#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200690.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200690_Fobs loop_ _publ_author_name 'Ravikumar, B.' 'Sridhar, B.' 'Rajaram, R. K.' _publ_section_title ; DL-Phenylalaninium dihydrogen phosphate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1078 _journal_page_last o1080 _journal_volume 57 _journal_year 2001 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yc' _symmetry_space_group_name_H-M 'P 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.726 _cell_angle_gamma 90.000 _cell_length_a 13.8990 _cell_length_b 9.9560 _cell_length_c 9.0508 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8420 _[local]_cod_data_source_file na6096Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DL-PHENYLALANINE PHOSPHATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 154.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -15 0 0 52.76 58.81 4.30 o -14 0 0 113.57 119.75 4.97 o -13 0 0 34.39 33.74 3.41 o -12 0 0 36.54 40.92 2.94 o -11 0 0 143.69 144.44 4.33 o -10 0 0 94.39 100.83 3.42 o -9 0 0 121.73 119.15 3.42 o -8 0 0 69.34 65.23 2.55 o -7 0 0 227.86 244.40 3.93 o -6 0 0 253.94 258.07 3.72 o -5 0 0 1094.16 1007.68 9.02 o -4 0 0 6303.52 5745.73 22.78 o -3 0 0 23761.63 22898.30 164.09 o -2 0 0 268.87 248.03 2.54 o -1 0 0 6867.92 6567.81 49.73 o 1 0 0 6870.16 6806.33 50.49 o 2 0 0 268.50 242.68 2.34 o 3 0 0 23751.14 23160.53 165.09 o 4 0 0 6323.62 5775.94 22.83 o 5 0 0 1096.57 1044.29 9.15 o 6 0 0 253.18 251.80 3.67 o 7 0 0 223.87 248.81 3.94 o 8 0 0 69.48 64.37 2.50 o 9 0 0 124.72 113.88 3.39 o 10 0 0 92.09 88.05 3.40 o 11 0 0 140.74 136.76 4.20 o 12 0 0 39.50 40.13 3.07 o 13 0 0 34.23 38.52 3.23 o 14 0 0 111.50 117.38 4.80 o 15 0 0 52.79 64.47 4.31 o -15 1 0 2.20 -1.78 4.58 o -14 1 0 50.89 56.65 4.04 o -13 1 0 303.36 316.00 7.10 o -12 1 0 405.26 410.32 7.07 o -11 1 0 127.63 129.33 4.17 o -10 1 0 208.00 216.47 4.65 o -9 1 0 81.17 71.88 2.92 o -8 1 0 205.77 220.41 4.09 o -7 1 0 10.43 9.60 1.63 o -6 1 0 322.03 355.51 4.31 o -5 1 0 533.67 600.72 6.33 o -4 1 0 94.02 98.88 2.25 o -3 1 0 24.37 23.58 1.41 o -2 1 0 3559.61 3530.52 13.43 o -1 1 0 33.61 26.99 1.06 o 0 1 0 45.06 38.56 1.00 o 1 1 0 32.52 21.70 1.05 o 2 1 0 3563.53 3525.56 13.46 o 3 1 0 20.87 20.57 1.36 o 4 1 0 96.18 99.21 