#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:08:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/48/2204855.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204855_Fobs loop_ _publ_author_name 'Churakov, Andrei V.' 'Karlov, Sergey S.' 'Yakubova, Elmira Kh.' 'Selina, Anastasia A.' 'Zaitseva, Galina S.' _publ_section_title ; Tetrakis(phenylethynyl)germanium(IV) ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m52 _journal_page_last m54 _journal_volume 61 _journal_year 2005 _space_group_IT_number 82 _symmetry_space_group_name_Hall 'I -4' _symmetry_space_group_name_H-M 'I -4' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.5320 _cell_length_b 13.5320 _cell_length_c 6.7460 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.8418 _cod_data_source_file ci6492Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' r in I-4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 3818.86 3536.69 60.96 o 0 2 0 154.03 170.36 1.77 o 2 2 0 2265.83 2192.91 15.48 o 1 3 0 32.58 25.43 1.08 o 3 3 0 14.63 12.46 1.17 o -2 4 0 17695.59 16412.00 197.08 o 0 4 0 2800.10 2814.91 36.02 o 2 4 0 488.29 474.98 5.10 o 4 4 0 1196.84 1054.28 8.26 o -3 5 0 2313.96 2238.15 20.61 o -1 5 0 1358.82 1208.78 12.52 o 1 5 0 4926.97 4544.96 21.90 o 3 5 0 181.62 155.16 2.09 o 5 5 0 197.97 185.42 2.52 o -4 6 0 2211.86 1993.43 18.31 o -2 6 0 2937.52 2757.67 19.45 o 0 6 0 895.37 827.87 7.78 o 2 6 0 2150.58 1976.37 16.59 o 4 6 0 571.38 469.49 4.77 o 6 6 0 239.30 249.20 3.17 o -5 7 0 899.11 819.26 12.06 o -3 7 0 4972.90 4977.28 29.20 o -1 7 0 234.22 223.17 3.45 o 1 7 0 126.00 101.83 2.28 o 3 7 0 1147.11 1039.33 9.98 o 5 7 0 2241.79 2159.10 19.07 o 7 7 0 424.91 408.04 4.63 o -6 8 0 392.78 376.94 4.53 o -4 8 0 2179.15 2070.51 15.34 o -2 8 0 502.57 471.29 9.19 o 0 8 0 1876.85 1777.46 13.10 o 2 8 0 558.58 510.51 5.02 o 4 8 0 438.84 402.58 4.10 o 6 8 0 906.80 839.01 8.03 o 8 8 0 239.65 228.04 9.03 o -7 9 0 53.03 57.05 5.72 o -5 9 0 672.77 628.62 5.89 o -3 9 0 1170.55 1082.53 10.83 o -1 9 0 857.70 797.16 8.29 o 1 9 0 790.25 774.19 8.16 o 3 9 0 629.85 578.44 8.34 o 5 9 0 382.84 373.10 4.66 o 7 9 0 286.07 269.85 4.64 o 9 9 0 681.73 701.72 6.96 o -8 10 0 275.85 274.43 5.25 o -6 10 0 737.43 702.26 11.02 o -4 10 0 598.01 599.89 6.04 o -2 10 0 363.58 