#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/33/2203343.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203343_Fobs loop_ _publ_author_name 'Gary, John Brannon' 'Kautz, Jason A.' 'Klausmeyer, Kevin K.' 'Wong, Ching-Wah' _publ_section_title ; Diisothiocyanatotetrapyridinecopper(II) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m328 _journal_page_last m329 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.481 _cell_angle_gamma 90.000 _cell_length_a 12.1203 _cell_length_b 12.8678 _cell_length_c 15.5017 _exptl_crystal_F_000 1020.00 _reflns_d_resolution_high 0.7699 _[local]_cod_data_source_file om6214Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'sq1150 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 386.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7091.76 7226.81 135.34 o 4 0 0 2460.19 2221.83 40.33 o 6 0 0 13474.04 12446.59 244.40 o 8 0 0 5641.18 5929.03 121.25 o 10 0 0 6382.23 6735.95 132.86 o 12 0 0 3403.99 3388.42 87.85 o 14 0 0 810.53 937.92 53.17 o 3 1 0 10622.38 11640.76 166.09 o 5 1 0 1224.79 1204.70 15.79 o 7 1 0 1339.91 1459.97 21.07 o 9 1 0 8.42 17.12 2.93 o 11 1 0 10.39 12.50 4.09 o 13 1 0 347.05 371.13 11.04 o 0 2 0 8554.31 9489.87 313.31 o 2 2 0 32815.27 33405.83 562.60 o 4 2 0 32665.67 34226.76 510.24 o 6 2 0 26522.85 28117.28 445.60 o 8 2 0 5483.80 5440.97 92.52 o 10 2 0 2497.00 2479.23 46.42 o 12 2 0 1376.68 1364.74 37.60 o 14 2 0 1065.90 1068.57 25.04 o 1 3 0 26255.97 27969.76 750.49 o 3 3 0 201.15 166.44 3.71 o 5 3 0 24.05 18.36 1.81 o 7 3 0 8128.20 8192.75 138.75 o 9 3 0 55.13 71.81 4.27 o 11 3 0 970.88 905.07 19.09 o 13 3 0 450.86 423.41 12.47 o 0 4 0 1600.70 1992.34 54.44 o 2 4 0 31123.32 32074.57 541.61 o 4 4 0 27520.73 28960.23 490.14 o 6 4 0 3096.30 3069.96 56.95 o 8 4 0 9977.71 9853.31 196.39 o 10 4 0 1955.53 1979.86 37.71 o 12 4 0 1903.32 1862.53 39.25 o 14 4 0 2437.85 2579.89 55.20 o 1 5 0 451.33 481.00 9.76 o 3 5 0 8.08 4.17 2.14 o 5 5 0 519.10 491.91 14.12 o 7 5 0 872.57 933.63 17.36 o 9 5 0 1394.37 1377.87 25.11 o 11 5 0 1062.63 1077.84 20.80 o 13 5 0 152.50 146.44 9.79 o 0 6 0 83.90 128.36 5.19 o 2 6 0 17287.87 17015.47 288.52 o 4 6 0 4597.11 4230.06 72.41 o 6 6 0 381.41 359.83 9.10 o 8 6 0 4397.62 4425.45 76.18 o 10 6 0 4754.93 4725.68 81.26 o 12 6 0 2034.93 2043.24 39.69 o 14 6 0 1632.91 1604.76 44.96 o 1 7 0 3255.57 3001.95 47.90 o 3 7 0 3161.31 3670.96 63.41 o 5 7 0 3810.38 3756.48 60.87 o 7 7 0 5199.44 5245.50 89.47 o 9 7 0 26.34 28.76 4.12 o 11 7 0 733.93 730.24 24.29 o 13 7 0 88.95 96.42 8.64 o 0 8 0 1446.46 1316.81 44.66 o 2 8 0 2849.17 2514.17 43.08 o 4 8 0 2691.45 2672.42 43.65 o 