#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/49/2204970.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204970_Fobs loop_ _publ_author_name 'Pitchumony, Tamil Selvi' 'Stoeckli-Evans, Helen' _publ_section_title ; An orthorhombic polymorph of naphthalene-2,3-dicarbonitrile ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o40 _journal_page_last o41 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 3.8144 _cell_length_b 12.1750 _cell_length_c 18.8061 _exptl_crystal_F_000 368.00 _reflns_d_resolution_high 0.8087 _[local]_cod_data_source_file sj6037Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BPB1 IPDS2 -120DEGC' _shelx_refln_list_code 4 _shelx_f_calc_maximum 64.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 278.79 267.33 8.71 o 4 0 0 67.19 65.76 3.97 o 1 1 0 35.72 34.52 1.28 o 2 1 0 1.67 1.74 1.13 o 3 1 0 59.94 63.32 2.72 o 4 1 0 2.11 2.11 0.84 o 1 2 0 570.00 506.04 6.80 o 2 2 0 14.52 13.75 0.96 o 3 2 0 100.45 103.25 1.79 o 4 2 0 1.09 0.85 0.98 o 1 3 0 240.32 211.99 33.23 o 2 3 0 187.91 184.54 2.66 o 3 3 0 42.16 41.64 1.10 o 4 3 0 6.17 5.78 1.04 o 1 4 0 38.02 36.94 1.07 o 2 4 0 18.04 17.42 1.58 o 3 4 0 28.03 28.96 4.17 o 4 4 0 0.00 0.55 1.01 o 1 5 0 29.79 32.61 0.97 o 2 5 0 81.04 76.26 4.75 o 3 5 0 0.01 0.93 0.82 o 4 5 0 0.21 0.47 1.04 o 0 6 0 762.52 808.26 4.87 o 1 6 0 618.58 596.23 21.22 o 2 6 0 24.41 23.86 1.02 o 3 6 0 50.94 49.57 2.90 o 4 6 0 113.65 116.45 5.68 o 1 7 0 0.18 -0.35 0.98 o 2 7 0 50.86 51.52 0.92 o 3 7 0 2.06 3.06 0.89 o 4 7 0 0.68 1.59 1.24 o 0 8 0 35.91 42.11 1.11 o 1 8 0 11.51 15.05 0.77 o 2 8 0 35.71 36.38 1.34 o 3 8 0 0.07 0.98 0.81 o 1 9 0 15.25 18.54 1.43 o 2 9 0 25.80 27.88 0.88 o 3 9 0 7.43 7.24 0.85 o 0 10 0 14.65 12.81 1.17 o 1 10 0 7.63 9.74 0.84 o 2 10 0 3.62 4.28 0.89 o 3 10 0 1.78 1.34 0.86 o 1 11 0 46.17 40.06 3.88 o 2 11 0 0.22 -0.06 0.82 o 3 11 0 4.07 3.66 0.82 o 0 12 0 5.43 5.20 1.16 o 1 12 0 70.27 71.53 3.80 o 2 12 0 0.17 0.23 0.84 o 1 13 0 1.27 1.41 0.84 o 2 13 0 1.08 0.72 0.79 o 0 14 0 0.93 1.42 1.19 o 1 14 0 11.20 9.67 0.85 o 1 0 1 474.02 410.08 2.70 o 2 0 1 3.74 4.22 0.93 o 3 0 1 22.16 22.42 1.28 o 4 0 1 105.85 109.90 1.91 o 0 1 1 76.26 64.78 1.85 o 1 1 1 2480.75 