#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:08:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180969 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/49/2204971.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204971_Fobs loop_ _publ_author_name 'Zhang, Zhu-Yan' 'Gao, Shan' 'Huo, Li-Hua' 'Zhao, Hui' 'Zhao, Jing-Gui' _publ_section_title ; Hexaaquamanganese(II) bis[(4-oxo-4H-pyridin-1-yl)acetate] dihydrate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m85 _journal_page_last m86 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.684 _cell_angle_gamma 90.000 _cell_length_a 12.5609 _cell_length_b 12.9491 _cell_length_c 6.8547 _exptl_crystal_F_000 526.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file sj6038Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zz in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1791.29 1699.53 19.83 o 3 0 0 1631.47 1686.95 39.92 o 4 0 0 11886.34 12410.68 53.65 o 5 0 0 10650.76 10940.17 152.70 o 6 0 0 43.94 74.27 2.40 o 7 0 0 4543.99 5017.98 102.54 o 8 0 0 1096.28 1098.06 28.59 o 9 0 0 710.26 715.35 11.09 o 10 0 0 689.78 686.49 5.48 o 11 0 0 1637.74 1443.56 31.50 o 12 0 0 7.94 12.42 1.33 o 13 0 0 91.95 106.27 11.85 o 14 0 0 2.66 6.19 2.09 o 15 0 0 37.68 31.06 3.61 o 16 0 0 38.15 42.03 7.64 o 2 1 0 321.07 333.92 4.55 o 3 1 0 1.56 2.47 0.20 o 4 1 0 15.82 11.89 0.21 o 5 1 0 59.89 67.73 0.71 o 6 1 0 202.70 172.99 1.67 o 7 1 0 1711.15 1849.24 10.70 o 8 1 0 68.23 78.73 1.29 o 9 1 0 8.41 4.78 0.41 o 10 1 0 44.18 38.56 0.91 o 11 1 0 114.69 106.73 3.73 o 12 1 0 117.66 116.67 1.58 o 13 1 0 11.28 10.59 1.02 o 14 1 0 58.35 69.57 3.65 o 15 1 0 40.61 44.68 5.52 o 16 1 0 0.12 -1.11 2.10 o 0 2 0 497.09 392.75 1.05 o 1 2 0 1062.06 1009.86 7.32 o 2 2 0 5346.22 5707.34 48.62 o 3 2 0 1866.76 1940.70 28.60 o 4 2 0 355.46 363.66 2.93 o 5 2 0 2651.63 2811.74 47.27 o 6 2 0 3933.57 4276.48 51.48 o 7 2 0 1536.32 1497.71 21.98 o 8 2 0 23.02 20.40 1.15 o 9 2 0 1.23 8.98 2.59 o 10 2 0 59.08 66.46 1.79 o 11 2 0 238.61 246.36 3.20 o 12 2 0 270.49 271.38 7.31 o 13 2 0 232.30 221.45 6.53 o 14 2 0 50.15 51.81 3.79 o 15 2 0 9.31 10.63 3.75 o 16 2 0 53.19 64.28 5.73 o 1 3 0 700.69 746.50 5.56 o 2 3 0 548.29 498.02 4.15 o 3 3 0 15.09 14.03 0.42 o 4 3 0 1301.31 1323.73 10.80 o 5 3 0 874.63 948.08 4.56 o 6 3 0 38.62 45.35 0.76 o 7 3 0 55.80 63.75 1.08 o 8 