#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2204836.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204836_Fobs loop_ _publ_author_name 'Zhang, Guang-Wen' 'Liao, Cheng-Zhu' 'Yao, Xin-Sheng' 'Kurihara, Hiroshi' 'Su, Jing-Yu' 'Zeng, Long-Mei' _publ_section_title ; 8\b-Hydroxy-2,6,6-trimethyl-5\bH,10\bH-eudesma-1,7(11)-dien-12,8-olide ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o172 _journal_page_last o173 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.1843 _cell_length_b 8.7554 _cell_length_c 21.3099 _exptl_crystal_F_000 536.00 _reflns_d_resolution_high 0.7831 _[local]_cod_data_source_file ac6144Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 04182m in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1342.50 1353.46 14.39 o 4 0 0 187.27 225.53 2.68 o 6 0 0 11.58 12.45 0.56 o 8 0 0 18.21 17.41 1.07 o 1 1 0 6959.76 5473.99 81.09 o 2 1 0 3770.99 3550.37 42.83 o 3 1 0 888.44 1041.23 7.89 o 4 1 0 970.33 1039.09 7.92 o 5 1 0 17.79 20.19 0.42 o 6 1 0 61.02 60.79 1.10 o 7 1 0 114.52 97.03 1.30 o 8 1 0 0.98 2.14 0.45 o 9 1 0 19.72 20.49 1.09 o 0 2 0 2407.01 2291.49 29.48 o 1 2 0 135.37 138.88 1.76 o 2 2 0 5.76 4.59 0.24 o 3 2 0 16.69 19.61 0.35 o 4 2 0 619.46 675.00 5.23 o 5 2 0 48.63 42.08 0.71 o 6 2 0 27.67 25.08 0.61 o 7 2 0 10.23 10.18 0.53 o 8 2 0 0.16 -0.01 0.34 o 9 2 0 0.00 -0.28 0.61 o 1 3 0 1615.17 1630.87 11.00 o 2 3 0 590.17 589.74 5.27 o 3 3 0 1127.65 1157.30 12.45 o 4 3 0 19.28 20.81 0.63 o 5 3 0 14.14 11.27 0.43 o 6 3 0 16.03 15.59 0.52 o 7 3 0 3.23 2.02 0.36 o 8 3 0 0.56 1.19 0.50 o 0 4 0 408.60 425.81 3.84 o 1 4 0 458.77 500.08 3.17 o 2 4 0 210.28 223.76 2.19 o 3 4 0 447.99 437.30 4.99 o 4 4 0 21.34 23.71 0.69 o 5 4 0 147.20 159.38 1.78 o 6 4 0 47.16 46.90 0.84 o 7 4 0 4.19 3.36 0.52 o 8 4 0 1.56 2.71 0.52 o 1 5 0 44.97 41.88 0.42 o 2 5 0 105.31 105.97 1.06 o 3 5 0 0.01 -0.12 0.26 o 4 5 0 29.34 28.39 0.78 o 5 5 0 5.86 5.75 0.49 o 6 5 0 0.17 0.65 0.43 o 7 5 0 1.35 1.01 0.43 o 8 5 0 25.65 25.96 1.15 o 0 6 0 825.38 827.51 8.08 o 1 6 0 266.10 269.35 1.84 o 2 6 0 106.67 109.55 1.13 o 3 6 0 7.65 8.19 0.35 o 4 6 0 48.99 45.29 1.01 o 5 6 0 27.35 24.40 0.81 o 6 6 0 2.28 1.04 0.70 o 7 6 0 2.40 1.31 0.52 o 1 7 0 5.78 4.17 0.29 o 2 7 0 345.36 343.99 2.93 o 3 7 0 0.21 0.10 0.25 o 4 7 0 92.80 91.94 1.29 o 5 7 0 46.74 47.10 1.12 o 6 7 0 2.13 2.13 0.84 o 7 7 0 1.86 2.51 0.57 o 0 8 0 447.33 425.60 7.19 o 1 8 0 56.93 48.27 0.73 o 2 8 0 53.47 53.68 0.79 o 3 8 0 306.27 306.08 2.75 o 4 8 0 11.56 11.84 0.75 o 5 8 0 2.83 3.60 0.44 o 6 8 0 4.05 4.47 0.62 o 1 9 0 0.64 1.10 0.40 o 2 9 0 10.45 11.18 