#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/34/2203489.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203489_Fobs loop_ _publ_author_name 'Liu, Jia-Geng' 'Xu, Duan-Jun' _publ_section_title ; Bis(2,2'-diamino-4,4'-bi-1,3-thiazole-\k^2^N,N')(isothiocyanato-\kN)(methanol)nickel(II) chloride ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m403 _journal_page_last m405 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.422 _cell_angle_gamma 90.000 _cell_length_a 8.6493 _cell_length_b 32.0885 _cell_length_c 8.3107 _exptl_crystal_F_000 1184.00 _reflns_d_resolution_high 0.8130 _[local]_cod_data_source_file om6223Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' l5 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 327.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14045.45 13918.55 891.76 o 2 0 0 352.91 250.48 126.66 o 3 0 0 27995.38 23072.49 4681.86 o 4 0 0 6549.47 5179.81 1966.56 o 5 0 0 3410.16 3216.08 673.82 o 6 0 0 7288.67 7160.54 269.88 o 7 0 0 1568.81 1514.34 164.82 o 8 0 0 9.44 -28.80 102.99 o 9 0 0 3505.04 3167.77 356.31 o 10 0 0 6.91 36.61 155.22 o 1 1 0 1649.57 1276.67 341.47 o 2 1 0 4811.21 4400.19 1120.12 o 3 1 0 7689.74 6606.64 1599.54 o 4 1 0 1927.87 1364.52 366.62 o 5 1 0 1536.90 1280.94 368.06 o 6 1 0 691.88 372.87 142.04 o 7 1 0 2351.25 2422.30 155.13 o 8 1 0 1890.93 2114.74 211.63 o 9 1 0 1803.48 2100.39 231.04 o 10 1 0 42.09 34.30 111.47 o 0 2 0 39.97 31.73 19.52 o 1 2 0 454.97 456.46 18.85 o 2 2 0 3975.50 4135.08 94.05 o 3 2 0 945.59 842.01 59.90 o 4 2 0 418.73 400.16 48.45 o 5 2 0 3542.89 3181.39 206.52 o 6 2 0 6544.22 5862.14 630.17 o 7 2 0 918.06 629.81 227.23 o 8 2 0 47.89 57.16 80.89 o 9 2 0 632.90 575.39 144.74 o 10 2 0 387.49 409.99 145.03 o 1 3 0 1796.85 1720.89 39.66 o 2 3 0 1349.83 1293.51 43.30 o 3 3 0 3776.58 3480.25 108.48 o 4 3 0 712.80 897.25 68.63 o 5 3 0 3805.90 3603.20 127.70 o 6 3 0 1419.32 1333.33 102.58 o 7 3 0 852.60 920.79 97.01 o 8 3 0 17.52 22.37 75.73 o 9 3 0 181.53 158.53 111.67 o 10 3 0 695.14 649.43 167.70 o 0 4 0 5452.39 5127.01 133.74 o 1 4 0 16403.45 16489.10 230.16 o 2 4 0 3.04 13.52 14.99 o 3 4 0 8.92 11.72 23.63 o 4 4 0 35.50 11.16 25.06 o 5 4 0 7580.31 7291.67 171.80 o 6 4 0 2880.42 2871.03 125.54 o 7 4 0 2523.94 2362.69 149.13 o 8 4 0 1754.72 1981.23 168.22 o 9 4 0 309.47 271.48 118.98 o 10 4 0 147.41 244.67 135.44 o 1 5 0 279.96 314.44 23.75 o 2 5 0 23038.96 22751.32 