2167.55 21.14 o 2 1 1 23.87 24.69 0.99 o 3 1 1 64.06 71.29 1.56 o 4 1 1 47.64 42.45 0.87 o 0 2 1 128.43 109.54 1.90 o 1 2 1 2046.03 1742.12 22.68 o 2 2 1 233.05 237.31 3.49 o 3 2 1 39.31 38.57 0.96 o 4 2 1 9.36 9.79 0.67 o 0 3 1 19.62 18.71 1.18 o 1 3 1 238.39 215.11 1.65 o 2 3 1 6.92 7.05 0.68 o 3 3 1 1.03 1.75 0.66 o 4 3 1 10.55 9.32 0.68 o 0 4 1 1035.56 872.82 7.38 o 1 4 1 47.27 41.70 0.91 o 2 4 1 90.55 90.98 1.69 o 3 4 1 29.17 32.68 1.98 o 4 4 1 58.01 51.29 4.31 o 0 5 1 439.31 419.15 5.50 o 1 5 1 756.37 717.13 10.33 o 2 5 1 21.08 20.54 0.66 o 3 5 1 30.36 31.34 1.69 o 4 5 1 112.48 103.98 13.75 o 0 6 1 40.43 50.46 1.15 o 1 6 1 233.10 218.48 9.35 o 2 6 1 45.86 51.40 0.76 o 3 6 1 92.85 96.62 2.30 o 4 6 1 83.58 76.33 4.74 o 0 7 1 501.47 529.33 3.13 o 1 7 1 12.16 13.07 0.57 o 2 7 1 21.23 22.27 0.63 o 3 7 1 29.34 33.57 1.04 o 4 7 1 44.46 38.86 3.10 o 0 8 1 0.77 -0.14 0.79 o 1 8 1 33.88 35.46 0.78 o 2 8 1 17.03 17.26 0.59 o 3 8 1 7.20 7.29 0.54 o 0 9 1 0.10 0.12 0.73 o 1 9 1 0.67 0.97 0.55 o 2 9 1 2.85 3.27 0.60 o 3 9 1 19.68 21.24 1.11 o 0 10 1 32.43 29.21 1.03 o 1 10 1 9.40 9.17 0.58 o 2 10 1 0.82 1.56 0.54 o 3 10 1 1.25 2.29 0.69 o 0 11 1 32.62 25.89 0.95 o 1 11 1 25.95 22.47 1.06 o 2 11 1 14.02 14.34 1.04 o 3 11 1 24.04 23.12 1.13 o 0 12 1 52.88 46.96 0.93 o 1 12 1 6.76 6.33 0.61 o 2 12 1 2.68 3.61 0.62 o 0 13 1 125.36 123.73 1.97 o 1 13 1 18.14 17.72 0.60 o 2 13 1 0.94 1.37 0.60 o 0 14 1 47.16 40.48 3.75 o 1 14 1 4.68 4.15 0.56 o 0 15 1 1.67 3.95 0.88 o 0 0 2 447.61 398.49 8.97 o 1 0 2 12.37 12.77 1.25 o 2 0 2 0.07 0.88 0.98 o 3 0 2 15.43 16.50 1.10 o 4 0 2 1.03 1.13 0.89 o 0 1 2 2886.90 2424.41 19.85 o 2 1 2 133.00 130.41 2.94 o 3 1 2 36.20 38.90 0.85 o 4 1 2 1.01 1.49 0.69 o 0 2 2 444.59 375.19 3.64 o 1 2 2 4160.57 3568.52 27.58 o 2 2 2 58.41 65.21 0.86 o 3 2 2 67.21 77.31 1.90 o 4 2 2 4.58 4.41 0.64 o 0 3 2 705.36 663.01 10.48 o 1 3 2 46.26 38.51 2.37 o 2 3 2 1.50 2.06 0.62 o 3 3 2 5.77 5.86 0.68 o 4 3 2 3.99 3.34 0.65 o 0 4 2 670.71 568.70 4.55 o 1 4 2 560.02 531.74 11.06 o 2 4 2 237.72 245.76 4.55 o 3 4 2 56.33 62.23 1.97 o 4 4 2 3.60 3.63 0.74 o 0 5 2 581.85 554.21 2.66 o 1 5 2 459.23 458.80 2.68 o 2 5 2 42.71 44.12 0.66 o 3 5 2 