#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:08:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/48/2204833.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204833_Fobs loop_ _publ_author_name 'Rozycka-Sokolowska, Ewa' 'Marciniak, Bernard' 'Pavlyuk, Volodymyr' _publ_section_title ; Naphthalene-2,7-diol ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o114 _journal_page_last o115 _journal_volume 61 _journal_year 2005 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.8720 _cell_length_b 17.4630 _cell_length_c 5.7540 _exptl_crystal_F_000 336.00 _reflns_d_resolution_high 0.7711 _cod_data_source_file ac6141Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '2,7-dihydroxynaphthalene in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 118.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14075.68 15377.20 76.50 o 4 0 0 8.40 11.72 1.54 o 6 0 0 0.20 -0.29 1.03 o 8 0 0 0.76 0.15 1.03 o 10 0 0 0.10 -0.06 1.55 o 1 1 0 58.70 52.52 2.57 o 2 1 0 1481.95 1262.21 12.01 o 3 1 0 6.10 6.18 1.03 o 4 1 0 200.47 178.56 4.62 o 5 1 0 3.86 6.22 1.55 o 6 1 0 46.35 49.37 2.57 o 7 1 0 7.32 10.76 1.03 o 8 1 0 5.42 8.69 1.03 o 9 1 0 0.95 3.53 1.13 o 10 1 0 0.12 -0.47 2.06 o 0 2 0 852.96 877.26 13.66 o 1 2 0 334.43 325.45 6.19 o 2 2 0 860.06 879.74 9.83 o 3 2 0 354.97 308.83 5.65 o 4 2 0 79.89 79.63 3.08 o 5 2 0 37.56 40.11 2.05 o 6 2 0 128.43 129.03 3.59 o 7 2 0 0.54 -0.44 0.52 o 8 2 0 2.57 5.60 0.52 o 9 2 0 0.17 0.15 2.09 o 10 2 0 0.70 3.53 1.55 o 1 3 0 1022.14 910.42 9.89 o 2 3 0 1.96 5.61 0.52 o 3 3 0 140.16 148.87 4.10 o 4 3 0 31.86 32.71 2.05 o 5 3 0 27.39 30.86 2.05 o 6 3 0 72.07 79.00 3.08 o 7 3 0 8.13 7.40 1.03 o 8 3 0 13.49 13.57 1.54 o 9 3 0 0.00 -0.15 1.03 o 10 3 0 0.08 0.35 1.03 o 0 4 0 27.31 32.72 2.57 o 1 4 0 306.92 306.64 5.66 o 2 4 0 534.04 486.94 7.21 o 3 4 0 207.15 174.90 4.62 o 4 4 0 26.72 24.08 1.54 o 5 4 0 19.29 19.75 1.54 o 6 4 0 0.03 -0.18 2.16 o 7 4 0 1.72 2.46 0.52 o 8 4 0 11.58 11.11 1.03 o 9 4 0 1.07 6.44 0.72 o 10 4 0 1.48 5.60 0.93 o 1 5 0 271.82 250.02 5.14 o 2 5 0 136.82 124.78 3.59 o 3 5 0 91.15 96.32 3.08 o 4 5 0 11.05 11.55 1.03 o 5 5 0 120.49 128.42 3.59 o 6 5 0 8.45 9.70 1.03 o 7 5 0 62.23 64.18 2.57 