2.22 o 5 1 0 533.11 591.89 5.76 o 6 1 0 320.87 349.47 4.30 o 7 1 0 9.55 10.22 1.54 o 8 1 0 211.18 225.26 4.15 o 9 1 0 77.09 69.16 2.83 o 10 1 0 207.33 201.48 4.46 o 11 1 0 126.96 126.56 4.06 o 12 1 0 404.08 425.88 7.07 o 13 1 0 303.01 308.19 6.98 o 14 1 0 51.03 62.58 3.97 o 15 1 0 2.31 5.73 4.62 o -15 2 0 36.83 38.00 3.89 o -14 2 0 129.91 147.15 5.55 o -13 2 0 90.95 97.58 4.52 o -12 2 0 100.11 107.71 4.03 o -11 2 0 466.62 477.33 7.24 o -10 2 0 72.08 80.62 3.28 o -9 2 0 23.89 25.04 2.31 o -8 2 0 374.32 345.74 5.13 o -7 2 0 542.42 554.69 5.94 o -6 2 0 71.60 74.33 2.26 o -5 2 0 37.36 37.31 1.83 o -4 2 0 494.65 459.67 4.53 o -3 2 0 6834.26 6708.00 24.16 o -2 2 0 570.99 513.71 5.31 o -1 2 0 3306.40 3228.10 13.93 o 0 2 0 5321.71 5636.82 18.20 o 1 2 0 3312.33 3194.75 13.84 o 2 2 0 571.91 528.72 5.37 o 3 2 0 6827.18 6759.51 24.34 o 4 2 0 490.49 435.07 4.41 o 5 2 0 40.58 41.09 1.82 o 6 2 0 72.05 65.73 2.27 o 7 2 0 535.71 541.98 5.85 o 8 2 0 376.84 341.31 5.08 o 9 2 0 22.99 17.94 2.27 o 10 2 0 71.78 76.38 3.20 o 11 2 0 463.37 455.48 7.16 o 12 2 0 103.07 106.78 4.25 o 13 2 0 90.93 96.66 4.45 o 14 2 0 128.38 148.29 5.48 o 15 2 0 38.22 39.63 3.89 o -15 3 0 11.16 13.70 3.23 o -14 3 0 39.00 47.19 3.90 o -13 3 0 98.26 124.65 4.94 o -12 3 0 15.09 18.41 2.59 o -11 3 0 69.63 65.93 3.44 o -10 3 0 609.36 621.21 7.91 o -9 3 0 235.95 223.86 4.72 o -8 3 0 393.70 401.71 5.62 o -7 3 0 775.74 752.64 7.59 o -6 3 0 526.24 516.40 5.52 o -5 3 0 1165.44 1150.20 10.74 o -4 3 0 189.17 184.81 3.04 o -3 3 0 183.86 218.05 3.09 o -2 3 0 2675.56 2441.40 14.97 o -1 3 0 8496.08 8713.14 28.20 o 0 3 0 851.49 839.72 8.38 o 1 3 0 8475.14 8811.38 28.43 o 2 3 0 2689.99 2475.91 15.07 o 3 3 0 181.65 215.15 3.11 o 4 3 0 187.08 177.78 3.03 o 5 3 0 1167.27 1140.84 10.70 o 6 3 0 525.69 522.83 5.57 o 7 3 0 779.49 753.57 7.62 o 8 3 0 395.56 417.59 5.82 o 9 3 0 233.15 225.68 4.71 o 10 3 0 612.36 641.92 8.06 o 11 3 0 69.72 71.93 3.43 o 12 3 0 15.27 17.01 2.53 o 13 3 0 98.73 107.13 4.79 o 14 3 0 38.38 40.74 3.86 o 15 3 0 11.16 14.84 3.40 o -14 4 0 80.57 78.21 4.85 o -13 4 0 128.44 152.71 5.31 o -12 4 0 125.68 131.63 5.00 o -11 4 0 562.17 573.17 8.20 o -10 4 0 134.98 143.47 4.25 o -9 4 0 221.72 217.77 4.83 o -8 4 0 556.02 558.44 6.88 o -7 4 0 524.99 513.82 6.25 o -6 4 0 28.38 27.53 2.02 o -5 4 0 601.74 