79.93 87.37 3.02 o 4 5 2 14.68 13.44 1.89 o 0 6 2 97.48 93.07 1.41 o 1 6 2 273.53 249.57 1.18 o 2 6 2 0.48 1.61 0.50 o 3 6 2 49.66 53.19 1.64 o 4 6 2 9.54 9.73 0.90 o 0 7 2 298.36 314.64 4.66 o 1 7 2 89.54 97.17 0.85 o 2 7 2 11.09 11.96 0.60 o 3 7 2 210.31 228.34 7.29 o 4 7 2 14.02 12.39 1.10 o 0 8 2 50.63 51.88 0.93 o 1 8 2 39.40 41.70 0.66 o 2 8 2 87.68 91.30 1.26 o 3 8 2 32.03 36.10 1.10 o 0 9 2 13.93 13.11 0.83 o 1 9 2 50.72 49.84 1.51 o 2 9 2 28.87 30.81 0.93 o 3 9 2 4.82 6.19 0.62 o 0 10 2 1.81 0.81 0.88 o 1 10 2 1.93 1.66 0.57 o 2 10 2 2.80 2.91 0.56 o 3 10 2 15.03 13.67 0.69 o 0 11 2 1.80 0.33 0.76 o 1 11 2 17.89 16.47 0.78 o 2 11 2 6.13 7.00 0.55 o 3 11 2 123.86 109.63 6.40 o 0 12 2 0.39 2.14 0.65 o 1 12 2 0.17 1.02 0.51 o 2 12 2 1.91 1.52 0.54 o 0 13 2 0.07 1.27 0.72 o 1 13 2 9.35 8.96 0.59 o 2 13 2 5.02 5.95 0.61 o 0 14 2 1.49 1.46 0.85 o 1 14 2 2.40 2.39 0.67 o 1 0 3 2470.34 2240.84 42.46 o 2 0 3 64.68 65.00 2.22 o 3 0 3 91.67 100.13 3.04 o 4 0 3 11.83 11.90 1.00 o 0 1 3 26.58 22.21 1.61 o 1 1 3 2031.14 1840.94 24.36 o 2 1 3 1492.70 1468.16 28.47 o 3 1 3 55.03 57.51 0.91 o 4 1 3 1.15 1.51 0.73 o 0 2 3 42.89 37.78 1.48 o 1 2 3 1450.91 1241.53 73.94 o 2 2 3 22.95 21.36 1.42 o 3 2 3 20.71 21.94 0.74 o 4 2 3 0.47 0.71 0.65 o 0 3 3 178.69 169.31 1.68 o 1 3 3 836.46 772.97 10.38 o 2 3 3 571.72 567.74 6.94 o 3 3 3 10.62 12.46 1.20 o 4 3 3 1.15 1.27 0.65 o 0 4 3 0.59 0.72 0.96 o 1 4 3 141.12 125.62 1.67 o 2 4 3 60.17 65.01 1.26 o 3 4 3 2.66 3.55 0.67 o 4 4 3 0.20 0.73 0.66 o 0 5 3 0.06 0.54 0.87 o 1 5 3 254.23 258.42 1.09 o 2 5 3 386.39 378.25 14.50 o 3 5 3 60.87 68.16 1.72 o 4 5 3 1.50 1.43 0.76 o 0 6 3 0.01 0.92 0.96 o 1 6 3 201.17 209.46 1.62 o 2 6 3 218.05 240.01 4.56 o 3 6 3 88.16 98.54 3.92 o 4 6 3 6.51 6.24 0.92 o 0 7 3 187.92 184.27 2.12 o 1 7 3 63.57 66.47 0.85 o 2 7 3 80.53 86.74 1.68 o 3 7 3 179.36 195.31 6.54 o 4 7 3 1.01 0.24 0.76 o 0 8 3 0.86 1.71 0.97 o 1 8 3 116.06 122.12 2.47 o 2 8 3 134.43 139.10 3.53 o 3 8 3 23.64 26.79 1.18 o 0 9 3 32.76 31.10 0.78 o 1 9 3 6.26 8.25 0.56 o 2 9 3 36.34 37.13 0.65 o 3 9 3 11.05 10.12 0.68 o 0 10 3 3.23 5.00 1.17 o 1 10 3 4.07 3.07 0.60 o 2 10 3 76.47 85.15 1.42 o 3 10 3 15.38 17.21 