#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/40/2204052.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204052_Fobs loop_ _publ_author_name 'Venkatraman, Ramaiyer' 'Ray, Paresh Chandra' 'Fronczek, Frank R.' _publ_section_title ; The tetrachlorodiphenylstannate(IV) salt of protonated di-2-pyridyl ketone N^4^-ethylthiosemicarbazone ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1035 _journal_page_last m1037 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 110.872 _cell_angle_beta 102.803 _cell_angle_gamma 100.404 _cell_length_a 7.4878 _cell_length_b 12.0090 _cell_length_c 13.5850 _exptl_crystal_F_000 502.00 _reflns_d_resolution_high 0.6396 _[local]_cod_data_source_file lh6238Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Venkat1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 155.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 68.02 64.25 1.74 o 2 0 0 105.98 92.40 3.50 o 3 0 0 998.21 1051.65 19.23 o 4 0 0 2840.99 2598.64 45.88 o 5 0 0 412.52 428.30 17.85 o 6 0 0 98.24 105.71 7.35 o 7 0 0 127.03 131.32 8.15 o 8 0 0 1246.16 1367.99 30.81 o 9 0 0 255.26 274.77 14.43 o 10 0 0 13.07 0.09 16.78 o -11 1 0 186.58 201.17 24.01 o -10 1 0 11.09 -0.87 21.87 o -9 1 0 689.10 672.94 25.21 o -8 1 0 249.88 258.11 14.20 o -7 1 0 345.06 350.85 14.04 o -6 1 0 165.13 199.28 10.09 o -5 1 0 1538.97 1496.94 25.72 o -4 1 0 605.23 611.91 11.33 o -3 1 0 11258.65 11424.73 162.29 o -2 1 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