6 8 0 3104.16 3068.98 50.12 o 8 8 0 1530.31 1563.37 28.42 o 10 8 0 2851.91 2850.19 49.93 o 12 8 0 2682.96 2784.20 57.64 o 1 9 0 1102.68 1231.65 20.76 o 3 9 0 393.30 376.97 8.73 o 5 9 0 640.72 652.17 14.43 o 7 9 0 170.75 127.92 5.79 o 9 9 0 183.08 193.10 9.55 o 11 9 0 243.91 217.70 11.12 o 0 10 0 21025.32 21009.79 459.98 o 2 10 0 351.34 378.85 8.60 o 4 10 0 899.48 918.22 19.22 o 6 10 0 7419.14 7431.82 146.75 o 8 10 0 1094.38 1015.30 23.13 o 10 10 0 905.84 920.74 24.51 o 12 10 0 1262.24 1309.48 38.11 o 1 11 0 335.43 336.33 9.57 o 3 11 0 976.00 892.63 34.10 o 5 11 0 1405.39 1291.73 28.16 o 7 11 0 678.60 642.56 18.23 o 9 11 0 259.15 248.65 10.99 o 11 11 0 78.08 88.13 10.22 o 0 12 0 3279.79 3215.07 82.23 o 2 12 0 1421.69 1422.97 30.05 o 4 12 0 2424.99 2244.59 52.02 o 6 12 0 2613.92 2613.87 59.75 o 8 12 0 299.00 327.67 17.80 o 10 12 0 882.52 988.07 30.80 o 1 13 0 1490.51 1529.80 29.32 o 3 13 0 3.85 0.15 6.67 o 5 13 0 614.23 598.56 17.70 o 7 13 0 56.35 50.93 8.32 o 9 13 0 139.96 146.48 11.97 o 0 14 0 834.72 814.26 30.72 o 2 14 0 4846.72 4788.04 107.71 o 4 14 0 1427.47 1464.31 36.13 o 6 14 0 8.99 11.50 8.01 o 8 14 0 2115.40 2247.75 61.02 o 1 15 0 320.54 302.24 12.96 o 3 15 0 137.59 130.45 10.14 o 5 15 0 118.85 175.87 11.42 o 0 16 0 19.70 46.80 19.58 o 2 16 0 2423.84 2373.11 77.45 o 4 16 0 803.85 878.84 28.73 o -15 1 1 2416.02 2371.49 83.97 o -13 1 1 484.44 532.72 15.02 o -11 1 1 977.12 1004.29 19.90 o -9 1 1 17533.66 17755.84 261.32 o -7 1 1 1094.43 990.80 14.68 o -5 1 1 12684.25 13122.11 160.54 o -3 1 1 37609.86 37551.16 522.12 o -1 1 1 33880.05 27794.65 1296.24 o 1 1 1 16263.93 16085.96 750.40 o 3 1 1 3336.71 3038.27 45.09 o 5 1 1 279.63 407.12 5.92 o 7 1 1 4814.93 4666.11 69.11 o 9 1 1 12858.94 12669.07 200.10 o 11 1 1 438.63 425.96 11.69 o 13 1 1 1190.48 1206.61 36.76 o -14 2 1 377.09 400.21 12.57 o -12 2 1 597.41 578.06 14.99 o -10 2 1 2446.42 2407.00 41.81 o -8 2 1 890.36 817.55 14.59 o -6 2 1 834.57 857.70 13.61 o -4 2 1 300.61 342.49 7.13 o -2 2 1 39252.07 40865.31 607.13 o 0 2 1 2361.66 2440.34 51.11 o 2 2 1 9931.49 10728.76 193.70 o 4 2 1 838.98 768.34 12.88 o 6 2 1 1842.49 1813.51 31.35 o 8 2 1 362.57 375.19 8.25 o 10 2 1 1660.80 1702.90 32.55 o 12 2 1 196.10 217.74 8.23 o 14 2 1 298.17 297.04 17.97 o -13 3 1 2319.36 2249.83 48.69 o -11 3 1 975.86 983.83 20.43 o -9 3 1 2789.54 2886.28 53.23 o -7 3 1 16329.75 16805.54 280.48 o -5 3 1 13427.25 13886.09 248.23 o -3 3 1 318.85 462.89 7.49 o -1 3 1 4358.47 4150.28 86.88 o 1 3 1 25384.70 25903.86 480.64 o 3 3 1 18490.60 18374.79 359.44 o 5 3 1 17717.84 17938.04 324.37 o 7 3 1 2142.14 1869.13 35.80 o 9 3 1 83.61 85.81 