0.54 o 3 9 0 12.75 18.21 0.54 o 4 9 0 23.10 24.66 0.75 o 5 9 0 0.00 -0.44 0.72 o 0 10 0 13.19 14.02 1.06 o 1 10 0 26.66 28.69 1.43 o 2 10 0 1.39 2.17 0.63 o 3 10 0 28.08 30.60 0.83 o 4 10 0 4.97 5.43 0.64 o 1 11 0 4.58 3.42 0.59 o 1 0 1 1756.02 1592.93 14.23 o 2 0 1 5531.30 4961.50 41.64 o 3 0 1 1309.81 1365.71 12.55 o 4 0 1 0.03 0.02 0.16 o 5 0 1 101.85 115.64 1.14 o 6 0 1 183.28 177.39 1.66 o 7 0 1 72.17 68.89 1.31 o 8 0 1 1.37 1.21 0.59 o 9 0 1 18.04 17.86 0.83 o 0 1 1 3736.74 3229.59 31.69 o 1 1 1 920.78 881.72 5.49 o 2 1 1 534.18 519.50 3.02 o 3 1 1 1063.67 1135.37 6.07 o 4 1 1 227.53 243.13 1.43 o 5 1 1 19.99 19.90 0.29 o 6 1 1 174.45 166.89 1.31 o 7 1 1 27.45 27.96 0.47 o 8 1 1 40.38 38.55 0.72 o 9 1 1 3.70 3.35 0.48 o 0 2 1 380.39 360.15 2.86 o 1 2 1 5805.63 5127.30 49.16 o 2 2 1 602.65 592.99 4.10 o 3 2 1 648.22 708.14 4.12 o 4 2 1 94.18 89.18 0.63 o 5 2 1 7.81 8.26 0.28 o 6 2 1 0.32 0.13 0.20 o 7 2 1 16.61 13.36 0.48 o 8 2 1 11.89 12.28 0.39 o 9 2 1 6.37 6.46 0.53 o 0 3 1 78.76 95.26 0.68 o 1 3 1 153.84 151.51 0.80 o 2 3 1 101.43 94.37 0.81 o 3 3 1 366.00 349.71 2.84 o 4 3 1 157.75 180.16 1.45 o 5 3 1 87.05 94.27 0.84 o 6 3 1 39.89 31.05 0.48 o 7 3 1 16.91 19.98 0.48 o 8 3 1 4.46 4.18 0.37 o 0 4 1 328.31 360.01 2.32 o 1 4 1 290.74 307.58 1.42 o 2 4 1 103.47 107.73 0.76 o 3 4 1 65.46 59.89 0.90 o 4 4 1 31.07 34.10 0.56 o 5 4 1 52.50 53.26 0.67 o 6 4 1 17.17 16.49 0.44 o 7 4 1 5.14 5.33 0.46 o 8 4 1 5.49 6.48 0.46 o 0 5 1 283.02 303.86 2.01 o 1 5 1 69.75 56.95 0.36 o 2 5 1 86.70 93.01 0.68 o 3 5 1 122.73 124.65 1.11 o 4 5 1 31.95 33.97 0.60 o 5 5 1 44.44 40.63 0.69 o 6 5 1 68.97 64.98 1.00 o 7 5 1 1.17 1.06 0.33 o 8 5 1 3.65 4.12 0.46 o 0 6 1 34.35 31.30 0.40 o 1 6 1 118.32 124.08 0.68 o 2 6 1 100.16 97.97 0.74 o 3 6 1 77.64 76.05 0.69 o 4 6 1 39.79 38.96 0.66 o 5 6 1 28.83 28.64 0.60 o 6 6 1 1.01 0.29 0.29 o 7 6 1 0.13 -0.34 0.34 o 0 7 1 73.01 68.88 0.66 o 1 7 1 54.84 49.63 0.46 o 2 7 1 184.35 175.03 1.18 o 3 7 1 87.04 83.95 0.72 o 4 7 1 1.52 1.61 0.23 o 5 7 1 1.56 1.97 0.31 o 6 7 1 21.87 22.58 0.61 o 7 7 1 3.68 2.54 0.41 o 0 8 1 34.11 32.87 0.89 o 1 8 1 100.86 94.53 0.83 o 2 8 1 97.29 96.14 0.79 o 3 8 1 15.07 12.70 0.33 o 4 8 1 0.08 -0.15 0.22 o 5 8 1 36.24 35.16 0.59 o 6 8 1 9.07 10.80 0.43 o 0 9 1 1.71 2.56 0.64 o 1 9 1 20.01 18.89 0.52 o 2 9 1 27.56 27.59 0.47 o 3 9 1 25.82 24.89 0.47 o 4 9 1 3.95 4.69 0.32 o 5 9 1 1.14 1.80 0.35 o 0 10 1 19.97 21.83 0.85 o 1 10 1 23.88 27.59 0.77 o 2 10 1 30.79 30.29 0.70 o 3 10 1 7.42 7.34 0.37 o 4 10 1 1.53 1.14 0.43 o 0 11 1 0.70 0.81 0.54 o 1 11 1 12.18 13.72 0.59 