#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:04:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180955 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/35/2203528.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203528_Fobs loop_ _publ_author_name 'Gao, Shan' 'Zhang, Zhu-Yan' 'Huo, Li-Hua' 'Zhao, Hui' 'Zhao, Jing-Gui' _publ_section_title ; Hexaaquazinc(II) bis[(4-oxo-4H-pyridin-1-yl)acetate] dihydrate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m444 _journal_page_last m446 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.620 _cell_angle_gamma 90.000 _cell_length_a 12.4269 _cell_length_b 12.8331 _cell_length_c 6.7816 _exptl_crystal_F_000 536.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file ww6176Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gao388 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 130.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2997.79 2765.25 60.76 o 3 0 0 2438.53 2590.25 48.59 o 4 0 0 13528.23 11589.20 569.44 o 5 0 0 13137.12 11543.63 359.34 o 6 0 0 9.78 10.89 2.10 o 7 0 0 5763.81 6003.70 63.30 o 8 0 0 1892.52 1969.29 11.59 o 9 0 0 1069.64 1107.92 18.86 o 10 0 0 850.02 875.14 10.36 o 11 0 0 2297.37 2222.40 31.29 o 12 0 0 97.47 119.19 1.60 o 13 0 0 248.48 240.86 10.98 o 14 0 0 30.73 33.94 1.34 o 15 0 0 64.24 55.24 2.16 o 2 1 0 351.53 392.05 4.97 o 3 1 0 8.50 10.17 1.22 o 4 1 0 14.78 9.74 0.61 o 5 1 0 62.60 63.77 1.72 o 6 1 0 209.90 178.34 1.73 o 7 1 0 1588.97 1791.84 17.43 o 8 1 0 112.95 142.11 1.05 o 9 1 0 27.19 19.85 0.65 o 10 1 0 69.04 58.96 1.41 o 11 1 0 158.44 148.93 2.60 o 12 1 0 79.10 72.67 2.26 o 13 1 0 25.14 25.51 1.26 o 14 1 0 50.13 50.19 1.28 o 15 1 0 52.02 41.63 1.34 o 0 2 0 1462.34 1304.38 21.55 o 1 2 0 2268.11 2201.45 17.19 o 2 2 0 7593.29 7016.55 110.71 o 3 2 0 3148.62 3244.67 66.67 o 4 2 0 788.37 830.43 9.39 o 5 2 0 3539.01 3797.90 66.29 o 6 2 0 5652.47 5747.86 45.42 o 7 2 0 3000.35 3111.48 46.63 o 8 2 0 284.32 281.59 2.30 o 9 2 0 39.76 38.48 0.71 o 10 2 0 140.16 151.33 1.19 o 11 2 0 382.59 396.04 4.84 o 12 2 0 435.89 434.98 7.70 o 13 2 0 425.57 408.58 9.90 o 14 2 0 142.60 144.68 1.90 o 15 2 0 30.55 29.18 1.16 o 1 3 0 793.51 859.59 8.81 o 2 3 0 544.69 535.64 6.39 o 3 3 0 8.45 9.02 0.66 o 4 3 0 1236.19 1315.13 9.73 o 