o 8 5 0 1.80 4.15 0.52 o 9 5 0 0.55 2.07 0.52 o 0 6 0 36.89 37.65 3.08 o 1 6 0 117.98 114.27 3.59 o 2 6 0 271.68 245.48 5.14 o 3 6 0 2.97 -0.44 2.06 o 4 6 0 19.10 18.51 1.54 o 5 6 0 141.97 146.33 4.10 o 6 6 0 4.32 3.70 0.52 o 7 6 0 11.20 11.11 1.03 o 8 6 0 0.19 0.29 1.03 o 9 6 0 0.16 -0.63 1.13 o 1 7 0 600.83 538.80 7.72 o 2 7 0 112.85 102.50 3.59 o 3 7 0 11.79 12.96 1.54 o 4 7 0 0.01 0.44 1.03 o 5 7 0 22.50 23.45 1.54 o 6 7 0 2.66 2.46 0.52 o 7 7 0 2.16 5.60 0.52 o 8 7 0 0.64 6.44 0.52 o 9 7 0 0.04 -0.44 1.03 o 0 8 0 856.29 866.25 13.41 o 1 8 0 95.47 109.29 3.59 o 2 8 0 523.73 532.46 7.71 o 3 8 0 300.98 315.22 6.16 o 4 8 0 62.32 64.80 2.57 o 5 8 0 5.50 8.91 1.13 o 6 8 0 0.03 -0.50 1.56 o 7 8 0 1.17 3.53 0.52 o 8 8 0 0.08 -0.34 1.03 o 9 8 0 0.29 0.48 2.06 o 1 9 0 0.06 4.98 1.13 o 2 9 0 181.58 191.49 4.62 o 3 9 0 248.25 256.40 5.13 o 4 9 0 23.15 27.15 2.05 o 5 9 0 47.82 45.67 2.57 o 6 9 0 2.17 2.46 0.52 o 7 9 0 4.77 4.32 1.03 o 8 9 0 1.37 1.24 0.52 o 9 9 0 0.04 0.00 0.10 o 0 10 0 11.32 11.11 1.54 o 1 10 0 240.34 226.13 5.13 o 2 10 0 12.00 11.72 1.03 o 3 10 0 6.82 7.40 1.03 o 4 10 0 3.66 4.32 1.03 o 5 10 0 24.86 25.92 1.54 o 6 10 0 10.02 8.63 1.03 o 7 10 0 3.07 3.09 0.52 o 8 10 0 10.68 10.49 1.03 o 9 10 0 4.39 3.70 0.52 o 1 11 0 33.03 33.95 2.05 o 2 11 0 0.04 0.00 0.10 o 3 11 0 7.17 6.78 1.03 o 4 11 0 1.15 1.24 0.52 o 5 11 0 8.63 8.03 1.03 o 6 11 0 24.49 22.83 1.54 o 7 11 0 0.09 0.00 0.10 o 8 11 0 10.26 8.63 1.03 o 0 12 0 47.26 46.90 3.08 o 1 12 0 60.12 60.49 2.57 o 2 12 0 6.77 6.18 1.03 o 3 12 0 1.50 1.24 0.52 o 4 12 0 33.79 36.41 2.05 o 5 12 0 30.36 30.23 2.05 o 6 12 0 3.04 3.09 0.52 o 7 12 0 2.51 2.46 0.52 o 8 12 0 10.52 9.87 1.03 o 1 13 0 0.85 0.61 0.52 o 2 13 0 54.79 57.40 2.57 o 3 13 0 55.12 58.62 2.57 o 4 13 0 70.17 68.50 3.08 o 5 13 0 40.84 39.49 2.05 o 6 13 0 0.46 0.00 0.52 o 7 13 0 0.91 0.61 0.52 o 8 13 0 0.03 0.00 0.10 o 0 14 0 18.83 19.75 2.05 o 1 14 0 3.08 3.70 0.52 o 2 14 0 107.74 112.35 3.59 o 3 14 0 93.16 91.97 3.08 o 4 14 0 50.60 48.75 2.57 o 5 14 0 15.95 14.20 1.54 o 6 14 0 2.73 2.46 0.52 o 7 14 0 0.65 0.61 0.52 o 8 14 0 0.21 0.00 0.52 o 1 15 0 69.77 70.36 3.08 o 2 15 0 87.82 89.49 3.08 o 3 15 0 89.61 87.03 3.08 o 4 15 0 9.85 