o 0 0 2 28.64 33.04 0.62 o 1 0 2 1221.15 1178.08 24.84 o 2 0 2 1040.86 1023.56 8.97 o 3 0 2 629.11 730.14 5.58 o 4 0 2 153.05 148.55 1.33 o 5 0 2 21.30 22.25 0.43 o 6 0 2 18.32 17.79 0.45 o 7 0 2 177.90 152.14 2.19 o 8 0 2 7.93 9.65 0.63 o 9 0 2 0.80 0.74 0.52 o 0 1 2 8057.25 6014.49 167.28 o 1 1 2 5410.77 4770.56 50.02 o 2 1 2 1025.09 1063.75 6.09 o 3 1 2 607.26 628.71 3.66 o 4 1 2 173.30 182.19 1.12 o 5 1 2 172.01 165.42 1.07 o 6 1 2 75.96 69.09 0.71 o 7 1 2 7.46 7.98 0.31 o 8 1 2 9.15 9.08 0.43 o 9 1 2 8.67 9.05 0.49 o 0 2 2 7820.13 6626.55 56.06 o 1 2 2 2758.05 2631.86 14.19 o 2 2 2 42.34 38.66 0.43 o 3 2 2 68.79 74.76 0.69 o 4 2 2 535.97 576.50 3.41 o 5 2 2 17.45 18.44 0.35 o 6 2 2 97.43 96.30 0.97 o 7 2 2 21.23 19.75 0.42 o 8 2 2 16.50 15.95 0.52 o 9 2 2 24.37 26.46 0.78 o 0 3 2 3105.72 3054.09 18.76 o 1 3 2 927.27 1007.10 4.84 o 2 3 2 416.10 412.53 2.65 o 3 3 2 169.20 171.99 1.34 o 4 3 2 85.70 88.64 0.84 o 5 3 2 81.64 84.09 0.78 o 6 3 2 13.08 10.30 0.33 o 7 3 2 7.44 9.01 0.39 o 8 3 2 16.72 16.29 0.48 o 0 4 2 3707.12 3823.88 23.43 o 1 4 2 16.24 15.85 0.26 o 2 4 2 16.08 16.57 0.23 o 3 4 2 142.31 153.61 1.42 o 4 4 2 155.04 150.09 1.27 o 5 4 2 37.93 39.11 0.65 o 6 4 2 3.56 4.45 0.30 o 7 4 2 32.13 35.26 0.72 o 8 4 2 1.62 1.94 0.35 o 0 5 2 122.69 144.32 1.04 o 1 5 2 121.71 136.00 0.70 o 2 5 2 207.32 221.83 1.36 o 3 5 2 357.05 380.26 2.81 o 4 5 2 30.94 32.48 0.58 o 5 5 2 287.90 272.07 2.46 o 6 5 2 0.75 1.53 0.32 o 7 5 2 32.59 29.91 0.67 o 8 5 2 3.14 3.05 0.40 o 0 6 2 9.66 9.60 0.25 o 1 6 2 518.67 538.16 2.69 o 2 6 2 46.26 42.95 0.44 o 3 6 2 69.98 64.99 0.63 o 4 6 2 264.01 253.72 2.30 o 5 6 2 2.88 2.57 0.33 o 6 6 2 8.88 8.95 0.44 o 7 6 2 0.72 0.80 0.36 o 0 7 2 177.09 173.49 1.44 o 1 7 2 280.56 278.36 1.60 o 2 7 2 120.60 120.77 0.89 o 3 7 2 18.05 22.40 0.39 o 4 7 2 5.31 6.21 0.29 o 5 7 2 7.29 7.39 0.41 o 6 7 2 3.75 4.29 0.50 o 7 7 2 7.86 9.61 0.57 o 0 8 2 65.51 61.32 0.96 o 1 8 2 83.85 83.47 0.76 o 2 8 2 16.65 15.10 0.33 o 3 8 2 25.94 24.60 0.43 o 4 8 2 14.65 16.33 0.41 o 5 8 2 2.21 2.33 0.28 o 6 8 2 8.80 10.36 0.45 o 0 9 2 63.07 60.83 1.26 o 1 9 2 9.08 8.42 0.40 o 2 9 2 43.80 44.53 0.58 o 3 9 2 31.74 31.16 0.55 o 4 9 2 1.40 1.09 0.26 o 5 9 2 4.98 4.01 0.37 o 0 10 2 0.83 1.28 0.47 o 1 10 2 7.61 9.75 0.47 o 2 10 2 1.29 0.89 0.39 o 3 10 2 8.04 6.73 0.45 o 4 10 2 7.04 8.65 0.49 o 0 11 2 20.96 24.02 0.98 o 1 11 2 3.67 5.29 0.59 o 1 0 3 12202.78 9424.61 144.67 o 2 0 3 1060.52 1062.23 9.31 o 3 0 3 119.98 111.21 1.16 o 4 0 3 299.35 311.06 2.54 o 5 0 3 74.38 79.21 0.87 o 6 0 3 5.32 4.53 0.30 o 7 0 3 80.47 71.06 1.33 o 8 0 