354.32 o 3 5 0 1020.43 1084.19 57.77 o 4 5 0 1147.56 1143.82 86.48 o 5 5 0 1727.35 1608.36 105.07 o 6 5 0 427.92 345.59 62.51 o 7 5 0 2745.51 2813.57 170.46 o 8 5 0 725.38 713.29 113.38 o 9 5 0 1251.25 1463.43 205.98 o 10 5 0 20.71 -34.84 105.61 o 0 6 0 159.42 238.19 47.35 o 1 6 0 29260.39 31409.05 250.20 o 2 6 0 1213.41 1377.73 46.86 o 3 6 0 459.41 505.23 41.01 o 4 6 0 1468.18 1375.88 74.03 o 5 6 0 37.69 4.50 32.64 o 6 6 0 1415.57 1406.95 131.04 o 7 6 0 49.53 5.77 52.46 o 8 6 0 1100.32 1188.39 141.48 o 9 6 0 15.48 -25.27 89.07 o 10 6 0 25.32 31.78 114.69 o 1 7 0 76.54 51.00 34.34 o 2 7 0 3735.99 3623.66 80.10 o 3 7 0 5563.55 5234.75 104.32 o 4 7 0 4307.98 4422.80 123.71 o 5 7 0 1924.22 1909.45 95.57 o 6 7 0 4406.93 4503.46 157.77 o 7 7 0 449.52 305.88 81.54 o 8 7 0 3783.91 3701.83 203.57 o 9 7 0 71.51 28.63 96.18 o 10 7 0 105.00 -0.98 162.05 o 0 8 0 9371.41 10741.15 285.54 o 1 8 0 7233.40 7436.31 168.66 o 2 8 0 7064.80 6907.74 112.66 o 3 8 0 482.56 453.34 40.17 o 4 8 0 4700.70 4414.17 124.47 o 5 8 0 53.08 14.45 33.39 o 6 8 0 5308.78 5168.54 165.01 o 7 8 0 157.19 53.28 59.93 o 8 8 0 183.58 151.60 84.08 o 9 8 0 475.95 488.48 139.95 o 10 8 0 1907.37 1949.47 360.71 o 1 9 0 2835.11 2749.10 110.62 o 2 9 0 49.94 54.42 21.51 o 3 9 0 5784.63 5572.32 110.81 o 4 9 0 971.49 1009.42 63.81 o 5 9 0 1899.45 1554.42 89.38 o 6 9 0 249.21 150.72 52.51 o 7 9 0 519.41 516.69 94.40 o 8 9 0 288.84 274.44 89.26 o 9 9 0 133.53 149.07 111.25 o 10 9 0 10.86 41.49 160.10 o 0 10 0 535.64 575.47 88.83 o 1 10 0 224.53 205.32 45.21 o 2 10 0 1357.58 1349.79 58.46 o 3 10 0 1974.94 1850.93 68.49 o 4 10 0 880.47 847.61 60.95 o 5 10 0 803.74 797.57 75.26 o 6 10 0 1960.36 1879.12 111.16 o 7 10 0 1375.36 1488.75 142.88 o 8 10 0 338.89 291.98 93.48 o 9 10 0 962.65 1130.15 182.91 o 10 10 0 589.55 509.58 229.90 o 1 11 0 5945.86 6390.25 184.75 o 2 11 0 5018.90 4886.97 123.50 o 3 11 0 10400.17 10202.70 154.13 o 4 11 0 193.75 200.24 39.17 o 5 11 0 1766.90 1814.64 98.79 o 6 11 0 2625.34 2575.80 149.34 o 7 11 0 1158.40 948.36 119.17 o 8 11 0 566.52 527.69 108.26 o 9 11 0 1043.85 857.10 251.86 o 10 11 0 556.17 497.37 235.26 o 0 12 0 442.05 506.16 91.76 o 1 12 0 2418.49 2444.38 123.73 o 2 12 0 5485.35 4770.05 1197.36 o 3 12 0 1706.91 1860.57 73.13 o 4 12 0 12670.28 13107.68 197.10 o 5 12 0 11341.88 11013.69 230.11 o 6 12 0 1024.73 1030.08 114.77 o 7 12 0 52.03 14.18 61.24 o 8 12 0 576.26 509.68 111.28 