#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:52:51 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180926 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/06/2200673.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200673_Fobs loop_ _publ_author_name 'Wang, Wenguo' 'Huang, Deguang' 'Zhu, Hongping' 'Chen, Changneng' 'Liu, Qiutian' _publ_section_title ; Monoclinic form of dichlorobis(quinoline-N)cobalt(II) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m587 _journal_page_last m588 _journal_volume 57 _journal_year 2001 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yac' _symmetry_space_group_name_H-M 'P 1 2/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.174 _cell_angle_gamma 90.000 _cell_length_a 7.7864 _cell_length_b 7.0874 _cell_length_c 14.5616 _exptl_crystal_F_000 414.00 _reflns_d_resolution_high 0.8404 _cod_data_source_file cv6072Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 120.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9739.65 9596.04 269.08 o 4 0 0 2650.19 2806.95 81.49 o 6 0 0 3.02 4.50 3.90 o 8 0 0 546.46 560.00 20.67 o 0 1 0 4743.02 4013.85 84.56 o 1 1 0 3368.03 3482.35 59.57 o 2 1 0 14575.07 13699.10 225.22 o 3 1 0 1568.05 1485.90 31.42 o 4 1 0 510.29 582.84 13.97 o 5 1 0 638.91 624.83 15.00 o 6 1 0 653.18 681.32 16.40 o 7 1 0 44.43 42.37 5.58 o 8 1 0 9.35 9.01 5.10 o 9 1 0 50.80 38.56 6.60 o 0 2 0 3592.33 3563.83 74.00 o 1 2 0 410.59 399.47 7.26 o 2 2 0 7.40 14.62 2.05 o 3 2 0 1360.00 1386.59 21.42 o 4 2 0 659.12 717.72 13.78 o 5 2 0 307.13 312.66 8.84 o 6 2 0 176.20 184.10 11.75 o 7 2 0 206.58 168.94 9.69 o 8 2 0 16.71 10.42 5.23 o 9 2 0 0.28 1.89 5.36 o 0 3 0 806.42 857.24 19.65 o 1 3 0 62.52 56.80 2.39 o 2 3 0 1149.00 1048.11 19.60 o 3 3 0 221.52 199.93 5.54 o 4 3 0 169.24 194.69 9.67 o 5 3 0 2.81 5.53 2.79 o 6 3 0 127.29 132.78 5.93 o 7 3 0 16.88 17.41 5.40 o 8 3 0 12.64 10.55 6.00 o 0 4 0 65.17 84.54 4.18 o 1 4 0 276.83 238.38 7.04 o 2 4 0 2110.07 2170.45 38.53 o 3 4 0 259.63 262.90 7.45 o 4 4 0 143.01 139.88 4.83 o 5 4 0 310.93 322.17 9.98 o 6 4 0 139.45 151.82 6.61 o 7 4 0 58.40 61.80 7.29 o 8 4 0 15.21 23.63 6.43 o 0 5 0 1464.24 1471.26 32.59 o 1 5 0 0.35 0.65 2.10 o 2 5 0 359.95 358.61 8.62 o 3 5 0 4.10 3.78 2.37 o 4 5 0 690.15 727.35 14.96 o 5 5 0 