#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:01:15 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180943 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/23/2202359.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202359_Fobs loop_ _publ_author_name 'Ugur, Derya' 'Fl\"orke, Ulrich' 'K\"ulc\"u, Nevzat' 'Arslan, Hakan' _publ_section_title ; 3-[4-(3,3-Diethylthioureidocarbonoyl)benzoyl]-1,1-diethylthiourea ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1345 _journal_page_last o1346 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.168 _cell_angle_gamma 90.000 _cell_length_a 6.7980 _cell_length_b 15.2735 _cell_length_c 10.0275 _exptl_crystal_F_000 420.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file bt6329Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C18 H26 N4 O2 S2 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 109.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10144.90 10245.17 297.56 o 4 0 0 12.49 3.58 0.43 o 6 0 0 228.88 232.94 10.99 o 8 0 0 3.14 0.89 1.15 o 1 1 0 2217.00 2251.26 48.10 o 2 1 0 745.60 818.32 23.97 o 3 1 0 110.16 142.60 3.68 o 4 1 0 304.67 298.58 5.27 o 5 1 0 52.31 43.99 1.94 o 6 1 0 43.01 38.41 3.19 o 7 1 0 18.84 14.53 1.36 o 8 1 0 26.46 25.56 2.43 o 0 2 0 117.34 153.05 4.29 o 1 2 0 8277.31 8372.42 245.36 o 2 2 0 566.44 585.79 11.87 o 3 2 0 27.64 19.26 0.51 o 4 2 0 7.90 4.57 0.29 o 5 2 0 6.32 3.85 0.70 o 6 2 0 92.55 70.89 4.09 o 7 2 0 0.04 -0.26 0.80 o 1 3 0 692.93 798.46 21.50 o 2 3 0 190.36 198.62 4.67 o 3 3 0 0.35 2.12 0.22 o 4 3 0 0.04 0.74 0.39 o 5 3 0 466.33 439.08 10.96 o 6 3 0 3.71 4.37 0.89 o 7 3 0 82.52 86.67 3.77 o 0 4 0 1715.02 1687.70 66.96 o 1 4 0 6972.61 7040.79 166.14 o 2 4 0 93.48 89.98 2.66 o 3 4 0 321.04 282.05 5.87 o 4 4 0 16.92 16.81 0.62 o 5 4 0 367.23 346.31 10.66 o 6 4 0 28.17 28.92 1.69 o 7 4 0 124.19 128.24 4.74 o 1 5 0 42.02 47.86 1.32 o 2 5 0 309.64 347.31 8.11 o 3 5 0 265.19 267.40 6.34 o 4 5 0 905.30 905.60 18.45 o 5 5 0 92.92 91.54 3.40 o 6 5 0 112.24 122.74 4.86 o 7 5 0 1.56 0.77 0.92 o 0 6 0 4004.72 4125.73 163.43 o 1 6 0 119.10 109.08 2.73 o 2 6 0 28.88 25.38 0.89 o 3 6 0 871.10 904.44 20.80 o 4 6 0 2.35 2.08 0.38 o 5 6 0 550.19 554.15 16.71 o 6 6 0 42.39 44.97 2.20 o 7 6 0 2.48 3.85 1.07 o 1 7 0 