o 9 12 0 145.72 103.48 156.68 o 1 13 0 18659.98 20676.48 287.85 o 2 13 0 5441.34 5826.93 145.60 o 3 13 0 276.04 267.11 38.18 o 4 13 0 4910.43 4711.68 122.87 o 5 13 0 5174.60 5079.30 139.83 o 6 13 0 146.06 70.38 55.52 o 7 13 0 1902.29 1949.76 163.59 o 8 13 0 4789.98 4961.30 240.26 o 9 13 0 267.88 172.63 124.13 o 0 14 0 364.34 434.90 94.69 o 1 14 0 3588.04 4010.28 132.69 o 2 14 0 1117.61 1114.89 74.14 o 3 14 0 60.37 90.31 33.99 o 4 14 0 385.18 438.44 52.15 o 5 14 0 3098.47 2970.78 128.12 o 6 14 0 3918.88 3750.65 186.31 o 7 14 0 0.71 -23.59 61.12 o 8 14 0 1563.66 1568.58 166.45 o 9 14 0 343.18 291.81 133.74 o 1 15 0 4549.73 4676.50 148.97 o 2 15 0 7286.28 6631.34 164.24 o 3 15 0 5728.75 5546.62 134.78 o 4 15 0 3764.22 3721.74 116.23 o 5 15 0 160.70 157.16 53.35 o 6 15 0 2985.73 2895.79 168.21 o 7 15 0 4318.98 4210.64 212.28 o 8 15 0 3018.88 2955.81 262.41 o 9 15 0 987.37 992.26 192.31 o 0 16 0 14632.43 15059.86 469.55 o 1 16 0 3810.71 4114.12 142.16 o 2 16 0 4676.77 4790.71 147.63 o 3 16 0 1022.56 1043.65 82.67 o 4 16 0 4037.75 3850.46 119.09 o 5 16 0 1686.70 1660.71 111.56 o 6 16 0 27.62 13.43 55.80 o 7 16 0 16.02 18.45 64.78 o 8 16 0 60.66 46.06 101.08 o 9 16 0 29.55 7.89 114.71 o 1 17 0 845.81 879.80 83.10 o 2 17 0 126.91 90.78 40.67 o 3 17 0 116.64 87.50 42.58 o 4 17 0 428.44 389.53 53.84 o 5 17 0 431.65 444.77 72.73 o 6 17 0 2.24 -11.25 55.75 o 7 17 0 1615.95 1666.41 163.95 o 8 17 0 546.15 486.03 144.96 o 9 17 0 381.26 449.56 156.98 o 0 18 0 11888.97 14181.28 492.49 o 1 18 0 5.50 17.88 35.94 o 2 18 0 1140.94 1166.54 92.88 o 3 18 0 319.53 292.06 58.53 o 4 18 0 1381.82 1443.81 125.53 o 5 18 0 185.44 180.00 67.53 o 6 18 0 254.29 223.92 77.84 o 7 18 0 6.94 1.49 67.87 o 8 18 0 11.60 -20.12 99.07 o 9 18 0 43.07 12.26 121.30 o 1 19 0 5767.46 5860.78 184.58 o 2 19 0 30.01 3.02 34.43 o 3 19 0 4255.34 4265.93 158.44 o 4 19 0 31.62 33.87 50.95 o 5 19 0 2300.41 2304.39 158.25 o 6 19 0 472.36 389.27 94.37 o 7 19 0 3388.41 3266.19 257.92 o 8 19 0 584.00 625.72 167.24 o 9 19 0 558.94 427.06 166.23 o 0 20 0 9288.68 9421.32 414.89 o 1 20 0 437.57 568.87 76.34 o 2 20 0 2776.98 2674.19 126.38 o 3 20 0 1416.90 1491.26 109.49 o 4 20 0 29.34 13.86 50.94 o 5 20 0 2410.61 2407.22 160.26 o 6 20 0 307.29 227.93 83.06 o 7 20 0 39.92 21.86 94.87 o 8 20 0 9.66 -8.49 108.13 o 1 21 0 106.33 70.66 46.99 o 2 21 0 875.52 926.28 92.29 o 3 21 0 1670.79 1744.60 156.07 o 4 21 0 1294.83 1418.27 