14.05 11.04 3.53 o 6 5 0 20.99 25.21 4.11 o 7 5 0 7.85 13.68 6.09 o 0 6 0 236.25 233.49 12.05 o 1 6 0 333.73 324.73 8.16 o 2 6 0 26.91 26.09 3.56 o 3 6 0 66.15 66.36 5.23 o 4 6 0 111.29 108.68 5.13 o 5 6 0 97.54 108.50 8.94 o 6 6 0 0.11 0.27 3.40 o 1 7 0 142.63 141.92 6.93 o 2 7 0 1.69 -2.46 3.19 o 3 7 0 77.70 79.46 4.38 o 4 7 0 252.05 266.56 13.70 o 5 7 0 3.32 7.59 3.64 o 0 8 0 7.33 3.60 5.19 o 1 8 0 7.89 7.14 4.16 o 2 8 0 218.15 224.45 9.22 o -7 0 1 66.90 53.01 5.83 o -5 0 1 1044.69 1044.73 32.81 o -3 0 1 1236.98 1173.27 35.77 o -1 0 1 3833.40 3799.91 107.99 o 1 0 1 4509.97 4624.49 130.90 o 3 0 1 697.52 650.24 21.27 o 5 0 1 832.52 859.32 27.88 o 7 0 1 110.00 97.14 7.12 o -9 1 1 0.35 0.43 4.98 o -8 1 1 46.33 43.19 6.13 o -7 1 1 81.69 71.88 6.73 o -6 1 1 5.44 2.53 2.76 o -5 1 1 3.99 -0.64 2.33 o -4 1 1 8046.28 7747.37 154.51 o -3 1 1 131.93 134.24 4.88 o -2 1 1 6671.23 6424.65 106.52 o -1 1 1 283.65 293.27 6.33 o 0 1 1 3119.33 3041.95 51.14 o 1 1 1 850.86 879.07 13.88 o 2 1 1 5895.08 5959.60 86.47 o 3 1 1 831.50 877.00 16.16 o 4 1 1 1674.54 1776.73 90.07 o 5 1 1 17.72 16.67 3.53 o 6 1 1 278.09 274.11 8.40 o 7 1 1 70.96 54.85 6.05 o 8 1 1 296.78 296.96 13.64 o 9 1 1 1.23 6.73 5.96 o -8 2 1 0.33 -1.24 4.67 o -7 2 1 112.29 98.00 7.68 o -6 2 1 1197.09 1233.01 39.20 o -5 2 1 332.95 304.56 8.67 o -4 2 1 65.50 70.27 3.79 o -3 2 1 666.72 630.97 21.65 o -2 2 1 4411.05 4395.07 73.44 o -1 2 1 665.99 654.20 10.83 o 0 2 1 780.07 819.29 13.17 o 1 2 1 839.82 815.80 13.13 o 2 2 1 4453.40 4421.76 64.65 o 3 2 1 314.35 290.89 6.61 o 4 2 1 50.63 43.52 3.07 o 5 2 1 67.09 64.44 3.45 o 6 2 1 647.54 671.25 23.63 o 7 2 1 75.74 74.15 6.86 o 8 2 1 0.20 2.83 4.50 o -8 3 1 46.54 23.46 5.66 o -7 3 1 192.79 181.55 10.55 o -6 3 1 15.64 15.84 3.30 o -5 3 1 142.48 140.60 7.21 o -4 3 1 30.90 30.84 2.68 o -3 3 1 300.71 288.66 8.77 o -2 3 1 2587.49 2635.50 46.07 o -1 3 1 676.60 680.47 13.96 o 0 3 1 321.96 350.16 6.91 o 1 3 1 1158.58 1191.01 18.69 o 2 3 1 15.33 3.14 1.55 o 3 3 1 999.25 1047.44 41.55 o 4 3 1 90.67 94.70 3.80 o 5 3 1 114.91 123.13 5.56 o 6 3 1 275.83 282.08 12.91 o 7 3 1 54.48 58.20 6.69 o 8 3 1 16.01 10.64 5.49 o -8 4 1 0.66 -4.20 4.20 o -7 4 1 17.26 16.43 5.36 o -6 4 1 243.75 261.20 8.98 o -5 4 1 0.49 -1.26 2.74 o -4 4 1 153.08 151.92 6.24 o -3 4 