3 14.47 12.59 0.68 o 9 0 3 25.89 33.15 1.05 o 0 1 3 145.32 153.15 1.24 o 1 1 3 2420.56 2393.65 14.59 o 2 1 3 42.63 37.61 0.33 o 3 1 3 1412.63 1527.53 8.71 o 4 1 3 330.82 343.69 1.96 o 5 1 3 15.41 17.48 0.29 o 6 1 3 170.46 157.61 1.25 o 7 1 3 1.42 1.63 0.24 o 8 1 3 3.02 2.83 0.33 o 9 1 3 11.63 14.12 0.65 o 0 2 3 396.30 393.04 2.47 o 1 2 3 723.73 738.40 4.27 o 2 2 3 163.78 164.72 0.97 o 3 2 3 451.20 461.85 2.73 o 4 2 3 32.95 40.85 0.60 o 5 2 3 129.72 144.51 1.13 o 6 2 3 58.67 50.78 0.60 o 7 2 3 55.79 57.80 0.72 o 8 2 3 3.10 3.18 0.36 o 0 3 3 3811.23 3789.67 23.27 o 1 3 3 302.42 305.43 1.62 o 2 3 3 458.99 487.64 3.12 o 3 3 3 2.24 0.77 0.11 o 4 3 3 86.95 95.45 0.88 o 5 3 3 20.91 24.49 0.58 o 6 3 3 22.71 21.70 0.41 o 7 3 3 26.59 29.12 0.56 o 8 3 3 3.13 2.74 0.36 o 0 4 3 343.95 325.81 2.11 o 1 4 3 709.86 741.34 3.28 o 2 4 3 1063.18 1097.78 6.92 o 3 4 3 56.64 69.20 0.70 o 4 4 3 28.29 29.66 0.52 o 5 4 3 141.20 139.79 1.43 o 6 4 3 52.59 55.35 0.73 o 7 4 3 57.35 53.41 0.77 o 8 4 3 11.94 12.71 0.52 o 0 5 3 416.09 432.14 2.79 o 1 5 3 357.03 374.70 1.73 o 2 5 3 476.82 473.56 2.52 o 3 5 3 198.44 185.30 1.52 o 4 5 3 88.12 85.05 1.00 o 5 5 3 64.70 66.76 1.08 o 6 5 3 1.60 1.32 0.29 o 7 5 3 4.86 5.98 0.41 o 8 5 3 8.62 9.40 0.51 o 0 6 3 34.07 33.01 0.39 o 1 6 3 159.03 149.02 0.83 o 2 6 3 116.13 109.25 0.80 o 3 6 3 42.11 43.25 0.50 o 4 6 3 115.77 115.31 1.27 o 5 6 3 84.92 79.45 1.04 o 6 6 3 32.56 32.14 0.69 o 7 6 3 7.31 5.98 0.42 o 0 7 3 133.25 132.28 1.17 o 1 7 3 12.44 12.34 0.26 o 2 7 3 71.89 73.09 0.64 o 3 7 3 123.04 121.19 0.99 o 4 7 3 14.97 14.13 0.42 o 5 7 3 7.51 8.29 0.48 o 6 7 3 3.70 3.17 0.38 o 7 7 3 0.92 2.01 0.53 o 0 8 3 40.34 44.86 0.80 o 1 8 3 145.41 143.09 1.03 o 2 8 3 43.41 45.27 0.55 o 3 8 3 44.80 38.42 0.52 o 4 8 3 16.18 13.84 0.40 o 5 8 3 17.38 15.40 0.48 o 6 8 3 12.93 13.34 0.81 o 0 9 3 22.51 20.99 0.77 o 1 9 3 6.64 6.74 0.34 o 2 9 3 35.56 37.35 0.54 o 3 9 3 2.04 1.45 0.25 o 4 9 3 6.50 7.12 0.42 o 5 9 3 5.01 4.44 0.37 o 0 10 3 1.39 1.41 0.49 o 1 10 3 0.43 -0.01 0.30 o 2 10 3 19.38 20.91 0.72 o 3 10 3 2.48 2.54 0.36 o 0 11 3 10.37 12.69 1.15 o 1 11 3 42.87 47.37 1.06 o 0 0 4 449.43 417.62 6.56 o 1 0 4 561.43 566.35 5.02 o 2 0 4 1483.20 1514.91 31.86 o 3 0 4 5.59 4.21 0.28 o 4 0 4 574.74 620.55 4.83 o 5 0 4 72.73 73.20 1.09 o 6 0 4 38.20 30.66 0.56 o 7 0 4 2.14 1.90 0.42 o 8 0 4 37.76 37.98 1.02 o 9 0 4 46.29 47.57 1.23 o 0 1 4 157.73 174.80 1.41 o 1 1 4 97.46 96.47 0.62 o 2 1 4 1444.85 1462.43 8.33 o 3 1 4 412.36 440.65 2.61 o 4 1 4 906.51 923.95 5.36 o 5 1 4 138.04 131.97 0.90 o 6 1 4 11.77 8.97 0.32 o 7 1 4 44.91 