133.14 o 5 21 0 87.49 55.73 63.99 o 6 21 0 112.76 120.97 79.14 o 7 21 0 1255.03 1177.48 191.89 o 8 21 0 571.15 392.11 151.17 o 0 22 0 21.33 24.69 56.99 o 1 22 0 2645.38 2884.23 147.47 o 2 22 0 11.16 36.22 43.75 o 3 22 0 1893.64 1875.54 163.62 o 4 22 0 2.97 5.87 51.54 o 5 22 0 407.16 462.54 103.14 o 6 22 0 1436.00 1381.93 201.14 o 7 22 0 0.47 -12.65 96.58 o 8 22 0 107.88 42.62 114.48 o 1 23 0 6819.79 6677.46 222.01 o 2 23 0 10701.86 10953.31 265.58 o 3 23 0 10.56 -3.97 56.71 o 4 23 0 21.12 9.78 53.44 o 5 23 0 908.48 1002.33 135.62 o 6 23 0 54.97 20.16 89.92 o 7 23 0 137.55 108.64 110.32 o 8 23 0 5265.78 5358.16 362.27 o 0 24 0 3133.25 3184.35 202.89 o 1 24 0 1624.84 1833.97 127.86 o 2 24 0 10.03 3.86 55.54 o 3 24 0 0.72 -8.18 61.36 o 4 24 0 355.79 321.43 86.68 o 5 24 0 367.13 369.52 94.93 o 6 24 0 1309.95 1547.07 225.24 o 7 24 0 1106.91 1244.87 205.78 o 8 24 0 97.86 56.96 124.98 o 1 25 0 430.92 372.45 78.22 o 2 25 0 553.98 498.70 105.00 o 3 25 0 3492.35 3349.19 216.20 o 4 25 0 214.68 186.77 77.36 o 5 25 0 21.13 28.09 72.05 o 6 25 0 553.92 562.43 157.88 o 7 25 0 30.80 5.85 112.13 o 8 25 0 741.64 690.16 186.95 o 0 26 0 881.27 945.25 137.17 o 1 26 0 2829.46 2760.17 194.43 o 2 26 0 449.63 397.14 101.47 o 3 26 0 60.94 98.60 77.31 o 4 26 0 1913.56 2102.16 177.21 o 5 26 0 676.36 599.15 148.98 o 6 26 0 4.32 -51.61 93.93 o 7 26 0 43.66 45.46 114.46 o 1 27 0 705.98 689.69 176.20 o 2 27 0 23.63 55.94 71.67 o 3 27 0 5033.95 4812.71 264.04 o 4 27 0 2898.93 2783.58 189.23 o 5 27 0 210.29 171.07 107.42 o 6 27 0 670.21 655.32 171.28 o 7 27 0 747.58 698.04 179.96 o 0 28 0 3439.06 3726.09 237.72 o 1 28 0 2170.90 2292.93 200.42 o 2 28 0 6763.27 6715.06 316.56 o 3 28 0 725.54 534.15 123.82 o 4 28 0 1990.70 2189.55 184.21 o 5 28 0 5.86 -21.56 95.62 o 6 28 0 1559.77 1562.02 232.22 o 7 28 0 356.79 286.47 152.96 o 1 29 0 21.80 8.45 75.02 o 2 29 0 8.21 4.83 70.21 o 3 29 0 562.12 443.54 120.42 o 4 29 0 383.25 336.08 124.11 o 5 29 0 174.41 136.13 112.09 o 6 29 0 1.58 -28.78 108.42 o 7 29 0 5.63 -61.28 112.01 o 0 30 0 4062.95 4583.96 336.30 o 1 30 0 9.71 -27.56 71.34 o 2 30 0 1517.22 1647.16 194.13 o 3 30 0 444.17 553.72 131.67 o 4 30 0 16.80 -28.63 87.45 o 5 30 0 901.24 958.62 189.13 o 6 30 0 631.69 563.98 176.01 o 1 31 0 53.74 44.89 68.05 o 2 31 0 2225.39 2406.29 217.35 o 3 31 0 1161.82 1113.98 173.06 o 4 31 0 162.12 65.07 101.07 o 5 31 0 34.68 2.53 105.93 o 6 31 0 180.23 85.78 