#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:06:57 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180963 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/43/2204349.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204349_Fobs loop_ _publ_author_name 'Wu, Chuan-Bao' _publ_section_title ; Tetrapyridinedithiocyanatozinc(II) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1490 _journal_page_last m1491 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.478 _cell_angle_gamma 90.000 _cell_length_a 12.3961 _cell_length_b 13.0221 _cell_length_c 15.1478 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.7964 _cod_data_source_file hb6098Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wu1 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 360.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6612.53 6616.53 159.83 o 4 0 0 3009.20 2450.66 95.50 o 6 0 0 8219.71 6999.44 216.11 o 8 0 0 3297.30 3184.09 146.81 o 10 0 0 3288.74 3056.19 160.61 o 12 0 0 478.78 603.05 95.19 o 1 1 0 158.56 145.84 8.18 o 3 1 0 8325.28 9774.67 372.91 o 5 1 0 1009.75 1178.85 48.87 o 7 1 0 1243.20 1326.17 61.96 o 9 1 0 30.22 63.75 49.45 o 11 1 0 1.04 -11.16 29.46 o 13 1 0 75.96 129.04 40.21 o 0 2 0 9398.03 10583.96 220.14 o 2 2 0 36757.21 42797.28 414.04 o 8 2 0 3283.10 2498.25 134.41 o 10 2 0 735.32 700.47 199.82 o 12 2 0 342.87 368.74 65.13 o 14 2 0 193.49 233.80 51.89 o 1 3 0 30109.12 39212.89 554.87 o 3 3 0 815.38 997.24 50.66 o 5 3 0 49.33 112.07 19.49 o 9 3 0 0.44 -4.51 21.30 o 11 3 0 95.93 103.81 33.21 o 13 3 0 14.07 50.97 30.83 o 0 4 0 2071.06 3080.99 100.77 o 2 4 0 34528.95 40226.87 480.80 o 4 4 0 24745.65 27205.32 342.32 o 6 4 0 3502.53 3182.41 72.32 o 8 4 0 5178.39 4467.82 95.45 o 10 4 0 492.60 499.69 61.70 o 12 4 0 649.82 593.25 67.08 o 14 4 0 445.41 474.97 69.35 o 1 5 0 410.40 657.08 29.41 o 3 5 0 10.61 23.91 11.47 o 5 5 0 110.00 117.63 17.99 o 7 5 0 459.69 464.74 31.37 o 9 5 0 1405.14 1122.31 131.85 o 11 5 0 310.50 183.97 43.48 o 13 5 0 61.00 74.01 36.31 o 0 6 0 612.48 340.60 30.99 o 2 6 0 12991.77 13152.92 193.19 o 4 6 0 2998.33 2538.69 66.79 o 6 6 0 720.15 625.44 35.83 o 8 6 0 3136.18 2736.17 77.48 o 10 6 0 2001.50 1676.24 90.92 o 12 6 0 671.36 614.00 69.94 o 1 7 0 2667.32 2748.93 71.52 o 3 7 0 2398.54 2805.78 73.37 o 5 7 0 1858.08 2034.45 89.81 o 7 7 0 1430.43 1189.69 56.34 o 9 7 0 110.91 111.98 31.90 o 11 7 0 141.13 163.35 41.02 o 13 7 0 2.95 -45.72 26.53 o 0 8 0 3127.40 3017.80 164.72 o 2 8 0 2441.17 2013.67 65.17 o 4 8 0 1848.99 1677.02 59.87 o 6 8 0 1471.70 1385.52 56.46 o 8 8 0 332.58 353.88 36.65 o 10 8 0 1727.41 1617.10 92.44 o 12 8 0 684.29 685.13 77.63 o 1 9 0 399.12 439.06 37.69 o 3 9 0 197.78 182.72 27.22 o 5 9 0 283.86 229.53 30.53 o 7 9 0 1.16 6.65 17.39 o 9 9 0 42.79 27.72 27.79 o 11 9 0 79.15 44.47 30.68 o 0 10 0 7362.02 6966.73 255.33 o 2 10 0 176.59 180.25 30.00 o 4 10 0 1380.80 1197.27 68.73 o 6 10 0 2621.29 2306.34 80.00 o 8 10 0 457.74 435.58 42.52 o 10 10 0 269.84 371.80 83.40 o 1 11 0 145.30 149.13 34.60 o 3 11 0 87.17 69.26 29.28 o 5 11 0 335.32 294.94 37.54 o 7 11 0 227.96 229.08 37.03 o 9 11 0 178.33 131.11 89.30 o 0 12 0 480.49 537.01 86.04 o 2 12 0 904.08 957.18 73.50 o 4 12 0 556.16 597.94 66.54 o 6 12 0 763.01 706.23 55.58 o 8 12 0 227.59 235.20 35.71 o 10 12 0 85.25 24.09 32.61 o 1 13 0 432.70 452.02 61.85 o 3 13 0 58.73 32.39 30.79 o 5 13 0 78.61 70.06 27.69 o 7 13 0 19.17 4.22 19.98 o 9 13 0 13.58 -6.24 30.77 o 0 14 0 289.73 340.59 79.53 o 2 14 0 1123.70 1069.95 89.79 o 4 14 0 243.76 276.17 53.16 o 6 14 0 2.53 24.96 23.81 o 1 15 0 61.28 25.53 34.28 o 3 15 0 0.04 -5.17 31.09 o 5 15 0 11.37 44.15 37.55 o 0 16 0 153.21 164.02 74.26 o 2 16 0 298.60 329.31 61.64 o -15 1 1 343.74 380.50 147.17 o -13 1 1 377.25 487.25 66.41 o -11 1 1 386.38 383.38 51.63 o -9 1 1 9310.88 9619.68 480.27 o -7 1 1 2188.51 1976.35 71.49 o -5 1 1 13773.87 14102.07 137.16 o -3 1 1 46694.59 50626.97 427.41 o -1 1 1 37769.71 43670.50 367.99 o 1 1 1 19056.29 22626.54 265.05 o 3 1 1 1664.76 1040.85 52.40 o 5 1 1 128.18 361.97 40.93 o 7 1 1 3940.94 3772.10 165.41 o 9 1 1 4677.40 4920.14 143.92 o 11 1 1 130.57 135.03 47.59 o 13 1 1 250.69 307.03 129.84 o -14 2 1 4.99 26.28 37.36 o -12 2 1 347.83 337.62 78.44 o -10 2 1 1130.21 1111.90 86.43 o -8 2 1 175.35 171.30 18.31 o -6 2 1 884.09 859.94 25.85 o -4 2 1 1623.64 1657.11 32.96 o -2 2 1 29959.21 35836.82 305.49 o 0 2 1 2357.23 2486.25 32.77 o 2 2 1 9058.07 12108.10 155.91 o 4 2 1 280.17 196.99 47.37 o 6 2 1 1964.62 1953.18 103.56 o 8 2 1 370.46 369.45 48.89 o 10 2 1 298.44 405.37 67.27 o 12 2 1 95.36 82.18 32.44 o 14 2 1 31.71 69.42 53.06 o -13 3 1 537.65 499.23 109.45 o -11 3 1 610.74 568.94 186.17 o -9 3 1 1866.26 1506.55 107.43 o -3 3 1 104.68 318.20 12.18 o -1 3 1 5868.87 5157.59 55.87 o 1 3 1 23336.67 25450.06 403.15 o 3 3 1 15487.10 16411.35 213.55 