o 1 7 1 55.93 117.77 14.47 o 2 7 1 572.03 691.32 23.98 o 3 7 1 681.21 790.13 34.33 o 4 7 1 137.93 121.21 22.61 o 5 7 1 2.05 -31.18 31.18 o 6 7 1 6.91 1.33 38.83 o 7 7 1 8.80 40.17 45.91 o 8 7 1 2.71 27.26 52.93 o 9 7 1 14.60 -27.27 60.87 o 10 7 1 8.88 57.99 69.65 o 11 7 1 53.62 44.25 88.76 o 12 7 1 17.49 -135.08 182.55 o 0 8 1 6720.52 6203.09 79.02 o 1 8 1 6353.76 6109.64 70.79 o 2 8 1 703.81 866.36 27.47 o 3 8 1 1469.46 1569.23 40.96 o 4 8 1 3918.26 3871.09 79.92 o 5 8 1 539.08 533.91 42.08 o 6 8 1 0.15 1.23 37.39 o 7 8 1 2106.01 2207.86 81.39 o 8 8 1 1849.57 1854.85 83.44 o 9 8 1 943.86 954.33 74.88 o 10 8 1 39.36 126.25 79.32 o 11 8 1 96.01 117.70 91.12 o 12 8 1 244.53 147.52 291.38 o 1 9 1 916.46 1230.88 34.24 o 2 9 1 4308.40 4608.86 63.13 o 3 9 1 2294.14 2311.90 58.40 o 4 9 1 6.37 -25.74 28.55 o 5 9 1 990.70 993.24 50.14 o 6 9 1 1037.01 1010.45 57.99 o 7 9 1 474.06 473.97 54.20 o 8 9 1 3.17 41.63 56.22 o 9 9 1 161.98 305.25 67.43 o 10 9 1 236.37 260.69 77.94 o 11 9 1 180.40 366.78 99.38 o 0 10 1 6846.81 5947.00 92.74 o 1 10 1 7170.97 6720.20 68.90 o 2 10 1 458.87 365.68 27.41 o 3 10 1 844.31 929.82 34.88 o 4 10 1 1343.96 1310.04 55.68 o 5 10 1 827.36 791.19 48.00 o 6 10 1 13.05 25.18 41.04 o 7 10 1 1628.15 1585.29 75.28 o 8 10 1 1130.09 1079.82 69.47 o 9 10 1 559.87 567.45 75.26 o 10 10 1 4.54 7.76 86.51 o 11 10 1 55.40 -52.77 139.23 o 1 11 1 3193.62 3154.91 57.25 o 2 11 1 4658.56 4134.31 65.23 o 3 11 1 1613.24 1714.57 49.81 o 4 11 1 12.66 7.87 33.90 o 5 11 1 1375.02 1308.31 60.33 o 6 11 1 2835.34 2741.14 84.96 o 7 11 1 1546.51 1347.76 71.47 o 8 11 1 0.37 -58.78 58.78 o 9 11 1 133.01 178.81 74.85 o 10 11 1 275.25 283.91 93.34 o 0 12 1 87.13 141.71 32.20 o 1 12 1 30.46 82.15 24.34 o 2 12 1 124.91 113.62 25.91 o 3 12 1 1815.97 1907.18 58.37 o 4 12 1 1553.04 1525.63 63.22 o 5 12 1 772.05 695.20 51.26 o 6 12 1 11.01 0.75 49.02 o 7 12 1 55.66 17.27 55.75 o 8 12 1 41.61 22.85 68.67 o 9 12 1 0.57 50.56 90.27 o 10 12 1 12.01 -9.99 99.37 o 1 13 1 1826.91 1791.29 50.23 o 2 13 1 4268.68 3904.42 75.23 o 3 13 1 2009.32 1989.15 76.00 o 4 13 1 29.70 16.06 40.54 o 5 13 1 1017.77 1073.09 78.97 o 6 13 1 2194.79 2000.84 82.89 o 7 13 1 921.78 861.66 68.91 o 8 13 1 1.04 -38.62 74.77 o 9 13 1 132.91 125.50 92.15 o 0 14 1 243.24 202.67 41.93 o 1 14 1 76.91 94.87 33.90 o 2 14 1 3.41 13.40 37.88 o 