125.50 o 0 32 0 124.92 164.12 99.74 o 1 32 0 17.02 0.36 67.50 o 2 32 0 174.83 147.78 103.83 o 3 32 0 120.55 91.76 138.62 o 4 32 0 1.53 16.42 101.80 o 5 32 0 785.41 757.20 186.03 o 6 32 0 1075.85 1011.43 217.60 o 1 33 0 10.65 8.08 74.27 o 2 33 0 0.59 -79.30 79.30 o 3 33 0 1885.31 1864.54 331.91 o 4 33 0 181.68 152.68 115.47 o 5 33 0 225.28 155.54 136.59 o 0 34 0 717.18 822.78 162.91 o 1 34 0 1034.32 970.26 136.78 o 2 34 0 10.55 17.06 95.60 o 3 34 0 567.34 696.03 228.43 o 4 34 0 402.34 447.14 153.16 o 5 34 0 1352.33 1408.04 231.22 o 1 35 0 450.60 395.28 106.58 o 2 35 0 188.72 158.14 161.56 o 3 35 0 2126.73 2191.08 353.87 o 4 35 0 2654.58 2901.60 305.42 o 0 36 0 4501.71 4510.17 292.70 o 1 36 0 56.19 12.63 84.79 o 2 36 0 224.86 68.62 88.50 o 3 36 0 1544.13 1628.79 331.42 o 4 36 0 101.22 9.82 124.48 o 1 37 0 10.22 -36.38 91.53 o 2 37 0 25.86 -66.60 99.50 o 3 37 0 693.26 666.31 170.15 o 0 38 0 77.99 99.08 156.19 o 1 38 0 72.05 13.55 112.55 o 2 38 0 19.29 -3.80 111.98 o 1 39 0 528.13 338.40 143.35 o -10 1 1 38.33 0.12 103.01 o -9 1 1 2351.01 2380.92 248.43 o -8 1 1 2734.13 2619.59 220.36 o -7 1 1 20.26 20.37 63.94 o -6 1 1 46.81 12.48 35.28 o -5 1 1 4434.64 4263.95 124.30 o -4 1 1 1983.30 1906.54 74.04 o -3 1 1 19525.17 20360.46 195.89 o -2 1 1 750.10 758.68 45.45 o -1 1 1 18902.58 20131.40 550.80 o 0 1 1 0.94 1.16 5.36 o 1 1 1 19114.42 20299.93 251.72 o 2 1 1 3068.70 3180.48 82.57 o 3 1 1 1413.73 1404.02 65.93 o 4 1 1 53.15 83.89 33.22 o 5 1 1 562.91 512.64 64.46 o 6 1 1 61.73 53.23 46.49 o 7 1 1 6374.12 6572.71 218.56 o 8 1 1 1712.28 1827.53 172.23 o 9 1 1 57.93 32.47 100.32 o -10 2 1 484.73 448.89 150.45 o -9 2 1 91.88 108.81 100.19 o -8 2 1 15.62 70.11 82.38 o -7 2 1 326.77 341.31 81.46 o -6 2 1 2212.09 2126.26 125.83 o -5 2 1 4423.23 4454.41 172.54 o -4 2 1 2227.72 2269.58 84.05 o -3 2 1 46.38 45.39 19.78 o -2 2 1 8475.48 9207.23 158.17 o -1 2 1 6770.56 7127.64 95.38 o 0 2 1 32906.21 26272.97 3152.69 o 1 2 1 11052.27 11766.82 185.01 o 2 2 1 47.59 52.35 20.88 o 3 2 1 4779.99 4842.19 117.81 o 4 2 1 9613.52 9917.50 249.97 o 5 2 1 1692.63 1772.48 99.17 o 6 2 1 6830.07 7239.22 207.45 o 7 2 1 365.19 405.93 92.46 o 8 2 1 2.80 -32.09 66.69 o 9 2 1 882.17 1052.41 181.13 o 10 2 1 13.84 -35.14 156.19 o -10 3 1 280.44 384.06 148.86 o -9 3 1 1436.54 1433.35 203.93 o -8 3 1 9042.64 9021.38 379.68 o -7 3 1 1073.37 985.88 120.13 o -6 3 1 1776.71 1779.75 101.21 o -5 3 1 