117.56 115.42 2.88 o 2 7 0 154.04 138.34 3.47 o 3 7 0 2.73 2.21 0.62 o 4 7 0 0.11 0.44 0.32 o 5 7 0 57.50 59.12 2.81 o 6 7 0 65.99 66.77 2.93 o 7 7 0 33.30 33.05 2.05 o 0 8 0 0.41 2.94 0.64 o 1 8 0 591.57 642.83 14.85 o 2 8 0 505.47 512.17 11.95 o 3 8 0 48.68 45.45 1.48 o 4 8 0 702.67 678.95 13.99 o 5 8 0 10.14 8.51 1.01 o 6 8 0 238.02 243.19 8.00 o 7 8 0 1.69 1.78 0.95 o 1 9 0 0.09 0.18 0.26 o 2 9 0 227.26 233.48 5.65 o 3 9 0 175.48 175.22 4.43 o 4 9 0 76.21 73.51 1.96 o 5 9 0 834.13 852.47 25.31 o 6 9 0 69.19 63.10 2.89 o 7 9 0 240.12 240.65 8.11 o 0 10 0 285.22 234.35 9.97 o 1 10 0 5.61 4.42 0.49 o 2 10 0 22.51 15.44 0.88 o 3 10 0 2.24 4.33 0.54 o 4 10 0 31.21 31.35 1.58 o 5 10 0 9.79 9.03 1.13 o 6 10 0 8.27 9.66 1.23 o 1 11 0 26.57 25.56 1.05 o 2 11 0 0.31 0.25 0.75 o 3 11 0 114.08 104.56 2.90 o 4 11 0 431.27 415.89 8.83 o 5 11 0 0.21 0.80 0.75 o 6 11 0 354.36 357.79 14.82 o 0 12 0 1.05 1.41 0.89 o 1 12 0 238.56 233.54 7.14 o 2 12 0 1.17 1.66 0.84 o 3 12 0 333.16 323.41 7.89 o 4 12 0 99.05 97.54 2.54 o 5 12 0 62.59 67.20 3.26 o 6 12 0 25.87 23.61 1.75 o 1 13 0 0.02 0.61 0.67 o 2 13 0 21.74 23.65 1.13 o 3 13 0 7.49 5.91 0.73 o 4 13 0 1.10 0.93 0.61 o 5 13 0 50.30 52.06 2.58 o 0 14 0 12.40 13.03 1.66 o 1 14 0 337.93 313.99 9.49 o 2 14 0 322.19 317.91 7.84 o 3 14 0 21.89 22.43 1.05 o 4 14 0 154.61 165.09 3.96 o 5 14 0 7.96 6.30 1.08 o 1 15 0 74.29 80.45 3.45 o 2 15 0 175.69 168.96 3.98 o 3 15 0 18.90 22.97 1.12 o 4 15 0 230.33 228.57 7.80 o 0 16 0 73.03 72.45 4.22 o 1 16 0 207.37 195.09 6.77 o 2 16 0 190.48 191.34 6.28 o 3 16 0 105.64 105.71 2.83 o 4 16 0 134.88 141.14 6.05 o 1 17 0 158.02 147.65 5.10 o 2 17 0 22.13 25.74 1.71 o 3 17 0 139.41 138.98 3.97 o 0 18 0 0.02 0.64 1.15 o 1 18 0 12.81 18.19 1.79 o 2 18 0 71.92 74.63 3.12 o -5 0 1 409.18 400.68 12.07 o -3 0 1 320.91 328.39 13.29 o -1 0 1 3650.28 3644.25 144.39 o 1 0 1 10088.34 10296.94 441.09 o 3 0 1 9.58 9.57 2.04 o 5 0 1 116.22 106.82 5.49 o -8 1 1 43.33 42.17 3.19 o -7 1 1 37.71 36.35 1.98 o -6 1 1 6.44 3.41 0.81 o -5 1 1 0.01 -0.07 0.37 o -4 1 1 1099.46 1177.09 27.80 o -3 1 1 626.71 679.39 19.24 o -2 1 1 559.01 646.63 18.25 o -1 1 1 1210.24 1288.93 30.31 o 0 1 1 5.53 8.93 0.35 o 1 1 1 4436.46 4781.90 259.01 o 2 1 1 1521.46 1575.70 32.53 o 3 1 1 1664.57 