3 14 1 161.49 78.07 42.25 o 4 14 1 20.65 26.35 44.70 o 5 14 1 6.80 -24.39 51.82 o 6 14 1 24.43 13.37 57.83 o 7 14 1 0.32 -19.03 69.41 o 8 14 1 14.42 143.09 86.03 o 9 14 1 27.45 -0.14 102.28 o 1 15 1 1128.59 1045.57 55.03 o 2 15 1 2485.41 2419.54 99.74 o 3 15 1 1119.89 1109.67 66.60 o 4 15 1 7.26 44.69 48.68 o 5 15 1 442.87 522.58 60.63 o 6 15 1 1005.28 973.01 110.07 o 7 15 1 279.17 227.76 84.38 o 8 15 1 0.85 83.24 97.43 o 0 16 1 339.57 228.41 94.98 o 1 16 1 5.42 82.23 48.64 o 2 16 1 22.36 21.53 46.99 o 3 16 1 348.04 380.13 53.92 o 4 16 1 409.83 368.40 58.72 o 5 16 1 481.93 534.71 64.09 o 6 16 1 88.28 25.16 72.16 o 7 16 1 1.20 -90.98 90.98 o 8 16 1 64.66 5.22 226.82 o 1 17 1 288.70 329.83 71.83 o 2 17 1 676.51 621.36 62.62 o 3 17 1 334.72 453.52 59.53 o 4 17 1 0.00 6.15 61.33 o 5 17 1 153.84 160.11 74.97 o 6 17 1 326.49 279.87 89.20 o 7 17 1 89.37 88.16 98.90 o 0 18 1 709.35 933.57 300.10 o 1 18 1 419.68 379.15 82.72 o 2 18 1 10.66 13.82 80.42 o 3 18 1 362.39 306.25 68.43 o 4 18 1 723.97 704.98 77.64 o 5 18 1 422.26 320.93 91.54 o 6 18 1 11.62 -6.83 97.78 o 1 19 1 58.34 104.23 90.60 o 2 19 1 63.17 96.91 141.53 o 3 19 1 0.33 -40.92 97.72 o 4 19 1 1.97 5.13 103.72 o 5 19 1 33.05 50.46 113.08 o 6 19 1 76.82 129.83 291.38 o 0 20 1 1077.01 1252.32 164.44 o 1 20 1 532.19 387.66 103.22 o 2 20 1 0.69 36.24 104.58 o 3 20 1 119.85 253.61 123.78 o 4 20 1 270.02 342.43 218.10 o 1 21 1 4.78 61.65 114.15 o 2 21 1 9.16 6.18 138.27 o 0 0 2 1858.28 793.33 282.43 o 1 0 2 136685.84 130479.81 1289.83 o 2 0 2 26351.59 27465.55 225.92 o 3 0 2 38775.48 33678.49 479.65 o 4 0 2 181.40 394.65 32.16 o 5 0 2 25630.31 23103.07 248.90 o 6 0 2 1555.01 1414.61 78.57 o 7 0 2 9605.47 9467.25 251.68 o 8 0 2 264.43 190.28 48.65 o 9 0 2 8488.14 8102.56 152.58 o 10 0 2 10.52 61.40 90.34 o 11 0 2 121.77 132.60 198.91 o 12 0 2 0.05 -153.62 174.98 o 13 0 2 501.90 642.08 303.59 o 1 1 2 9537.55 8421.88 80.41 o 2 1 2 960.94 1370.29 32.25 o 3 1 2 82.93 50.26 11.83 o 4 1 2 1.61 44.94 15.16 o 5 1 2 177.05 171.06 22.05 o 6 1 2 18.37 26.04 24.05 o 7 1 2 999.86 1068.93 47.61 o 8 1 2 62.40 24.30 32.54 o 9 1 2 20.15 -33.97 41.18 o 10 1 2 5.57 12.18 71.49 o 11 1 2 17.96 132.91 101.15 o 12 1 2 3.03 -75.71 119.04 o 13 1 2 9.80 -19.91 293.12 o 0 2 2 7977.06 6265.32 116.40 o 1 2 2 35111.11 34901.62 425.85 o 2 2 2 23.80 36.71 7.65 o 3 