#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2204368.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204368_Fobs loop_ _publ_author_name 'Parvez, Masood' Sadiq-ur-Rehman 'Shahid, Khadija' 'Ali, Saqib' 'Mazhar, Muhammad' _publ_section_title ; Tetrabutylbis[3-(4-methoxyphenyl)-2-phenyl-2-propenoato]distannoxane dimer ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1465 _journal_page_last m1467 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.490 _cell_angle_beta 96.820 _cell_angle_gamma 118.531 _cell_length_a 12.9710 _cell_length_b 13.4290 _cell_length_c 15.0880 _exptl_crystal_F_000 1012.00 _reflns_d_resolution_high 0.7496 _[local]_cod_data_source_file lh6275Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SAQIB-52 COLORLESS BLOCK' _shelx_refln_list_code 4 _shelx_f_calc_maximum 300.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 46.62 10.06 7.17 o 3 0 0 1601.48 1647.55 44.39 o 4 0 0 6353.98 6352.40 117.84 o 5 0 0 10877.78 10416.73 190.91 o 6 0 0 7333.76 7027.44 271.40 o 7 0 0 1337.87 1324.52 49.76 o 8 0 0 115.70 50.30 23.79 o 9 0 0 145.36 98.36 39.01 o 10 0 0 215.16 107.39 48.60 o 11 0 0 177.57 121.67 58.36 o 12 0 0 59.15 121.60 78.87 o 13 0 0 3.88 92.85 93.07 o 14 0 0 37.90 136.91 142.01 o -15 1 0 47.40 98.45 142.20 o -14 1 0 280.74 229.69 92.08 o -13 1 0 3.05 60.26 77.27 o -12 1 0 667.78 785.55 210.14 o -11 1 0 565.81 633.79 78.70 o -10 1 0 958.26 990.88 67.66 o -9 1 0 1515.84 1489.10 110.78 o -8 1 0 347.39 352.98 38.52 o -7 1 0 5545.07 5660.00 241.90 o -6 1 0 15516.33 15411.16 422.77 o -5 1 0 8076.38 7879.46 140.04 o -4 1 0 96.88 127.75 21.04 o -3 1 0 7213.18 7193.96 128.20 o 2 1 0 6548.13 6278.10 107.41 o 3 1 0 169.34 140.84 41.20 o 4 1 0 1618.86 1549.09 115.93 o 5 1 0 2455.47 2513.32 91.99 o 6 1 0 2750.11 3020.74 74.43 o 7 1 0 78.70 15.84 26.42 o 8 1 0 522.90 506.48 62.36 o 9 1 0 310.64 300.22 50.94 o 10 1 0 166.71 183.19 55.38 o 11 1 0 384.62 319.42 98.43 o 12 1 0 104.72 315.21 208.28 o 13 1 0 32.01 181.29 173.60 o 14 1 0 89.32 -9.04 216.71 o -15 2 0 446.48 303.00 221.26 o -14 2 0 165.37 78.91 171.09 o -13 2 0 312.22 357.66 80.06 o -12 2 0 2157.48 2287.31 165.17 o -11 2 0 1953.81 1809.31 119.05 o -10 2 0 1906.03 1981.92 83.34 o -9 2 0 1699.76 1659.55 78.47 o -8 2 0 475.37 467.76 51.08 o -7 2 0 10563.27 10308.68 172.85 o -6 2 0 16518.28 17204.90 320.15 o -5 2 0 5320.10 5593.07 109.24 o -4 2 0 65.30 70.04 96.94 o -3 2 0 3106.84 