0.86 o 0 11 3 0.12 1.34 0.89 o 1 11 3 26.35 23.56 0.55 o 2 11 3 3.71 4.24 0.61 o 3 11 3 88.74 85.37 4.09 o 0 12 3 0.68 0.32 1.03 o 1 12 3 31.64 31.28 0.63 o 2 12 3 48.04 45.49 1.81 o 0 13 3 26.49 30.79 0.95 o 1 13 3 32.32 31.35 0.71 o 2 13 3 17.43 18.68 1.12 o 0 14 3 0.13 0.47 0.84 o 1 14 3 5.06 3.81 0.76 o 0 0 4 1569.00 1304.16 24.19 o 1 0 4 34.85 37.12 2.52 o 2 0 4 446.95 473.45 11.12 o 3 0 4 35.29 40.64 1.24 o 4 0 4 0.30 1.34 0.97 o 0 1 4 154.78 137.52 3.34 o 1 1 4 91.17 79.93 1.86 o 2 1 4 887.21 883.44 62.37 o 3 1 4 50.12 50.38 1.05 o 4 1 4 2.25 2.40 0.68 o 0 2 4 844.93 737.84 10.49 o 1 2 4 250.55 226.31 4.44 o 2 2 4 261.00 262.75 5.01 o 3 2 4 43.47 47.62 2.82 o 4 2 4 0.09 0.23 0.71 o 0 3 4 2701.63 2849.34 387.42 o 1 3 4 63.64 55.64 0.96 o 2 3 4 1679.67 1713.16 21.44 o 3 3 4 60.48 62.22 1.36 o 4 3 4 13.60 13.49 0.81 o 0 4 4 86.90 84.20 1.32 o 1 4 4 18.85 19.25 0.78 o 2 4 4 7.32 8.31 0.61 o 3 4 4 15.49 15.51 0.68 o 4 4 4 1.16 1.10 0.63 o 0 5 4 6.64 7.61 1.01 o 1 5 4 46.98 46.15 1.14 o 2 5 4 85.85 102.36 2.76 o 3 5 4 42.58 46.66 0.98 o 4 5 4 1.79 1.79 0.73 o 0 6 4 272.97 268.13 4.55 o 1 6 4 197.87 208.70 2.22 o 2 6 4 37.68 39.78 0.71 o 3 6 4 53.54 57.76 2.28 o 4 6 4 6.94 4.67 0.81 o 0 7 4 309.19 299.35 3.49 o 1 7 4 43.31 46.55 0.72 o 2 7 4 205.63 215.89 2.80 o 3 7 4 12.36 14.14 1.22 o 4 7 4 3.40 1.79 0.75 o 0 8 4 4.80 5.35 0.75 o 1 8 4 6.59 6.35 0.60 o 2 8 4 28.88 28.73 0.90 o 3 8 4 28.78 30.46 1.92 o 0 9 4 2.55 2.07 0.98 o 1 9 4 1.66 2.40 0.62 o 2 9 4 196.72 220.07 5.11 o 3 9 4 6.76 7.69 0.58 o 0 10 4 1.09 1.75 0.75 o 1 10 4 0.07 1.20 0.57 o 2 10 4 126.31 132.61 4.36 o 3 10 4 3.32 2.94 0.56 o 0 11 4 0.49 0.07 1.13 o 1 11 4 33.92 33.34 0.64 o 2 11 4 17.20 21.53 0.64 o 3 11 4 15.86 13.45 0.70 o 0 12 4 0.61 0.08 0.98 o 1 12 4 13.96 14.39 0.74 o 2 12 4 120.35 124.78 6.25 o 0 13 4 0.01 0.73 1.19 o 1 13 4 1.48 1.84 0.52 o 2 13 4 10.13 11.15 0.66 o 0 14 4 1.74 1.58 0.78 o 1 14 4 9.25 8.11 0.63 o 1 0 5 21.82 24.56 1.53 o 2 0 5 174.57 195.64 12.84 o 3 0 5 1.81 1.61 1.10 o 4 0 5 12.01 9.96 2.09 o 0 1 5 27.69 25.86 1.26 o 1 1 5 115.68 105.82 1.31 o 2 1 5 244.72 249.77 5.75 o 3 1 5 26.26 26.90 1.86 o 4 1 5 7.18 7.07 0.75 o 0 2 5 9.07 8.11 1.03 