3 0 9.08 7.46 0.41 o 9 3 0 22.87 19.64 0.61 o 10 3 0 77.00 80.79 1.81 o 11 3 0 325.90 325.79 3.20 o 12 3 0 20.26 18.86 1.38 o 13 3 0 3.59 1.84 0.74 o 14 3 0 0.37 0.41 1.09 o 15 3 0 11.02 10.69 3.04 o 0 4 0 8599.27 9223.64 202.31 o 1 4 0 13507.25 14103.09 114.66 o 2 4 0 695.37 651.09 4.72 o 3 4 0 293.37 321.84 2.54 o 4 4 0 98.32 83.47 0.94 o 5 4 0 60.29 47.19 0.69 o 6 4 0 2678.05 2800.24 14.62 o 7 4 0 63.22 70.81 0.89 o 8 4 0 292.71 302.08 3.67 o 9 4 0 210.84 199.97 4.31 o 10 4 0 202.26 201.41 2.15 o 11 4 0 57.51 57.55 3.75 o 12 4 0 677.12 660.93 8.63 o 13 4 0 3.40 4.97 1.24 o 14 4 0 33.33 33.90 4.01 o 15 4 0 36.76 47.86 2.62 o 1 5 0 2115.23 2165.93 6.14 o 2 5 0 93.78 97.03 0.86 o 3 5 0 995.01 966.88 3.06 o 4 5 0 324.76 316.02 1.86 o 5 5 0 68.35 62.14 0.72 o 6 5 0 17.91 21.70 0.65 o 7 5 0 15.89 17.13 0.71 o 8 5 0 19.43 18.65 0.67 o 9 5 0 0.35 0.04 0.52 o 10 5 0 45.04 42.60 1.32 o 11 5 0 19.73 17.98 1.07 o 12 5 0 4.58 3.04 0.94 o 13 5 0 0.61 1.96 1.22 o 14 5 0 4.11 6.72 1.28 o 15 5 0 1.00 2.25 2.42 o 0 6 0 1343.32 1353.78 37.43 o 1 6 0 3288.80 3294.25 25.37 o 2 6 0 362.70 328.68 2.77 o 3 6 0 35.89 25.43 3.73 o 4 6 0 778.94 737.17 10.48 o 5 6 0 1392.37 1387.98 14.95 o 6 6 0 1550.54 1536.52 8.03 o 7 6 0 204.72 202.09 1.63 o 8 6 0 295.86 300.79 3.80 o 9 6 0 604.28 614.18 3.81 o 10 6 0 541.42 515.97 8.91 o 11 6 0 213.94 216.15 5.14 o 12 6 0 293.31 311.39 5.91 o 13 6 0 148.72 159.15 4.55 o 14 6 0 83.60 87.77 2.07 o 15 6 0 40.82 43.55 2.88 o 1 7 0 35.68 34.17 0.78 o 2 7 0 236.02 240.24 2.07 o 3 7 0 48.86 55.17 3.18 o 4 7 0 44.51 35.41 0.80 o 5 7 0 118.98 123.26 1.08 o 6 7 0 276.07 265.21 1.84 o 7 7 0 53.08 54.95 0.93 o 8 7 0 14.49 15.17 0.67 o 9 7 0 70.47 67.75 1.30 o 10 7 0 33.58 34.72 1.06 o 11 7 0 10.15 8.02 0.71 o 12 7 0 0.04 1.03 0.78 o 13 7 0 8.00 6.92 1.27 o 14 7 0 0.99 5.48 1.80 o 0 8 0 3225.74 3186.22 6.74 o 1 8 0 376.12 404.95 4.08 o 2 8 0 1234.52 1214.30 8.99 o 3 8 0 883.63 879.39 7.50 o 4 8 0 246.20 226.41 1.47 o 5 8 0 1006.10 957.71 5.45 o 6 8 0 330.80 285.21 2.83 o 7 8 0 1385.98 1419.59 15.22 o 8 8 0 101.73 100.16 1.67 o 9 8 0 4.42 6.34 1.18 o 10 8 0 134.23 140.55 2.49 o 11 8 0 366.67 388.76 4.07 o 12 8 0 54.73 56.90 3.11 o 13 8 0 279.55 284.35 5.87 o 14 8 0 63.77 67.09 4.99 o 1 9 0 282.97 267.59 2.27 o 2 9 0 3.58 4.78 0.90 o 3 9 0 38.94 38.70 1.09 o 4 9 0 77.92 76.70 2.38 o 5 9 0 188.99 