3117.61 46.23 o -2 2 0 6113.99 4281.07 1377.98 o 0 2 0 3157.06 2779.29 423.74 o 1 2 0 6179.54 6495.08 120.74 o 2 2 0 1309.44 1234.27 30.87 o 3 2 0 295.61 346.60 20.55 o 4 2 0 32.57 14.56 33.28 o 5 2 0 3986.03 3861.64 115.35 o 6 2 0 720.33 764.50 82.16 o 7 2 0 582.70 683.15 117.12 o 8 2 0 0.26 -11.84 52.92 o 9 2 0 1962.41 1907.58 92.16 o 10 2 0 1524.32 1622.36 186.00 o 11 2 0 2145.85 1975.17 191.05 o 12 2 0 528.55 483.96 114.57 o 13 2 0 34.99 116.64 200.66 o -16 3 0 1023.50 807.97 214.04 o -15 3 0 581.22 518.56 122.87 o -14 3 0 108.92 132.16 80.17 o -13 3 0 578.81 766.75 108.22 o -12 3 0 6861.69 6878.94 423.07 o -11 3 0 2790.27 2739.05 91.66 o -10 3 0 2494.66 2513.98 90.29 o -9 3 0 1313.84 1315.38 81.40 o -8 3 0 1043.32 1003.95 44.94 o -7 3 0 6446.36 6533.56 108.21 o -6 3 0 8873.85 9130.69 193.87 o -5 3 0 4343.73 4421.59 73.10 o -4 3 0 1659.36 1408.39 34.04 o -3 3 0 6532.21 6418.95 108.07 o -2 3 0 408.15 408.61 21.44 o -1 3 0 3.38 41.03 9.03 o 0 3 0 806.24 864.01 31.21 o 1 3 0 2140.51 2346.02 53.19 o 2 3 0 1781.41 1940.22 68.17 o 3 3 0 3313.93 3343.33 67.41 o 4 3 0 8356.43 7834.16 126.65 o 5 3 0 1907.26 1924.52 51.13 o 6 3 0 1477.78 1430.90 54.10 o 7 3 0 715.06 694.30 48.00 o 8 3 0 580.41 585.48 62.60 o 9 3 0 3490.81 3614.68 173.19 o 10 3 0 3233.70 3596.43 164.76 o 11 3 0 1601.72 1795.50 178.16 o 12 3 0 311.47 315.39 124.39 o 13 3 0 21.48 -48.11 190.74 o -16 4 0 407.87 366.87 159.57 o -15 4 0 371.41 62.28 129.87 o -14 4 0 0.25 -11.51 68.06 o -13 4 0 609.09 694.69 103.00 o -12 4 0 2658.19 2605.39 112.18 o -11 4 0 1226.64 1269.03 78.07 o -10 4 0 1539.08 1687.54 59.25 o -9 4 0 514.72 529.09 31.10 o -8 4 0 30.28 9.28 18.64 o -7 4 0 4479.65 5114.04 124.54 o -6 4 0 76.00 46.88 15.19 o -5 4 0 1983.32 2144.75 47.60 o -4 4 0 1932.43 1840.11 49.86 o -3 4 0 34.02 24.07 8.08 o -2 4 0 2910.66 2894.54 55.55 o -1 4 0 2200.79 2240.13 65.13 o 0 4 0 2450.52 2407.52 48.60 o 1 4 0 2045.28 1989.63 64.74 o 2 4 0 590.26 586.95 28.99 o 3 4 0 10899.89 10849.69 211.22 o 4 4 0 6071.93 6075.70 123.02 o 5 4 0 5878.63 6058.31 129.79 o 6 4 0 995.17 1126.25 188.17 o 7 4 0 23.15 -2.92 46.25 o 8 4 0 669.40 680.56 72.63 o 9 4 0 2423.10 2917.81 170.05 o 10 4 0 2174.40 1792.45 134.27 o 11 4 0 677.27 549.26 124.65 o 12 4 0 106.93 74.10 209.73 o -16 5 0 235.60 393.11 151.39 o -15 5 0 61.60 225.80 93.99 o -14 5 0 20.75 -15.67 63.56 o -13 5 0 101.91 195.31 110.54 o -12 5 0 135.60 210.71 46.10 o -11 5 0 