1 44.23 42.47 3.12 o -2 4 1 431.91 428.82 9.54 o -1 4 1 0.70 -0.46 1.55 o 0 4 1 113.37 93.93 3.12 o 1 4 1 1.79 0.09 1.67 o 2 4 1 784.74 810.66 15.90 o 3 4 1 87.98 77.85 4.44 o 4 4 1 162.52 158.45 5.10 o 5 4 1 5.35 1.21 2.96 o 6 4 1 253.27 276.64 9.23 o 7 4 1 45.57 43.75 6.39 o -7 5 1 7.35 -1.24 4.63 o -6 5 1 38.06 36.75 4.28 o -5 5 1 215.21 215.99 9.46 o -4 5 1 130.28 131.21 6.89 o -3 5 1 134.25 129.04 5.58 o -2 5 1 579.19 572.20 12.17 o -1 5 1 373.85 378.96 8.85 o 0 5 1 239.13 221.78 5.15 o 1 5 1 519.81 541.97 11.56 o 2 5 1 115.65 103.45 4.25 o 3 5 1 329.61 332.65 8.24 o 4 5 1 379.43 388.44 9.32 o 5 5 1 440.42 450.26 12.88 o 6 5 1 1.90 7.25 7.78 o 7 5 1 30.20 22.00 6.26 o -6 6 1 22.76 17.22 3.88 o -5 6 1 0.22 -0.96 3.00 o -4 6 1 446.36 422.08 10.13 o -3 6 1 112.67 111.01 8.24 o -2 6 1 0.52 -1.66 2.32 o -1 6 1 117.68 119.33 4.71 o 0 6 1 1098.52 1123.72 27.26 o 1 6 1 59.17 56.84 3.53 o 2 6 1 19.75 23.71 2.98 o 3 6 1 101.96 91.40 5.85 o 4 6 1 258.19 296.80 9.86 o 5 6 1 54.25 47.21 4.70 o 6 6 1 3.06 3.44 4.52 o -5 7 1 35.36 34.45 4.58 o -4 7 1 42.76 39.79 5.61 o -3 7 1 48.32 51.24 3.88 o -2 7 1 150.71 145.87 7.05 o -1 7 1 17.75 9.80 3.66 o 0 7 1 30.82 28.87 4.11 o 1 7 1 5.80 5.57 3.74 o 2 7 1 194.34 193.47 11.45 o 3 7 1 26.66 25.49 3.25 o 4 7 1 62.63 72.40 5.23 o 5 7 1 79.03 85.27 6.03 o -2 8 1 7.75 12.54 4.38 o -1 8 1 58.89 58.51 5.50 o 0 8 1 49.29 45.86 5.18 o 1 8 1 19.11 26.46 4.52 o 2 8 1 0.21 1.31 8.77 o -6 0 2 18.12 21.87 4.33 o -4 0 2 2039.66 1942.27 57.47 o -2 0 2 11260.53 10684.14 299.32 o 0 0 2 196.89 246.10 9.48 o 2 0 2 148.06 127.80 4.47 o 4 0 2 5889.82 5890.74 121.14 o 6 0 2 1.11 4.89 3.99 o 8 0 2 114.01 132.66 8.62 o -9 1 2 43.43 43.49 6.91 o -8 1 2 34.65 27.71 5.79 o -7 1 2 83.87 82.22 6.78 o -6 1 2 5.57 4.60 2.82 o -5 1 2 488.60 478.37 12.14 o -4 1 2 1729.98 1665.59 38.99 o -3 1 2 769.08 712.56 19.47 o -2 1 2 84.27 70.18 3.44 o -1 1 2 1751.06 1883.03 39.90 o 0 1 2 1263.31 1398.33 24.43 o 1 1 2 1398.90 1439.18 41.41 o 2 1 2 1590.62 1521.94 23.14 o 3 1 2 625.48 605.27 11.73 o 4 1 2 86.80 93.37 3.50 o 5 1 2 829.32 896.19 16.85 o 6 1 2 187.90 173.82 6.52 o 7 1 2 83.29 72.35 6.78 o 8 1 2 6.64 2.74 4.46 o 9 1 2 40.38 34.48 6.30 o -8 2 2 209.92 201.88 10.98 o -7 2 2 48.79 34.65 5.45 o -6 2 2 1060.53 1001.20 32.68 o -5 2 