2 2 30903.22 31079.29 297.65 o 4 2 2 51.77 4.54 15.82 o 5 2 2 24191.33 21458.11 199.10 o 6 2 2 52.70 73.01 26.22 o 7 2 2 2931.38 2697.74 65.10 o 8 2 2 1.15 -17.40 32.65 o 9 2 2 3799.63 3933.73 104.03 o 10 2 2 19.01 32.57 63.30 o 11 2 2 386.20 305.34 98.91 o 12 2 2 2.59 4.92 124.34 o 13 2 2 419.55 242.88 171.62 o 1 3 2 18598.97 15536.57 159.12 o 2 3 2 14190.05 15128.02 108.22 o 3 3 2 25250.56 21393.52 109.66 o 4 3 2 128.95 134.21 17.29 o 5 3 2 7610.89 6667.81 75.71 o 6 3 2 16.17 42.06 24.16 o 7 3 2 5255.38 4891.18 82.18 o 8 3 2 12.29 36.50 35.87 o 9 3 2 357.89 400.27 56.96 o 10 3 2 6.07 8.71 63.69 o 11 3 2 513.09 592.17 81.91 o 12 3 2 4.51 -77.86 146.28 o 13 3 2 44.55 397.81 307.08 o 0 4 2 1045.42 831.62 23.41 o 1 4 2 24482.54 22915.21 160.63 o 2 4 2 919.82 1132.32 29.54 o 3 4 2 23816.23 22407.02 426.95 o 4 4 2 1052.63 1094.44 36.09 o 5 4 2 19222.15 18774.44 192.31 o 6 4 2 470.09 577.91 34.25 o 7 4 2 414.07 503.39 39.59 o 8 4 2 187.78 182.86 44.71 o 9 4 2 889.41 1016.05 86.96 o 10 4 2 7.04 34.45 65.53 o 11 4 2 521.43 597.95 82.71 o 12 4 2 3.99 -11.11 120.00 o 13 4 2 184.36 387.34 300.10 o 1 5 2 37428.02 34353.67 224.20 o 2 5 2 1368.82 1366.22 30.20 o 3 5 2 32396.24 30233.63 248.54 o 4 5 2 487.78 540.02 40.06 o 5 5 2 9069.23 9068.58 121.51 o 6 5 2 84.31 77.26 26.39 o 7 5 2 7013.95 6980.20 142.52 o 8 5 2 30.07 30.32 49.71 o 9 5 2 927.99 1162.73 77.38 o 10 5 2 0.14 -1.22 69.43 o 11 5 2 1377.46 1633.37 131.72 o 12 5 2 2.71 -17.52 98.14 o 0 6 2 146.15 190.43 18.20 o 1 6 2 3872.68 3771.18 44.69 o 2 6 2 30.86 20.54 12.33 o 3 6 2 2.19 11.81 17.12 o 4 6 2 301.09 405.46 26.30 o 5 6 2 103.07 130.72 24.85 o 6 6 2 27.82 24.22 28.81 o 7 6 2 1030.19 1098.88 63.95 o 8 6 2 30.99 86.06 51.86 o 9 6 2 164.29 178.50 62.94 o 10 6 2 48.88 48.44 65.23 o 11 6 2 55.75 249.22 90.46 o 12 6 2 1.37 -90.58 101.20 o 1 7 2 19293.17 16489.26 99.52 o 2 7 2 95.96 137.61 14.18 o 3 7 2 35365.17 33866.72 454.93 o 4 7 2 139.64 157.37 23.44 o 5 7 2 7536.67 7095.62 113.64 o 6 7 2 24.62 36.34 35.56 o 7 7 2 7255.67 7495.86 192.74 o 8 7 2 19.14 44.81 48.81 o 9 7 2 798.77 777.67 68.62 o 10 7 2 0.12 -2.81 75.92 o 11 7 2 1220.21 1329.53 101.31 o 12 7 2 2.60 107.14 145.39 o 0 8 2 260.55 323.21 26.11 o 1 8 2 577.02 678.56 24.04 o 2 8 2 1670.83 1811.48 35.48 o 3 8 2 4663.29 5066.89 62.85 o 4 8 2 252.17 297.81 27.39 o 5 8 2 3008.61 