373.46 5.69 o 0 10 0 405.22 382.15 5.15 o 2 10 0 431.55 399.81 4.67 o 4 10 0 966.05 968.09 9.33 o 6 10 0 329.11 326.77 5.02 o 8 10 0 213.05 220.99 5.01 o 10 10 0 16.26 31.66 10.99 o -9 11 0 5.52 0.00 11.49 o -7 11 0 71.21 80.28 5.20 o -5 11 0 979.23 974.26 9.82 o -3 11 0 425.15 409.75 5.35 o -1 11 0 220.52 199.40 4.23 o 1 11 0 395.33 395.62 7.70 o 3 11 0 487.49 492.74 5.58 o 5 11 0 283.55 283.00 5.01 o 7 11 0 209.06 218.00 5.06 o 9 11 0 151.25 144.28 8.89 o 11 11 0 15.27 3.61 13.38 o -10 12 0 70.14 88.09 9.56 o -8 12 0 2.14 18.54 11.33 o -6 12 0 62.42 70.60 4.34 o -4 12 0 220.51 212.70 4.89 o -2 12 0 303.66 311.90 5.69 o 0 12 0 382.46 395.84 5.49 o 2 12 0 305.36 320.02 6.09 o 4 12 0 234.84 219.45 4.91 o 6 12 0 119.00 117.26 4.55 o 8 12 0 304.65 344.51 6.29 o 10 12 0 0.89 21.87 12.39 o -9 13 0 38.99 37.78 8.39 o -7 13 0 74.32 87.40 9.80 o -5 13 0 89.62 107.19 4.84 o -3 13 0 37.01 39.13 4.14 o -1 13 0 92.79 104.04 4.61 o 1 13 0 181.57 187.41 5.93 o 3 13 0 418.79 414.43 8.48 o 5 13 0 144.87 164.34 5.16 o 7 13 0 167.57 194.20 6.21 o 9 13 0 1.40 0.00 13.10 o -6 14 0 91.56 79.83 6.11 o -4 14 0 42.26 47.55 9.89 o -2 14 0 32.18 39.94 5.97 o 0 14 0 52.66 42.88 7.67 o 2 14 0 144.51 153.84 5.17 o 4 14 0 103.64 118.48 5.30 o 6 14 0 189.44 196.73 6.06 o -5 15 0 75.23 77.92 6.42 o -3 15 0 2.79 25.86 12.04 o -1 15 0 52.92 52.87 8.32 o 1 15 0 76.31 85.85 5.17 o 3 15 0 27.73 45.92 12.71 o 5 15 0 60.13 63.91 7.14 o 0 16 0 11.85 0.00 13.61 o 1 0 1 1902.89 2286.57 57.68 o 3 0 1 12835.77 13277.99 264.12 o 5 0 1 2125.14 2126.29 46.70 o 7 0 1 2409.84 2332.72 31.59 o 9 0 1 284.05 276.66 3.59 o 11 0 1 506.64 493.00 9.88 o 13 0 1 144.02 141.98 7.85 o 15 0 1 68.58 78.00 8.56 o -14 1 1 147.41 154.87 6.49 o -12 1 1 411.05 420.34 5.71 o -10 1 1 429.60 415.05 7.10 o -8 1 1 649.01 614.87 5.89 o -6 1 1 264.65 270.29 4.85 o -4 1 1 4035.26 4087.79 68.80 o -2 1 1 22108.08 21699.42 604.94 o 0 1 1 1843.60 2202.80 30.06 o 2 1 1 425.44 490.49 6.42 o 4 1 1 4187.89 4538.89 100.43 o 6 1 1 5723.77 5583.45 63.59 o 8 1 1 1964.55 1800.85 24.80 o 10 1 1 477.03 482.69 10.60 o 12 1 1 99.77 91.29 4.12 o 14 1 1 92.05 100.08 10.44 o -15 2 1 52.27 56.83 12.91 o -13 2 1 93.94 96.82 4.51 o -11 2 1 564.32 554.65 7.07 o -9 2 1 843.44 809.03 15.24 o -7 2 1 962.00 940.36 9.53 o -5 2 1 850.23 801.80 11.47 o -3 2 1 2961.14 2995.45 52.83 o -1 2 1 476.85 555.96 9.77 o 1 2 1 22084.74 21979.88 275.06 o 3 2 1 2877.49 2853.49 41.25 o 5 2 1 268.75 263.63 4.15 o 7 2 1 2483.39 2525.52 21.05 o 9 2 1 1173.29 1148.11 16.02 o 11 2 1 947.51 899.54 9.62 o 13 2 1 150.36 175.43 5.51 o 15 2 1 50.65 55.04 8.91 o -14 3 1 106.21 114.73 5.68 o -12 3 1 217.69 224.50 4.93 o -10 3 1 430.36 412.13 5.28 o -8 3 1 1719.66 1714.82 13.72 o -6 3 1 242.45 217.44 2.66 o -4 3 1 743.88 698.62 15.39 o -2 3 1 2912.91 2884.86 36.39 o 0 3 1 13084.49 13486.18 202.52 o 2 3 1 2847.56 2859.08 32.00 o 4 3 1 1445.79 1447.37 13.12 o 6 3 1 1838.17 1734.60 23.13 o 8 3 1 557.51 531.71 8.03 o 10 3 1 1171.34 1132.00 11.15 o 12 3 1 198.15 199.26 4.80 o 14 3 1 62.99 56.39 8.05 o -15 4 1 106.95 101.77 5.67 o -13 4 1 227.42 241.05 5.50 o -11 4 1 245.71 246.53 4.66 o -9 4 1 406.75 382.25 6.95 o -7 4 1 795.92 744.01 7.49 o -5 4 1 3075.95 2991.89 46.00 o -3 4 1 1490.75 1497.91 34.12 o -1 4 1 4399.15 4823.86 41.91 o 1 4 1 3949.94 3935.13 39.34 o 3 4 1 724.78 675.06 6.63 o 5 4 1 3149.55 3068.32 37.12 o 7 4 1 902.04 849.48 8.34 o 9 4 1 1086.31 1011.92 15.28 o 11 4 1 76.13 81.07 3.89 o 13 4 1 204.15 201.42 5.40 o 15 4 1 121.75 120.47 5.90 o -14 5 1 86.92 102.37 8.50 o -12 5 1 351.62 355.10 5.77 o -10 5 1 458.83 462.40 5.72 o -8 5 1 302.82 284.69 5.01 o -6 5 1 981.36 941.56 20.53 o -4 5 1 3118.20 3071.47 49.49 o -2 5 1 286.50 292.20 5.81 o 0 5 1 2126.59 2173.86 23.03 o 2 5 1 900.95 853.73 7.63 o 4 5 1 3114.73 2995.12 21.06 o 6 5 1 707.04 635.11 6.20 o 8 5 1 760.38 752.61 14.46 o 10 5 1 377.11 382.62 8.44 o 12 5 1 440.68 410.02 6.16 o 14 5 1 107.71 105.38 11.43 o -13 6 1 159.46 179.81 6.81 o -11 6 1 336.67 338.09 6.28 o -9 6 1 655.62 628.22 8.08 o -7 6 1 381.56 367.29 5.04 o -5 6 1 713.00 635.64 8.35 o -3 6 1 1847.89 1705.94 16.76 o -1 6 1 5738.72 5631.92 87.51 o 1 6 1 224.53 234.52 4.12 o 3 6 1 256.23 236.21 2.68 o 5 6 1 991.63 935.03 10.09 o 7 6 1 1099.71 1062.84 16.35 o 9 6 1 920.64 869.79 10.10 o 11 6 1 165.16 177.46 4.76 o 13 6 1 96.23 90.55 5.00 o -14 7 1 22.62 12.36 13.46 o -12 7 1 111.00 117.77 4.97 o -10 7 1 381.75 397.21 5.53 o -8 7 1 371.84 359.26 4.82 o -6 7 1 1081.03 1051.01 10.15 o -4 7 1 888.45 834.49 11.29 o -2 7 1 2586.09 2617.92 21.33 o 0 