5 3 0 1018.10 1119.33 15.34 o 6 3 0 2.05 6.43 0.48 o 7 3 0 50.22 62.16 0.88 o 8 3 0 12.41 11.94 0.60 o 9 3 0 17.35 18.54 0.88 o 10 3 0 68.64 74.05 0.92 o 11 3 0 332.81 333.82 1.57 o 12 3 0 61.21 57.73 1.26 o 13 3 0 8.49 6.98 1.41 o 14 3 0 1.63 1.79 1.02 o 15 3 0 15.23 12.08 1.87 o 0 4 0 6854.69 6469.08 135.52 o 1 4 0 16228.27 13821.69 198.21 o 2 4 0 164.76 151.39 1.49 o 3 4 0 56.34 66.71 0.81 o 4 4 0 292.78 267.63 4.20 o 5 4 0 205.00 179.43 2.31 o 6 4 0 3909.50 4322.04 40.73 o 7 4 0 7.20 6.50 0.77 o 8 4 0 538.54 584.00 6.27 o 9 4 0 412.53 436.05 1.66 o 10 4 0 370.23 380.67 3.45 o 11 4 0 99.62 111.56 1.71 o 12 4 0 1031.35 1015.74 17.37 o 13 4 0 59.55 61.29 1.22 o 14 4 0 85.74 78.33 3.08 o 15 4 0 64.16 65.09 1.98 o 1 5 0 2005.06 2139.06 13.87 o 2 5 0 98.33 100.99 0.81 o 3 5 0 999.51 987.56 2.27 o 4 5 0 337.14 339.56 4.34 o 5 5 0 60.93 55.96 0.72 o 6 5 0 19.65 24.13 0.72 o 7 5 0 8.68 8.26 0.67 o 8 5 0 16.89 17.22 1.11 o 9 5 0 6.39 6.36 0.71 o 10 5 0 46.18 43.03 2.27 o 11 5 0 13.20 11.40 0.78 o 12 5 0 6.72 5.14 0.49 o 13 5 0 0.02 0.95 0.60 o 14 5 0 6.38 10.31 1.76 o 15 5 0 2.99 1.11 2.20 o 0 6 0 2129.66 2207.62 18.39 o 1 6 0 4415.27 4622.52 44.69 o 2 6 0 724.42 706.28 3.82 o 3 6 0 152.74 123.14 1.11 o 4 6 0 1149.19 1084.49 11.04 o 5 6 0 1889.27 1909.15 28.60 o 6 6 0 2115.73 2252.91 33.11 o 7 6 0 429.91 445.60 5.44 o 8 6 0 523.47 557.30 5.95 o 9 6 0 868.06 893.36 16.67 o 10 6 0 711.90 727.35 9.66 o 11 6 0 312.73 295.03 12.95 o 12 6 0 468.71 483.02 8.22 o 13 6 0 275.70 296.13 6.47 o 14 6 0 150.83 153.25 6.08 o 1 7 0 45.46 45.21 0.51 o 2 7 0 210.52 228.41 1.22 o 3 7 0 40.77 44.74 1.03 o 4 7 0 53.85 42.27 0.43 o 5 7 0 118.91 129.58 3.37 o 6 7 0 337.59 332.70 3.18 o 7 7 0 12.36 14.57 1.00 o 8 7 0 16.77 19.34 1.27 o 9 7 0 63.49 63.92 1.81 o 10 7 0 47.49 52.48 1.64 o 11 7 0 1.31 0.23 1.66 o 12 7 0 0.23 0.41 2.10 o 13 7 0 5.12 8.81 2.20 o 14 7 0 3.70 3.28 3.26 o 0 8 0 4426.12 4619.06 67.30 o 1 8 0 124.25 155.29 0.90 o 2 8 0 1861.42 1919.41 11.62 o 3 8 0 1396.99 1432.68 18.47 o 4 8 0 531.43 490.12 7.15 o 5 8 0 1630.61 1578.39 12.37 o 6 8 0 677.53 637.45 5.97 o 7 8 0 2127.15 2238.75 21.53 o 8 8 0 326.02 328.73 3.54 o 9 8 0 46.54 51.57 1.37 o 10 8 0 208.66 216.95 2.13 o 11 8 0 559.78 595.40 6.91 o 12 8 0 112.23 120.61 2.21 o 