o 5 3 1 12845.88 12077.30 173.16 o 7 3 1 861.40 699.14 33.97 o 9 3 1 44.67 79.92 42.08 o 11 3 1 1283.66 1160.46 328.59 o 13 3 1 158.72 161.18 43.14 o -14 4 1 13.67 11.58 32.51 o -12 4 1 10.20 5.53 23.40 o -10 4 1 331.59 239.93 109.38 o -8 4 1 10.61 15.52 11.65 o -6 4 1 670.11 789.48 25.59 o -4 4 1 185.37 227.03 13.61 o -2 4 1 4628.40 5360.84 67.20 o 0 4 1 1591.63 1732.89 71.16 o 2 4 1 4589.06 5750.71 94.62 o 4 4 1 10265.87 12136.65 174.79 o 6 4 1 477.86 565.12 31.65 o 8 4 1 198.02 217.25 24.78 o 10 4 1 192.10 191.06 38.33 o 12 4 1 213.66 216.06 63.17 o 14 4 1 8.29 15.12 33.67 o -13 5 1 505.49 536.90 68.29 o -11 5 1 3803.99 3654.78 137.54 o -9 5 1 253.47 268.33 41.95 o -7 5 1 4469.97 4036.99 198.83 o -5 5 1 2196.37 1798.71 37.14 o -3 5 1 10968.60 12259.14 140.16 o -1 5 1 11363.74 10830.26 123.87 o 1 5 1 2212.91 1697.82 46.63 o 3 5 1 6290.90 7345.34 121.77 o 5 5 1 10702.18 9468.41 152.52 o 7 5 1 1366.78 1196.13 46.47 o 9 5 1 255.99 217.39 38.69 o 11 5 1 1884.40 1922.53 99.37 o 13 5 1 226.14 224.61 48.16 o -14 6 1 29.35 11.81 43.72 o -12 6 1 104.37 118.76 37.71 o -10 6 1 2.85 -13.45 20.68 o -8 6 1 0.45 25.28 14.42 o -6 6 1 443.42 502.06 34.52 o -4 6 1 3945.95 4440.24 92.60 o -2 6 1 5228.87 5703.86 71.21 o 0 6 1 5841.72 6824.73 301.57 o 2 6 1 3712.80 4553.65 91.18 o 4 6 1 799.93 719.78 35.88 o 6 6 1 783.27 773.71 42.98 o 8 6 1 571.16 506.25 37.98 o 10 6 1 0.18 43.12 25.58 o 12 6 1 7.75 -11.11 25.31 o -13 7 1 187.68 168.42 43.81 o -11 7 1 559.99 635.10 69.01 o -9 7 1 850.67 825.22 64.92 o -7 7 1 980.57 926.70 49.61 o -5 7 1 1575.78 1407.60 53.08 o -3 7 1 3290.62 2545.91 101.24 o -1 7 1 5178.36 4896.75 69.03 o 1 7 1 1016.54 666.31 35.57 o 3 7 1 3155.59 2840.26 74.22 o 5 7 1 2563.01 2721.80 75.23 o 7 7 1 4066.04 3502.10 224.45 o 9 7 1 1586.93 1298.04 78.33 o 11 7 1 1097.98 1033.63 80.45 o 13 7 1 56.51 98.07 40.27 o -12 8 1 3.18 44.73 31.79 o -10 8 1 810.17 625.09 117.04 o -8 8 1 193.13 204.29 29.57 o -6 8 1 4.55 25.64 16.40 o -4 8 1 32.82 25.90 25.76 o -2 8 1 100.84 50.50 18.51 o 0 8 1 2365.18 2513.26 72.20 o 2 8 1 505.66 585.95 38.94 o 4 8 1 57.04 36.64 16.69 o 6 8 1 251.44 246.51 30.71 o 8 8 1 5.40 13.29 16.09 o 10 8 1 97.17 130.11 38.11 o 12 8 1 67.76 62.73 33.58 o -11 9 1 84.69 100.66 35.45 o -9 9 1 2231.53 2232.20 108.97 o -7 9 1 6.32 -7.31 15.33 o -5 9 1 444.04 446.42 39.31 o -3 9 1 3124.61 2928.16 83.93 o -1 9 1 702.50 616.84 50.57 o 1 9 1 4229.23 3992.46 98.07 