655.94 6.67 o -4 4 0 47.96 55.14 2.12 o -3 4 0 461.10 505.60 4.95 o -2 4 0 174.96 164.16 2.92 o -1 4 0 3678.64 3951.39 21.11 o 0 4 0 6092.82 7179.07 28.58 o 1 4 0 3667.16 4001.75 21.23 o 2 4 0 174.48 164.80 2.89 o 3 4 0 454.70 491.46 4.91 o 4 4 0 45.97 44.80 1.98 o 5 4 0 595.02 657.85 6.66 o 6 4 0 29.88 28.73 2.02 o 7 4 0 523.74 507.57 6.22 o 8 4 0 556.00 545.83 6.82 o 9 4 0 222.61 217.44 4.80 o 10 4 0 137.28 134.24 4.33 o 11 4 0 562.45 559.74 8.24 o 12 4 0 124.46 126.73 4.91 o 13 4 0 127.26 134.96 5.42 o 14 4 0 81.22 88.76 4.85 o -14 5 0 10.89 4.51 4.95 o -13 5 0 103.96 120.13 5.12 o -12 5 0 26.61 24.71 3.21 o -11 5 0 10.71 12.69 2.85 o -10 5 0 358.19 365.91 6.59 o -9 5 0 378.16 377.48 6.43 o -8 5 0 118.50 121.93 3.71 o -7 5 0 256.26 254.09 4.79 o -6 5 0 477.74 462.68 5.97 o -5 5 0 685.52 646.00 6.67 o -4 5 0 215.21 209.90 3.82 o -3 5 0 369.79 392.59 4.87 o -2 5 0 529.14 506.61 5.34 o -1 5 0 734.93 720.20 7.15 o 0 5 0 138.88 131.73 2.82 o 1 5 0 728.35 704.84 7.15 o 2 5 0 529.72 488.86 5.30 o 3 5 0 363.59 397.45 4.93 o 4 5 0 211.90 214.66 3.87 o 5 5 0 680.88 650.53 6.73 o 6 5 0 480.59 487.23 6.16 o 7 5 0 258.82 260.79 4.92 o 8 5 0 117.71 114.03 3.76 o 9 5 0 377.45 376.67 6.44 o 10 5 0 360.63 375.36 6.79 o 11 5 0 10.65 8.09 4.29 o 12 5 0 27.44 31.81 3.25 o 13 5 0 103.80 125.52 5.16 o 14 5 0 10.53 6.40 4.86 o -13 6 0 69.42 78.20 4.57 o -12 6 0 47.85 45.07 3.80 o -11 6 0 88.74 88.13 4.56 o -10 6 0 61.14 63.34 3.55 o -9 6 0 144.71 138.90 4.47 o -8 6 0 119.69 118.92 4.05 o -7 6 0 150.19 154.11 4.23 o -6 6 0 67.79 70.10 3.03 o -5 6 0 171.17 173.50 3.98 o -4 6 0 352.49 355.60 5.25 o -3 6 0 37.60 42.17 2.27 o -2 6 0 175.75 174.79 3.74 o -1 6 0 70.57 74.26 2.62 o 0 6 0 208.36 224.79 4.04 o 1 6 0 68.09 69.36 2.52 o 2 6 0 173.90 167.85 3.64 o 3 6 0 38.85 39.54 2.17 o 4 6 0 350.44 349.56 5.29 o 5 6 0 169.76 174.40 4.05 o 6 6 0 69.95 78.47 3.16 o 7 6 0 152.65 144.16 4.15 o 8 6 0 121.40 117.84 4.08 o 9 6 0 146.81 149.69 4.49 o 10 6 0 62.90 65.24 3.52 o 11 6 0 88.50 84.93 4.50 o 12 6 0 48.58 52.97 3.96 o 13 6 0 70.63 75.32 4.72 o -12 7 0 150.43 154.16 6.09 o -11 7 0 137.28 153.58 5.46 o -10 7 0 4.02 3.33 2.75 o -9 7 0 107.11 107.38 4.53 o -8 7 0 288.08 281.84 5.84 o -7 7 0 322.53 348.32 6.24 o -6 7 0 14.68 20.18 2.41 o -5 7 0 5.52 -1.98 3.51 o -4 7 0 150.90 146.12 