8.63 1.03 o 5 15 0 6.96 6.78 1.03 o 6 15 0 1.15 1.24 0.52 o 7 15 0 0.04 0.00 0.10 o 0 16 0 6.70 7.40 1.03 o 1 16 0 7.45 8.63 1.03 o 2 16 0 8.81 9.87 1.03 o 3 16 0 21.61 21.59 1.54 o 4 16 0 5.15 5.55 1.03 o 5 16 0 5.21 4.32 1.03 o 6 16 0 0.19 0.00 0.52 o 7 16 0 0.28 0.00 0.52 o 1 17 0 0.51 0.61 0.52 o 2 17 0 2.95 3.09 0.52 o 3 17 0 2.15 1.85 0.52 o 4 17 0 5.98 6.18 1.03 o 5 17 0 0.00 0.00 0.10 o 6 17 0 0.47 0.61 0.52 o 0 18 0 9.35 10.49 1.54 o 1 18 0 0.02 0.00 0.10 o 2 18 0 0.93 0.61 0.52 o 3 18 0 2.98 2.46 0.52 o 4 18 0 0.69 0.61 0.52 o 5 18 0 2.96 2.46 0.52 o 6 18 0 0.50 0.61 0.52 o 1 19 0 0.10 0.00 0.10 o 2 19 0 1.19 1.24 0.52 o 3 19 0 0.01 0.00 0.10 o 4 19 0 2.41 2.46 0.52 o 5 19 0 0.44 0.61 0.52 o 0 20 0 1.11 1.85 0.52 o 1 20 0 1.00 0.61 0.52 o 2 20 0 1.30 1.24 0.52 o 3 20 0 1.51 1.24 0.52 o 4 20 0 0.52 0.61 0.52 o 1 21 0 0.37 0.61 0.52 o 2 21 0 1.85 1.85 0.52 o 3 21 0 0.02 0.00 0.10 o 0 22 0 13.20 12.96 2.05 o 1 22 0 0.07 0.00 0.10 o 2 22 0 2.60 2.46 0.52 o 2 0 1 11256.54 11407.61 56.76 o 4 0 1 945.35 1012.45 14.43 o 6 0 1 23.77 19.14 2.05 o 8 0 1 2.06 1.24 0.52 o 10 0 1 0.27 0.00 0.52 o 0 1 1 1110.92 982.29 14.64 o 1 1 1 6101.22 5996.86 29.84 o 2 1 1 658.84 566.75 7.74 o 3 1 1 1428.14 1423.04 12.44 o 4 1 1 368.21 376.03 6.68 o 5 1 1 38.65 43.81 2.05 o 6 1 1 15.56 15.43 1.54 o 7 1 1 0.76 0.61 0.52 o 8 1 1 0.31 0.61 0.52 o 9 1 1 1.15 0.61 0.52 o 10 1 1 1.19 1.24 0.52 o 1 2 1 512.26 462.95 7.23 o 2 2 1 490.39 499.85 7.21 o 3 2 1 112.84 120.43 3.59 o 4 2 1 615.35 622.49 8.23 o 5 2 1 21.80 23.45 1.54 o 6 2 1 1.16 0.61 0.52 o 7 2 1 11.35 10.49 1.03 o 8 2 1 1.06 1.24 0.52 o 9 2 1 1.13 1.24 0.52 o 10 2 1 0.77 0.61 0.52 o 0 3 1 32.17 24.69 2.05 o 1 3 1 1220.12 1062.83 10.92 o 2 3 1 104.44 88.32 3.08 o 3 3 1 615.71 599.43 8.23 o 4 3 1 105.76 129.65 4.10 o 5 3 1 51.03 54.31 2.57 o 6 3 1 31.46 33.95 2.05 o 7 3 1 13.73 12.96 1.54 o 8 3 1 9.91 9.87 1.03 o 9 3 1 10.82 8.63 1.03 o 10 3 1 2.35 2.46 0.52 o 1 4 1 372.83 345.68 6.17 o 2 4 1 10.54 12.34 1.03 o 3 4 1 67.15 63.58 2.57 o 4 4 1 127.85 129.05 3.59 o 5 4 1 5.60 4.32 1.03 o 6 4 1 13.54 13.57 1.54 o 7 4 1 6.19 4.32 1.03 o 8 4 1 1.01 0.61 0.52 o 9 4 1 4.82 4.32 1.03 o 0 5 1 263.01 238.80 7.20 o 1 5 