o 3 9 1 4034.83 3780.94 112.51 o 5 9 1 532.26 632.08 44.68 o 7 9 1 983.79 970.67 74.48 o 9 9 1 1804.13 1560.33 155.65 o 11 9 1 85.02 77.45 34.53 o -10 10 1 59.30 38.30 29.49 o -8 10 1 4.44 38.35 19.42 o -6 10 1 42.31 43.65 25.52 o -4 10 1 0.16 10.37 17.00 o -2 10 1 2220.18 2090.74 116.97 o 0 10 1 158.13 164.16 28.44 o 2 10 1 2174.93 2144.88 74.25 o 4 10 1 350.44 348.38 37.86 o 6 10 1 0.97 6.56 16.07 o 8 10 1 82.99 78.60 22.98 o 10 10 1 13.38 -5.22 28.22 o -11 11 1 53.27 113.38 39.66 o -9 11 1 553.89 565.17 68.92 o -7 11 1 315.15 328.32 39.22 o -5 11 1 1235.65 1148.10 104.50 o -3 11 1 1131.41 1069.01 74.21 o -1 11 1 24.68 52.89 28.33 o 1 11 1 724.43 657.81 50.04 o 3 11 1 2755.79 2643.65 87.56 o 5 11 1 1162.33 1084.08 56.80 o 7 11 1 491.73 430.22 44.11 o 9 11 1 409.81 491.57 63.96 o -10 12 1 19.90 -5.17 30.01 o -8 12 1 612.96 520.01 50.76 o -6 12 1 9.73 17.66 19.97 o -4 12 1 249.10 266.50 59.22 o -2 12 1 133.75 121.16 51.00 o 0 12 1 267.79 360.21 68.13 o 2 12 1 3.96 23.64 20.51 o 4 12 1 33.75 32.91 20.76 o 6 12 1 20.58 32.34 21.04 o 8 12 1 1.34 30.26 29.74 o -9 13 1 25.07 24.78 35.68 o -7 13 1 395.63 410.04 49.81 o -5 13 1 545.24 562.57 83.95 o -3 13 1 130.05 167.86 45.05 o -1 13 1 1760.22 1646.83 119.99 o 1 13 1 1395.69 1349.55 85.78 o 3 13 1 4.72 1.39 19.18 o 5 13 1 526.83 555.40 52.93 o 7 13 1 107.42 154.38 32.04 o -6 14 1 1.01 10.75 32.51 o -4 14 1 25.83 4.31 30.61 o -2 14 1 0.63 23.60 30.86 o 0 14 1 18.18 39.89 31.79 o 2 14 1 3.89 30.94 31.12 o 4 14 1 8.78 8.95 21.02 o 6 14 1 3.18 35.82 23.92 o -5 15 1 116.16 94.94 43.14 o -3 15 1 156.15 281.05 56.99 o -1 15 1 602.52 562.20 72.18 o 1 15 1 210.49 265.05 53.69 o 3 15 1 37.33 42.37 32.94 o 5 15 1 136.16 178.89 37.15 o -2 16 1 142.00 81.99 42.39 o 0 16 1 70.66 35.00 38.79 o 2 16 1 71.27 71.63 42.63 o -14 0 2 613.61 742.42 116.58 o -12 0 2 1535.80 1687.93 129.91 o -10 0 2 97.57 159.06 49.61 o -8 0 2 4759.41 4603.40 113.86 o -6 0 2 8497.71 7609.47 183.47 o -4 0 2 25.71 161.71 17.69 o -2 0 2 10330.44 10076.42 149.41 o 0 0 2 28290.21 34040.23 599.02 o 2 0 2 25244.40 33878.39 699.94 o 4 0 2 679.39 263.54 34.26 o 6 0 2 7029.62 7103.62 218.59 o 8 0 2 267.71 244.79 55.34 o 10 0 2 1065.50 1086.27 96.74 o 14 0 2 129.90 293.85 94.58 o -15 1 2 14.14 21.83 37.64 o -13 1 2 7.53 42.32 43.87 o -11 1 2 331.20 335.79 49.13 o -9 1 2 441.24 568.26 66.04 o -7 1 2 2442.07 2668.50 43.65 o -5 1 2 7592.32 8859.43 93.41 o -3 1 2 10789.43 