695.48 639.34 59.87 o -10 5 0 0.23 -13.73 315.33 o -9 5 0 559.49 528.80 25.65 o -8 5 0 1490.18 1444.24 40.10 o -7 5 0 3080.50 3163.19 117.27 o -6 5 0 7260.02 7024.63 130.45 o -5 5 0 10816.00 10937.70 145.98 o -4 5 0 5850.40 6161.56 105.04 o -3 5 0 1403.74 1317.09 30.01 o -2 5 0 3940.94 3946.72 87.76 o -1 5 0 17306.72 17425.70 299.59 o 0 5 0 11795.82 12026.39 205.67 o 1 5 0 4098.96 4157.37 96.92 o 2 5 0 863.59 841.12 35.42 o 3 5 0 6001.86 5633.09 290.08 o 4 5 0 8871.81 8907.84 174.16 o 5 5 0 4558.05 4565.71 114.34 o 6 5 0 1197.75 1392.99 120.84 o 7 5 0 52.27 46.73 60.21 o 8 5 0 1217.11 946.53 104.56 o 9 5 0 779.98 781.48 136.51 o 10 5 0 400.75 689.55 251.44 o 11 5 0 44.30 -4.03 109.42 o 12 5 0 29.55 -1.04 321.17 o -16 6 0 121.35 133.84 104.03 o -15 6 0 100.74 13.32 89.17 o -14 6 0 6.01 32.93 80.07 o -13 6 0 242.05 230.80 68.99 o -12 6 0 1651.03 1779.69 71.35 o -11 6 0 753.52 843.58 94.59 o -10 6 0 439.05 578.37 45.48 o -9 6 0 15.22 12.94 25.39 o -8 6 0 6377.41 6437.06 115.35 o -7 6 0 13225.33 13082.17 346.06 o -6 6 0 15901.75 16075.83 239.33 o -5 6 0 9402.67 10256.73 178.38 o -4 6 0 88.97 29.05 32.80 o -3 6 0 2007.00 2036.04 40.77 o -2 6 0 4054.60 3636.74 65.36 o -1 6 0 20805.26 20902.91 494.92 o 0 6 0 16941.36 17297.94 295.71 o 1 6 0 771.12 785.36 33.28 o 2 6 0 2660.07 2756.00 69.43 o 3 6 0 3066.67 3124.46 82.30 o 4 6 0 3060.47 3139.34 122.23 o 5 6 0 2771.32 2955.54 187.56 o 6 6 0 260.92 453.89 123.45 o 7 6 0 146.26 173.97 70.64 o 8 6 0 96.82 135.87 85.23 o 9 6 0 7.57 123.01 113.18 o 10 6 0 13.52 184.31 230.62 o 11 6 0 1.59 -84.30 184.52 o -17 7 0 6.96 29.32 109.38 o -16 7 0 7.87 -68.60 84.75 o -15 7 0 0.34 118.34 103.46 o -14 7 0 584.82 557.59 106.27 o -13 7 0 1213.93 1127.40 81.90 o -12 7 0 3074.05 3110.68 115.08 o -11 7 0 4052.27 4366.70 168.38 o -10 7 0 75.74 125.08 47.85 o -9 7 0 1322.12 1314.79 45.44 o -8 7 0 3420.98 3302.63 88.01 o -7 7 0 16351.00 16922.52 249.57 o -6 7 0 10050.29 10050.99 157.20 o -5 7 0 1853.03 1949.12 75.99 o -4 7 0 508.49 568.40 25.46 o -3 7 0 8022.95 7703.96 124.94 o -2 7 0 3017.72 3006.22 61.13 o -1 7 0 3266.49 3192.83 71.43 o 0 7 0 359.75 409.86 62.30 o 1 7 0 6.60 21.99 26.83 o 2 7 0 188.92 238.58 34.52 o 3 7 0 931.30 855.00 64.00 o 4 7 0 19.06 -50.75 44.33 o 5 7 0 0.03 84.72 75.33 o 6 7 0 8.37 -40.01 98.81 o 7 7 0 0.03 -73.75 165.15 o 8 7 0 20.18 25.70 129.31 o 9 7 0 381.39 397.17 171.07 o 10 7 0 213.41 245.63 195.18 o -17 8 0 561.60 