4.32 o 11 3 1 4196.68 4032.22 74.61 o 13 3 1 943.07 961.19 22.56 o -14 4 1 435.97 412.21 13.36 o -12 4 1 3.63 -10.30 6.87 o -10 4 1 481.56 476.31 11.34 o -8 4 1 501.20 482.53 13.53 o -6 4 1 1526.29 1734.94 30.30 o -2 4 1 7967.35 8358.71 142.22 o 0 4 1 2338.72 2405.66 49.63 o 2 4 1 4674.17 4951.94 79.60 o 4 4 1 21939.29 23518.53 424.62 o 6 4 1 1484.61 1588.18 32.71 o 8 4 1 390.03 341.82 8.23 o 10 4 1 890.07 827.48 17.40 o 12 4 1 800.72 705.41 17.71 o 14 4 1 11.35 25.85 7.90 o -13 5 1 3121.17 3198.52 65.56 o -11 5 1 9166.31 9617.08 162.91 o -9 5 1 1179.22 1161.42 21.44 o -7 5 1 6413.83 6048.24 103.18 o -5 5 1 2700.45 2583.50 44.67 o -3 5 1 13990.69 14877.85 250.88 o -1 5 1 12910.49 12696.12 216.19 o 1 5 1 1988.75 1750.77 33.23 o 3 5 1 5504.09 5885.58 88.92 o 5 5 1 18635.33 17534.40 317.05 o 7 5 1 4202.55 4151.16 71.30 o 9 5 1 574.11 588.48 12.21 o 11 5 1 8106.99 8399.65 142.94 o 13 5 1 1361.84 1337.55 31.16 o -14 6 1 100.55 105.67 9.72 o -12 6 1 20.55 13.85 6.10 o -10 6 1 158.19 165.06 6.19 o -8 6 1 3.89 3.72 3.23 o -6 6 1 1358.89 1330.14 22.43 o -4 6 1 3868.22 4117.96 84.88 o -2 6 1 3454.00 3638.81 66.87 o 0 6 1 10032.56 11303.63 177.89 o 2 6 1 4757.10 5333.23 91.17 o 4 6 1 1244.27 1196.32 20.12 o 6 6 1 689.97 753.94 13.44 o 8 6 1 2825.33 2812.33 48.98 o 10 6 1 12.54 15.01 4.22 o 12 6 1 195.29 223.81 9.95 o -13 7 1 863.16 866.89 27.84 o -11 7 1 1634.52 1715.51 33.82 o -9 7 1 518.19 573.53 12.39 o -7 7 1 4684.88 4752.81 76.64 o -5 7 1 3426.38 3441.12 59.27 o -3 7 1 2411.44 2049.45 35.71 o -1 7 1 6242.45 6153.95 97.09 o 1 7 1 1101.55 795.78 15.87 o 3 7 1 5703.12 5457.82 93.51 o 5 7 1 6411.11 6673.58 106.78 o 7 7 1 9282.46 9375.54 159.55 o 9 7 1 2840.32 2737.42 47.69 o 11 7 1 6514.01 6543.90 112.10 o 13 7 1 467.09 425.61 13.78 o -12 8 1 55.36 64.08 11.25 o -10 8 1 2682.95 2685.45 47.35 o -8 8 1 340.72 372.26 9.81 o -6 8 1 17.22 24.65 3.60 o -4 8 1 348.23 310.41 6.94 o -2 8 1 709.72 608.01 14.02 o 0 8 1 2926.62 3028.04 51.39 o 2 8 1 2131.72 2148.75 37.63 o 4 8 1 760.58 700.28 13.17 o 6 8 1 763.46 797.90 14.76 o 8 8 1 186.71 142.09 7.53 o 10 8 1 248.45 276.82 8.21 o 12 8 1 1374.30 1216.11 28.25 o -11 9 1 710.76 671.07 19.40 o -9 9 1 8356.39 8277.29 157.65 o -7 9 1 111.10 98.90 6.57 o -5 9 1 652.03 681.79 13.92 o -3 9 1 6447.20 6162.17 103.66 o -1 9 1 1123.02 1082.07 31.09 o 1 9 1 10278.23 10396.66 163.59 o 3 9 1 7844.02 7979.60 136.32 o 5 9 1 1588.75 1574.35 28.59 o 7 9 1 1900.23 1888.75 36.63 o 9 9 1 6629.49 6448.71 121.38 o 11 9 1 142.15 132.72 9.91 o -12 10 1 0.73 -0.42 10.41 o -10 10 1 474.46 468.68 15.45 o -8 10 1 12.39 16.62 6.17 o -6 10 1 64.38 64.02 5.87 o -4 