o 1 2 5 161.20 149.10 9.26 o 2 2 5 544.46 556.71 8.82 o 3 2 5 176.20 181.46 2.14 o 4 2 5 1.58 1.48 0.86 o 0 3 5 111.47 102.31 2.32 o 1 3 5 757.62 719.03 6.50 o 2 3 5 87.74 87.29 1.22 o 3 3 5 80.09 88.13 2.21 o 4 3 5 5.97 6.21 0.91 o 0 4 5 40.83 41.38 1.29 o 1 4 5 210.57 209.51 3.37 o 2 4 5 149.86 148.56 2.82 o 3 4 5 103.23 109.68 3.38 o 4 4 5 1.26 1.03 0.82 o 0 5 5 19.92 19.50 1.08 o 1 5 5 148.20 150.19 1.22 o 2 5 5 204.19 213.56 4.34 o 3 5 5 37.05 41.60 1.31 o 4 5 5 4.20 4.07 0.71 o 0 6 5 71.81 70.77 1.45 o 1 6 5 28.13 26.88 0.69 o 2 6 5 232.05 245.95 3.64 o 3 6 5 7.15 8.50 0.69 o 4 6 5 4.01 2.88 0.90 o 0 7 5 111.62 118.54 2.05 o 1 7 5 272.78 268.89 2.35 o 2 7 5 168.56 176.63 9.60 o 3 7 5 31.20 31.41 3.08 o 4 7 5 1.22 0.78 0.81 o 0 8 5 4.71 5.16 0.89 o 1 8 5 173.50 179.22 2.10 o 2 8 5 133.72 128.45 2.46 o 3 8 5 17.17 18.15 0.82 o 0 9 5 0.42 0.99 0.97 o 1 9 5 110.10 111.71 2.21 o 2 9 5 284.88 297.62 8.43 o 3 9 5 20.88 19.57 0.71 o 0 10 5 49.00 54.92 2.20 o 1 10 5 94.63 100.80 1.60 o 2 10 5 62.34 73.90 2.18 o 3 10 5 15.83 14.32 0.98 o 0 11 5 1.54 2.17 0.88 o 1 11 5 16.77 19.21 1.01 o 2 11 5 70.36 72.33 2.15 o 3 11 5 2.01 1.77 0.69 o 0 12 5 29.94 32.27 1.11 o 1 12 5 2.67 2.81 0.53 o 2 12 5 35.88 38.90 1.51 o 0 13 5 6.72 7.23 1.02 o 1 13 5 3.45 3.81 0.51 o 2 13 5 11.71 11.84 0.69 o 0 14 5 3.13 3.46 0.88 o 1 14 5 21.81 23.39 1.30 o 0 0 6 1409.69 1290.77 20.55 o 1 0 6 29.27 27.92 10.17 o 2 0 6 62.40 62.11 1.43 o 3 0 6 0.04 0.76 1.38 o 4 0 6 15.67 17.14 2.44 o 0 1 6 453.81 389.36 4.10 o 1 1 6 250.09 232.24 3.29 o 2 1 6 89.48 88.31 4.05 o 3 1 6 22.23 23.35 0.76 o 4 1 6 1.54 2.12 0.75 o 0 2 6 626.54 567.76 4.05 o 1 2 6 725.85 684.11 10.82 o 2 2 6 174.73 187.56 3.43 o 3 2 6 393.95 415.36 4.56 o 4 2 6 9.25 9.53 0.72 o 0 3 6 45.08 43.37 1.25 o 1 3 6 196.71 190.79 3.25 o 2 3 6 1.10 1.29 0.61 o 3 3 6 112.87 124.43 3.21 o 4 3 6 0.43 0.39 0.69 o 0 4 6 688.16 822.26 130.56 o 1 4 6 983.24 970.61 39.97 o 2 4 6 170.55 183.68 2.45 o 3 4 6 154.17 174.89 7.43 o 4 4 6 22.72 21.35 0.85 o 0 5 6 117.39 113.96 1.26 o 1 5 6 219.80 203.31 8.76 o 2 5 6 82.53 88.38 2.02 o 3 5 6 19.95 21.46 0.83 o 4 5 6 2.22 1.68 0.75 o 0 6 6 206.69 196.92 3.22 o 1 6 6 41.30 40.95 0.70 