3016.98 77.76 o 6 8 2 295.83 350.66 42.53 o 7 8 2 109.81 137.50 43.24 o 8 8 2 6.65 -37.71 52.11 o 9 8 2 90.69 86.63 62.47 o 10 8 2 58.86 -27.01 77.05 o 11 8 2 14.78 -75.46 93.35 o 12 8 2 0.84 -265.21 265.21 o 1 9 2 15721.17 14238.04 136.28 o 2 9 2 71.96 25.45 17.49 o 3 9 2 11651.70 11238.53 141.60 o 4 9 2 65.22 78.60 26.09 o 5 9 2 4072.96 4049.63 89.14 o 6 9 2 1.47 -41.40 41.40 o 7 9 2 5328.64 5233.63 114.32 o 8 9 2 5.73 -33.36 54.55 o 9 9 2 649.16 724.98 80.69 o 10 9 2 3.61 -20.06 83.81 o 11 9 2 483.78 576.95 105.08 o 0 10 2 458.61 507.95 39.53 o 1 10 2 12635.56 12088.91 108.72 o 2 10 2 68.84 94.79 19.48 o 3 10 2 1777.63 1879.67 49.38 o 4 10 2 45.36 81.19 34.95 o 5 10 2 2730.85 3049.24 78.30 o 6 10 2 143.55 206.36 41.85 o 7 10 2 1122.76 986.27 63.47 o 8 10 2 40.32 52.20 57.87 o 9 10 2 1079.06 1265.09 87.37 o 10 10 2 0.46 -9.15 81.98 o 11 10 2 12.33 97.01 146.35 o 1 11 2 2141.86 1997.37 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21 187.10 296.27 88.42 o 8 9 21 16.93 159.77 97.14 o 9 9 21 5.05 63.02 149.75 o 0 10 21 2205.87 2352.07 115.51 o 1 10 21 1323.65 1495.94 72.12 o 2 10 21 3.83 73.48 49.46 o 3 10 21 197.51 262.40 56.03 o 4 10 21 396.38 480.47 67.45 o 5 10 21 394.21 349.87 66.52 o 6 10 21 0.01 -29.35 69.86 o 7 10 21 362.11 425.13 93.34 o 8 10 21 225.28 302.86 104.70 o 1 11 21 989.12 989.56 67.38 o 2 11 21 1099.51 1266.31 73.20 o 3 11 21 535.58 751.32 89.89 o 4 11 21 4.61 -49.86 64.53 o 5 11 21 229.61 373.95 75.08 o 6 11 21 433.87 511.21 119.39 o 7 11 21 470.31 495.88 99.65 o 8 11 21 26.79 -125.21 181.46 o 0 12 21 20.71 113.05 129.46 o 1 12 21 38.04 47.57 56.77 o 2 12 21 55.00 30.02 56.76 o 3 12 21 240.90 298.12 64.63 o 4 12 21 233.92 350.43 71.84 o 5 12 21 148.03 253.00 85.51 o 6 12 21 0.17 -91.02 91.02 o 7 12 21 28.03 167.66 97.01 o 8 12 21 5.47 174.48 293.12 o 1 13 21 899.49 928.85 78.36 o 2 13 21 1071.67 1023.73 75.14 o 3 13 21 783.72 871.97 77.03 o 4 13 21 0.41 8.85 74.37 o 5 13 21 339.24 235.51 93.12 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22 2643.84 2591.24 90.23 o 4 4 22 115.78 127.69 45.48 o 5 4 22 1691.34 1637.34 82.98 o 6 4 22 4.62 28.55 58.86 o 7 4 22 107.89 43.75 68.54 o 8 4 22 5.76 -13.36 77.98 o 9 4 22 96.71 145.32 111.30 o 1 5 22 3753.29 3497.79 83.21 o 2 5 22 108.56 124.66 38.26 o 3 5 22 3413.82 3013.82 89.85 o 4 5 22 17.24 82.39 51.68 