2 8.59 9.09 4.12 o -4 2 2 2410.26 2373.99 49.08 o -3 2 2 639.52 654.03 12.59 o -2 2 2 175.18 181.67 5.29 o -1 2 2 1038.37 999.26 18.06 o 0 2 2 220.90 212.42 4.55 o 1 2 2 594.64 581.35 9.83 o 2 2 2 1385.51 1446.26 22.55 o 3 2 2 639.60 649.21 12.64 o 4 2 2 1364.11 1403.70 34.86 o 5 2 2 38.85 39.77 2.79 o 6 2 2 79.08 85.13 7.38 o 7 2 2 179.60 170.83 9.86 o 8 2 2 24.91 25.78 5.96 o -8 3 2 95.60 65.96 7.03 o -7 3 2 143.61 127.51 8.66 o -6 3 2 792.75 803.61 27.45 o -5 3 2 11.90 15.05 4.63 o -4 3 2 0.73 0.41 2.79 o -3 3 2 244.87 229.71 10.59 o -2 3 2 3665.63 3503.51 51.70 o -1 3 2 439.95 429.21 7.82 o 0 3 2 533.55 594.75 10.18 o 1 3 2 294.84 290.04 5.83 o 2 3 2 4008.70 4058.31 59.65 o 3 3 2 226.59 224.19 5.42 o 4 3 2 1.26 0.39 2.00 o 5 3 2 2.22 2.99 2.67 o 6 3 2 328.49 387.50 16.17 o 7 3 2 60.71 62.02 6.60 o 8 3 2 3.14 -0.64 4.63 o -8 4 2 80.79 65.28 7.38 o -7 4 2 49.61 57.86 6.69 o -6 4 2 136.31 123.83 6.00 o -5 4 2 257.07 239.42 6.68 o -4 4 2 111.42 106.89 4.26 o -3 4 2 444.72 462.24 10.23 o -2 4 2 331.66 303.10 7.45 o -1 4 2 1180.85 1222.60 19.33 o 0 4 2 1693.42 1733.79 26.62 o 1 4 2 1149.01 1125.41 20.19 o 2 4 2 529.04 512.93 15.17 o 3 4 2 418.19 411.56 14.87 o 4 4 2 35.84 34.28 2.97 o 5 4 2 140.41 150.05 6.47 o 6 4 2 356.55 382.65 16.08 o 7 4 2 20.85 22.39 5.66 o 8 4 2 3.53 -0.73 4.76 o -7 5 2 1.14 0.17 4.85 o -6 5 2 1.02 4.75 3.35 o -5 5 2 82.91 79.12 5.21 o -4 5 2 167.68 165.27 5.51 o -3 5 2 62.70 64.56 3.64 o -2 5 2 139.70 124.87 4.67 o -1 5 2 0.10 -1.59 2.09 o 0 5 2 1541.75 1534.16 23.96 o 1 5 2 0.54 -0.86 2.10 o 2 5 2 264.52 270.15 7.08 o 3 5 2 0.65 0.39 2.24 o 4 5 2 678.60 677.05 17.28 o 5 5 2 6.72 5.20 3.35 o 6 5 2 213.19 213.59 11.58 o 7 5 2 7.92 6.99 5.06 o -6 6 2 2.72 2.58 3.77 o -5 6 2 50.99 54.04 6.78 o -4 6 2 14.95 12.52 2.93 o -3 6 2 17.12 17.41 3.04 o -2 6 2 14.57 14.88 2.72 o -1 6 2 269.80 257.94 7.06 o 0 6 2 658.48 632.86 22.65 o 1 6 2 743.22 776.74 15.78 o 2 6 2 306.39 302.52 7.90 o 3 6 2 350.23 361.88 11.45 o 4 6 2 384.49 394.55 16.17 o 5 6 2 195.85 195.66 7.91 o 6 6 2 14.39 12.14 4.22 o -5 7 2 19.57 22.19 4.23 o -4 7 2 125.94 130.94 5.44 o -3 7 2 115.93 112.39 7.35 o -2 7 2 2.59 1.47 3.38 o -1 7 2 67.51 70.44 5.53 o 0 7 2 154.96 145.49 7.04 o 1 7 2 220.52 209.55 8.46 o 2 7 2 174.78 151.70 7.72 o 3 7 2 406.99 