3.97 o -3 7 0 160.11 157.49 4.02 o -2 7 0 47.03 47.41 2.57 o -1 7 0 58.07 60.21 2.72 o 0 7 0 331.86 319.10 5.15 o 1 7 0 60.14 55.59 2.70 o 2 7 0 47.03 46.73 2.61 o 3 7 0 159.52 154.51 3.90 o 4 7 0 146.72 155.64 4.06 o 5 7 0 5.49 8.67 1.95 o 6 7 0 14.61 16.96 2.32 o 7 7 0 318.08 339.36 6.18 o 8 7 0 283.73 276.10 5.84 o 9 7 0 106.62 114.68 4.65 o 10 7 0 4.30 1.87 4.30 o 11 7 0 135.55 130.19 5.53 o 12 7 0 148.44 154.40 5.83 o -11 8 0 25.50 24.27 3.40 o -10 8 0 36.96 48.48 3.99 o -9 8 0 12.28 16.35 2.77 o -8 8 0 9.00 5.66 4.79 o -7 8 0 299.70 326.04 6.56 o -6 8 0 108.81 100.40 3.57 o -5 8 0 20.37 19.08 2.30 o -4 8 0 23.77 24.67 2.47 o -3 8 0 94.19 84.22 3.29 o -2 8 0 331.31 310.32 5.50 o -1 8 0 136.10 129.14 3.79 o 0 8 0 852.45 888.24 8.80 o 1 8 0 139.06 134.51 3.74 o 2 8 0 329.23 317.65 5.50 o 3 8 0 94.97 94.51 3.44 o 4 8 0 22.73 23.67 2.40 o 5 8 0 20.84 19.80 2.36 o 6 8 0 111.52 106.54 3.82 o 7 8 0 300.16 289.30 6.00 o 8 8 0 9.09 12.14 2.53 o 9 8 0 13.27 12.17 2.82 o 10 8 0 37.94 40.75 3.39 o 11 8 0 25.30 21.57 3.21 o -10 9 0 130.51 128.85 5.59 o -9 9 0 92.19 89.17 4.62 o -8 9 0 9.49 8.47 2.82 o -7 9 0 119.04 114.85 4.62 o -6 9 0 207.95 204.53 5.63 o -5 9 0 46.86 51.58 3.36 o -4 9 0 115.95 110.57 4.00 o -3 9 0 92.12 85.91 3.63 o -2 9 0 39.62 29.74 2.60 o -1 9 0 91.83 91.45 3.56 o 0 9 0 218.35 203.34 4.93 o 1 9 0 89.11 82.40 3.41 o 2 9 0 39.33 28.47 2.58 o 3 9 0 91.42 92.15 3.50 o 4 9 0 112.72 112.40 3.91 o 5 9 0 47.65 57.27 3.41 o 6 9 0 206.48 208.05 5.63 o 7 9 0 115.91 107.57 4.62 o 8 9 0 9.33 -1.24 4.82 o 9 9 0 92.73 103.65 4.79 o 10 9 0 130.27 137.89 5.49 o -8 10 0 53.37 62.30 3.95 o -7 10 0 28.82 29.37 3.35 o -6 10 0 11.01 17.78 2.66 o -5 10 0 3.76 1.52 3.23 o -4 10 0 74.68 80.36 4.06 o -3 10 0 19.94 17.66 2.64 o -2 10 0 103.16 96.36 4.16 o -1 10 0 128.68 123.70 4.57 o 0 10 0 96.41 93.12 4.18 o 1 10 0 130.53 123.21 4.58 o 2 10 0 104.05 99.42 4.23 o 3 10 0 19.14 23.16 2.54 o 4 10 0 74.19 69.01 4.04 o 5 10 0 3.61 2.74 3.76 o 6 10 0 11.15 12.49 2.93 o 7 10 0 29.32 30.58 3.16 o 8 10 0 53.11 54.20 4.10 o -5 11 0 49.15 55.46 4.03 o -4 11 0 61.84 65.84 3.98 o -3 11 0 28.04 32.66 3.38 o -2 11 0 54.47 60.83 3.85 o -1 11 0 81.82 72.96 4.10 o 0 11 0 70.88 71.45 4.12 o 1 11 0 78.21 68.24 4.14 o 2 11 0 55.06 49.30 3.91 o 3 11 0 27.93 30.19 3.41 o 4 11 0 