1 280.64 241.90 5.14 o 2 5 1 197.03 174.27 4.62 o 3 5 1 139.46 128.47 3.59 o 4 5 1 91.81 91.36 3.08 o 5 5 1 35.40 39.50 2.05 o 6 5 1 11.60 9.87 1.03 o 7 5 1 4.39 4.32 1.03 o 8 5 1 0.47 0.61 0.52 o 9 5 1 3.89 4.32 1.03 o 1 6 1 74.96 62.36 2.57 o 2 6 1 323.71 317.28 6.16 o 3 6 1 102.77 111.13 3.59 o 4 6 1 85.77 88.90 3.08 o 5 6 1 25.47 24.68 1.54 o 6 6 1 14.49 14.81 1.54 o 7 6 1 6.77 11.15 1.03 o 8 6 1 2.24 4.76 0.52 o 9 6 1 0.32 -0.15 1.55 o 0 7 1 500.43 509.18 10.80 o 1 7 1 251.15 229.33 5.14 o 2 7 1 79.45 98.15 3.59 o 3 7 1 239.21 239.12 5.13 o 4 7 1 12.48 15.42 1.54 o 5 7 1 1.27 1.24 0.52 o 6 7 1 7.81 7.40 1.03 o 7 7 1 0.74 4.98 1.13 o 8 7 1 0.92 6.44 1.13 o 9 7 1 0.23 -0.34 2.58 o 1 8 1 96.13 89.52 3.08 o 2 8 1 33.38 40.11 2.05 o 3 8 1 51.54 50.62 2.57 o 4 8 1 62.30 59.86 2.57 o 5 8 1 52.68 53.07 2.57 o 6 8 1 11.35 9.87 1.03 o 7 8 1 0.76 2.07 1.55 o 8 8 1 1.09 3.53 1.55 o 9 8 1 0.04 0.34 1.75 o 0 9 1 435.10 447.94 9.76 o 1 9 1 471.03 489.47 7.20 o 2 9 1 94.18 95.69 3.08 o 3 9 1 42.48 40.73 2.05 o 4 9 1 37.64 40.73 2.05 o 5 9 1 47.58 46.90 2.57 o 6 9 1 8.43 8.63 1.03 o 7 9 1 3.77 6.00 0.52 o 8 9 1 0.30 -0.03 1.55 o 9 9 1 1.43 5.60 0.52 o 1 10 1 61.51 59.87 2.57 o 2 10 1 3.41 3.70 0.52 o 3 10 1 2.57 1.85 0.52 o 4 10 1 29.68 28.39 2.05 o 5 10 1 20.73 20.36 1.54 o 6 10 1 24.74 24.68 1.54 o 7 10 1 16.25 14.81 1.54 o 8 10 1 2.82 3.09 0.52 o 9 10 1 0.77 0.61 0.52 o 0 11 1 0.07 -0.15 1.13 o 1 11 1 63.36 63.57 2.57 o 2 11 1 6.30 6.78 1.03 o 3 11 1 36.82 36.41 2.05 o 4 11 1 18.72 18.51 1.54 o 5 11 1 20.64 20.36 1.54 o 6 11 1 9.54 10.94 1.03 o 7 11 1 12.93 13.18 1.03 o 8 11 1 1.18 4.15 0.62 o 1 12 1 28.94 30.23 2.05 o 2 12 1 37.71 38.87 2.05 o 3 12 1 12.60 12.34 1.03 o 4 12 1 2.07 2.46 0.52 o 5 12 1 6.16 5.55 1.03 o 6 12 1 30.33 29.01 2.05 o 7 12 1 9.12 8.63 1.03 o 8 12 1 7.28 6.18 1.03 o 0 13 1 115.98 120.38 5.13 o 1 13 1 101.05 106.17 3.59 o 2 13 1 109.57 114.20 3.59 o 3 13 1 44.25 45.04 2.57 o 4 13 1 34.97 35.17 2.05 o 5 13 1 12.14 12.34 1.03 o 6 13 1 11.97 11.11 1.03 o 7 13 1 2.03 1.85 0.52 o 8 13 1 0.59 0.61 0.52 o 1 14 1 29.22 28.39 2.05 o 2 14 1 53.75 54.93 2.57 o 3 14 1 15.62 14.81 1.54 o 4 14 1 19.31 18.51 1.54 o 5 14 1 8.71 8.63 1.03 o 6 