423.82 182.56 o -16 8 0 306.30 405.41 129.08 o -15 8 0 1.59 -66.19 74.48 o -14 8 0 812.19 856.27 88.05 o -13 8 0 3225.29 3416.32 182.74 o -12 8 0 3024.79 3036.36 219.78 o -11 8 0 2782.69 2883.56 264.86 o -10 8 0 1043.15 1008.61 42.93 o -9 8 0 568.81 538.77 39.03 o -8 8 0 5397.62 5599.26 107.50 o -7 8 0 10011.97 9836.45 237.98 o -6 8 0 7515.02 8136.84 161.42 o -5 8 0 1201.57 1125.77 34.20 o -4 8 0 221.54 199.24 19.81 o -3 8 0 161.36 187.59 22.41 o -2 8 0 379.86 404.22 30.39 o -1 8 0 77.73 115.11 23.49 o 0 8 0 20.19 17.41 27.72 o 1 8 0 1.18 5.21 28.28 o 2 8 0 400.95 425.88 63.33 o 3 8 0 1.43 -19.26 46.08 o 4 8 0 1059.26 1099.80 85.96 o 5 8 0 895.44 915.52 122.12 o 6 8 0 97.82 121.76 85.82 o 7 8 0 145.94 198.74 101.47 o 8 8 0 286.01 103.70 223.64 o 9 8 0 490.98 467.91 177.06 o -17 9 0 1025.44 481.38 209.21 o -16 9 0 360.45 173.73 115.33 o -15 9 0 1.50 -130.56 87.04 o -14 9 0 658.60 978.70 93.07 o -13 9 0 2963.00 2713.47 256.30 o -12 9 0 3136.94 3100.06 88.75 o -11 9 0 1451.61 1527.18 73.87 o -10 9 0 423.65 373.89 51.45 o -9 9 0 275.35 313.31 32.68 o -8 9 0 693.38 692.80 26.16 o -7 9 0 2971.16 3091.13 67.37 o -6 9 0 1738.70 1725.56 43.80 o -5 9 0 835.60 924.57 62.74 o -4 9 0 350.07 306.08 25.42 o -3 9 0 223.81 272.67 27.71 o -2 9 0 1051.04 1094.02 60.27 o -1 9 0 852.49 911.61 177.79 o 0 9 0 153.17 148.97 41.25 o 1 9 0 44.25 55.62 55.94 o 2 9 0 3397.98 3369.71 117.73 o 3 9 0 2107.93 2427.31 108.40 o 4 9 0 2706.46 2598.38 143.34 o 5 9 0 846.18 1242.28 140.61 o 6 9 0 6.84 -18.66 91.97 o 7 9 0 344.08 327.04 130.89 o 8 9 0 558.80 434.11 146.10 o -17 10 0 528.29 384.48 139.46 o -16 10 0 43.58 -205.16 180.77 o -15 10 0 51.73 133.55 83.81 o -14 10 0 37.40 -10.85 121.38 o -13 10 0 1230.79 1099.85 90.75 o -12 10 0 297.30 218.23 67.12 o -11 10 0 26.51 -2.69 44.63 o -10 10 0 5.92 -1.49 49.73 o -9 10 0 70.44 75.03 31.35 o -8 10 0 277.91 276.73 30.41 o -7 10 0 1.16 -7.97 38.13 o -6 10 0 1.57 -19.85 20.87 o -5 10 0 33.70 11.00 23.87 o -4 10 0 76.06 79.14 34.30 o -3 10 0 2722.29 2445.52 114.77 o -2 10 0 4131.72 4099.04 101.61 o -1 10 0 1842.14 1838.63 70.60 o 0 10 0 237.64 238.14 39.76 o 1 10 0 68.55 74.21 39.20 o 2 10 0 2505.66 2458.49 198.46 o 3 10 0 2843.23 3333.86 201.16 o 4 10 0 2516.69 2792.20 142.87 o 5 10 0 599.33 832.61 124.10 o 6 10 0 25.72 -27.68 98.41 o 7 10 0 256.74 272.58 113.19 o -16 11 0 4.03 -110.53 352.59 o -15 11 0 9.93 30.15 112.98 o -14 11 0 10.95 86.93 64.70 o -13 11 0 0.29 -27.76 69.42 o -12 11 0 315.89 328.81 58.45 o -11 11 0 681.37 760.67 118.79 o -10 11 0 52.96 -8.80 35.58 o -9 11 0 1430.21 1467.85 55.56 o -8 11 0 3324.28 3415.25 231.58 o -7 11 0 1753.47 1931.77 76.13 o -6 11 0 1006.40 1011.32 41.69 o -5 11 0 142.76 119.52 28.27 o -4 11 0 1850.94 1772.11 58.34 o -3 11 0 3727.60 3814.23 110.39 o -2 11 0 4145.97 4468.52 109.28 o -1 11 0 2236.93 2446.38 87.06 o 0 11 0 211.35 246.64 53.76 o 1 11 0 357.53 266.30 58.20 o 2 11 0 1822.54 2002.43 114.60 o 3 11 0 1243.36 1343.71 132.91 o 4 11 0 996.83 1088.09 129.14 o 5 11 0 287.68 329.53 87.41 o 6 11 0 89.78 92.87 149.11 o -16 12 0 70.06 163.85 216.38 o -15 12 0 90.48 261.18 128.07 o -14 12 0 521.36 548.31 152.16 o -13 12 0 833.94 870.67 84.90 o -12 12 0 708.84 709.12 126.67 o -11 12 0 280.40 137.09 49.02 o -10 12 0 90.88 127.98 26.91 o -9 12 0 409.47 502.34 44.68 o -8 12 0 6292.34 6201.50 213.36 o -7 12 0 5058.23 4842.25 165.76 o -6 12 0 911.68 853.68 50.91 o -5 12 0 70.55 111.51 37.50 o -4 12 0 1607.28 1612.21 109.43 o -3 12 0 5146.22 4969.52 213.64 o -2 12 0 4607.44 4691.87 116.71 o -1 12 0 1028.52 968.05 114.80 o 0 12 0 7.30 14.92 56.48 o 1 12 0 180.90 224.54 76.72 o 2 12 0 343.87 351.31 102.31 o 3 12 0 242.74 72.88 84.61 o 4 12 0 170.43 117.66 93.04 o 5 12 0 80.33 175.40 206.58 o -16 13 0 0.14 93.04 392.63 o -15 13 0 555.04 345.43 137.09 o -14 13 0 1747.83 1765.85 156.36 o -13 13 0 1911.85 1930.25 229.56 o -12 13 0 857.50 626.60 78.61 o -11 13 0 158.10 139.67 51.09 o -10 13 0 653.37 542.59 59.54 o -9 13 0 1474.88 1494.93 77.42 o -8 13 0 4311.88 4365.00 151.45 o -7 13 0 1735.99 1573.83 74.46 o -6 13 0 182.73 228.78 37.68 o -5 13 0 325.95 373.45 56.81 o -4 13 0 390.81 256.78 49.36 o -3 13 0 1180.77 1099.90 68.80 o -2 13 0 1458.23 1200.12 91.40 o -1 13 0 232.15 76.96 64.65 o 0 13 0 35.88 216.30 75.59 o 1 13 0 17.89 67.48 115.62 o 2 13 0 0.68 -27.83 80.36 o 3 13 0 39.32 61.24 130.16 o 4 13 0 17.07 163.87 172.81 o -15 14 0 685.59 454.05 218.52 o -14 14 0 2009.02 2149.07 210.95 o -13 14 0 1675.11 2099.70 216.66 o -12 14 0 619.27 680.82 116.60 o -11 14 0 126.82 164.47 219.82 o -10 14 0 264.48 194.46 56.65 o -9 14 0 790.27 686.17 132.33 o -8 14 0 2614.00 2483.66 163.82 o -7 14 0 583.91 515.78 56.81 o -6 14 0 4.82 98.25 54.42 o -5 14 0 1.43 -5.84 59.78 o -4 14 0 123.62 89.04 53.08 o -3 14 0 44.96 14.73 71.46 o -2 14 0 31.31 15.41 58.89 o -1 14 0 38.90 52.93 71.27 o 0 14 0 10.65 