5011.20 4834.59 164.41 o -4 3 1 106.08 72.23 29.17 o -3 3 1 531.91 421.91 36.47 o -2 3 1 1890.00 1993.74 76.61 o -1 3 1 1554.71 1672.96 54.83 o 0 3 1 246.97 236.31 14.36 o 1 3 1 5025.27 4940.24 121.46 o 2 3 1 6652.31 6702.90 114.18 o 3 3 1 88.47 38.08 23.69 o 4 3 1 148.82 134.13 37.96 o 5 3 1 39.90 48.79 38.21 o 6 3 1 140.24 148.87 53.27 o 7 3 1 45.52 -11.60 48.17 o 8 3 1 5277.04 5218.26 239.22 o 9 3 1 979.21 942.32 172.21 o 10 3 1 146.67 149.36 172.30 o -10 4 1 224.32 161.92 125.33 o -9 4 1 135.74 147.10 104.40 o -8 4 1 19.15 -11.51 72.89 o -7 4 1 1051.40 1054.36 115.93 o -6 4 1 1036.50 890.78 172.33 o -5 4 1 392.22 275.17 59.07 o -4 4 1 4968.22 4575.17 538.51 o -3 4 1 1953.50 1921.73 89.61 o -2 4 1 81.44 106.87 29.03 o -1 4 1 5256.72 5167.13 74.07 o 0 4 1 3067.50 2939.13 85.34 o 1 4 1 7122.28 7011.76 229.88 o 2 4 1 12616.49 13171.48 161.44 o 3 4 1 4818.18 4903.20 117.77 o 4 4 1 130.44 85.98 33.52 o 5 4 1 2896.49 2930.38 121.83 o 6 4 1 2327.77 2268.12 119.18 o 7 4 1 954.60 880.40 97.31 o 8 4 1 467.75 604.49 110.37 o 9 4 1 468.65 547.65 212.32 o 10 4 1 656.72 910.31 268.46 o -10 5 1 520.60 513.09 159.40 o -9 5 1 420.38 427.47 135.45 o -8 5 1 1298.64 1273.31 171.12 o -7 5 1 5049.44 4914.37 204.77 o -6 5 1 5557.58 5205.76 246.70 o -5 5 1 78.69 44.28 33.07 o -4 5 1 4239.07 3314.26 323.55 o -3 5 1 5585.90 5412.42 144.92 o -2 5 1 24808.32 24716.22 585.18 o -1 5 1 20992.13 22322.52 387.87 o 0 5 1 1494.02 1469.92 41.27 o 1 5 1 459.01 448.38 32.05 o 2 5 1 19750.81 19522.01 257.10 o 3 5 1 167.49 184.05 34.94 o 4 5 1 176.83 143.87 39.62 o 5 5 1 1513.56 1650.61 112.30 o 6 5 1 844.70 747.38 96.00 o 7 5 1 890.29 748.84 210.62 o 8 5 1 2765.07 2602.02 176.07 o 9 5 1 145.10 137.64 158.14 o 10 5 1 54.77 0.49 159.12 o -10 6 1 1380.27 1342.96 220.35 o -9 6 1 704.21 716.46 158.61 o -8 6 1 205.50 151.25 93.51 o -7 6 1 9.31 -32.54 47.33 o -6 6 1 2944.19 2451.91 447.14 o -5 6 1 7985.38 8328.20 175.04 o -4 6 1 10319.77 10350.70 153.20 o -3 6 1 336.91 308.09 47.90 o -2 6 1 27522.23 28082.36 397.03 o -1 6 1 47103.58 50867.84 367.93 o 0 6 1 6060.81 6451.03 162.39 o 1 6 1 5950.35 5977.94 120.03 o 2 6 1 2.74 3.43 18.66 o 3 6 1 1348.94 1453.44 69.10 o 4 6 1 368.15 396.71 51.73 o 5 6 1 13602.28 13804.35 252.58 o 6 6 1 1491.33 1307.38 358.74 o 7 6 1 1978.15 1766.22 501.11 o 8 6 1 468.75 449.41 101.45 o 9 6 1 317.36 195.24 158.14 o 10 6 1 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