13 8 0 426.66 446.06 6.38 o 1 9 0 365.81 339.53 3.46 o 2 9 0 0.25 1.17 0.59 o 3 9 0 41.08 38.30 0.92 o 4 9 0 93.74 93.99 1.49 o 5 9 0 308.18 287.79 3.09 o 6 9 0 36.14 36.96 1.12 o 7 9 0 144.69 145.20 2.10 o 8 9 0 90.07 92.09 1.48 o 9 9 0 30.47 26.48 1.41 o 10 9 0 3.29 3.83 1.66 o 11 9 0 113.46 121.88 2.53 o 12 9 0 36.72 36.97 3.24 o 13 9 0 5.39 6.17 2.18 o 0 10 0 2904.81 2833.46 17.04 o 1 10 0 280.41 268.80 1.78 o 2 10 0 34.06 35.11 0.68 o 3 10 0 196.57 196.12 2.69 o 4 10 0 203.09 198.88 2.64 o 5 10 0 174.98 171.65 2.33 o 6 10 0 16.56 16.97 0.57 o 7 10 0 388.05 411.39 4.59 o 8 10 0 332.51 329.68 2.38 o 9 10 0 89.66 90.74 3.04 o 10 10 0 205.25 215.27 2.88 o 11 10 0 473.78 512.84 15.36 o 12 10 0 103.55 108.97 2.39 o 1 11 0 710.39 705.49 3.98 o 2 11 0 262.72 262.69 1.75 o 3 11 0 5.95 5.87 0.84 o 4 11 0 34.69 32.26 1.19 o 5 11 0 63.35 53.72 2.10 o 6 11 0 76.42 66.54 0.94 o 7 11 0 6.53 4.02 1.59 o 8 11 0 0.44 -0.67 1.42 o 9 11 0 47.32 45.46 1.64 o 10 11 0 0.02 -0.97 1.69 o 11 11 0 0.02 1.48 2.12 o 0 12 0 46.43 50.52 1.19 o 1 12 0 981.47 990.28 9.19 o 2 12 0 482.07 491.42 5.27 o 3 12 0 272.68 286.48 4.51 o 4 12 0 409.86 430.39 7.60 o 5 12 0 328.98 324.36 8.10 o 6 12 0 811.72 828.87 4.61 o 7 12 0 91.42 90.80 2.62 o 8 12 0 73.97 88.65 4.91 o 9 12 0 230.65 243.75 7.35 o 10 12 0 43.84 50.70 2.16 o 11 12 0 17.78 19.31 2.27 o 1 13 0 10.27 12.53 1.67 o 2 13 0 5.79 7.95 1.39 o 3 13 0 41.55 38.53 1.08 o 4 13 0 3.96 5.65 0.84 o 5 13 0 18.51 15.17 1.59 o 6 13 0 5.16 6.17 1.73 o 7 13 0 71.49 73.78 2.08 o 8 13 0 63.78 65.64 4.78 o 9 13 0 49.46 54.03 2.43 o 0 14 0 354.21 348.33 10.28 o 1 14 0 736.91 742.06 16.69 o 2 14 0 349.17 352.14 5.24 o 3 14 0 235.08 239.21 5.31 o 4 14 0 545.48 535.37 12.63 o 5 14 0 267.37 278.69 6.10 o 6 14 0 290.39 309.87 2.72 o 7 14 0 129.08 129.97 3.09 o 8 14 0 136.70 150.22 2.65 o 1 15 0 53.31 49.36 2.07 o 2 15 0 5.85 7.69 1.03 o 3 15 0 36.08 32.28 1.54 o 4 15 0 24.68 24.08 1.86 o 5 15 0 5.37 3.43 1.92 o 6 15 0 3.34 1.76 2.04 o 0 16 0 181.26 155.35 7.47 o 1 16 0 51.98 49.22 1.59 o 2 16 0 279.93 255.73 5.44 o 3 16 0 197.22 197.58 2.74 o 4 16 0 15.27 19.78 1.96 o -16 1 1 60.74 55.53 1.92 o -15 1 1 108.66 97.11 4.19 o -14 1 1 208.15 196.57 4.45 o -13 1 1 286.87 277.15 2.85 o -12 1 1 802.58 772.61 9.20 o -11 