47.22 0.61 o 8 1 4 1.07 0.77 0.31 o 9 1 4 3.30 3.06 0.53 o 0 2 4 1447.20 1490.91 9.17 o 1 2 4 34.50 38.04 0.38 o 2 2 4 8.13 10.67 0.25 o 3 2 4 236.82 236.66 1.47 o 4 2 4 242.49 251.23 1.59 o 5 2 4 7.25 6.03 0.62 o 6 2 4 129.33 124.53 1.07 o 7 2 4 6.84 6.63 0.31 o 8 2 4 2.31 3.24 0.49 o 0 3 4 75.34 73.91 0.56 o 1 3 4 401.99 393.98 1.95 o 2 3 4 1165.67 1276.51 7.39 o 3 3 4 50.61 46.36 0.44 o 4 3 4 254.11 247.40 1.71 o 5 3 4 108.20 95.75 0.93 o 6 3 4 15.26 13.50 0.41 o 7 3 4 119.96 116.73 1.22 o 8 3 4 3.36 3.63 0.34 o 0 4 4 369.98 386.32 2.48 o 1 4 4 95.75 112.02 0.65 o 2 4 4 152.51 136.20 0.86 o 3 4 4 79.94 75.67 0.89 o 4 4 4 0.02 -0.11 0.23 o 5 4 4 111.55 106.50 1.19 o 6 4 4 12.46 12.95 0.46 o 7 4 4 9.60 8.95 0.40 o 8 4 4 6.05 6.01 0.61 o 0 5 4 126.61 146.14 2.20 o 1 5 4 566.61 605.63 2.72 o 2 5 4 175.69 178.28 1.15 o 3 5 4 38.72 37.79 0.53 o 4 5 4 236.32 225.41 2.05 o 5 5 4 31.14 28.66 0.60 o 6 5 4 27.14 24.74 0.60 o 7 5 4 18.97 20.76 0.60 o 8 5 4 4.60 4.68 0.44 o 0 6 4 76.41 75.38 0.66 o 1 6 4 71.79 69.42 0.50 o 2 6 4 247.66 247.41 1.53 o 3 6 4 147.05 140.94 1.07 o 4 6 4 141.38 134.96 1.42 o 5 6 4 18.05 17.50 0.51 o 6 6 4 44.06 38.79 0.74 o 7 6 4 25.59 26.46 0.67 o 0 7 4 52.61 67.01 0.73 o 1 7 4 384.55 389.55 2.69 o 2 7 4 33.65 30.90 0.40 o 3 7 4 16.49 13.87 0.33 o 4 7 4 32.41 32.36 0.52 o 5 7 4 68.77 67.09 0.98 o 6 7 4 3.13 3.82 0.44 o 7 7 4 41.09 46.01 0.90 o 0 8 4 44.63 44.02 0.80 o 1 8 4 25.28 24.29 0.38 o 2 8 4 11.63 10.71 0.32 o 3 8 4 8.41 7.97 0.30 o 4 8 4 12.83 13.73 0.44 o 5 8 4 4.94 5.26 0.36 o 6 8 4 4.62 5.44 0.39 o 0 9 4 10.56 10.57 0.63 o 1 9 4 12.16 11.99 0.37 o 2 9 4 28.33 28.12 0.65 o 3 9 4 0.39 0.59 0.35 o 4 9 4 0.97 1.31 0.34 o 5 9 4 3.83 5.44 0.59 o 0 10 4 0.20 -0.02 0.44 o 1 10 4 1.78 2.79 0.40 o 2 10 4 0.80 0.55 0.38 o 3 10 4 14.16 15.51 0.50 o 0 11 4 0.75 -0.18 0.74 o 1 0 5 1215.78 1222.83 10.71 o 2 0 5 3655.27 3479.47 30.32 o 3 0 5 22.57 27.00 0.42 o 4 0 5 254.56 285.51 2.54 o 5 0 5 312.97 302.25 2.55 o 6 0 5 1.77 3.75 0.29 o 7 0 5 4.07 5.03 0.47 o 8 0 5 1.22 1.71 0.46 o 9 0 5 2.96 4.35 0.79 o 0 1 5 95.73 102.03 0.88 o 1 1 5 865.76 864.01 4.98 o 2 1 5 880.24 915.74 5.70 o 3 1 5 310.16 309.98 1.88 o 4 1 5 1111.78 1126.25 6.50 o 5 1 5 34.54 41.73 0.60 o 6 1 5 105.74 107.13 0.95 o 7 1 5 16.73 17.01 0.40 o 8 1 5 3.99 4.26 0.43 o 0 2 5 469.55 438.38 2.76 o 1 2 5 465.10 482.53 2.64 o 2 2 5 382.94 447.18 2.47 o 3 2 5 13.67 12.74 0.20 o 4 2 5 170.47 178.64 1.18 o 5 2 5 13.42 13.21 0.53 o 6 2 5 38.13 34.77 0.51 o 7 2 5 75.92 70.84 0.87 o 8 2 5 25.73 26.77 0.64 o 0 3 5 3.59 4.37 0.12 o 1 3 5 675.48 756.21 