o 5 5 22 1396.39 1246.91 76.99 o 6 5 22 3.06 43.38 62.45 o 7 5 22 1014.19 695.10 76.51 o 8 5 22 1.60 -11.28 78.86 o 9 5 22 401.81 295.17 92.80 o 0 6 22 41.06 78.19 51.63 o 1 6 22 469.92 458.42 44.56 o 2 6 22 0.13 21.23 39.55 o 3 6 22 41.68 64.10 45.95 o 4 6 22 13.25 5.17 49.49 o 5 6 22 8.77 46.31 57.73 o 6 6 22 7.52 36.98 61.95 o 7 6 22 153.08 132.25 73.12 o 8 6 22 5.92 91.97 82.74 o 9 6 22 16.05 81.83 103.73 o 1 7 22 3536.47 3384.20 90.74 o 2 7 22 24.93 -23.90 42.49 o 3 7 22 2895.37 2412.84 93.29 o 4 7 22 25.39 19.58 50.50 o 5 7 22 1299.84 1311.88 80.72 o 6 7 22 20.58 33.10 65.51 o 7 7 22 968.29 646.41 80.69 o 8 7 22 2.29 10.41 92.89 o 9 7 22 375.40 297.61 137.41 o 10 7 22 5.08 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251.25 o 0 12 22 41.53 40.44 89.80 o 1 12 22 1599.90 1492.49 101.44 o 2 12 22 24.20 35.94 59.00 o 3 12 22 472.50 452.07 68.64 o 4 12 22 0.02 57.90 85.10 o 5 12 22 620.49 573.57 93.62 o 6 12 22 0.41 80.11 95.80 o 7 12 22 247.32 204.78 147.80 o 1 13 22 1.31 16.62 71.27 o 2 13 22 11.97 -17.74 66.48 o 3 13 22 2.50 -30.96 68.95 o 4 13 22 0.39 -43.04 77.95 o 5 13 22 6.04 70.05 89.35 o 6 13 22 2.67 108.98 102.37 o 0 14 22 0.11 64.08 145.06 o 1 14 22 488.78 478.60 77.20 o 2 14 22 2.55 -19.51 75.72 o 3 14 22 876.56 806.71 81.70 o 4 14 22 20.62 49.27 92.55 o 5 14 22 650.95 607.39 108.22 o 6 14 22 7.28 48.85 282.66 o 1 15 22 44.07 -18.87 82.75 o 2 15 22 0.02 20.99 85.68 o 3 15 22 102.94 94.47 94.56 o 4 15 22 0.99 38.87 128.85 o 5 15 22 26.94 103.64 164.68 o 0 16 22 3.35 81.58 129.31 o 1 16 22 381.52 390.01 87.56 o 2 16 22 0.15 -30.16 95.77 o 3 16 22 383.60 406.23 185.01 o 1 17 22 126.21 157.03 258.23 o 1 1 23 2014.40 2199.37 70.98 o 2 1 23 6401.26 6383.21 119.95 o 3 1 23 1987.27 2335.49 79.14 o 4 1 23 36.24 116.78 41.65 o 5 1 23 849.00 1000.68 64.70 o 6 1 23 1972.39 2363.10 110.41 o 7 1 23 743.65 954.70 87.39 o 8 1 23 148.07 242.41 96.22 o 9 1 23 161.16 106.13 113.77 o 10 1 23 299.76 589.74 258.23 o 0 2 23 6291.22 5685.65 134.47 o 1 2 23 333.56 351.42 42.04 o 2 2 23 242.97 283.69 38.68 o 3 2 23 86.76 137.93 39.39 o 4 2 23 359.03 448.18 50.54 o 5 2 23 237.51 285.02 52.78 o 6 2 23 27.77 4.62 58.52 o 7 2 23 77.18 43.04 76.11 o 8 2 23 438.49 205.44 101.30 o 9 2 23 75.37 -53.42 110.95 o 10 2 23 61.85 289.64 268.70 o 1 3 23 656.49 786.75 61.18 o 2 3 23 3745.04 3610.76 