62.66 67.14 4.03 o 5 11 0 49.24 54.20 3.92 o -16 1 1 24.12 23.87 3.37 o -15 1 1 4.25 8.19 2.52 o -14 1 1 25.58 24.53 3.21 o -13 1 1 109.73 108.79 4.01 o -12 1 1 530.94 513.03 7.41 o -11 1 1 45.98 41.89 2.72 o -10 1 1 58.02 56.22 2.74 o -9 1 1 3.35 5.19 1.65 o -8 1 1 21.06 15.87 1.78 o -7 1 1 124.75 121.37 2.83 o -6 1 1 1005.15 967.60 9.24 o -5 1 1 1965.62 1892.39 13.58 o -4 1 1 398.62 355.54 3.62 o -3 1 1 2755.13 2566.47 12.71 o -2 1 1 1363.22 1306.54 7.92 o -1 1 1 283.85 298.54 2.84 o 0 1 1 169.43 162.27 1.69 o 1 1 1 2185.42 2066.01 10.03 o 2 1 1 3444.91 3401.54 14.67 o 3 1 1 3028.32 2854.26 15.05 o 4 1 1 431.22 447.77 4.44 o 5 1 1 1163.32 1095.43 9.83 o 6 1 1 265.59 242.44 3.74 o 7 1 1 124.91 123.72 3.01 o 8 1 1 617.46 603.84 6.59 o 9 1 1 153.73 138.42 3.75 o 10 1 1 30.05 29.20 2.40 o 11 1 1 46.02 39.58 2.82 o 12 1 1 3.63 -3.91 3.91 o 13 1 1 0.79 -3.23 3.89 o 14 1 1 29.23 28.70 3.34 o 15 1 1 18.22 22.36 3.28 o -15 2 1 69.64 70.67 4.25 o -14 2 1 94.83 100.51 4.44 o -13 2 1 15.77 15.26 2.63 o -12 2 1 112.80 104.41 3.89 o -11 2 1 24.92 19.49 2.35 o -10 2 1 344.39 336.67 5.43 o -9 2 1 605.30 590.86 6.63 o -8 2 1 520.17 491.85 5.67 o -7 2 1 355.81 360.35 4.53 o -6 2 1 287.83 283.39 3.76 o -5 2 1 67.35 85.16 2.16 o -4 2 1 351.47 327.04 3.42 o -3 2 1 405.69 423.41 4.15 o -2 2 1 660.65 654.08 5.76 o -1 2 1 2587.68 2645.66 12.62 o 0 2 1 6995.80 7074.37 21.41 o 1 2 1 2008.80 1756.36 10.77 o 2 2 1 1126.47 1055.26 8.95 o 3 2 1 280.33 270.45 3.20 o 4 2 1 129.24 127.72 2.51 o 5 2 1 338.54 336.46 4.11 o 6 2 1 343.55 342.18 4.48 o 7 2 1 90.96 93.43 2.76 o 8 2 1 109.89 106.98 3.11 o 9 2 1 63.70 61.54 2.84 o 10 2 1 144.95 135.26 4.06 o 11 2 1 115.49 114.24 3.87 o 12 2 1 5.07 3.54 4.01 o 13 2 1 41.30 40.05 3.39 o 14 2 1 5.45 8.49 2.77 o -15 3 1 18.38 20.02 2.96 o -14 3 1 65.74 69.39 4.26 o -13 3 1 281.79 263.90 6.37 o -12 3 1 387.82 377.83 6.58 o -11 3 1 60.30 60.80 3.03 o -10 3 1 208.33 190.53 4.34 o -9 3 1 193.30 176.78 3.95 o -8 3 1 83.88 88.12 2.76 o -7 3 1 149.48 136.86 3.07 o -6 3 1 546.61 558.32 5.45 o -5 3 1 89.70 96.32 2.37 o -4 3 1 522.17 470.68 4.71 o -3 3 1 412.52 392.64 3.85 o -2 3 1 876.92 760.17 7.11 o -1 3 1 1103.68 1057.72 9.39 o 0 3 1 1729.28 1592.63 11.47 o 1 3 1 1031.53 1042.26 9.56 o 2 3 1 4491.62 4498.78 20.89 o 3 3 1 1791.20 1643.55 13.20 o 