1 1 331.88 347.22 2.94 o -10 1 1 56.26 61.35 0.91 o -9 1 1 219.06 219.72 1.91 o -8 1 1 1294.52 1269.94 13.51 o -7 1 1 2254.43 2241.90 14.83 o -6 1 1 2593.91 2572.98 35.63 o -5 1 1 1211.43 1235.53 14.29 o -4 1 1 1788.25 1838.60 25.99 o -3 1 1 571.20 533.59 4.74 o -2 1 1 2446.00 2465.29 21.79 o -1 1 1 8751.83 8331.75 61.15 o 0 1 1 679.29 596.91 4.73 o 1 1 1 8907.74 8302.08 193.70 o 2 1 1 4588.50 4607.67 43.47 o 3 1 1 1405.88 1491.18 5.77 o 4 1 1 2488.29 2606.44 7.14 o 5 1 1 5683.16 5966.45 31.13 o 6 1 1 7950.13 8538.77 31.66 o 7 1 1 1685.93 1618.30 10.08 o 8 1 1 123.37 137.10 3.03 o 9 1 1 1258.16 1324.68 15.95 o 10 1 1 559.63 617.62 10.72 o 11 1 1 639.20 638.36 4.43 o 12 1 1 835.53 820.27 11.10 o 13 1 1 325.78 326.64 7.55 o 14 1 1 132.80 139.84 2.18 o 15 1 1 28.21 22.40 1.37 o -16 2 1 9.59 11.40 1.77 o -15 2 1 3.37 2.42 1.03 o -14 2 1 0.36 0.42 0.75 o -13 2 1 7.76 3.81 0.70 o -12 2 1 318.49 279.03 4.42 o -11 2 1 270.75 241.07 3.63 o -10 2 1 6.04 5.34 0.55 o -9 2 1 6.78 11.45 0.74 o -8 2 1 17.29 17.96 1.23 o -7 2 1 2084.89 2268.28 13.66 o -6 2 1 569.19 705.89 5.45 o -5 2 1 2.51 1.89 0.44 o -4 2 1 309.51 311.21 1.34 o -3 2 1 3.96 11.81 0.34 o -2 2 1 210.63 181.09 1.79 o -1 2 1 3514.95 3529.48 42.10 o 0 2 1 5365.47 5400.91 77.14 o 1 2 1 2883.80 3078.11 26.80 o 2 2 1 336.81 377.80 6.37 o 3 2 1 3898.55 4182.89 43.76 o 4 2 1 9.57 11.77 0.96 o 5 2 1 33.70 41.14 0.74 o 6 2 1 0.35 1.81 0.54 o 7 2 1 154.73 171.04 3.97 o 8 2 1 50.65 49.48 0.79 o 9 2 1 195.70 189.46 2.98 o 10 2 1 393.88 417.63 4.52 o 11 2 1 263.87 250.87 1.73 o 12 2 1 8.65 10.02 1.09 o 13 2 1 47.91 45.44 1.34 o 14 2 1 5.93 5.20 1.42 o 15 2 1 17.13 19.93 1.31 o -15 3 1 28.78 28.24 1.87 o -14 3 1 93.13 92.10 5.34 o -13 3 1 195.14 186.50 5.93 o -12 3 1 45.76 44.06 2.53 o -11 3 1 583.25 567.14 7.74 o -10 3 1 969.48 954.83 13.44 o -9 3 1 274.42 281.76 4.95 o -8 3 1 79.42 73.70 1.47 o -7 3 1 660.63 680.68 10.66 o -6 3 1 1840.62 1829.59 29.92 o -5 3 1 972.62 884.73 10.66 o -4 3 1 932.74 1029.80 3.09 o -3 3 1 249.85 249.50 6.19 o -2 3 1 3741.56 3914.57 15.37 o -1 3 1 3118.38 3139.84 11.05 o 0 3 1 16926.64 14958.59 269.55 o 1 3 1 196.76 198.77 1.92 o 2 3 1 11.25 11.74 0.56 o 3 3 1 53.87 32.66 0.58 o 4 3 1 1962.76 1876.40 5.09 o 5 3 1 3122.70 3210.36 49.55 o 6 3 1 428.17 