88.53 o 3 3 23 1604.12 1631.24 72.35 o 4 3 23 2.78 -31.37 46.90 o 5 3 23 590.80 732.12 65.87 o 6 3 23 922.39 1133.32 79.25 o 7 3 23 255.03 226.62 72.57 o 8 3 23 29.77 -4.36 92.69 o 9 3 23 54.42 146.61 127.93 o 10 3 23 344.32 90.73 275.68 o 0 4 23 4949.82 4751.72 158.85 o 1 4 23 1012.27 1167.72 55.71 o 2 4 23 49.66 143.78 42.46 o 3 4 23 676.75 756.16 54.22 o 4 4 23 3041.87 3078.93 106.50 o 5 4 23 817.76 777.88 67.06 o 6 4 23 78.35 64.74 63.90 o 7 4 23 119.44 68.99 71.90 o 8 4 23 467.85 516.93 85.05 o 9 4 23 188.66 301.19 120.11 o 1 5 23 126.38 98.59 40.00 o 2 5 23 947.60 1124.97 57.54 o 3 5 23 433.68 513.39 54.96 o 4 5 23 0.29 4.05 54.79 o 5 5 23 174.39 302.08 60.40 o 6 5 23 297.60 386.37 67.32 o 7 5 23 49.02 106.85 72.82 o 8 5 23 0.60 100.84 84.35 o 9 5 23 5.48 -107.84 107.84 o 0 6 23 4078.79 3877.66 125.46 o 1 6 23 1705.07 1790.55 70.25 o 2 6 23 106.71 143.71 42.70 o 3 6 23 1102.19 1228.41 85.82 o 4 6 23 4983.57 4739.86 120.32 o 5 6 23 929.26 860.58 74.07 o 6 6 23 277.07 277.39 70.95 o 7 6 23 168.45 156.03 76.82 o 8 6 23 574.99 748.32 91.68 o 9 6 23 249.23 246.09 138.16 o 1 7 23 22.13 -18.34 43.57 o 2 7 23 10.01 55.53 44.24 o 3 7 23 26.39 27.23 54.37 o 4 7 23 23.49 -18.87 57.58 o 5 7 23 0.80 86.78 63.86 o 6 7 23 35.41 39.08 68.38 o 7 7 23 3.26 9.69 78.17 o 8 7 23 7.57 52.62 98.67 o 9 7 23 1.46 -142.82 142.82 o 0 8 23 3928.00 3987.14 198.57 o 1 8 23 1365.64 1444.61 67.47 o 2 8 23 66.45 62.98 49.50 o 3 8 23 798.19 728.16 67.51 o 4 8 23 1355.95 1510.58 83.29 o 5 8 23 470.42 422.36 76.07 o 6 8 23 4.14 11.12 71.84 o 7 8 23 232.49 376.03 85.57 o 8 8 23 863.15 791.52 105.23 o 9 8 23 186.01 192.19 146.36 o 1 9 23 147.65 104.60 50.68 o 2 9 23 447.08 562.99 58.37 o 3 9 23 214.11 272.91 63.92 o 4 9 23 13.65 45.68 63.88 o 5 9 23 82.42 140.13 76.83 o 6 9 23 89.14 171.96 85.34 o 7 9 23 67.28 -5.05 90.94 o 8 9 23 34.64 66.08 133.69 o 0 10 23 2167.32 2167.45 119.72 o 1 10 23 467.88 455.29 58.29 o 2 10 23 96.96 128.24 55.99 o 3 10 23 384.94 494.53 61.30 o 4 10 23 540.11 482.59 69.88 o 5 10 23 275.32 306.23 86.61 o 6 10 23 0.01 -89.75 89.75 o 7 10 23 116.19 224.18 106.23 o 8 10 23 454.59 205.78 218.10 o 1 11 23 669.15 590.19 71.87 o 2 11 23 828.52 971.98 73.72 o 3 11 23 325.20 281.97 62.81 o 4 11 23 30.99 15.64 71.08 o 5 11 23 124.13 166.82 81.18 o 6 11 23 500.26 599.49 104.73 o 7 11 23 217.56 