13581.38 142.92 o -1 1 2 64.24 72.93 4.52 o 1 1 2 1832.92 2317.72 36.25 o 3 1 2 17201.00 20073.46 314.38 o 5 1 2 837.59 1050.18 72.55 o 7 1 2 813.02 983.48 56.91 o 9 1 2 99.18 130.07 42.01 o 11 1 2 21.33 45.91 27.98 o 13 1 2 102.86 112.83 74.62 o -14 2 2 197.31 278.58 51.75 o -12 2 2 367.16 429.21 100.94 o -10 2 2 1615.48 1689.58 83.85 o -8 2 2 3410.03 2888.16 83.04 o -6 2 2 9952.56 10075.51 116.90 o -4 2 2 57.65 300.21 36.94 o -2 2 2 43.50 388.96 12.48 o 0 2 2 9138.63 8476.84 111.03 o 2 2 2 52.32 30.05 6.49 o 6 2 2 404.02 235.30 51.67 o 8 2 2 1792.98 1652.87 74.67 o 10 2 2 487.58 559.42 134.85 o 12 2 2 89.76 161.54 42.64 o 14 2 2 166.92 198.95 48.90 o -15 3 2 78.52 93.37 40.33 o -13 3 2 3.30 46.17 91.16 o -11 3 2 1106.52 1078.94 70.32 o -9 3 2 1981.12 1822.65 117.36 o -7 3 2 144.25 219.81 33.28 o -5 3 2 5095.75 5313.05 63.84 o -3 3 2 5.43 32.62 9.28 o -1 3 2 3163.68 3908.65 46.02 o 1 3 2 15662.82 18699.00 191.71 o 3 3 2 120.41 57.65 20.09 o 5 3 2 1375.77 1432.60 44.61 o 7 3 2 617.20 671.36 113.88 o 9 3 2 1993.92 1776.98 83.04 o 11 3 2 78.02 119.90 41.63 o 13 3 2 85.98 128.50 45.01 o -14 4 2 272.27 307.12 56.40 o -12 4 2 327.78 320.89 122.08 o -10 4 2 882.13 854.35 145.90 o -8 4 2 1304.25 1207.39 139.75 o -6 4 2 38.74 21.00 7.73 o -4 4 2 20196.01 19923.45 187.08 o -2 4 2 3561.97 3008.64 41.07 o 0 4 2 26.99 130.50 10.11 o 2 4 2 32448.47 35066.34 534.55 o 4 4 2 285.33 200.07 19.93 o 6 4 2 561.64 548.87 32.06 o 8 4 2 484.73 548.82 37.15 o 10 4 2 447.26 546.86 82.16 o 12 4 2 884.06 972.05 84.19 o -13 5 2 8.55 0.46 27.09 o -11 5 2 259.87 297.66 48.84 o -9 5 2 22.28 20.38 20.56 o -7 5 2 1209.17 1151.78 41.87 o -5 5 2 490.34 657.41 23.77 o -3 5 2 8.63 17.59 6.33 o -1 5 2 288.12 299.71 17.94 o 1 5 2 1809.41 2232.08 40.19 o 3 5 2 1054.50 1310.50 42.88 o 5 5 2 593.54 572.53 32.62 o 7 5 2 669.33 656.79 36.43 o 9 5 2 34.31 39.48 14.74 o 11 5 2 117.96 131.05 36.56 o 13 5 2 51.16 81.48 40.14 o -14 6 2 42.63 106.34 39.66 o -12 6 2 113.26 152.33 40.04 o -10 6 2 1240.78 1381.08 93.40 o -8 6 2 549.57 478.53 36.12 o -6 6 2 433.86 325.04 29.29 o -4 6 2 9461.06 8838.19 112.56 o -2 6 2 3933.15 3435.28 52.70 o 0 6 2 494.25 1098.56 40.53 o 2 6 2 9616.24 9226.26 148.61 o 4 6 2 3926.20 3702.15 84.08 o 6 6 2 3554.92 3723.64 137.27 o 8 6 2 1740.16 1676.94 83.49 o 10 6 2 42.51 134.08 34.40 o 12 6 2 300.73 399.25 59.24 o -13 7 2 8.42 -6.43 29.48 o -11 7 2 139.13 192.72 41.46 o -9 7 2 