14 1 8.89 8.03 1.03 o 7 14 1 0.93 0.61 0.52 o 0 15 1 148.74 151.88 5.64 o 1 15 1 144.82 146.93 4.10 o 2 15 1 10.49 9.87 1.03 o 3 15 1 9.86 9.26 1.03 o 4 15 1 2.60 2.46 0.52 o 5 15 1 5.98 4.94 1.03 o 6 15 1 1.53 4.15 0.52 o 7 15 1 0.79 2.07 0.52 o 1 16 1 3.74 3.70 0.52 o 2 16 1 7.68 8.03 1.03 o 3 16 1 2.84 2.46 0.52 o 4 16 1 4.63 4.94 1.03 o 5 16 1 3.10 3.09 0.52 o 6 16 1 0.21 -0.15 1.55 o 7 16 1 1.28 1.24 0.52 o 0 17 1 27.33 27.15 2.57 o 1 17 1 6.20 6.18 1.03 o 2 17 1 9.95 9.26 1.03 o 3 17 1 2.00 1.85 0.52 o 4 17 1 5.82 4.94 1.03 o 5 17 1 1.59 4.15 0.52 o 6 17 1 3.21 6.00 0.52 o 1 18 1 0.72 3.53 0.62 o 2 18 1 3.93 3.70 0.52 o 3 18 1 1.51 2.69 0.52 o 4 18 1 0.85 1.24 0.52 o 5 18 1 0.29 -0.29 1.55 o 6 18 1 0.74 0.61 0.52 o 0 19 1 4.62 4.94 1.03 o 1 19 1 1.52 1.85 0.52 o 2 19 1 1.07 1.24 0.52 o 3 19 1 0.10 -0.04 1.03 o 4 19 1 0.78 0.61 0.52 o 5 19 1 0.38 0.15 0.52 o 1 20 1 0.14 0.00 0.52 o 2 20 1 0.68 0.61 0.52 o 3 20 1 0.11 0.15 1.03 o 4 20 1 1.16 1.24 0.52 o 0 21 1 2.34 2.46 0.52 o 1 21 1 3.45 3.09 0.52 o 2 21 1 0.22 0.00 0.52 o 3 21 1 1.39 1.24 0.52 o 1 22 1 0.45 0.61 0.52 o 2 22 1 1.67 1.85 0.52 o 0 0 2 413.85 446.04 13.89 o 2 0 2 820.71 788.10 12.89 o 4 0 2 1200.30 1282.13 16.50 o 6 0 2 147.52 150.64 5.64 o 8 0 2 1.29 0.61 0.52 o 1 1 2 139.97 165.57 4.10 o 2 1 2 367.67 385.51 6.68 o 3 1 2 782.90 841.02 9.78 o 4 1 2 64.21 61.10 2.57 o 5 1 2 278.33 278.64 5.64 o 6 1 2 7.95 8.03 1.03 o 7 1 2 18.41 17.27 1.54 o 8 1 2 2.49 1.85 0.52 o 9 1 2 0.72 0.61 0.52 o 0 2 2 846.81 821.52 12.91 o 1 2 2 936.71 875.93 9.81 o 2 2 2 363.82 338.45 6.16 o 3 2 2 146.81 157.48 4.10 o 4 2 2 8.27 11.11 1.03 o 5 2 2 68.83 67.89 3.08 o 6 2 2 20.46 20.99 1.54 o 7 2 2 8.77 9.26 1.03 o 8 2 2 7.26 6.78 1.03 o 9 2 2 4.24 3.69 1.03 o 1 3 2 113.22 123.52 3.59 o 2 3 2 134.53 132.17 4.10 o 3 3 2 14.77 16.66 1.54 o 4 3 2 38.35 37.65 2.05 o 5 3 2 48.56 49.99 2.57 o 6 3 2 33.24 36.41 2.05 o 7 3 2 35.73 32.08 2.05 o 8 3 2 11.43 11.11 1.03 o 9 3 2 2.24 1.85 0.52 o 0 4 2 63.98 75.31 4.10 o 1 4 2 228.51 195.32 4.62 o 2 4 2 169.52 184.08 4.62 o 3 4 2 8.72 9.26 1.03 o 4 4 2 32.92 33.32 2.05 o 5 4 2 29.86 25.92 1.54 o 6 4 2 27.06 26.53 2.05 o 7 4 2 11.24 10.49 1.03 o 8 4 2 3.25 2.46 0.52 