134.74 75.92 o 1 14 0 129.56 24.32 121.16 o 2 14 0 76.25 -34.65 177.31 o -15 15 0 1027.09 847.70 200.27 o -14 15 0 990.28 1060.14 224.41 o -13 15 0 784.01 591.45 186.07 o -12 15 0 421.86 439.39 152.41 o -11 15 0 6.23 97.55 87.00 o -10 15 0 45.37 136.86 95.79 o -9 15 0 43.97 27.01 80.69 o -8 15 0 125.54 83.89 76.94 o -7 15 0 34.44 30.30 69.50 o -6 15 0 9.89 -1.66 84.87 o -5 15 0 250.58 290.73 70.55 o -4 15 0 250.42 303.09 87.53 o -3 15 0 431.79 581.30 78.24 o -2 15 0 280.11 381.00 86.83 o -1 15 0 82.05 -26.38 88.79 o 0 15 0 15.27 108.77 101.85 o 1 15 0 317.33 103.62 244.61 o -14 16 0 402.74 191.34 282.08 o -13 16 0 120.43 240.55 143.68 o -12 16 0 26.96 -83.78 131.56 o -11 16 0 53.23 135.67 108.72 o -10 16 0 138.43 186.12 112.71 o -9 16 0 315.59 398.79 131.93 o -8 16 0 318.96 132.97 131.95 o -7 16 0 89.98 269.86 136.69 o -6 16 0 0.21 4.28 193.22 o -5 16 0 485.12 431.85 116.03 o -4 16 0 1091.79 982.49 170.04 o -3 16 0 1129.05 1060.36 167.51 o -2 16 0 290.93 413.82 191.64 o -1 16 0 17.31 86.79 163.02 o -12 17 0 1.69 208.71 382.15 o -11 17 0 204.77 150.44 140.83 o -10 17 0 430.22 366.74 123.29 o -9 17 0 923.80 895.85 147.55 o -8 17 0 1197.60 1473.91 243.89 o -7 17 0 509.13 469.02 144.06 o -6 17 0 11.09 126.49 117.31 o -5 17 0 417.20 419.43 161.62 o -4 17 0 1459.17 1317.40 185.23 o 4 -17 1 262.25 235.68 152.77 o 5 -17 1 13.44 98.82 129.51 o 6 -17 1 190.55 275.00 111.32 o 7 -17 1 354.74 610.41 135.56 o 8 -17 1 241.56 157.47 142.83 o 9 -17 1 33.31 -130.14 134.19 o 10 -17 1 3.95 84.12 106.40 o 11 -17 1 126.27 34.30 147.74 o 12 -17 1 83.81 132.95 204.24 o 1 -16 1 162.42 312.40 213.27 o 2 -16 1 248.73 274.20 114.99 o 3 -16 1 168.46 119.91 115.09 o 4 -16 1 49.62 174.67 197.44 o 5 -16 1 11.32 6.36 118.91 o 6 -16 1 31.23 -64.77 91.83 o 7 -16 1 31.24 126.42 93.99 o 8 -16 1 58.84 -83.13 80.65 o 9 -16 1 26.71 170.26 153.78 o 10 -16 1 0.04 39.89 91.10 o 11 -16 1 243.44 196.88 100.83 o 12 -16 1 501.38 621.09 194.27 o 13 -16 1 1016.03 722.16 236.49 o 14 -16 1 786.90 994.23 229.41 o -1 -15 1 14.04 136.86 137.98 o 0 -15 1 0.59 94.24 156.85 o 1 -15 1 0.44 185.87 116.89 o 2 -15 1 1.62 241.44 86.93 o 3 -15 1 1.41 80.18 168.10 o 4 -15 1 25.68 159.57 74.05 o 5 -15 1 48.38 103.41 62.24 o 6 -15 1 190.89 92.25 166.71 o 7 -15 1 709.87 706.57 97.47 o 8 -15 1 1358.23 1250.25 137.51 o 9 -15 1 319.81 108.04 125.68 o 10 -15 1 30.78 74.46 77.90 o 11 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