169.78 1.72 o 6 9 0 105.49 98.59 2.79 o 7 9 0 203.85 188.39 3.21 o 8 9 0 84.38 79.94 2.10 o 9 9 0 23.00 22.88 0.86 o 10 9 0 1.93 2.21 1.04 o 11 9 0 81.07 88.57 4.09 o 12 9 0 11.26 14.04 1.39 o 13 9 0 0.08 -0.51 1.56 o 0 10 0 2214.41 2173.81 27.57 o 1 10 0 121.47 118.48 1.73 o 2 10 0 1.45 4.28 0.99 o 3 10 0 83.15 84.35 2.15 o 4 10 0 89.93 79.09 1.71 o 5 10 0 67.27 57.62 1.21 o 6 10 0 1.97 1.92 1.52 o 7 10 0 205.63 222.83 6.91 o 8 10 0 176.84 169.90 5.00 o 9 10 0 40.05 35.90 1.54 o 10 10 0 114.00 110.60 3.55 o 11 10 0 266.90 291.72 2.91 o 12 10 0 25.80 28.99 1.77 o 1 11 0 687.05 670.70 11.11 o 2 11 0 227.54 219.14 1.97 o 3 11 0 9.29 9.00 1.14 o 4 11 0 30.10 29.83 1.18 o 5 11 0 57.53 50.21 1.30 o 6 11 0 69.90 61.17 2.11 o 7 11 0 7.18 4.81 1.02 o 8 11 0 0.04 1.69 1.01 o 9 11 0 40.81 36.58 2.39 o 10 11 0 0.21 0.88 0.99 o 11 11 0 0.98 2.96 1.24 o 12 11 0 69.04 69.80 2.19 o 0 12 0 81.70 79.55 2.22 o 1 12 0 786.98 788.88 6.86 o 2 12 0 393.56 402.30 4.73 o 3 12 0 213.06 217.96 3.80 o 4 12 0 317.89 330.37 4.11 o 5 12 0 244.58 240.50 3.42 o 6 12 0 582.99 586.83 6.55 o 7 12 0 34.05 33.71 1.35 o 8 12 0 37.20 41.41 1.54 o 9 12 0 158.19 180.02 3.50 o 10 12 0 15.34 15.31 1.77 o 11 12 0 7.88 7.27 1.35 o 1 13 0 12.52 14.32 3.49 o 2 13 0 11.45 13.32 1.42 o 3 13 0 25.30 25.83 1.62 o 4 13 0 0.00 3.07 1.34 o 5 13 0 29.76 28.44 1.48 o 6 13 0 4.87 7.51 1.38 o 7 13 0 49.13 47.05 2.22 o 8 13 0 31.34 32.28 1.98 o 9 13 0 11.49 15.90 1.83 o 10 13 0 65.76 59.05 3.96 o 0 14 0 200.35 191.36 3.26 o 1 14 0 472.26 465.98 6.82 o 2 14 0 193.26 203.26 2.24 o 3 14 0 137.45 133.63 2.04 o 4 14 0 360.90 357.13 5.87 o 5 14 0 133.52 141.51 3.57 o 6 14 0 153.34 155.89 5.26 o 7 14 0 69.10 63.26 3.73 o 8 14 0 90.16 96.36 3.71 o 1 15 0 50.61 48.03 1.88 o 2 15 0 4.65 8.64 1.94 o 3 15 0 37.46 34.57 1.96 o 4 15 0 27.20 30.05 1.76 o 5 15 0 3.52 6.44 1.63 o 6 15 0 2.57 4.51 1.62 o 7 15 0 0.34 1.47 1.43 o 0 16 0 65.26 61.14 3.67 o 1 16 0 7.14 6.90 2.05 o 2 16 0 146.00 148.34 5.18 o 3 16 0 94.81 94.01 2.25 o 4 16 0 0.48 2.99 1.76 o -16 1 1 38.83 41.63 3.19 o -15 1 1 57.14 61.41 2.63 o -14 1 1 103.26 117.44 5.19 o -13 1 1 141.02 155.17 5.73 o -12 1 1 479.86 520.94 9.70 o -11 1 1 278.30 318.73 8.23 o -10 1 1 9.04 10.92 0.33 o -9 1 1 35.43 31.58 0.94 o -8 1 1 564.76 548.79 7.39 o -7 1 1 1393.94 1403.45 15.51 o -6 1 1 1582.36 1568.38 13.78 o -5 1 