o 2 6 6 7.54 7.32 0.56 o 3 6 6 3.15 3.00 0.57 o 4 6 6 1.23 1.73 0.79 o 0 7 6 12.61 16.31 1.11 o 1 7 6 52.19 51.72 0.92 o 2 7 6 14.84 16.34 0.62 o 3 7 6 7.37 7.08 0.84 o 0 8 6 28.53 29.19 0.82 o 1 8 6 591.86 607.24 7.76 o 2 8 6 202.87 218.83 7.94 o 3 8 6 30.40 32.09 1.04 o 0 9 6 1.92 3.26 0.90 o 1 9 6 20.06 19.32 0.57 o 2 9 6 2.95 3.03 0.65 o 3 9 6 32.22 31.51 2.29 o 0 10 6 2.06 3.22 0.82 o 1 10 6 351.32 370.28 6.09 o 2 10 6 19.15 20.90 0.80 o 3 10 6 2.43 2.52 0.64 o 0 11 6 0.61 0.78 0.86 o 1 11 6 38.99 40.21 0.87 o 2 11 6 27.82 28.56 1.07 o 0 12 6 0.03 0.24 0.88 o 1 12 6 9.79 10.37 0.63 o 2 12 6 19.47 18.52 1.02 o 0 13 6 4.47 3.71 0.91 o 1 13 6 0.11 0.09 0.59 o 2 13 6 9.43 9.06 1.15 o 0 14 6 0.16 -0.53 0.74 o 1 14 6 52.01 49.04 2.33 o 1 0 7 21.77 23.21 1.81 o 2 0 7 0.90 0.50 1.13 o 3 0 7 0.00 1.62 0.86 o 4 0 7 28.20 27.37 3.53 o 0 1 7 297.47 266.13 1.82 o 1 1 7 144.48 144.55 1.81 o 2 1 7 8.18 8.05 1.04 o 3 1 7 63.53 68.63 3.17 o 4 1 7 21.86 22.02 1.34 o 0 2 7 0.07 -0.50 1.23 o 1 2 7 62.41 67.78 1.51 o 2 2 7 139.15 145.16 1.82 o 3 2 7 55.76 60.00 0.98 o 4 2 7 36.14 35.42 3.28 o 0 3 7 150.00 149.87 1.42 o 1 3 7 187.24 191.23 2.82 o 2 3 7 15.20 15.90 2.02 o 3 3 7 240.94 256.90 11.95 o 4 3 7 76.25 63.54 2.58 o 0 4 7 336.86 326.26 1.87 o 1 4 7 58.28 65.06 0.83 o 2 4 7 43.40 44.00 0.88 o 3 4 7 31.33 32.12 1.24 o 4 4 7 39.48 33.15 1.39 o 0 5 7 0.83 0.56 0.89 o 1 5 7 1.32 1.03 0.57 o 2 5 7 16.30 15.39 0.63 o 3 5 7 26.23 28.22 1.21 o 4 5 7 15.31 13.17 1.62 o 0 6 7 49.09 42.86 1.14 o 1 6 7 98.58 96.99 0.88 o 2 6 7 27.91 27.91 0.66 o 3 6 7 5.89 6.14 0.71 o 4 6 7 6.45 4.84 0.80 o 0 7 7 115.84 116.33 1.72 o 1 7 7 60.60 58.37 1.37 o 2 7 7 4.64 4.83 0.57 o 3 7 7 27.69 28.83 1.32 o 0 8 7 179.29 182.70 2.20 o 1 8 7 218.77 219.77 4.17 o 2 8 7 5.17 4.96 0.58 o 3 8 7 8.17 7.47 0.70 o 0 9 7 591.82 610.02 10.00 o 1 9 7 197.32 204.51 3.40 o 2 9 7 5.66 7.16 0.85 o 3 9 7 0.76 1.90 0.59 o 0 10 7 110.65 114.88 2.78 o 1 10 7 303.36 315.05 6.27 o 2 10 7 1.69 1.78 0.60 o 3 10 7 25.20 23.18 1.48 o 0 11 7 73.06 83.03 2.78 o 1 11 7 42.19 43.18 1.77 o 2 11 7 1.22 1.15 0.54 o 0 12 7 45.94 48.28 1.59 o 1 12 7 14.63 15.21 0.62 o 2 12 7 0.17 0.73 0.61 o 0 13 7 85.09 85.07 