3.87 o 2 3 5 228.15 237.01 1.48 o 3 3 5 82.59 88.60 0.64 o 4 3 5 568.45 578.21 3.72 o 5 3 5 47.24 40.35 0.64 o 6 3 5 35.27 35.66 0.63 o 7 3 5 1.34 0.87 0.28 o 8 3 5 24.76 26.05 0.59 o 0 4 5 2961.62 3123.75 19.05 o 1 4 5 341.69 347.38 1.90 o 2 4 5 28.10 28.42 0.29 o 3 4 5 13.85 16.62 0.29 o 4 4 5 177.19 176.18 2.67 o 5 4 5 27.51 24.76 0.54 o 6 4 5 106.19 99.54 1.19 o 7 4 5 70.37 73.46 0.93 o 8 4 5 1.55 2.42 0.35 o 0 5 5 66.40 60.31 0.53 o 1 5 5 348.33 408.91 1.98 o 2 5 5 34.80 40.67 0.39 o 3 5 5 94.85 96.53 0.94 o 4 5 5 69.83 69.33 0.98 o 5 5 5 146.67 128.79 1.39 o 6 5 5 119.83 115.76 1.35 o 7 5 5 33.29 32.84 0.73 o 8 5 5 7.57 9.71 0.53 o 0 6 5 19.55 17.26 0.38 o 1 6 5 49.97 51.80 0.39 o 2 6 5 352.69 359.03 2.12 o 3 6 5 16.72 14.98 0.31 o 4 6 5 32.82 32.66 0.62 o 5 6 5 45.39 43.81 0.75 o 6 6 5 37.64 35.28 0.73 o 7 6 5 8.30 10.21 0.54 o 0 7 5 50.14 53.43 0.63 o 1 7 5 240.38 234.52 1.49 o 2 7 5 7.44 7.54 0.24 o 3 7 5 41.10 40.24 0.50 o 4 7 5 97.32 91.48 1.01 o 5 7 5 23.55 21.40 0.58 o 6 7 5 96.45 96.66 1.51 o 0 8 5 13.48 14.30 0.51 o 1 8 5 32.47 30.87 0.41 o 2 8 5 4.23 4.53 0.25 o 3 8 5 18.30 16.76 0.45 o 4 8 5 14.04 13.90 0.40 o 5 8 5 29.58 28.76 0.60 o 6 8 5 6.10 8.21 0.44 o 0 9 5 2.38 2.50 0.35 o 1 9 5 9.92 9.77 0.38 o 2 9 5 10.89 9.60 0.36 o 3 9 5 2.66 3.07 0.32 o 4 9 5 10.01 10.63 0.44 o 5 9 5 1.33 1.43 0.37 o 0 10 5 27.92 29.67 1.35 o 1 10 5 12.17 11.96 0.74 o 2 10 5 6.13 5.31 0.37 o 3 10 5 8.36 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13 13.20 13.39 0.50 o 2 8 13 18.19 19.23 0.51 o 3 8 13 18.10 19.63 0.52 o 4 8 13 2.65 1.88 0.50 o 0 9 13 1.56 0.95 0.49 o 1 9 13 34.07 33.36 0.74 o 2 9 13 16.74 16.29 0.59 o 3 9 13 7.64 7.23 0.43 o 0 0 14 4.64 3.93 0.26 o 1 0 14 89.19 101.70 1.56 o 2 0 14 13.16 11.09 0.71 o 3 0 14 11.43 16.00 0.43 o 4 0 14 27.80 23.17 0.54 o 5 0 14 18.44 20.62 0.71 o 6 0 14 2.55 3.02 0.50 o 7 0 14 10.29 10.40 0.73 o 0 1 14 1.44 1.79 0.24 o 1 1 14 8.55 8.16 0.34 o 2 1 14 15.61 18.09 0.28 o 3 1 14 154.82 140.84 1.12 o 4 1 14 79.64 75.49 0.82 o 5 1 14 14.16 13.53 0.40 o 6 1 14 5.40 6.13 0.41 o 7 1 14 35.65 35.40 0.91 o 0 2 14 1198.94 1180.29 13.77 o 1 2 14 28.59 31.40 0.38 o 2 2 14 24.27 25.47 0.39 o 3 2 14 6.51 5.34 0.28 o 4 2 14 115.95 109.77 0.98 o 5 2 14 96.40 90.08 0.99 o 6 2 14 10.68 11.16 0.48 o 7 2 14 12.17 12.48 0.47 o 0 3 14 74.12 66.85 0.91 o 1 3 14 107.85 105.77 0.85 o 2 3 14 297.89 280.88 1.98 o 3 3 14 208.87 195.43 1.38 o 4 3 14 105.51 91.97 0.98 o 5 3 14 1.26 1.05 0.28 o 6 3 14 23.10 24.33 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5.38 0.36 o 2 6 19 9.90 8.82 0.36 