10 1 225.22 232.59 9.13 o -2 10 1 1110.42 1072.40 19.84 o 0 10 1 25.87 22.39 4.13 o 2 10 1 5313.63 5139.50 104.16 o 4 10 1 311.84 364.73 10.29 o 6 10 1 83.69 94.26 7.15 o 8 10 1 602.19 542.63 15.25 o 10 10 1 30.10 26.13 7.17 o -11 11 1 174.07 179.58 12.31 o -9 11 1 3803.11 3816.56 85.49 o -7 11 1 552.29 527.10 15.53 o -5 11 1 3530.94 3408.57 69.06 o -3 11 1 3338.58 3286.71 65.41 o -1 11 1 731.55 690.82 24.19 o 1 11 1 1406.03 1423.98 26.97 o 3 11 1 7480.04 7056.43 156.05 o 5 11 1 741.40 722.03 16.28 o 7 11 1 2131.79 2098.97 48.44 o 9 11 1 3324.19 3535.93 80.29 o 11 11 1 19.03 19.13 10.17 o -10 12 1 127.41 131.36 11.36 o -8 12 1 1706.71 1655.64 39.90 o -6 12 1 0.66 -3.36 6.45 o -4 12 1 849.45 859.37 22.99 o -2 12 1 1473.76 1404.89 29.78 o 0 12 1 1801.66 1745.16 32.65 o 2 12 1 28.10 35.15 6.17 o 4 12 1 337.82 356.33 12.26 o 6 12 1 1.84 19.57 6.71 o 8 12 1 1.40 6.21 7.18 o 10 12 1 166.90 125.97 11.11 o -9 13 1 253.17 249.71 25.99 o -7 13 1 2538.61 2432.03 56.26 o -5 13 1 2807.17 2882.45 76.61 o -3 13 1 1036.79 1035.10 26.72 o -1 13 1 4269.13 4290.15 76.64 o 1 13 1 3554.92 3437.84 77.29 o 3 13 1 18.21 12.46 6.47 o 5 13 1 2087.35 2053.96 60.47 o 7 13 1 494.89 531.76 17.13 o 9 13 1 411.13 382.94 17.47 o -8 14 1 442.39 484.72 19.43 o -6 14 1 4.67 -1.76 7.75 o -4 14 1 47.40 64.66 7.89 o -2 14 1 295.76 306.10 12.23 o 0 14 1 40.38 49.42 6.47 o 2 14 1 94.36 67.75 8.15 o 4 14 1 208.36 170.88 11.22 o 6 14 1 422.13 522.49 17.23 o -5 15 1 967.25 990.26 27.16 o -3 15 1 623.36 615.87 34.58 o -1 15 1 2466.56 2387.28 81.77 o 1 15 1 1086.63 1172.79 30.74 o 3 15 1 216.99 223.36 11.70 o 5 15 1 1514.95 1525.04 38.01 o -4 16 1 343.69 297.70 18.57 o -2 16 1 933.28 1017.49 29.05 o 0 16 1 791.96 701.85 31.90 o 2 16 1 782.66 740.76 28.63 o 4 16 1 351.77 329.85 39.29 o -14 0 2 2515.38 2616.56 136.18 o -12 0 2 4613.36 4654.07 101.81 o -10 0 2 19.41 25.39 5.18 o -8 0 2 8445.43 8222.55 161.90 o -6 0 2 6907.51 6433.89 127.05 o -4 0 2 1006.72 1422.69 25.06 o 2 0 2 25034.79 28413.94 643.97 o 6 0 2 11903.13 11610.88 227.82 o 8 0 2 13.87 10.69 3.24 o 10 0 2 3032.22 3051.37 61.25 o 12 0 2 472.71 482.37 21.91 o 14 0 2 234.76 212.03 22.29 o -15 1 2 213.56 219.18 16.97 o -13 1 2 19.74 20.46 5.45 o -11 1 2 535.52 550.47 12.55 o -9 1 2 583.67 600.14 11.28 o -7 1 2 2553.58 2864.29 40.53 o -5 1 2 7677.26 8359.22 99.17 o -3 1 2 10718.39 11175.29 149.73 o -1 1 2 172.29 163.36 4.10 o 1 1 2 2143.77 2086.68 48.69 o 3 1 2 22395.07 23437.92 363.86 o 5 1 2 857.49 1012.66 14.99 o 7 1 2 1629.34 1678.97 27.32 o 9 1 2 136.95 125.32 4.33 o 11 1 2 32.64 27.07 4.93 o 13 1 2 305.81 286.14 14.09 o -14 2 2 390.26 456.89 13.60 