2.65 o 1 13 7 20.07 20.05 1.43 o 0 14 7 12.06 13.97 0.85 o 0 0 8 296.26 273.02 3.81 o 1 0 8 3.85 3.07 1.20 o 2 0 8 1.75 2.67 2.41 o 3 0 8 2.76 2.65 1.37 o 4 0 8 40.42 33.24 2.95 o 0 1 8 337.19 352.19 3.23 o 1 1 8 8.00 8.51 0.80 o 2 1 8 73.31 74.04 1.16 o 3 1 8 13.30 14.00 0.92 o 4 1 8 2.09 2.32 0.85 o 0 2 8 125.77 126.80 1.53 o 1 2 8 263.13 240.84 3.82 o 2 2 8 14.36 14.34 0.70 o 3 2 8 6.12 6.76 0.75 o 4 2 8 21.07 21.42 0.93 o 0 3 8 1834.77 1913.07 25.28 o 1 3 8 57.31 55.87 1.08 o 2 3 8 28.16 32.92 0.92 o 3 3 8 39.74 41.85 1.56 o 4 3 8 47.74 48.37 5.41 o 0 4 8 48.18 48.87 1.01 o 1 4 8 22.29 22.26 0.69 o 2 4 8 30.80 32.53 1.12 o 3 4 8 22.04 22.19 1.45 o 4 4 8 94.54 76.75 5.41 o 0 5 8 882.28 893.75 10.64 o 1 5 8 58.69 61.70 1.21 o 2 5 8 25.05 23.09 1.41 o 3 5 8 9.29 9.50 0.72 o 4 5 8 44.91 35.39 2.65 o 0 6 8 370.00 368.71 6.22 o 1 6 8 192.79 187.08 2.06 o 2 6 8 7.20 8.41 0.83 o 3 6 8 8.06 9.63 0.65 o 4 6 8 5.51 2.66 1.87 o 0 7 8 355.34 341.00 6.27 o 1 7 8 73.68 68.95 1.21 o 2 7 8 23.08 22.11 2.77 o 3 7 8 8.54 8.84 0.69 o 0 8 8 75.12 75.84 0.95 o 1 8 8 13.74 14.43 0.57 o 2 8 8 10.29 10.79 1.02 o 3 8 8 18.10 17.38 1.58 o 0 9 8 723.52 744.71 23.15 o 1 9 8 183.22 189.63 3.84 o 2 9 8 16.38 18.58 1.50 o 3 9 8 0.21 0.62 0.61 o 0 10 8 85.46 88.96 1.87 o 1 10 8 13.82 14.97 0.71 o 2 10 8 2.43 2.75 0.63 o 3 10 8 4.20 4.22 0.65 o 0 11 8 3.54 3.00 0.76 o 1 11 8 37.81 38.10 1.50 o 2 11 8 10.67 8.01 1.14 o 0 12 8 84.99 90.68 5.42 o 1 12 8 14.23 15.21 0.66 o 2 12 8 5.16 4.64 0.62 o 0 13 8 0.02 -0.08 0.78 o 1 13 8 5.13 4.50 0.59 o 0 14 8 0.36 0.55 1.05 o 1 0 9 27.78 25.80 1.17 o 2 0 9 5.99 5.78 1.39 o 3 0 9 1.14 0.28 1.09 o 4 0 9 11.72 9.11 1.26 o 0 1 9 7.50 7.43 1.26 o 1 1 9 93.92 100.30 2.22 o 2 1 9 52.50 51.47 0.83 o 3 1 9 9.83 9.72 0.82 o 4 1 9 48.26 41.50 2.55 o 0 2 9 71.77 80.71 1.37 o 1 2 9 214.87 208.89 3.53 o 2 2 9 23.94 24.07 0.77 o 3 2 9 33.31 34.21 1.20 o 4 2 9 74.32 70.15 1.44 o 0 3 9 15.65 17.55 0.91 o 1 3 9 242.70 236.26 3.78 o 2 3 9 7.45 8.26 0.77 o 3 3 9 18.55 21.32 0.85 o 4 3 9 100.92 104.05 7.49 o 0 4 9 179.54 175.33 3.17 o 1 4 9 281.15 292.39 3.32 o 2 4 9 8.93 8.93 0.66 o 3 4 9 25.95 28.11 1.25 o 4 4 9 71.45 66.34 3.41 o 0 5 9 330.26 