1799.22 37.13 o 4 1 1 793.33 826.13 25.52 o 5 1 1 12.60 16.33 1.16 o 6 1 1 219.31 219.27 7.36 o 7 1 1 30.27 26.23 1.80 o -8 2 1 101.45 102.48 5.49 o -7 2 1 294.61 264.59 8.53 o -6 2 1 202.87 202.33 6.57 o -5 2 1 70.91 83.45 1.71 o -4 2 1 403.62 396.33 6.85 o -3 2 1 1879.70 2057.99 34.57 o -2 2 1 294.17 309.08 5.75 o -1 2 1 1965.39 2049.83 37.36 o 0 2 1 2734.65 2787.58 50.63 o 1 2 1 432.95 413.71 9.73 o 2 2 1 409.75 454.32 9.46 o 3 2 1 129.34 128.56 2.85 o 4 2 1 297.58 314.79 10.03 o 5 2 1 144.97 152.73 5.29 o 6 2 1 28.26 27.43 3.32 o 7 2 1 39.31 32.66 1.98 o -8 3 1 37.06 30.04 2.00 o -7 3 1 4.73 4.89 1.07 o -6 3 1 36.45 45.19 2.15 o -5 3 1 443.86 451.55 7.30 o -4 3 1 203.10 215.03 3.81 o -3 3 1 131.92 114.21 2.09 o -2 3 1 63.60 75.06 1.92 o -1 3 1 189.06 189.29 4.45 o 0 3 1 799.26 834.99 15.21 o 1 3 1 865.29 900.13 16.44 o 2 3 1 102.05 102.82 2.29 o 3 3 1 243.17 247.15 4.69 o 4 3 1 44.06 37.41 1.63 o 5 3 1 461.80 437.59 10.97 o 6 3 1 47.34 40.73 2.68 o 7 3 1 114.89 114.73 4.36 o -8 4 1 89.87 99.43 4.04 o -7 4 1 0.70 1.09 0.89 o -6 4 1 246.64 242.92 7.78 o -5 4 1 0.37 0.11 0.36 o -4 4 1 1385.74 1484.27 29.94 o -3 4 1 491.83 535.15 12.39 o -2 4 1 266.76 268.97 6.32 o -1 4 1 7837.83 8004.14 185.90 o 0 4 1 3874.07 3986.61 72.29 o 1 4 1 17.32 20.40 0.81 o 2 4 1 162.49 163.66 3.47 o 3 4 1 636.02 712.88 13.14 o 4 4 1 178.28 165.88 4.42 o 5 4 1 49.13 47.28 3.13 o 6 4 1 616.91 594.26 24.41 o 7 4 1 25.01 27.16 1.84 o -7 5 1 63.57 66.00 2.91 o -6 5 1 52.87 48.32 2.24 o -5 5 1 88.54 93.74 2.56 o -4 5 1 90.03 78.30 2.16 o -3 5 1 120.98 119.55 3.05 o -2 5 1 73.27 89.17 2.28 o -1 5 1 408.85 412.40 9.54 o 0 5 1 1293.76 1322.35 26.60 o 1 5 1 5726.25 5877.76 106.52 o 2 5 1 476.77 491.88 9.12 o 3 5 1 1752.69 1881.20 37.89 o 4 5 1 7.77 7.47 0.80 o 5 5 1 49.42 41.29 1.96 o 6 5 1 60.13 59.01 3.26 o 7 5 1 37.44 34.79 2.09 o -7 6 1 12.27 14.34 1.47 o -6 6 1 19.65 21.75 1.53 o -5 6 1 605.93 626.40 14.66 o -4 6 1 8.07 8.86 0.59 o -3 6 1 563.24 572.67 13.28 o -2 6 1 1018.53 1062.26 26.36 o -1 6 1 117.25 117.64 2.90 o 0 6 1 151.82 137.91 2.95 o 1 6 1 320.92 340.23 6.35 o 2 6 1 513.09 572.90 11.73 o 3 6 1 152.13 162.57 3.21 o 4 6 1 102.62 103.27 3.67 o 5 6 1 41.59 35.85 2.68 o 6 6 1 53.91 49.67 2.42 o 7 6 1 42.06 48.25 2.49 o -7 7 1 45.57 