4 3 1 7.51 3.11 1.35 o 5 3 1 1206.83 1225.74 11.24 o 6 3 1 1218.92 1101.04 11.48 o 7 3 1 164.88 161.70 3.59 o 8 3 1 25.76 25.25 2.23 o 9 3 1 424.88 413.21 6.18 o 10 3 1 127.93 119.63 3.92 o 11 3 1 291.59 274.13 5.81 o 12 3 1 2.65 -1.99 3.80 o 13 3 1 29.48 29.63 3.17 o 14 3 1 32.55 32.28 3.63 o -15 4 1 132.89 130.29 5.49 o -14 4 1 89.63 101.00 4.52 o -13 4 1 55.87 58.71 3.73 o -12 4 1 98.90 100.63 3.97 o -11 4 1 321.68 312.82 5.80 o -10 4 1 77.93 73.12 3.17 o -9 4 1 16.11 15.68 2.13 o -8 4 1 45.88 43.73 2.44 o -7 4 1 71.37 68.51 2.51 o -6 4 1 388.98 359.23 4.70 o -5 4 1 894.50 885.39 8.67 o -4 4 1 1245.85 1356.59 13.17 o -3 4 1 233.69 217.86 3.30 o -2 4 1 553.13 554.10 5.62 o -1 4 1 624.62 663.55 6.61 o 0 4 1 285.90 289.76 3.55 o 1 4 1 67.72 68.20 2.12 o 2 4 1 105.54 99.87 2.32 o 3 4 1 1284.30 1330.78 12.96 o 4 4 1 956.67 921.21 8.87 o 5 4 1 164.02 145.02 3.20 o 6 4 1 45.86 50.31 2.29 o 7 4 1 490.65 469.18 5.97 o 8 4 1 352.39 346.22 5.59 o 9 4 1 119.95 111.57 3.60 o 10 4 1 22.82 20.95 2.42 o 11 4 1 57.11 57.07 3.25 o 12 4 1 72.23 78.16 4.01 o 13 4 1 62.95 57.51 4.00 o 14 4 1 7.88 7.03 4.25 o -14 5 1 9.73 12.48 2.79 o -13 5 1 21.41 15.69 3.09 o -12 5 1 34.35 34.62 3.21 o -11 5 1 57.67 51.82 3.25 o -10 5 1 10.85 10.01 2.09 o -9 5 1 443.83 417.98 6.33 o -8 5 1 730.52 695.90 7.62 o -7 5 1 60.31 56.83 2.68 o -6 5 1 513.22 477.54 5.78 o -5 5 1 2609.17 2437.91 19.93 o -4 5 1 621.70 555.05 5.71 o -3 5 1 282.55 269.60 3.93 o -2 5 1 578.87 535.97 5.31 o -1 5 1 464.81 398.89 4.57 o 0 5 1 4.82 3.95 1.39 o 1 5 1 815.83 839.55 8.36 o 2 5 1 449.14 453.10 4.99 o 3 5 1 168.10 167.53 3.32 o 4 5 1 180.18 168.37 3.50 o 5 5 1 0.17 1.97 2.28 o 6 5 1 327.42 313.82 5.06 o 7 5 1 849.64 814.82 8.26 o 8 5 1 583.98 519.62 7.00 o 9 5 1 148.32 138.14 4.11 o 10 5 1 408.70 385.73 6.80 o 11 5 1 74.08 78.95 4.14 o 12 5 1 12.23 14.53 2.98 o 13 5 1 17.72 9.15 5.41 o -13 6 1 52.65 64.85 4.14 o -12 6 1 28.24 27.48 3.19 o -11 6 1 339.05 334.34 6.94 o -10 6 1 95.65 105.30 3.91 o -9 6 1 73.69 74.79 3.31 o -8 6 1 442.39 434.03 6.44 o -7 6 1 689.37 643.26 7.50 o -6 6 1 432.94 410.42 5.83 o -5 6 1 148.29 162.31 3.74 o -4 6 1 339.08 316.82 4.81 o -3 6 1 1770.00 1642.78 14.56 o -2 6 1 531.72 488.51 5.60 o -1 6 1 64.20 65.14 2.44 o 0 6 1 273.42 249.97 4.05 o 1 6 1 314.04 271.95 4.22 o 2 6 1 