7 1 2331.04 2257.95 19.64 o 2 7 1 925.14 899.12 12.56 o 4 7 1 826.09 787.68 8.48 o 6 7 1 397.36 374.92 8.65 o 8 7 1 821.59 814.14 13.91 o 10 7 1 78.61 75.62 12.22 o 12 7 1 177.87 173.53 5.47 o 14 7 1 70.18 64.20 10.99 o -13 8 1 54.08 65.23 13.00 o -11 8 1 43.03 39.57 7.04 o -9 8 1 325.18 315.15 5.21 o -7 8 1 820.46 786.55 8.64 o -5 8 1 765.84 775.16 7.54 o -3 8 1 578.68 558.35 7.61 o -1 8 1 1907.20 1741.67 13.37 o 1 8 1 672.89 643.89 10.42 o 3 8 1 1722.12 1696.44 21.73 o 5 8 1 296.25 280.43 5.68 o 7 8 1 372.91 364.21 4.82 o 9 8 1 139.71 139.63 6.88 o 11 8 1 246.99 264.48 5.61 o 13 8 1 81.68 83.92 5.41 o -12 9 1 92.46 105.20 5.37 o -10 9 1 39.79 47.70 7.27 o -8 9 1 127.38 127.41 4.44 o -6 9 1 899.13 832.81 8.28 o -4 9 1 1117.38 1031.52 13.78 o -2 9 1 1170.48 1141.11 11.55 o 0 9 1 266.10 259.83 3.50 o 2 9 1 835.78 798.55 8.39 o 4 9 1 406.35 371.25 6.23 o 6 9 1 655.22 628.63 6.24 o 8 9 1 340.16 344.31 6.38 o 10 9 1 96.76 120.02 4.73 o 12 9 1 44.30 51.46 6.59 o -11 10 1 152.55 161.07 5.62 o -9 10 1 104.58 118.69 4.84 o -7 10 1 72.23 64.10 3.97 o -5 10 1 360.41 363.31 6.98 o -3 10 1 1184.22 1140.72 11.14 o -1 10 1 472.03 475.27 6.09 o 1 10 1 418.67 392.49 4.74 o 3 10 1 432.38 409.33 8.43 o 5 10 1 458.66 461.11 6.09 o 7 10 1 385.27 387.81 5.62 o 9 10 1 36.66 37.91 5.85 o 11 10 1 94.49 93.40 5.27 o -10 11 1 95.14 103.91 7.55 o -8 11 1 251.19 256.41 8.19 o -6 11 1 176.44 181.67 7.01 o -4 11 1 81.87 87.50 5.29 o -2 11 1 907.67 878.51 13.24 o 0 11 1 512.03 496.63 9.71 o 2 11 1 576.57 581.07 5.96 o 4 11 1 240.21 236.92 4.73 o 6 11 1 336.06 330.48 8.26 o 8 11 1 44.08 45.02 6.44 o 10 11 1 150.23 154.99 5.66 o -9 12 1 45.39 54.58 8.93 o -7 12 1 178.28 176.75 5.44 o -5 12 1 461.61 417.42 6.68 o -3 12 1 193.72 196.81 4.76 o -1 12 1 87.82 93.80 3.94 o 1 12 1 402.45 412.04 6.20 o 3 12 1 220.01 228.03 4.93 o 5 12 1 353.40 358.59 7.39 o 7 12 1 114.50 118.67 7.33 o 9 12 1 89.00 99.34 5.33 o -8 13 1 79.39 68.30 10.79 o -6 13 1 102.29 96.53 15.78 o -4 13 1 210.89 215.68 5.66 o -2 13 1 156.20 173.17 5.03 o 0 13 1 138.52 134.83 4.62 o 2 13 1 88.13 86.15 4.52 o 4 13 1 226.44 235.52 8.10 o 6 13 1 163.57 180.60 5.50 o 8 13 1 51.68 62.06 13.12 o -7 14 1 71.01 79.42 5.62 o -5 14 1 111.30 114.95 5.42 o -3 14 1 61.40 60.46 14.52 o -1 14 1 97.49 102.38 