o 9 4 2 1.28 1.24 0.52 o 1 5 2 74.95 72.23 3.08 o 2 5 2 145.62 153.16 4.10 o 3 5 2 91.62 106.80 3.59 o 4 5 2 21.73 18.51 1.54 o 5 5 2 14.90 14.20 1.54 o 6 5 2 8.60 8.03 1.03 o 7 5 2 0.36 0.61 0.52 o 8 5 2 5.11 4.32 1.03 o 9 5 2 1.73 1.85 0.52 o 0 6 2 958.93 919.96 13.92 o 1 6 2 358.36 386.57 6.68 o 2 6 2 71.31 72.83 3.08 o 3 6 2 144.28 155.00 4.10 o 4 6 2 5.81 4.94 1.03 o 5 6 2 6.56 6.78 1.03 o 6 6 2 0.87 0.61 0.52 o 7 6 2 0.39 0.61 0.52 o 8 6 2 1.54 1.24 0.52 o 9 6 2 0.18 0.00 0.52 o 1 7 2 146.70 146.36 4.10 o 2 7 2 41.43 40.73 2.05 o 3 7 2 21.98 23.45 1.54 o 4 7 2 1.12 1.24 0.52 o 5 7 2 13.61 12.96 1.54 o 6 7 2 0.02 0.00 0.10 o 7 7 2 0.59 0.61 0.52 o 8 7 2 0.05 0.00 0.10 o 9 7 2 0.12 0.00 0.10 o 0 8 2 240.24 237.27 7.19 o 1 8 2 31.08 35.80 2.05 o 2 8 2 91.92 96.30 3.08 o 3 8 2 93.06 91.36 3.08 o 4 8 2 24.39 25.92 1.54 o 5 8 2 12.62 11.72 1.03 o 6 8 2 4.96 4.94 1.03 o 7 8 2 3.35 3.09 0.52 o 8 8 2 0.41 0.61 0.52 o 9 8 2 0.03 0.00 0.10 o 1 9 2 155.62 161.17 4.10 o 2 9 2 111.47 122.24 3.59 o 3 9 2 106.90 108.65 3.59 o 4 9 2 62.65 61.71 2.57 o 5 9 2 10.91 10.49 1.03 o 6 9 2 10.37 9.26 1.03 o 7 9 2 12.34 11.11 1.03 o 8 9 2 1.02 1.24 0.52 o 0 10 2 19.47 20.36 2.05 o 1 10 2 3.64 4.32 1.03 o 2 10 2 39.35 41.96 2.05 o 3 10 2 87.14 89.50 3.08 o 4 10 2 57.55 59.86 2.57 o 5 10 2 15.28 14.20 1.54 o 6 10 2 10.71 10.49 1.03 o 7 10 2 0.87 0.61 0.52 o 8 10 2 0.69 0.61 0.52 o 1 11 2 19.30 19.75 1.54 o 2 11 2 25.48 26.53 2.05 o 3 11 2 30.22 31.47 2.05 o 4 11 2 26.84 25.92 1.54 o 5 11 2 42.74 40.11 2.05 o 6 11 2 1.99 1.85 0.52 o 7 11 2 6.11 5.55 1.03 o 8 11 2 0.06 0.00 0.10 o 0 12 2 31.12 32.08 2.57 o 1 12 2 38.85 40.73 2.05 o 2 12 2 1.59 1.85 0.52 o 3 12 2 9.96 10.49 1.03 o 4 12 2 50.53 49.98 2.57 o 5 12 2 1.96 1.85 0.52 o 6 12 2 14.60 12.96 1.54 o 7 12 2 0.85 0.61 0.52 o 8 12 2 1.23 1.24 0.52 o 1 13 2 11.36 11.72 1.03 o 2 13 2 22.54 23.45 1.54 o 3 13 2 3.38 3.70 0.52 o 4 13 2 15.11 15.42 1.54 o 5 13 2 3.16 3.09 0.52 o 6 13 2 4.05 3.70 0.52 o 7 13 2 6.34 5.55 1.03 o 0 14 2 273.10 283.51 7.69 o 1 14 2 98.93 95.05 3.08 o 2 14 2 67.31 66.65 2.57 o 3 14 2 11.38 11.11 1.03 o 4 14 2 5.80 5.55 1.03 o 5 14 2 3.77 3.09 0.52 o 6 14 2 0.88 0.61 0.52 o 7 14 2 2.76 2.46 