#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/34/2203448.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203448_Fobs loop_ _publ_author_name 'Meijboom, Reinout' 'Muller, Alfred' 'Roodt, Andreas' _publ_section_title ; trans-Carbonylchlorobis[tris(2,6-dimethylphenyl)phosphito]rhodium(I) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m455 _journal_page_last m457 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.685 _cell_angle_beta 89.773 _cell_angle_gamma 75.016 _cell_length_a 12.3892 _cell_length_b 13.1262 _cell_length_c 14.6675 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.7496 _[local]_cod_data_source_file hg6027Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rmvasm in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 239.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 176.23 126.55 84.44 o 2 0 0 17425.29 16398.10 332.54 o 3 0 0 720.51 792.11 24.08 o 4 0 0 3471.32 3526.21 72.14 o 5 0 0 87.51 81.92 10.05 o 6 0 0 15945.42 15938.96 392.04 o 7 0 0 584.51 638.58 22.52 o 8 0 0 622.98 530.43 32.87 o 9 0 0 0.62 10.88 21.67 o 10 0 0 263.65 277.30 30.58 o 11 0 0 11.36 12.88 28.51 o 12 0 0 984.52 991.34 72.63 o 13 0 0 38.86 76.64 48.49 o 14 0 0 543.75 513.67 68.92 o 15 0 0 30.75 11.20 70.06 o -15 1 0 220.84 267.97 68.25 o -14 1 0 24.03 46.51 58.72 o -13 1 0 866.39 1040.33 85.12 o -12 1 0 12.35 21.66 42.87 o -11 1 0 148.02 139.49 44.88 o -10 1 0 11.60 25.86 26.66 o 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154.79 14.63 o 5 5 0 3094.66 2969.27 50.86 o 6 5 0 93.09 67.84 23.58 o 7 5 0 1576.01 1281.43 267.10 o 8 5 0 59.34 37.46 16.33 o 9 5 0 1954.59 2114.69 44.35 o 10 5 0 125.61 176.53 27.84 o 11 5 0 1403.45 1579.66 71.23 o 12 5 0 106.12 34.67 50.37 o 13 5 0 498.47 434.75 59.11 o 14 5 0 21.03 -12.66 96.41 o 15 5 0 168.66 224.09 110.26 o 16 5 0 26.27 85.99 68.05 o -13 6 0 4.38 -89.55 88.15 o -12 6 0 159.74 110.22 58.38 o -11 6 0 9.43 16.72 42.48 o -10 6 0 991.11 1122.15 63.16 o -9 6 0 23.63 51.77 32.57 o -8 6 0 575.35 561.11 40.51 o -7 6 0 1.14 -3.72 24.24 o -6 6 0 392.08 404.75 31.05 o -5 6 0 331.13 336.73 26.18 o -4 6 0 3698.43 3729.97 61.48 o -3 6 0 18.15 73.32 26.03 o -2 6 0 759.70 704.56 23.05 o -1 6 0 7.16 6.50 9.82 o 0 6 0 2542.21 2698.33 108.86 o 1 6 0 1.37 11.21 21.97 o 2 6 0 6931.91 7157.51 285.92 o 3 6 0 25.57 30.19 12.44 o 4 6 0 794.88 727.12 28.37 o 5 6 0 18.24 33.00 17.80 o 6 6 0 4744.27 4768.03 130.20 o 7 6 0 368.66 313.85 48.76 o 8 6 0 1278.70 1104.80 84.02 o 9 6 0 28.01 13.01 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