4.84 o 1 14 1 152.21 152.64 6.68 o 3 14 1 101.98 123.09 5.05 o 5 14 1 86.09 95.06 7.06 o 7 14 1 22.27 25.84 6.73 o -4 15 1 117.90 120.94 12.04 o -2 15 1 52.12 51.82 8.59 o 0 15 1 73.22 75.16 5.23 o 2 15 1 54.63 64.36 7.69 o 4 15 1 107.09 108.62 5.81 o 0 0 2 36.03 40.03 1.87 o 2 0 2 3702.20 4364.07 81.43 o 4 0 2 3332.48 3689.60 77.59 o 6 0 2 643.42 698.42 18.70 o 8 0 2 1254.78 1229.97 24.31 o 10 0 2 1502.67 1454.88 30.74 o 12 0 2 169.26 175.57 4.76 o 14 0 2 35.10 47.43 6.34 o -15 1 2 85.25 94.85 6.34 o -13 1 2 150.90 150.85 7.00 o -11 1 2 219.79 214.55 5.34 o -9 1 2 803.48 808.13 11.19 o -7 1 2 1615.84 1651.23 27.83 o -5 1 2 3259.15 3542.55 73.76 o -3 1 2 2993.94 3267.69 65.05 o -1 1 2 666.56 662.80 13.15 o 1 1 2 684.99 576.67 96.87 o 3 1 2 1435.17 1645.12 23.63 o 5 1 2 2192.09 2331.35 52.71 o 7 1 2 493.78 476.02 9.93 o 9 1 2 930.10 908.27 13.33 o 11 1 2 330.58 312.55 5.28 o 13 1 2 217.04 214.16 5.37 o 15 1 2 72.53 86.52 9.34 o -14 2 2 119.84 121.60 6.99 o -12 2 2 47.07 49.57 4.48 o -10 2 2 356.43 348.04 4.91 o -8 2 2 497.79 463.54 5.48 o -6 2 2 2640.21 2721.28 27.81 o -4 2 2 2583.23 2840.63 70.96 o -2 2 2 1988.72 2261.97 39.63 o 0 2 2 3654.87 4154.21 215.20 o 2 2 2 1903.15 1961.13 116.17 o 4 2 2 1228.35 1331.11 30.01 o 6 2 2 658.92 634.55 11.43 o 8 2 2 1110.68 1080.96 17.66 o 10 2 2 34.50 34.46 3.76 o 12 2 2 455.41 444.97 7.75 o 14 2 2 295.60 279.20 6.34 o -15 3 2 65.84 68.56 14.79 o -13 3 2 145.02 150.65 5.11 o -11 3 2 511.97 515.35 6.93 o -9 3 2 222.25 208.82 4.05 o -7 3 2 178.62 171.30 3.38 o -5 3 2 2633.82 2647.36 53.61 o -3 3 2 5518.96 6059.12 141.45 o -1 3 2 1503.74 1745.74 45.65 o 1 3 2 3035.25 3156.65 148.09 o 3 3 2 5445.76 5816.42 109.13 o 5 3 2 890.53 991.01 14.94 o 7 3 2 672.64 687.66 10.60 o 9 3 2 775.88 738.96 13.10 o 11 3 2 389.09 367.62 5.51 o 13 3 2 90.33 109.87 6.55 o 15 3 2 102.73 98.10 5.80 o -14 4 2 85.61 77.84 10.75 o -12 4 2 222.19 221.75 5.16 o -10 4 2 554.92 550.86 5.82 o -8 4 2 406.53 399.52 7.87 o -6 4 2 706.59 687.05 10.36 o -4 4 2 1468.17 1514.86 34.63 o -2 4 2 1221.19 1334.59 17.24 o 0 4 2 3395.18 3698.38 85.56 o 2 4 2 2586.44 2784.68 77.55 o 4 4 2 1445.76 1502.19 27.90 o 6 4 2 985.53 953.55 9.65 o 8 4 2 372.41 338.73 4.35 o 10 4 2 144.96 152.37 5.20 o 12 4 2 104.96 100.79 4.62 o 14 4 