o -12 2 2 399.36 401.78 10.02 o -10 2 2 2998.65 3088.63 52.40 o -8 2 2 3827.39 3602.74 57.19 o -6 2 2 11260.07 11423.25 169.41 o -2 2 2 272.53 194.06 4.24 o 0 2 2 10799.84 10772.50 205.00 o 2 2 2 273.14 355.83 7.88 o 4 2 2 1810.15 1669.72 28.51 o 8 2 2 3650.97 3549.90 61.00 o 10 2 2 1820.55 1723.35 33.01 o 12 2 2 403.05 452.30 12.38 o 14 2 2 576.96 596.14 23.60 o -15 3 2 520.63 530.14 17.18 o -13 3 2 49.09 72.65 12.36 o -11 3 2 3140.16 2960.27 60.15 o -9 3 2 5348.09 5270.28 88.18 o -7 3 2 563.17 730.80 12.64 o -5 3 2 5846.13 6237.16 97.87 o -3 3 2 560.90 517.43 9.04 o -1 3 2 5471.43 5789.67 108.20 o 1 3 2 20683.82 21811.38 404.06 o 3 3 2 314.42 307.71 13.93 o 5 3 2 2671.64 2831.88 56.55 o 7 3 2 1613.76 1649.19 27.06 o 9 3 2 6425.88 6291.63 114.80 o 11 3 2 205.95 247.59 11.01 o 13 3 2 78.91 111.43 9.34 o -14 4 2 796.42 832.11 21.24 o -12 4 2 784.31 718.98 17.98 o -10 4 2 2141.22 2108.88 42.07 o -8 4 2 1055.54 984.45 17.77 o -6 4 2 399.24 327.20 6.74 o -4 4 2 24756.79 25531.51 400.43 o -2 4 2 3919.67 4000.11 67.15 o 0 4 2 25.56 53.83 7.78 o 2 4 2 35841.90 36314.72 733.19 o 4 4 2 1988.51 1697.72 34.35 o 6 4 2 612.29 527.24 12.54 o 8 4 2 1674.96 1670.14 31.66 o 10 4 2 1137.12 1132.64 22.74 o 12 4 2 2838.96 2854.74 58.67 o 14 4 2 2177.13 2419.70 50.43 o -13 5 2 58.90 63.31 7.58 o -11 5 2 304.21 295.36 9.90 o -9 5 2 45.37 42.85 3.94 o -7 5 2 744.97 823.07 14.57 o -5 5 2 136.34 157.26 3.73 o -3 5 2 83.04 88.24 3.90 o -1 5 2 167.50 139.13 4.17 o 1 5 2 1192.25 1347.09 25.91 o 3 5 2 1592.30 1878.51 35.01 o 5 5 2 638.34 633.09 14.58 o 7 5 2 930.95 947.09 20.73 o 9 5 2 159.65 170.47 5.45 o 11 5 2 212.85 205.64 8.71 o 13 5 2 30.83 25.60 7.50 o -14 6 2 575.23 555.33 18.15 o -12 6 2 557.50 564.42 15.28 o -10 6 2 3446.20 3391.49 58.99 o -8 6 2 1538.72 1475.03 27.19 o -6 6 2 319.97 361.14 7.56 o -4 6 2 18935.06 19541.32 309.88 o -2 6 2 3322.91 3178.41 57.38 o 0 6 2 1121.47 1580.54 33.05 o 2 6 2 23120.52 23553.41 437.47 o 4 6 2 6013.51 6335.27 101.19 o 6 6 2 8689.00 8647.07 170.32 o 8 6 2 5044.73 4937.36 84.88 o 10 6 2 19.78 29.75 3.87 o 12 6 2 962.74 1051.44 22.90 o -13 7 2 1.76 6.66 7.55 o -11 7 2 1340.95 1274.40 40.12 o -9 7 2 3710.58 3634.38 62.78 o -7 7 2 15.16 19.41 3.37 o -5 7 2 1642.56 1534.53 27.30 o -3 7 2 628.24 600.81 12.23 o -1 7 2 1789.74 2018.45 34.61 o 1 7 2 2458.06 2284.56 43.50 o 3 7 2 498.33 439.92 10.71 o 5 7 2 76.21 68.82 3.03 o 7 7 2 2716.82 2495.71 43.36 o 9 7 2 2999.93 2808.48 49.11 o 11 7 2 77.60 77.98 5.22 o 13 7 2 262.45 272.29 13.28 o -12 8 2 1984.70 2030.14 43.69 o -10 8 2 2957.24 2875.99 54.41 o -8 8 2 766.48 830.65 26.20 o -6 8 2 2719.22 2655.52 46.14 