409.57 10.11 o 4 7 2 33.81 44.14 5.75 o 5 7 2 63.39 69.75 5.50 o -2 8 2 126.00 127.08 7.14 o -1 8 2 4.77 9.75 4.16 o 0 8 2 0.95 2.45 5.15 o 1 8 2 9.27 15.08 4.50 o 2 8 2 157.05 174.06 8.23 o -7 0 3 40.79 33.02 5.28 o -5 0 3 518.16 496.52 17.80 o -3 0 3 651.99 614.81 20.42 o -1 0 3 1336.77 1446.47 43.10 o 1 0 3 3019.26 3075.95 88.35 o 3 0 3 860.92 801.51 25.69 o 5 0 3 738.82 775.26 25.69 o 7 0 3 28.69 29.89 5.28 o -9 1 3 2.41 0.94 4.89 o -8 1 3 221.91 212.17 11.24 o -7 1 3 25.62 19.26 5.23 o -6 1 3 1.28 2.01 3.15 o -5 1 3 3.95 3.10 2.56 o -4 1 3 522.28 472.24 11.92 o -3 1 3 180.76 179.98 12.01 o -2 1 3 246.12 268.53 11.67 o -1 1 3 202.42 203.77 5.06 o 0 1 3 10888.26 10057.22 165.85 o 1 1 3 73.48 71.79 2.88 o 2 1 3 28.05 27.96 1.86 o 3 1 3 342.03 359.90 7.76 o 4 1 3 1201.81 1172.52 21.17 o 5 1 3 6.69 6.87 2.72 o 6 1 3 20.45 17.05 3.09 o 7 1 3 53.76 52.67 6.39 o 8 1 3 285.65 308.54 14.07 o 9 1 3 0.29 -4.76 4.76 o -8 2 3 102.65 90.88 8.06 o -7 2 3 82.18 77.11 7.12 o -6 2 3 131.04 113.14 7.81 o -4 2 3 63.69 63.00 3.80 o -3 2 3 964.50 994.97 18.25 o -2 2 3 5205.10 5254.13 87.68 o -1 2 3 777.44 777.95 21.36 o 0 2 3 1311.96 1374.26 24.26 o 1 2 3 521.24 506.77 8.83 o 2 2 3 1505.12 1473.30 22.66 o 3 2 3 529.79 506.50 8.88 o 4 2 3 160.53 156.14 6.21 o 5 2 3 169.69 172.87 8.33 o 7 2 3 71.17 87.66 7.98 o 8 2 3 0.80 -0.86 4.93 o -8 3 3 98.58 67.72 7.46 o -7 3 3 81.43 83.46 7.55 o -6 3 3 510.93 474.05 18.18 o -5 3 3 245.21 225.30 10.81 o -4 3 3 7.26 10.04 2.89 o -3 3 3 761.77 799.83 15.12 o -2 3 3 884.07 850.13 15.87 o -1 3 3 1165.32 1159.41 48.65 o 0 3 3 108.30 122.37 3.81 o 1 3 3 552.02 551.32 9.61 o 2 3 3 2481.17 2627.97 39.28 o 3 3 3 452.66 435.69 8.02 o 4 3 3 31.73 33.53 3.38 o 5 3 3 92.95 94.80 5.02 o 6 3 3 179.42 185.67 10.46 o 7 3 3 94.80 98.17 8.15 o 8 3 3 1.00 -0.99 4.55 o -8 4 3 19.57 16.81 5.96 o -7 4 3 2.13 -0.56 3.43 o -6 4 3 314.01 336.07 10.52 o -5 4 3 0.04 0.40 2.26 o -4 4 3 933.07 942.85 18.45 o -3 4 3 216.15 215.20 6.15 o -2 4 3 2673.73 2730.27 48.00 o -1 4 3 58.79 61.24 3.30 o 0 4 3 783.59 825.65 12.16 o 1 4 3 27.78 26.30 2.18 o 2 4 3 825.42 808.50 13.46 o 3 4 3 58.32 55.25 3.20 o 4 4 3 276.54 307.07 9.55 o 5 4 3 1.66 -0.81 4.89 o 6 4 3 261.67 292.46 13.72 o 7 4 3 70.08 70.21 7.46 o -7 5 3 3.97 7.39 3.73 o -6 5 3 19.87 