45.26 2.43 o -6 7 1 62.17 64.78 2.82 o -5 7 1 70.69 71.23 2.14 o -4 7 1 92.95 82.19 2.33 o -3 7 1 11.82 12.03 0.64 o -2 7 1 381.75 377.68 8.87 o -1 7 1 40.26 49.38 1.43 o 0 7 1 2238.36 2297.73 46.19 o 1 7 1 37.52 23.22 0.66 o 2 7 1 2604.84 2846.67 57.26 o 3 7 1 0.66 1.65 0.31 o 4 7 1 512.45 510.95 12.35 o 5 7 1 10.25 9.65 2.17 o 6 7 1 155.44 148.58 5.31 o 7 7 1 19.47 20.50 1.69 o -7 8 1 10.78 11.09 1.38 o -6 8 1 68.59 73.50 3.09 o -5 8 1 11.51 12.65 0.83 o -4 8 1 213.55 191.44 7.87 o -3 8 1 158.78 151.61 3.86 o -2 8 1 508.90 544.33 12.68 o -1 8 1 26.06 25.19 0.91 o 0 8 1 145.91 156.48 3.41 o 1 8 1 4.37 6.59 0.41 o 2 8 1 64.43 67.08 1.67 o 3 8 1 335.04 342.90 7.23 o 4 8 1 29.80 27.91 1.01 o 5 8 1 134.17 126.79 4.60 o 6 8 1 41.91 41.34 2.27 o 7 8 1 12.10 9.28 1.29 o -7 9 1 9.05 8.68 1.41 o -6 9 1 135.40 138.41 5.00 o -5 9 1 94.60 92.44 3.30 o -4 9 1 254.33 245.33 8.04 o -3 9 1 7.29 7.32 0.61 o -2 9 1 157.52 148.78 3.76 o -1 9 1 46.23 49.38 1.47 o 0 9 1 1082.70 1023.46 24.30 o 1 9 1 257.68 246.53 5.24 o 2 9 1 888.11 866.04 17.67 o 3 9 1 15.28 19.24 0.94 o 4 9 1 28.39 32.35 1.38 o 5 9 1 330.61 330.46 10.44 o 6 9 1 3.62 2.64 0.95 o -7 10 1 55.91 61.40 2.89 o -6 10 1 32.61 33.89 2.03 o -5 10 1 49.14 51.20 1.82 o -4 10 1 559.99 546.02 12.88 o -3 10 1 101.90 101.14 2.80 o -2 10 1 567.54 578.57 13.52 o -1 10 1 640.35 662.21 19.02 o 0 10 1 116.77 120.00 3.22 o 1 10 1 75.48 79.80 2.40 o 2 10 1 5.40 8.90 0.72 o 3 10 1 98.21 89.97 2.25 o 4 10 1 253.38 257.23 5.66 o 5 10 1 7.58 8.64 1.11 o 6 10 1 48.05 49.89 2.60 o -6 11 1 67.59 61.99 2.89 o -5 11 1 38.61 42.08 1.47 o -4 11 1 168.46 168.59 4.40 o -3 11 1 175.91 164.22 4.25 o -2 11 1 1110.70 1162.11 26.78 o -1 11 1 597.64 589.98 17.03 o 0 11 1 12.16 10.19 0.69 o 1 11 1 443.85 421.04 8.80 o 2 11 1 49.59 54.21 1.53 o 3 11 1 217.32 215.63 4.81 o 4 11 1 270.33 277.64 7.14 o 5 11 1 12.23 14.57 1.38 o 6 11 1 0.16 0.88 1.02 o -6 12 1 14.11 14.22 1.44 o -5 12 1 150.71 151.43 3.68 o -4 12 1 75.36 74.52 2.33 o -3 12 1 93.49 88.68 2.58 o -2 12 1 21.46 20.20 1.03 o -1 12 1 18.98 18.90 1.22 o 0 12 1 141.20 137.48 4.47 o 1 12 1 24.94 26.26 1.01 o 2 12 1 132.93 143.50 3.34 o 3 12 1 154.90 148.85 3.50 o 4 12 1 52.82 56.51 2.82 o 5 12 1 233.96 237.07 7.91 o -6 13 1 76.26 82.09 3.53 o -5 13 1 46.28 