2 111.08 108.79 5.43 o -13 5 2 24.15 29.83 7.98 o -11 5 2 235.67 232.46 6.32 o -9 5 2 622.08 597.30 9.17 o -7 5 2 1315.22 1343.00 18.50 o -5 5 2 718.77 711.46 7.33 o -3 5 2 975.25 1056.41 13.47 o -1 5 2 2170.50 2304.79 34.02 o 1 5 2 3258.01 3498.86 52.28 o 3 5 2 2679.02 2726.47 53.64 o 5 5 2 705.72 699.76 7.04 o 7 5 2 1144.23 1106.79 17.31 o 9 5 2 56.38 54.27 8.37 o 11 5 2 166.96 180.62 5.52 o 13 5 2 172.38 181.15 8.38 o -14 6 2 25.71 15.65 8.71 o -12 6 2 126.75 135.36 7.50 o -10 6 2 151.33 159.99 4.47 o -8 6 2 351.32 331.94 4.68 o -6 6 2 1641.43 1570.98 19.20 o -4 6 2 994.82 955.89 23.29 o -2 6 2 675.47 651.43 14.30 o 0 6 2 694.45 762.72 8.59 o 2 6 2 2630.53 2761.99 44.57 o 4 6 2 685.20 655.33 6.88 o 6 6 2 1673.33 1602.26 15.22 o 8 6 2 294.59 293.56 6.44 o 10 6 2 401.14 377.84 5.62 o 12 6 2 95.94 95.84 5.32 o 14 6 2 32.47 56.61 6.79 o -13 7 2 90.09 91.31 12.99 o -11 7 2 113.64 113.41 5.40 o -9 7 2 81.09 81.64 3.99 o -7 7 2 686.76 638.23 7.26 o -5 7 2 1153.17 1116.47 22.47 o -3 7 2 653.69 663.08 7.38 o -1 7 2 503.40 498.86 7.11 o 1 7 2 1608.55 1657.82 12.95 o 3 7 2 167.95 158.19 2.98 o 5 7 2 1350.36 1366.10 19.95 o 7 7 2 704.07 669.10 9.85 o 9 7 2 361.64 360.50 5.35 o 11 7 2 98.86 103.30 4.76 o 13 7 2 92.18 85.27 5.38 o -12 8 2 79.63 77.21 6.25 o -10 8 2 174.71 181.93 6.44 o -8 8 2 259.27 263.35 4.83 o -6 8 2 284.65 279.38 4.52 o -4 8 2 370.79 331.51 4.33 o -2 8 2 1105.89 1060.48 12.83 o 0 8 2 1255.10 1241.85 12.14 o 2 8 2 487.44 457.13 4.98 o 4 8 2 404.63 408.93 4.81 o 6 8 2 358.71 336.24 6.32 o 8 8 2 271.31 278.65 5.28 o 10 8 2 271.19 260.49 6.08 o 12 8 2 194.31 195.28 6.03 o -11 9 2 95.14 94.28 5.22 o -9 9 2 132.18 128.10 4.84 o -7 9 2 369.98 361.35 5.42 o -5 9 2 58.70 60.97 7.22 o -3 9 2 742.90 719.59 9.95 o -1 9 2 935.85 926.42 12.72 o 1 9 2 797.84 814.44 8.09 o 3 9 2 215.41 202.99 4.50 o 5 9 2 626.36 601.93 6.26 o 7 9 2 85.52 86.62 4.14 o 9 9 2 132.42 133.49 4.87 o 11 9 2 210.74 227.28 6.02 o -10 10 2 59.76 70.87 10.08 o -8 10 2 267.60 248.98 5.48 o -6 10 2 416.90 397.68 5.66 o -4 10 2 152.12 162.21 4.22 o -2 10 2 31.62 38.55 3.74 o 0 10 2 1465.55 1418.28 20.74 o 2 10 2 346.69 339.83 4.86 o 4 10 2 573.95 582.15 7.49 o 6 10 2 155.77 167.28 4.50 o 8 10 2 167.30 172.45 6.10 o 10 10 2 60.07 68.06 6.32 o -11 11 2 61.92 