19.41 3.71 o -5 5 3 257.88 233.95 8.50 o -4 5 3 798.46 795.58 16.27 o -3 5 3 499.44 493.79 14.47 o -2 5 3 95.29 95.87 4.23 o -1 5 3 1130.98 1139.00 34.64 o 0 5 3 1041.37 1029.07 16.82 o 1 5 3 676.38 665.14 13.66 o 2 5 3 188.59 189.82 5.78 o 3 5 3 94.39 95.39 4.24 o 4 5 3 92.07 102.83 5.53 o 5 5 3 230.19 246.30 8.72 o 6 5 3 54.56 57.73 6.73 o 7 5 3 42.10 53.10 7.21 o -6 6 3 13.18 13.19 4.18 o -5 6 3 8.30 10.29 4.61 o -4 6 3 310.46 303.66 8.23 o -3 6 3 48.74 42.76 3.50 o -2 6 3 19.39 11.82 2.68 o -1 6 3 173.89 170.48 5.60 o 0 6 3 358.47 377.31 11.69 o 1 6 3 362.20 385.29 11.33 o 2 6 3 0.71 0.03 3.06 o 3 6 3 143.62 158.55 5.55 o 4 6 3 499.85 509.64 14.15 o 5 6 3 12.38 14.71 3.76 o 6 6 3 0.50 7.98 5.19 o -4 7 3 17.55 12.02 3.10 o -3 7 3 75.43 74.65 4.21 o -2 7 3 271.14 272.33 9.91 o -1 7 3 148.67 140.75 6.97 o 0 7 3 75.40 65.18 5.32 o 1 7 3 40.75 43.11 4.74 o 2 7 3 107.35 103.10 6.21 o 3 7 3 20.15 23.70 3.97 o 4 7 3 0.55 4.23 3.84 o -2 8 3 8.73 1.95 4.61 o -1 8 3 124.04 112.93 9.61 o 0 8 3 4.51 6.26 3.90 o 1 8 3 82.34 69.44 5.79 o 2 8 3 1.72 7.51 3.95 o -6 0 4 81.18 82.13 6.43 o -4 0 4 1385.68 1573.38 47.74 o -2 0 4 361.65 366.91 13.55 o 0 0 4 5228.72 5224.81 148.10 o 2 0 4 117.17 118.07 6.60 o 4 0 4 4890.09 4855.24 138.66 o 6 0 4 178.16 165.81 9.09 o 8 0 4 237.90 246.87 12.48 o -8 1 4 5.09 -1.03 4.50 o -7 1 4 60.59 57.86 6.35 o -6 1 4 263.55 253.81 8.07 o -5 1 4 411.13 413.34 11.03 o -4 1 4 233.66 222.31 7.00 o -3 1 4 575.77 500.29 12.27 o -2 1 4 48.53 36.67 4.07 o -1 1 4 883.74 855.84 19.05 o 0 1 4 2136.96 2216.45 38.01 o 1 1 4 1614.76 1624.30 34.46 o 2 1 4 1599.21 1578.93 27.67 o 3 1 4 427.00 431.20 7.71 o 4 1 4 3.58 2.44 1.91 o 5 1 4 673.13 715.54 17.05 o 6 1 4 323.97 312.41 9.35 o 7 1 4 118.24 126.22 8.53 o 8 1 4 4.81 7.33 5.23 o -8 2 4 68.09 69.91 7.42 o -7 2 4 88.69 79.86 7.21 o -6 2 4 27.72 20.11 5.06 o -5 2 4 69.06 63.07 4.17 o -4 2 4 534.15 560.87 24.94 o -3 2 4 401.65 401.25 10.37 o -2 2 4 1645.44 1785.36 31.17 o -1 2 4 279.42 263.27 8.63 o 0 2 4 3276.12 3283.49 55.52 o 1 2 4 34.90 30.37 2.88 o 2 2 4 1300.08 1311.11 20.40 o 3 2 4 542.69 529.08 9.26 o 4 2 4 942.99 968.10 18.00 o 5 2 4 24.58 21.24 3.12 o 6 2 4 96.02 96.76 7.55 o 8 2 4 0.75 6.26 5.15 o -8 3 4 14.04 22.86 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