o -4 8 2 905.76 773.47 13.03 o -2 8 2 10852.10 10868.10 170.86 o 0 8 2 10596.41 10890.05 171.51 o 2 8 2 2991.63 3009.24 52.20 o 4 8 2 7385.34 7274.37 132.66 o 6 8 2 2433.82 2591.13 45.28 o 8 8 2 3601.72 3515.14 63.68 o 10 8 2 2580.33 2657.06 46.85 o 12 8 2 247.50 253.68 15.50 o -13 9 2 37.44 36.22 10.12 o -11 9 2 51.41 61.62 8.11 o -9 9 2 354.91 368.95 12.57 o -7 9 2 36.15 45.10 7.22 o -5 9 2 332.50 310.92 10.67 o -3 9 2 9.92 10.43 3.45 o -1 9 2 466.41 484.15 10.37 o 1 9 2 1616.33 1666.27 29.07 o 3 9 2 88.12 109.04 7.19 o 5 9 2 46.17 58.86 4.11 o 7 9 2 18.86 17.24 3.83 o 9 9 2 940.35 863.77 25.89 o 11 9 2 36.38 69.85 8.35 o -12 10 2 1841.60 1892.43 103.98 o -10 10 2 15.11 9.46 7.07 o -8 10 2 2374.06 2288.15 52.21 o -6 10 2 5705.68 5714.91 113.54 o -4 10 2 12.00 14.48 3.83 o -2 10 2 6696.31 6608.79 110.98 o 0 10 2 14913.29 15122.96 270.11 o 2 10 2 14.03 12.76 3.81 o 4 10 2 6276.17 6570.54 131.28 o 6 10 2 3047.52 3151.71 68.90 o 8 10 2 10.75 7.15 4.92 o 10 10 2 2910.33 3063.24 58.07 o -11 11 2 721.23 664.57 21.09 o -9 11 2 54.96 49.52 7.93 o -7 11 2 358.45 328.03 16.13 o -5 11 2 113.93 102.16 8.54 o -3 11 2 21.96 34.28 4.87 o -1 11 2 1.77 3.66 4.68 o 1 11 2 202.48 202.85 6.81 o 3 11 2 292.60 260.54 8.79 o 5 11 2 1268.55 1128.79 25.07 o 7 11 2 1396.61 1285.80 49.77 o 9 11 2 465.91 446.73 14.94 o -10 12 2 634.49 693.02 23.22 o -8 12 2 2650.65 2751.59 65.07 o -6 12 2 3388.91 3336.52 74.46 o -4 12 2 2499.53 2533.68 77.13 o -2 12 2 511.55 499.17 17.27 o 0 12 2 2545.96 2435.94 44.47 o 2 12 2 1484.55 1526.82 36.53 o 4 12 2 1687.80 1649.71 39.32 o 6 12 2 1993.86 1998.83 51.91 o 8 12 2 1266.26 1333.53 33.43 o -9 13 2 309.65 307.33 18.36 o -7 13 2 57.81 54.23 8.41 o -5 13 2 337.25 360.61 11.94 o -3 13 2 1150.07 1135.44 28.89 o -1 13 2 265.47 248.91 9.81 o 1 13 2 3213.65 2875.09 65.84 o 3 13 2 200.16 229.92 12.50 o 5 13 2 10.30 13.40 7.12 o 7 13 2 734.61 773.19 21.99 o -8 14 2 928.34 948.87 30.54 o -6 14 2 472.07 473.22 17.14 o -4 14 2 4360.02 4461.28 90.40 o -2 14 2 674.86 745.78 21.13 o 0 14 2 445.86 484.75 20.27 o 2 14 2 3470.44 3377.78 77.02 o 4 14 2 103.97 118.19 12.61 o 6 14 2 344.04 309.37 12.92 o -5 15 2 10.88 11.55 10.98 o -3 15 2 160.40 165.12 16.60 o -1 15 2 6.84 5.84 11.05 o 1 15 2 113.70 108.88 9.78 o 3 15 2 0.41 4.46 9.27 o 5 15 2 209.24 208.77 13.53 o -4 16 2 1160.25 1192.10 37.01 o -2 16 2 984.36 901.09 38.70 o 0 16 2 272.30 303.37 14.01 o 2 16 2 2114.81 2077.04 56.50 o -15 1 3 3109.44 3243.08 95.68 o -13 1 3 241.32 269.67 8.61 o -11 1 3 5217.58 5192.94 93.24 o -9 1 3 7346.57 7053.51 130.87 o -7 1 3 601.98 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