0.52 o 1 15 2 17.88 17.27 1.54 o 2 15 2 19.03 18.51 1.54 o 3 15 2 15.25 14.20 1.54 o 4 15 2 4.18 4.32 1.03 o 5 15 2 1.24 1.24 0.52 o 6 15 2 0.31 0.61 0.52 o 7 15 2 1.55 1.24 0.52 o 0 16 2 10.17 9.87 1.54 o 1 16 2 20.95 21.59 1.54 o 2 16 2 13.65 13.57 1.54 o 3 16 2 2.32 2.46 0.52 o 4 16 2 1.26 1.24 0.52 o 5 16 2 0.46 0.61 0.52 o 6 16 2 1.11 1.24 0.52 o 1 17 2 0.54 0.61 0.52 o 2 17 2 1.75 1.85 0.52 o 3 17 2 2.18 1.85 0.52 o 4 17 2 0.86 0.61 0.52 o 5 17 2 0.00 0.00 0.10 o 6 17 2 0.46 0.61 0.52 o 0 18 2 1.87 1.85 0.52 o 1 18 2 4.21 3.09 0.52 o 2 18 2 1.47 1.85 0.52 o 3 18 2 1.10 1.24 0.52 o 4 18 2 0.76 0.61 0.52 o 5 18 2 0.28 0.00 0.52 o 1 19 2 0.35 0.61 0.52 o 2 19 2 1.81 1.85 0.52 o 3 19 2 2.05 1.85 0.52 o 4 19 2 0.64 0.61 0.52 o 0 20 2 0.81 0.61 0.52 o 1 20 2 0.61 0.61 0.52 o 2 20 2 0.92 1.24 0.52 o 3 20 2 0.54 0.61 0.52 o 1 21 2 0.08 0.00 0.10 o 2 21 2 0.89 0.61 0.52 o 2 0 3 126.97 135.23 5.64 o 4 0 3 26.95 29.01 2.57 o 6 0 3 112.63 112.95 5.13 o 8 0 3 25.26 23.44 2.05 o 0 1 3 529.59 521.94 10.80 o 1 1 3 158.61 176.02 4.62 o 2 1 3 249.70 249.65 5.13 o 3 1 3 10.80 10.49 1.03 o 4 1 3 6.63 5.55 1.03 o 5 1 3 48.75 49.37 2.57 o 6 1 3 3.44 3.09 0.52 o 7 1 3 23.75 21.59 1.54 o 8 1 3 1.88 1.85 0.52 o 9 1 3 2.77 2.46 0.52 o 1 2 3 6.78 8.03 1.03 o 2 2 3 66.83 73.45 3.08 o 3 2 3 4.21 4.94 1.03 o 4 2 3 0.84 0.61 0.52 o 5 2 3 13.86 15.42 1.54 o 6 2 3 44.92 43.81 2.05 o 7 2 3 17.24 16.05 1.54 o 8 2 3 9.12 8.03 1.03 o 9 2 3 0.72 0.61 0.52 o 0 3 3 332.12 363.55 8.73 o 1 3 3 170.65 178.51 4.62 o 2 3 3 27.71 32.71 2.05 o 3 3 3 68.74 75.29 3.08 o 4 3 3 45.92 49.98 2.57 o 5 3 3 72.67 74.07 3.08 o 6 3 3 37.43 36.41 2.05 o 7 3 3 3.95 3.70 0.52 o 8 3 3 1.69 1.85 0.52 o 9 3 3 0.96 0.61 0.52 o 1 4 3 22.89 22.21 1.54 o 2 4 3 4.52 4.32 1.03 o 3 4 3 73.15 79.62 3.08 o 4 4 3 71.57 75.29 3.08 o 5 4 3 46.44 47.52 2.57 o 6 4 3 7.54 6.18 1.03 o 7 4 3 9.77 9.26 1.03 o 8 4 3 0.53 0.61 0.52 o 9 4 3 0.47 0.61 0.52 o 0 5 3 416.01 450.89 9.76 o 1 5 3 230.83 229.83 5.13 o 2 5 3 30.58 32.71 2.05 o 3 5 3 7.15 6.18 1.03 o 4 5 3 14.90 16.05 1.54 o 5 5 3 7.98 8.63 1.03 o 6 5 3 3.47 3.09 0.52 o 7 5 3 1.08 1.24 0.52 o 8 5 3 0.90 0.61 0.52 o 9 5 3 0.94 0.61 0.52 o 1 6 3 43.98 46.29 2.57 o 2 