78.80 130.27 o 0 12 23 35.77 150.50 93.75 o 1 12 23 20.26 151.55 69.06 o 2 12 23 33.95 59.66 64.56 o 3 12 23 76.80 23.13 64.57 o 4 12 23 279.24 324.64 79.41 o 5 12 23 34.33 34.79 92.37 o 6 12 23 10.35 11.65 111.90 o 1 13 23 448.73 357.26 74.43 o 2 13 23 957.52 987.86 91.86 o 3 13 23 281.66 192.74 72.69 o 4 13 23 32.20 96.47 82.68 o 5 13 23 165.60 140.25 97.50 o 6 13 23 484.02 416.16 179.24 o 0 14 23 80.89 -7.35 106.59 o 1 14 23 0.34 -76.72 76.72 o 2 14 23 29.24 111.12 77.21 o 3 14 23 2.90 -84.65 84.65 o 4 14 23 2.53 -49.98 95.50 o 5 14 23 9.97 177.87 247.76 o 6 14 23 0.45 -258.23 272.19 o 1 15 23 280.81 274.16 86.98 o 2 15 23 651.72 830.33 88.44 o 3 15 23 235.22 331.27 98.08 o 4 15 23 10.23 -27.92 237.29 o 5 15 23 126.08 80.26 307.08 o 0 16 23 55.24 -74.56 130.81 o 1 16 23 52.09 -93.67 93.67 o 2 16 23 0.82 -10.96 132.94 o 1 17 23 70.41 -17.45 268.70 o 0 0 24 9921.58 8940.31 366.41 o 1 0 24 943.33 996.97 75.15 o 2 0 24 49.56 78.94 55.04 o 3 0 24 45.25 87.78 57.45 o 4 0 24 3023.94 3015.13 117.11 o 5 0 24 17.14 122.08 83.21 o 6 0 24 0.18 24.37 91.23 o 7 0 24 25.78 13.27 124.59 o 8 0 24 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1 5 34 443.59 339.55 100.21 o 2 5 34 11.52 8.39 130.96 o 3 5 34 360.70 94.23 133.14 o 4 5 34 0.11 -28.12 186.73 o 0 6 34 0.01 -140.63 155.51 o 1 6 34 5.36 21.74 117.48 o 2 6 34 1.12 118.71 116.65 o 3 6 34 30.58 79.29 159.88 o 4 6 34 11.06 52.34 237.29 o 1 7 34 457.73 374.08 165.45 o 2 7 34 17.95 187.83 163.74 o 3 7 34 337.57 280.87 164.08 o 1 8 34 33.75 -97.71 209.37 o 2 8 34 2.32 45.36 261.72 o 2 9 34 13.18 164.01 272.19 o 1 1 35 123.76 85.99 111.08 o 2 1 35 565.57 490.99 119.95 o 3 1 35 161.85 185.51 128.00 o 4 1 35 1.21 328.02 251.25 o 0 2 35 59.35 -34.90 181.46 o 1 2 35 80.95 -98.52 112.54 o 2 2 35 18.22 94.36 120.73 o 3 2 35 15.57 174.73 168.92 o 4 2 35 131.41 129.11 275.68 o 5 2 35 24.51 272.19 282.66 o 1 3 35 104.45 98.53 116.63 o 2 3 35 281.81 241.32 105.81 o 3 3 35 62.51 35.99 172.51 o 4 3 35 0.91 -111.67 261.72 o 0 4 35 461.96 212.22 159.88 o 1 4 35 150.05 94.29 123.90 o 2 4 35 0.02 -50.96 218.29 o 3 4 35 100.02 -50.94 171.48 o 1 5 35 42.63 -129.45 129.45 o 2 5 35 67.26 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1 2 37 39.65 136.09 275.68 o 2 2 37 9.31 125.62 268.70 o 1 3 37 101.49 -45.36 240.78 o 0 4 37 149.13 129.11 282.66 o