51.36 6.34 o -9 11 2 206.78 217.11 6.02 o -7 11 2 100.85 112.31 4.79 o -5 11 2 168.18 166.93 4.75 o -3 11 2 406.09 372.70 5.52 o -1 11 2 333.35 307.99 5.03 o 1 11 2 197.47 190.44 4.49 o 3 11 2 503.86 504.62 6.26 o 5 11 2 238.88 240.04 6.35 o 7 11 2 117.27 123.14 4.94 o 9 11 2 93.48 88.86 13.94 o 11 11 2 60.32 57.23 8.58 o -8 12 2 197.21 200.34 5.95 o -6 12 2 95.95 94.93 4.89 o -4 12 2 101.04 99.38 4.68 o -2 12 2 464.96 456.41 6.20 o 0 12 2 172.59 183.51 4.80 o 2 12 2 45.51 50.83 5.48 o 4 12 2 214.26 209.92 5.59 o 6 12 2 126.38 128.54 5.10 o 8 12 2 78.89 78.84 7.58 o -7 13 2 95.75 71.27 6.25 o -5 13 2 171.42 181.03 5.62 o -3 13 2 92.76 111.57 5.71 o -1 13 2 210.41 205.08 5.40 o 1 13 2 156.75 151.99 5.06 o 3 13 2 150.74 157.14 5.71 o 5 13 2 23.03 31.59 11.77 o 7 13 2 84.83 93.38 6.22 o -6 14 2 33.69 16.68 14.00 o -4 14 2 114.70 110.96 11.66 o -2 14 2 291.70 273.26 6.37 o 0 14 2 33.08 50.18 6.31 o 2 14 2 123.75 120.82 7.31 o 4 14 2 90.03 92.02 12.41 o 6 14 2 24.89 1.27 13.52 o -3 15 2 104.12 103.29 8.80 o -1 15 2 69.95 86.58 8.32 o 1 15 2 85.44 90.54 14.59 o 3 15 2 67.44 76.08 13.98 o 1 0 3 1781.18 2110.81 58.24 o 3 0 3 2434.66 2910.01 55.17 o 5 0 3 1114.30 1187.09 24.88 o 7 0 3 534.18 529.31 12.96 o 9 0 3 555.42 534.35 7.71 o 11 0 3 299.33 288.87 5.32 o 13 0 3 146.87 150.08 5.40 o -14 1 3 156.49 171.18 6.05 o -12 1 3 223.74 215.61 5.39 o -10 1 3 251.12 251.02 5.96 o -8 1 3 422.53 419.96 7.33 o -6 1 3 2827.57 3073.81 39.97 o -4 1 3 958.00 1103.67 11.59 o -2 1 3 390.63 439.10 11.92 o 0 1 3 1837.30 2157.01 54.58 o 2 1 3 788.42 838.17 16.41 o 4 1 3 949.70 984.33 21.79 o 6 1 3 1045.54 1099.28 11.98 o 8 1 3 452.58 446.77 11.37 o 10 1 3 217.46 206.37 6.79 o 12 1 3 156.53 157.50 5.07 o 14 1 3 129.91 120.60 5.68 o -13 2 3 104.29 112.92 8.63 o -11 2 3 173.12 185.06 4.86 o -9 2 3 537.76 525.18 5.77 o -7 2 3 1861.64 1900.74 49.49 o -5 2 3 1299.53 1360.22 21.28 o -3 2 3 1626.77 1880.69 49.32 o -1 2 3 805.96 871.45 18.34 o 1 2 3 415.01 422.29 23.32 o 3 2 3 2141.48 2425.22 32.66 o 5 2 3 2230.32 2497.69 25.98 o 7 2 3 210.79 190.05 3.68 o 9 2 3 141.79 146.92 3.92 o 11 2 3 223.57 212.29 6.93 o 13 2 3 172.85 170.05 5.63 o -14 3 3 18.30 18.52 13.37 o -12 3 3 121.89 122.47 5.01 o -10 3 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