46.03 1.61 o -4 13 1 52.20 46.55 1.72 o -3 13 1 574.20 577.65 13.70 o -2 13 1 15.86 14.52 1.55 o -1 13 1 792.97 785.38 22.63 o 0 13 1 48.01 49.07 2.08 o 1 13 1 376.09 347.81 9.18 o 2 13 1 8.23 9.40 0.67 o 3 13 1 385.58 400.77 8.58 o 4 13 1 1.58 2.15 0.85 o 5 13 1 366.41 407.17 12.78 o -5 14 1 70.27 60.32 2.69 o -4 14 1 1.63 0.97 0.57 o -3 14 1 0.33 0.81 0.52 o -2 14 1 5.53 5.76 0.89 o -1 14 1 75.39 69.65 2.71 o 0 14 1 10.26 9.38 1.04 o 1 14 1 55.64 58.06 2.39 o 2 14 1 5.31 4.52 0.59 o 3 14 1 19.76 17.39 0.94 o 4 14 1 0.12 -0.37 0.59 o 5 14 1 0.17 0.38 0.96 o -5 15 1 2.02 2.23 0.64 o -4 15 1 18.23 21.26 1.24 o -3 15 1 474.53 454.11 11.35 o -2 15 1 127.32 120.37 4.25 o -1 15 1 204.31 191.18 6.14 o 0 15 1 623.72 609.25 17.80 o 1 15 1 10.32 11.34 1.21 o 2 15 1 209.06 201.54 4.64 o 3 15 1 43.14 47.00 1.60 o 4 15 1 36.67 36.60 2.08 o -4 16 1 22.76 21.84 1.19 o -3 16 1 2.40 2.59 0.83 o -2 16 1 76.17 69.83 2.89 o -1 16 1 24.13 24.97 1.66 o 0 16 1 100.88 103.38 3.79 o 1 16 1 10.04 8.87 1.13 o 2 16 1 0.01 0.43 0.68 o 3 16 1 6.06 7.11 0.74 o 4 16 1 12.04 13.60 1.41 o -3 17 1 0.88 1.81 0.85 o -2 17 1 282.60 287.84 9.07 o -1 17 1 39.04 43.20 2.16 o 0 17 1 56.59 60.59 2.66 o 1 17 1 0.95 0.85 0.85 o 2 17 1 1.96 5.16 2.36 o 3 17 1 0.42 0.28 0.69 o -2 18 1 0.84 0.49 0.83 o -1 18 1 20.49 22.41 1.73 o 0 18 1 74.32 72.62 3.90 o 1 18 1 6.34 3.29 0.98 o 2 18 1 13.52 13.38 1.98 o 0 19 1 111.09 104.72 4.02 o -8 0 2 81.69 75.77 4.47 o -6 0 2 6.61 7.66 1.34 o -4 0 2 488.66 467.16 19.04 o -2 0 2 785.46 808.58 32.33 o 0 0 2 4258.42 3967.43 145.80 o 2 0 2 11961.28 12777.89 547.15 o 4 0 2 888.03 886.15 38.72 o 6 0 2 2.25 0.77 1.15 o -8 1 2 120.48 123.43 6.26 o -7 1 2 80.37 79.47 3.90 o -6 1 2 6.15 6.26 0.67 o -5 1 2 84.10 77.54 2.66 o -4 1 2 19.45 18.94 1.34 o -3 1 2 138.39 101.51 3.16 o -2 1 2 1031.89 1043.37 23.79 o -1 1 2 18.33 20.65 0.58 o 0 1 2 1403.91 1364.25 43.51 o 1 1 2 297.59 291.40 26.26 o 2 1 2 5.76 9.32 1.98 o 3 1 2 120.81 118.58 4.07 o 4 1 2 102.56 101.52 3.66 o 5 1 2 41.06 42.81 2.03 o 6 1 2 4.13 7.60 1.04 o 7 1 2 18.74 19.45 1.58 o -8 2 2 88.81 98.01 5.37 o -7 2 2 24.83 26.97 3.00 o -6 2 2 461.18 429.13 10.51 o -5 2 2 105.94 94.27 2.60 o -4 2 2 124.39 108.19 2.80 o -3 2 2 209.06 199.47 4.79 o -2 2 2 2697.85 2920.06 66.29 o -1 2 2 927.51 956.28 14.99 o 0 2 2 625.52 687.11 14.26 o 1 2 2 4253.12 4457.22 103.91 o 2 2 2 50.62 37.57 1.60 o 3 2 2 2036.84 2252.71 101.46 o 4 2 2 336.39 331.21 10.62 o 5 2 2 184.95 178.37 6.09 o 6 2 2 24.38 24.59 1.66 o 7 2 2 14.90 14.19 1.44 o -8 3 2 113.57 109.79 5.11 o -7 3 2 6.65 4.14 0.95 o -6 3 2 292.06 283.28 8.45 o -5 3 2 364.15 371.73 7.69 o -4 3 2 2.93 7.76 0.43 o -3 3 2 691.04 721.71 13.34 o -2 3 2 337.81 316.73 5.93 o -1 3 2 14.55 7.41 0.28 o 0 3 2 5508.85 5787.34 104.95 o 1 3 2 0.00 2.09 1.23 o 2 3 2 2.16 2.04 0.21 o 3 3 2 39.13 40.05 1.11 o 4 3 2 83.13 80.42 3.03 o 5 3 2 29.26 28.56 1.32 o 6 3 2 72.06 64.90 2.80 o 7 3 2 16.96 14.98 1.49 o -8 4 2 70.18 67.60 3.11 o -7 4 2 31.61 31.42 2.68 o -6 4 2 58.95 54.18 3.19 o -5 4 2 356.03 376.99 7.20 o -4 4 2 56.00 56.68 1.34 o -3 4 2 1459.31 1548.16 28.38 o -2 4 2 469.36 516.25 11.92 o -1 4 2 680.27 760.20 15.38 o 0 4 2 2384.48 2606.32 47.32 o 1 4 2 313.12 277.80 5.20 o 2 4 2 162.79 158.72 4.70 o 3 4 2 110.77 94.58 2.78 o 4 4 2 5.82 7.36 0.63 o 5 4 2 15.55 14.69 1.16 o 6 4 2 38.20 40.33 2.15 o 7 4 2 1.18 2.27 0.98 o -8 5 2 45.92 56.36 2.84 o -7 5 2 71.12 67.52 2.94 o -6 5 2 148.81 145.03 6.64 o -5 5 2 12.09 12.93 0.76 o -4 5 2 755.17 770.05 17.80 o -3 5 2 1294.21 1463.18 33.44 o -2 5 2 1011.55 996.03 22.79 o -1 5 2 2870.29 3184.94 72.28 o 0 5 2 150.89 148.98 2.86 o 1 5 2 224.72 240.85 4.53 o 2 5 2 77.54 96.13 1.97 o 3 5 2 3.87 2.87 0.28 o 4 5 2 298.73 284.61 17.82 o 5 5 2 54.16 51.92 3.13 o 6 5 2 64.46 73.42 3.09 o 7 5 2 79.47 78.79 3.40 o -7 6 2 0.03 -0.85 0.85 o -6 6 2 46.22 56.09 3.32 o -5 6 2 45.10 43.69 1.52 o -4 6 2 1524.11 1559.39 35.68 o -3 6 2 1093.64 1121.83 25.72 o -2 6 2 218.59 207.75 4.99 o -1 6 2 5100.73 5535.08 125.45 o 0 6 2 414.18 402.18 7.46 o 1 6 2 21.41 9.03 0.41 o 2 6 2 1081.44 1047.16 19.19 o 3 6 2 13.63 21.34 0.83 o 4 6 2 4.76 5.67 0.80 o 5 6 2 630.38 636.73 19.10 o 6 6 2 0.82 1.18 0.85 o 7 6 2 131.88 137.44 6.26 o -7 7 2 154.85 156.62 5.58 o -6 7 2 217.57 211.86 9.33 o -5 7 2 288.90 276.35 6.76 o -4 7 2 35.40 34.29 1.25 o -3 7 2 552.82 519.14 12.11 o -2 7 2 568.78 686.24 15.85 o -1 7 2 287.83 284.36 8.35 o 0 7 2 675.11 765.19 14.06 o 1 7 2 2.13 2.27 0.23 o 2 7 2 8.26 11.64 0.58 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