311.90 6.63 o 1 5 9 91.98 97.15 1.36 o 2 5 9 27.40 27.02 1.70 o 3 5 9 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7 11 15.74 16.31 0.94 o 1 7 11 303.87 308.02 7.40 o 2 7 11 54.17 52.27 2.56 o 3 7 11 11.56 10.88 0.77 o 0 8 11 26.13 25.91 1.25 o 1 8 11 85.32 90.04 2.63 o 2 8 11 13.41 12.67 1.55 o 3 8 11 5.61 4.86 0.64 o 0 9 11 23.35 23.36 1.33 o 1 9 11 67.16 73.10 2.52 o 2 9 11 2.23 2.51 0.52 o 3 9 11 1.42 1.52 0.63 o 0 10 11 0.18 0.34 0.80 o 1 10 11 82.15 86.30 2.23 o 2 10 11 37.30 33.69 1.51 o 0 11 11 0.32 0.62 0.98 o 1 11 11 88.58 87.78 2.97 o 2 11 11 18.36 18.32 1.49 o 0 12 11 1.26 1.16 0.78 o 1 12 11 36.04 33.30 2.02 o 0 13 11 10.75 9.24 1.56 o 0 0 12 6.61 8.14 1.39 o 1 0 12 16.52 17.04 0.93 o 2 0 12 368.49 375.02 2.23 o 3 0 12 15.99 17.21 1.24 o 4 0 12 0.43 0.60 0.95 o 0 1 12 18.54 18.00 0.98 o 1 1 12 15.26 17.48 0.72 o 2 1 12 166.48 175.60 3.58 o 3 1 12 36.43 37.05 1.75 o 4 1 12 2.26 1.44 0.87 o 0 2 12 89.67 83.24 2.03 o 1 2 12 26.25 29.91 0.93 o 2 2 12 124.10 131.56 3.46 o 3 2 12 31.46 33.83 1.33 o 0 3 12 0.03 -0.09 0.85 o 1 3 12 75.38 81.92 1.26 o 2 3 12 131.96 136.08 5.01 o 3 3 12 74.58 78.35 1.60 o 0 4 12 0.12 0.79 0.79 o 1 4 12 4.18 5.66 0.71 o 2 4 12 21.89 20.78 1.58 o 3 4 12 9.89 12.07 1.00 o 0 5 12 3.96 5.82 0.83 o 1 5 12 63.76 63.72 1.53 o 2 5 12 6.36 6.66 0.67 o 3 5 12 1.57 1.39 0.72 o 0 6 12 24.32 22.99 1.09 o 1 6 12 110.27 112.79 3.83 o 2 6 12 70.06 82.79 2.47 o 3 6 12 31.51 28.66 2.16 o 0 7 12 7.34 8.97 0.88 o 1 7 12 14.31 14.01 0.71 o 2 7 12 109.18 116.65 5.09 o 3 7 12 2.65 2.66 0.80 o 0 8 12 14.75 15.39 0.86 o 1 8 12 16.77 16.24 0.78 o 2 8 12 53.05 58.54 3.40 o 3 8 12 12.07 11.07 1.74 o 0 9 12 5.96 6.02 0.92 o 1 9 12 63.23 64.32 2.29 o 2 9 12 10.98 8.58 0.66 o 0 10 12 3.57 4.43 1.18 o 1 10 12 27.20 26.68 0.91 o 2 10 12 54.56 54.18 3.34 o 0 11 12 14.14 13.97 1.44 o 1 11 12 18.22 16.57 0.79 o 2 11 12 24.12 21.28 1.63 o 0 12 12 9.25 8.80 0.82 o 1 12 12 18.80 16.51 0.65 o 1 0 13 76.77 76.77 1.04 o 2 0 13 106.59 101.24 1.40 o 3 0 13 55.50 52.46 3.22 o 0 1 13 69.21 64.54 1.45 o 1 1 13 49.48 51.91 1.44 o 2 1 13 244.66 248.69 4.77 o 3 1 13 7.86 8.26 0.91 o 0 2 13 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