393.16 2.91 o 7 3 1 773.07 827.94 12.99 o 8 3 1 1367.73 1413.47 16.42 o 9 3 1 958.31 984.89 17.17 o 10 3 1 1051.15 1065.98 9.55 o 11 3 1 786.74 785.08 7.77 o 12 3 1 296.72 302.69 4.80 o 13 3 1 293.83 285.10 4.91 o 14 3 1 106.63 96.90 2.19 o 15 3 1 78.29 73.44 2.08 o -15 4 1 32.79 30.61 1.85 o -14 4 1 28.09 25.26 1.98 o -13 4 1 20.04 14.42 2.21 o -12 4 1 22.50 21.74 1.10 o -11 4 1 113.64 110.91 4.87 o -10 4 1 8.62 8.47 0.90 o -9 4 1 186.13 192.22 2.98 o -8 4 1 21.25 25.59 0.65 o -7 4 1 11.66 14.03 0.76 o -6 4 1 946.22 962.31 6.39 o -5 4 1 688.26 723.45 6.73 o -4 4 1 35.40 40.70 0.99 o -3 4 1 160.77 187.99 1.28 o -2 4 1 226.28 206.42 0.77 o -1 4 1 3192.86 3395.94 18.20 o 0 4 1 72.30 75.36 0.88 o 1 4 1 3054.03 3223.14 15.74 o 2 4 1 6437.70 6633.22 38.35 o 3 4 1 2948.44 3175.31 8.93 o 4 4 1 27.70 17.37 1.12 o 5 4 1 201.08 202.82 1.44 o 6 4 1 648.79 676.99 9.25 o 7 4 1 131.02 119.66 1.13 o 8 4 1 39.61 42.48 0.65 o 9 4 1 177.24 181.20 2.50 o 10 4 1 128.34 132.72 1.82 o 11 4 1 37.52 40.67 2.73 o 12 4 1 17.06 12.33 1.20 o 13 4 1 2.44 3.37 1.08 o 14 4 1 1.61 0.79 0.81 o 15 4 1 0.04 3.68 1.95 o -15 5 1 50.35 50.11 4.01 o -14 5 1 74.55 71.85 4.44 o -13 5 1 580.46 595.93 13.75 o -12 5 1 605.58 649.08 22.97 o -11 5 1 143.00 139.25 4.57 o -10 5 1 4.29 7.01 1.44 o -9 5 1 164.40 170.98 3.38 o -8 5 1 2235.01 2352.30 30.75 o -7 5 1 2214.69 2298.16 4.39 o -6 5 1 1252.17 1204.48 8.54 o -5 5 1 2369.88 2292.71 3.05 o -4 5 1 3249.95 3237.82 12.73 o -3 5 1 3723.74 3808.72 30.42 o -2 5 1 190.51 163.23 2.62 o -1 5 1 448.16 386.17 3.77 o 0 5 1 5018.53 5148.81 40.88 o 1 5 1 453.59 395.89 2.37 o 2 5 1 211.50 186.86 2.70 o 3 5 1 3008.80 3057.91 26.65 o 4 5 1 2517.29 2499.92 25.70 o 5 5 1 1355.21 1297.67 13.94 o 6 5 1 861.04 827.28 9.95 o 7 5 1 2096.63 2109.05 12.70 o 8 5 1 824.11 815.10 10.70 o 9 5 1 531.91 509.88 8.85 o 10 5 1 163.46 168.91 5.75 o 11 5 1 877.40 877.36 20.54 o 12 5 1 407.49 405.53 16.43 o 13 5 1 80.39 67.28 2.89 o 14 5 1 51.71 47.37 2.21 o -15 6 1 2.80 1.68 1.92 o -14 6 1 11.68 9.83 1.83 o -13 6 1 0.59 2.68 1.71 o -12 6 1 29.83 23.83 1.70 o -11 6 1 725.71 753.45 15.53 o -10 6 1 7.13 11.39 2.31 o -9 6 1 615.03 656.08 6.53 o -8 6 1 199.77 208.68 3.06 o -7 6 1 678.98 725.80 3.28 o -6 6 1 171.62 197.15 1.20 o -5 6 1 55.47 85.19 