103.19 94.98 2.85 o 3 6 1 363.27 380.76 5.19 o 4 6 1 797.69 746.25 7.37 o 5 6 1 356.37 329.89 5.30 o 6 6 1 196.53 184.28 4.28 o 7 6 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125.03 115.88 5.11 o -6 1 9 72.31 71.04 4.21 o -5 1 9 36.23 38.38 3.76 o -4 1 9 13.82 6.20 5.60 o -3 1 9 267.31 273.23 6.70 o -2 1 9 77.29 77.43 4.64 o -1 1 9 84.43 82.13 4.69 o 0 1 9 9.16 5.34 5.32 o 1 1 9 2.60 -4.88 5.07 o 2 1 9 1.09 6.41 5.10 o 3 1 9 7.68 13.85 3.22 o 4 1 9 6.67 11.51 3.02 o -12 2 9 10.39 5.01 4.97 o -11 2 9 4.47 7.19 4.63 o -10 2 9 3.61 -4.72 4.72 o -9 2 9 25.97 28.22 3.38 o -8 2 9 186.28 182.89 5.96 o -7 2 9 192.00 191.02 5.96 o -6 2 9 34.43 31.69 3.60 o -5 2 9 28.68 26.56 3.62 o -4 2 9 495.84 483.77 8.50 o -3 2 9 249.56 249.26 6.48 o -2 2 9 296.55 277.04 6.92 o -1 2 9 347.52 353.62 7.87 o 0 2 9 292.91 273.27 7.12 o 1 2 9 131.56 126.43 5.31 o 2 2 9 28.58 33.20 3.83 o 3 2 9 146.05 148.18 6.11 o -12 3 9 17.06 28.96 3.66 o -11 3 9 3.20 6.59 4.59 o -10 3 9 20.70 27.22 3.57 o -9 3 9 26.32 24.71 3.76 o -8 3 9 36.37 38.62 3.59 o -7 3 9 79.12 70.79 4.35 o -6 3 9 74.22 72.05 4.33 o -5 3 9 115.02 113.53 5.10 o -4 3 9 39.56 35.49 3.69 o -3 3 9 143.71 137.96 5.35 o -2 3 9 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o -8 0 10 55.46 55.78 4.18 o -7 0 10 170.39 158.53 5.92 o -6 0 10 214.48 206.46 6.35 o -5 0 10 39.11 36.11 3.86 o -4 0 10 71.85 64.24 4.72 o -3 0 10 113.93 110.12 5.13 o -2 0 10 48.46 44.29 4.36 o -1 0 10 3.53 5.55 5.55 o 0 0 10 36.79 37.50 4.28 o -10 1 10 4.95 8.39 5.78 o -9 1 10 143.79 134.13 5.84 o -8 1 10 318.25 303.99 7.87 o -7 1 10 281.62 245.03 7.20 o -6 1 10 9.54 11.63 3.65 o -5 1 10 412.03 390.29 8.49 o -4 1 10 171.32 157.07 5.90 o -3 1 10 42.80 44.76 4.24 o -2 1 10 68.75 71.39 4.76 o -1 1 10 180.52 178.48 6.35 o 0 1 10 56.73 48.61 4.87 o -10 2 10 84.80 84.66 4.96 o -9 2 10 57.21 59.62 4.45 o -8 2 10 5.04 -2.06 5.59 o -7 2 10 98.87 96.83 5.10 o -6 2 10 192.93 189.65 6.41 o -5 2 10 24.73 15.47 3.69 o -4 2 10 119.55 102.80 5.46 o -3 2 10 41.17 40.68 4.17 o -2 2 10 38.81 33.15 4.14 o -1 2 10 4.82 9.58 3.41 o 0 2 10 34.88 37.21 4.24 o -9 3 10 61.18 61.72 4.45 o -8 3 10 136.82 136.15 5.71 o -7 3 10 21.83 21.70 3.81 o -6 3 10 148.42 143.45 5.97 o -5 3 10 132.12 115.74 5.65 o -4 3 10 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