6 3 79.72 80.23 3.08 o 3 6 3 23.09 23.45 1.54 o 4 6 3 1.17 1.85 0.52 o 5 6 3 5.22 5.55 1.03 o 6 6 3 7.41 6.78 1.03 o 7 6 3 2.36 1.85 0.52 o 8 6 3 3.62 3.09 0.52 o 0 7 3 6.09 6.78 1.03 o 1 7 3 68.02 77.16 3.08 o 2 7 3 55.67 57.40 2.57 o 3 7 3 4.75 4.94 1.03 o 4 7 3 41.13 41.95 2.05 o 5 7 3 10.79 11.72 1.03 o 6 7 3 5.29 4.94 1.03 o 7 7 3 2.16 1.85 0.52 o 8 7 3 0.46 0.61 0.52 o 1 8 3 36.22 36.41 2.05 o 2 8 3 14.42 14.20 1.54 o 3 8 3 8.64 9.87 1.03 o 4 8 3 6.97 7.40 1.03 o 5 8 3 10.97 9.87 1.03 o 6 8 3 3.72 3.70 0.52 o 7 8 3 0.92 0.61 0.52 o 8 8 3 0.84 0.61 0.52 o 0 9 3 118.74 127.18 5.13 o 1 9 3 93.37 96.29 3.08 o 2 9 3 50.83 49.99 2.57 o 3 9 3 7.24 8.03 1.03 o 4 9 3 0.18 0.00 0.52 o 5 9 3 2.87 2.46 0.52 o 6 9 3 2.47 2.46 0.52 o 7 9 3 0.20 0.00 0.52 o 8 9 3 0.51 0.61 0.52 o 1 10 3 61.68 65.43 2.57 o 2 10 3 50.36 51.84 2.57 o 3 10 3 41.96 41.35 2.05 o 4 10 3 25.01 22.83 1.54 o 5 10 3 2.47 1.85 0.52 o 6 10 3 0.64 0.61 0.52 o 7 10 3 0.30 0.00 0.52 o 8 10 3 0.22 0.00 0.52 o 0 11 3 61.67 66.65 3.59 o 1 11 3 99.87 103.08 3.59 o 2 11 3 24.81 25.30 1.54 o 3 11 3 120.11 119.75 3.59 o 4 11 3 1.72 1.85 0.52 o 5 11 3 7.46 6.78 1.03 o 6 11 3 0.41 0.61 0.52 o 7 11 3 0.03 0.00 0.10 o 1 12 3 8.97 9.26 1.03 o 2 12 3 53.15 52.46 2.57 o 3 12 3 5.88 5.55 1.03 o 4 12 3 18.05 16.66 1.54 o 5 12 3 0.96 0.61 0.52 o 6 12 3 1.41 1.24 0.52 o 7 12 3 1.78 1.24 0.52 o 0 13 3 30.44 34.56 2.57 o 1 13 3 4.22 4.32 1.03 o 2 13 3 0.53 0.61 0.52 o 3 13 3 5.74 5.55 1.03 o 4 13 3 2.22 2.46 0.52 o 5 13 3 1.42 1.24 0.52 o 6 13 3 0.72 0.61 0.52 o 7 13 3 0.43 0.61 0.52 o 1 14 3 6.39 5.55 1.03 o 2 14 3 23.17 23.45 1.54 o 3 14 3 27.68 24.68 1.54 o 4 14 3 7.67 7.40 1.03 o 5 14 3 8.77 7.40 1.03 o 6 14 3 0.81 0.61 0.52 o 0 15 3 2.19 2.46 0.52 o 1 15 3 3.62 3.70 0.52 o 2 15 3 8.81 8.63 1.03 o 3 15 3 15.45 14.81 1.54 o 4 15 3 7.46 7.40 1.03 o 5 15 3 8.87 8.03 1.03 o 6 15 3 0.79 0.61 0.52 o 1 16 3 1.60 1.24 0.52 o 2 16 3 0.58 0.61 0.52 o 3 16 3 1.00 1.24 0.52 o 4 16 3 7.32 6.78 1.03 o 5 16 3 0.16 0.00 0.52 o 0 17 3 1.02 0.61 0.52 o 1 17 3 0.67 0.61 0.52 o 2 17 3 4.98 4.32 1.03 o 3 17 3 0.69 0.61 0.52 o 4 17 3 0.54 0.61 0.52 o 5 17 3 1.03 1.24 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