o 3 6 19 1.04 1.06 0.34 o 4 6 19 6.04 6.41 0.46 o 0 7 19 12.36 11.64 0.73 o 1 7 19 8.35 10.14 0.40 o 2 7 19 4.71 4.17 0.36 o 3 7 19 25.99 26.92 0.66 o 0 8 19 1.16 1.99 0.53 o 0 0 20 125.97 122.94 2.82 o 1 0 20 0.48 0.31 0.43 o 2 0 20 0.58 0.07 0.49 o 3 0 20 19.65 21.57 0.77 o 4 0 20 0.27 0.24 0.40 o 5 0 20 1.72 2.82 0.62 o 6 0 20 18.35 23.48 1.40 o 0 1 20 89.92 92.33 2.38 o 1 1 20 13.35 13.98 0.48 o 2 1 20 31.82 29.18 0.55 o 3 1 20 2.13 1.24 0.28 o 4 1 20 5.45 4.74 0.35 o 5 1 20 6.19 7.59 0.51 o 6 1 20 16.54 17.18 0.74 o 0 2 20 14.69 14.73 0.68 o 1 2 20 168.05 151.23 1.64 o 2 2 20 31.97 30.94 0.57 o 3 2 20 61.87 61.03 1.20 o 4 2 20 17.40 17.82 0.53 o 5 2 20 5.90 9.57 0.49 o 6 2 20 21.67 23.79 0.97 o 0 3 20 15.94 17.64 0.73 o 1 3 20 25.32 25.91 0.79 o 2 3 20 26.81 24.82 0.53 o 3 3 20 55.18 56.94 0.90 o 4 3 20 17.04 17.22 0.49 o 5 3 20 37.51 37.69 0.77 o 0 4 20 0.22 0.02 0.48 o 1 4 20 16.59 14.21 0.40 o 2 4 20 19.29 20.00 0.50 o 3 4 20 7.97 9.10 0.39 o 4 4 20 9.73 13.87 0.53 o 5 4 20 3.74 3.25 0.53 o 0 5 20 1.12 1.03 0.42 o 1 5 20 17.56 16.95 0.43 o 2 5 20 23.13 23.34 0.54 o 3 5 20 0.50 0.46 0.39 o 4 5 20 0.91 0.51 0.33 o 0 6 20 17.10 17.34 0.64 o 1 6 20 12.41 12.37 0.45 o 2 6 20 9.62 9.52 0.42 o 3 6 20 4.86 4.69 0.42 o 0 7 20 1.79 1.37 0.49 o 1 7 20 1.11 1.62 0.29 o 2 7 20 5.24 4.71 0.44 o 1 0 21 46.72 42.15 1.06 o 2 0 21 21.81 19.65 0.77 o 3 0 21 7.05 9.11 0.61 o 4 0 21 0.01 -0.37 0.37 o 5 0 21 0.91 0.48 0.59 o 0 1 21 248.70 245.59 4.78 o 1 1 21 50.76 52.23 0.85 o 2 1 21 2.94 2.91 0.32 o 3 1 21 47.03 46.27 0.80 o 4 1 21 0.56 0.26 0.29 o 5 1 21 36.91 38.73 0.92 o 0 2 21 2.07 2.47 0.45 o 1 2 21 26.03 23.45 0.83 o 2 2 21 42.13 42.19 0.68 o 3 2 21 5.62 4.98 0.37 o 4 2 21 12.41 11.44 0.58 o 5 2 21 21.43 21.82 0.65 o 0 3 21 2.76 2.00 0.44 o 1 3 21 7.35 7.21 0.40 o 2 3 21 2.17 2.34 0.29 o 3 3 21 5.58 4.54 0.37 o 4 3 21 29.20 29.88 0.69 o 5 3 21 31.76 35.22 0.77 o 0 4 21 1.70 0.97 0.58 o 1 4 21 16.56 16.24 0.47 o 2 4 21 4.84 5.83 0.39 o 3 4 21 67.04 71.84 1.07 o 4 4 21 11.39 11.50 0.51 o 0 5 21 29.17 31.00 0.97 o 1 5 21 3.11 4.21 0.46 o 2 5 21 12.98 13.93 0.47 o 3 5 21 12.14 12.06 0.46 o 4 5 21 4.71 4.44 0.43 o 0 6 21 2.69 2.94 0.53 o 1 6 21 8.16 9.81 0.48 o 2 6 21 15.29 16.51 0.52 o 3 6 21 4.68 4.42 0.43 o 0 7 21 35.96 39.98 1.71 o 1 7 21 0.98 1.50 0.43 o 0 0 22 0.17 0.94 0.60 o 1 0 22 13.36 11.40 1.07 o 2 0 22 2.90 2.65 0.45 o 3 0 22 67.56 61.98 1.35 o 4 0 22 2.67 1.24 0.44 o 5 0 22 12.44 12.38 1.15 o 0 1 22 3.44 4.83 0.68 o 1 1 22 105.89 99.07 1.27 o 2 1 22 4.33 4.55 0.39 o 3 1 22 26.74 26.81 0.64 o 4 1 22 3.85 4.75 