1007.26 1037.46 72.00 o -7 7 2 4.97 38.32 16.12 o -5 7 2 1097.10 984.71 45.09 o -3 7 2 820.82 817.70 30.34 o -1 7 2 1688.96 2186.64 47.27 o 1 7 2 1166.77 1017.54 42.32 o 3 7 2 870.77 794.08 39.66 o 5 7 2 4.38 25.10 15.03 o 7 7 2 1074.62 973.81 63.85 o 9 7 2 357.55 340.54 35.91 o 11 7 2 138.55 99.42 49.69 o -12 8 2 406.34 404.26 60.62 o -10 8 2 831.63 816.83 74.34 o -8 8 2 63.57 88.45 29.69 o -6 8 2 1420.03 1366.84 56.54 o -4 8 2 216.88 148.68 24.05 o -2 8 2 6729.98 6558.33 106.69 o 0 8 2 6006.96 6159.86 95.54 o 2 8 2 835.17 747.47 41.40 o 4 8 2 4515.08 4194.42 104.57 o 6 8 2 758.99 836.74 45.98 o 8 8 2 1349.58 1024.42 53.08 o 10 8 2 767.09 741.88 73.12 o 12 8 2 14.56 71.53 37.13 o -11 9 2 1.19 3.32 28.75 o -9 9 2 9.40 66.27 30.30 o -7 9 2 0.88 1.10 15.46 o -5 9 2 8.59 7.44 15.97 o -3 9 2 103.67 110.72 29.22 o -1 9 2 429.57 410.80 36.39 o 1 9 2 1125.11 1075.31 52.68 o 3 9 2 32.97 40.83 17.54 o 5 9 2 5.05 -4.92 13.52 o 7 9 2 53.09 47.71 20.19 o 9 9 2 11.68 37.30 18.49 o 11 9 2 12.94 27.50 33.72 o -12 10 2 164.60 159.58 45.15 o -10 10 2 8.70 33.67 33.00 o -8 10 2 679.65 680.16 51.03 o -6 10 2 1428.63 1414.80 63.55 o -4 10 2 49.53 56.34 38.21 o -2 10 2 1619.84 1577.37 89.31 o 0 10 2 4628.29 4416.84 109.88 o 2 10 2 124.27 151.44 26.77 o 4 10 2 3066.72 2895.87 99.68 o 6 10 2 1217.51 1283.06 59.95 o 8 10 2 4.03 17.63 18.23 o 10 10 2 438.70 459.69 63.40 o -11 11 2 130.73 38.25 39.12 o -9 11 2 9.35 32.61 32.69 o -7 11 2 57.22 69.55 22.45 o -5 11 2 71.90 109.85 34.03 o -3 11 2 57.32 22.31 24.50 o -1 11 2 12.36 14.81 18.25 o 1 11 2 18.34 28.44 18.91 o 3 11 2 287.33 332.97 70.63 o 5 11 2 281.03 234.71 34.74 o 7 11 2 164.19 129.97 27.18 o 9 11 2 134.29 203.33 44.99 o -10 12 2 37.90 106.09 43.28 o -8 12 2 493.09 453.74 65.77 o -6 12 2 512.97 465.12 62.28 o -4 12 2 1042.56 1043.71 77.06 o -2 12 2 112.87 163.80 42.55 o 0 12 2 1005.96 975.67 62.72 o 2 12 2 971.15 1003.34 57.95 o 4 12 2 328.83 335.36 53.30 o 6 12 2 368.31 336.86 49.11 o 8 12 2 182.21 285.97 39.47 o -9 13 2 3.94 5.51 70.07 o -7 13 2 44.70 19.41 45.35 o -5 13 2 0.09 4.18 28.88 o -3 13 2 180.63 228.43 47.02 o -1 13 2 100.13 110.28 34.08 o 1 13 2 358.54 389.75 45.62 o 3 13 2 24.58 1.62 19.22 o 5 13 2 8.96 5.57 20.14 o 7 13 2 31.80 30.98 21.42 o -8 14 2 203.81 176.80 50.06 o -6 14 2 47.30 21.61 52.86 o -4 14 2 857.00 829.18 82.60 o -2 14 2 216.65 247.90 51.84 o 0 14 2 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