1.27 o -4 6 1 509.73 501.64 6.93 o -3 6 1 1536.84 1621.95 17.57 o -2 6 1 330.46 308.45 3.09 o -1 6 1 333.22 413.93 5.23 o 0 6 1 4670.68 5197.09 24.60 o 1 6 1 21.64 22.02 0.44 o 2 6 1 151.73 163.06 0.75 o 3 6 1 348.34 323.60 4.69 o 4 6 1 117.56 106.02 1.12 o 5 6 1 275.26 286.96 2.53 o 6 6 1 11.73 9.80 2.52 o 7 6 1 402.54 412.00 5.11 o 8 6 1 1126.29 1112.22 18.16 o 9 6 1 14.36 17.27 0.93 o 10 6 1 7.30 6.84 0.81 o 11 6 1 74.85 69.71 4.19 o 12 6 1 0.12 -0.61 0.61 o 13 6 1 54.21 54.00 2.62 o 14 6 1 5.06 5.37 3.08 o -14 7 1 209.11 216.71 2.71 o -13 7 1 147.91 157.20 4.52 o -12 7 1 552.57 588.68 9.74 o -11 7 1 751.39 831.42 10.77 o -10 7 1 1271.63 1370.44 15.36 o -9 7 1 702.94 738.48 6.08 o -8 7 1 1287.14 1398.99 10.17 o -7 7 1 1117.33 1153.44 12.97 o -6 7 1 3301.64 3267.53 21.26 o -5 7 1 1448.94 1389.00 13.83 o -4 7 1 1010.01 982.77 14.30 o -3 7 1 2185.87 2183.16 51.36 o -2 7 1 2273.41 2263.36 23.88 o -1 7 1 8137.13 8339.97 65.59 o 0 7 1 1267.69 1238.25 8.87 o 1 7 1 5092.94 5426.35 23.68 o 2 7 1 948.51 967.19 13.02 o 3 7 1 166.79 138.44 0.95 o 4 7 1 195.89 174.28 2.28 o 5 7 1 1025.65 1011.71 11.23 o 6 7 1 1491.43 1562.06 11.52 o 7 7 1 29.32 27.73 1.54 o 8 7 1 86.50 80.29 3.02 o 9 7 1 568.62 548.63 13.69 o 10 7 1 638.26 652.41 19.30 o 11 7 1 52.19 45.43 2.49 o 12 7 1 72.76 71.01 2.40 o 13 7 1 74.14 66.63 2.12 o 14 7 1 47.07 50.67 2.23 o -14 8 1 1.54 4.98 2.12 o -13 8 1 15.77 17.80 2.54 o -12 8 1 23.12 25.81 2.17 o -11 8 1 0.14 0.83 1.71 o -10 8 1 17.58 19.93 1.78 o -9 8 1 41.94 39.79 1.65 o -8 8 1 0.02 0.99 1.30 o -7 8 1 26.12 24.36 1.43 o -6 8 1 124.77 107.11 1.25 o -5 8 1 176.92 185.60 1.29 o -4 8 1 20.04 16.61 0.74 o -3 8 1 619.57 641.70 1.58 o -2 8 1 741.11 735.38 5.22 o -1 8 1 1245.54 1248.60 9.95 o 0 8 1 470.38 486.29 2.93 o 1 8 1 60.18 58.64 0.63 o 2 8 1 1.21 1.37 0.50 o 3 8 1 194.02 193.91 1.60 o 4 8 1 470.41 502.22 4.56 o 5 8 1 50.33 56.50 1.82 o 6 8 1 57.44 61.59 2.10 o 7 8 1 0.67 0.60 0.50 o 8 8 1 257.58 243.06 6.46 o 9 8 1 17.60 15.66 0.81 o 10 8 1 41.89 38.20 2.23 o 11 8 1 25.88 21.65 1.78 o 12 8 1 36.78 34.09 1.97 o 13 8 1 0.28 2.64 2.05 o -13 9 1 116.27 104.30 3.35 o -12 9 1 287.59 290.14 7.32 o -11 9 1 197.11 195.64 4.10 o -10 9 1 88.10 91.50 2.90 o 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