0.49 o 5 1 22 0.78 1.30 0.41 o 0 2 22 4.16 4.01 0.49 o 1 2 22 55.84 56.15 0.91 o 2 2 22 9.41 10.90 0.48 o 3 2 22 5.29 4.89 0.37 o 4 2 22 4.07 4.59 0.46 o 5 2 22 4.41 5.43 0.47 o 0 3 22 27.22 28.00 1.21 o 1 3 22 12.58 12.56 0.49 o 2 3 22 33.93 37.58 0.67 o 3 3 22 19.03 20.75 0.62 o 4 3 22 35.70 40.77 0.82 o 0 4 22 1.12 1.72 0.44 o 1 4 22 1.19 0.75 0.30 o 2 4 22 67.27 70.22 1.06 o 3 4 22 13.04 14.93 0.56 o 4 4 22 4.97 4.95 0.70 o 0 5 22 3.03 3.04 0.52 o 1 5 22 26.75 26.88 0.77 o 2 5 22 4.30 5.57 0.48 o 3 5 22 3.81 5.54 0.76 o 0 6 22 0.49 0.39 0.66 o 1 6 22 4.58 3.98 0.47 o 2 6 22 6.81 7.95 0.50 o 1 0 23 35.44 34.06 1.02 o 2 0 23 3.68 2.97 0.82 o 3 0 23 1.45 1.73 0.47 o 4 0 23 1.07 0.98 0.52 o 0 1 23 0.29 0.27 0.40 o 1 1 23 4.47 5.05 0.37 o 2 1 23 5.87 5.44 0.40 o 3 1 23 8.18 8.83 0.44 o 4 1 23 6.79 7.72 0.46 o 0 2 23 23.51 22.36 1.33 o 1 2 23 28.94 28.94 0.68 o 2 2 23 7.96 9.17 0.46 o 3 2 23 0.09 0.56 0.32 o 4 2 23 14.74 15.01 0.68 o 0 3 23 0.25 0.13 0.70 o 1 3 23 6.47 6.61 0.54 o 2 3 23 19.13 19.82 0.60 o 3 3 23 47.94 53.09 0.94 o 4 3 23 4.33 5.75 0.77 o 0 4 23 1.63 0.91 0.47 o 1 4 23 1.05 0.47 0.31 o 2 4 23 37.32 42.13 0.84 o 3 4 23 18.57 21.19 0.65 o 0 5 23 2.99 2.39 0.53 o 1 5 23 0.32 0.19 0.38 o 2 5 23 12.56 14.10 0.61 o 0 0 24 22.24 21.60 1.23 o 1 0 24 7.28 8.35 0.65 o 2 0 24 0.29 0.50 0.39 o 3 0 24 16.98 17.74 0.83 o 4 0 24 4.59 3.95 0.56 o 0 1 24 2.85 2.49 0.52 o 1 1 24 39.45 40.67 0.79 o 2 1 24 12.80 13.38 0.59 o 3 1 24 5.43 6.10 0.64 o 4 1 24 9.70 10.13 0.61 o 0 2 24 1.38 2.63 0.49 o 1 2 24 16.72 20.59 0.61 o 2 2 24 0.84 0.52 0.32 o 3 2 24 0.57 1.09 0.34 o 4 2 24 25.44 27.50 1.00 o 0 3 24 22.21 23.73 1.07 o 1 3 24 20.65 22.87 0.65 o 2 3 24 5.01 5.93 0.43 o 3 3 24 19.91 22.19 0.66 o 0 4 24 1.51 1.12 0.57 o 1 4 24 2.25 2.64 0.35 o 2 4 24 53.00 58.16 1.29 o 0 5 24 3.37 2.78 0.55 o 1 5 24 0.98 0.42 0.42 o 1 0 25 0.00 -0.15 0.46 o 2 0 25 8.81 10.36 0.70 o 3 0 25 16.61 15.78 0.82 o 0 1 25 11.08 11.75 0.83 o 1 1 25 46.75 47.79 0.89 o 2 1 25 10.55 11.34 0.53 o 3 1 25 2.28 1.94 0.60 o 0 2 25 45.73 45.81 1.25 o 1 2 25 40.14 42.24 0.93 o 2 2 25 1.77 1.73 0.36 o 3 2 25 2.87 4.49 0.42 o 0 3 25 1.11 1.20 0.47 o 1 3 25 28.02 30.75 0.75 o 2 3 25 1.80 1.90 0.38 o 0 4 25 0.92 0.14 0.46 o 1 4 25 6.55 7.29 0.48 o 0 0 26 9.64 11.43 1.11 o 1 0 26 2.05 2.89 0.54 o 2 0 26 0.94 2.17 0.55 o 0 1 26 37.53 42.54 1.23 o 1 1 26 1.81 2.40 0.40 o 2 1 26 10.57 12.49 0.56 o 0 2 26 5.71 6.54 0.64 o 1 2 26 34.31 38.75 1.17 o 2 2 26 8.29 6.86 0.48 o 0 3 26 15.49 16.42 0.90 o 1 3 26 6.42 7.57 0.49 o 1 0 27 7.33 8.80 0.74 o 0 1 27 29.10 32.68 1.12 o