1 714.79 691.68 9.90 o -4 1 1 1099.90 1045.70 11.35 o -3 1 1 144.27 134.42 2.11 o -2 1 1 1308.99 1347.96 18.00 o -1 1 1 6656.52 6765.14 30.34 o 0 1 1 142.28 124.50 0.97 o 1 1 1 6337.08 6348.05 33.46 o 2 1 1 2976.01 3071.95 42.35 o 3 1 1 904.56 891.51 12.94 o 4 1 1 1954.46 1865.02 12.63 o 5 1 1 4440.61 4846.26 29.80 o 6 1 1 6032.90 6626.05 19.26 o 7 1 1 739.62 669.38 1.92 o 8 1 1 18.92 18.71 0.45 o 9 1 1 946.61 954.84 9.00 o 10 1 1 390.07 391.20 5.73 o 11 1 1 422.20 400.16 5.50 o 12 1 1 553.63 488.72 10.53 o 13 1 1 139.78 127.04 2.63 o 14 1 1 55.14 56.81 2.45 o 15 1 1 17.82 20.59 6.31 o -16 2 1 7.47 14.17 2.90 o -15 2 1 7.03 8.31 2.52 o -14 2 1 2.52 5.70 2.38 o -13 2 1 32.01 27.85 2.54 o -12 2 1 264.64 231.47 8.33 o -11 2 1 233.98 206.65 3.13 o -10 2 1 0.03 1.31 0.53 o -9 2 1 6.17 8.79 0.70 o -8 2 1 14.55 15.02 0.43 o -7 2 1 2378.20 2559.79 26.05 o -6 2 1 356.62 441.43 4.71 o -5 2 1 13.34 6.91 1.04 o -4 2 1 249.72 261.18 2.75 o -3 2 1 1.01 4.17 0.31 o -2 2 1 254.55 236.67 1.10 o -1 2 1 3708.64 3863.34 38.81 o 0 2 1 5509.36 5953.09 43.17 o 1 2 1 3195.54 3474.48 21.27 o 2 2 1 299.08 310.29 3.08 o 3 2 1 3626.46 3884.86 27.23 o 4 2 1 23.69 22.59 0.40 o 5 2 1 52.26 59.45 1.16 o 6 2 1 1.76 6.37 0.37 o 7 2 1 135.71 126.37 1.11 o 8 2 1 31.11 28.48 0.69 o 9 2 1 88.15 79.03 1.19 o 10 2 1 389.44 403.63 5.19 o 11 2 1 190.85 170.10 2.09 o 12 2 1 4.40 5.07 0.56 o 13 2 1 45.21 34.08 3.20 o 14 2 1 5.04 5.65 1.23 o 15 2 1 8.61 11.94 2.80 o -16 3 1 8.21 5.30 5.25 o -15 3 1 6.13 11.45 2.33 o -14 3 1 24.69 29.68 1.92 o -13 3 1 82.89 77.48 5.50 o -12 3 1 9.62 10.63 0.61 o -11 3 1 306.38 293.95 4.54 o -10 3 1 744.05 719.80 11.26 o -9 3 1 206.45 214.80 4.92 o -8 3 1 194.88 178.85 1.99 o -7 3 1 251.80 262.53 4.07 o -6 3 1 1360.89 1338.45 11.34 o -5 3 1 751.21 672.50 9.11 o -4 3 1 1219.02 1400.52 12.67 o -3 3 1 649.50 666.81 2.88 o -2 3 1 2559.93 2800.64 35.05 o -1 3 1 2054.25 2003.56 30.04 o 0 3 1 14797.57 15162.07 86.32 o 1 3 1 10.07 17.89 3.17 o 2 3 1 114.16 114.71 1.96 o 3 3 1 12.35 25.04 0.65 o 4 3 1 1343.39 1278.55 12.36 o 5 3 1 2206.39 2145.67 16.89 o 6 3 1 72.66 66.02 0.72 o 7 3 1 316.37 335.96 1.12 o 8 3 1 785.96 782.27 7.91 o 9 3 1 590.70 564.11 5.71 o 10 3 1 719.74 683.90 6.66 o 11 3 1 441.03 432.35 6.08 o 12 3 1 90.36 90.19 1.72 o 13 3 1 113.01 109.09 3.80 o 14 3 1 36.85 32.14 1.69 o 15 3 1 43.21 44.39 3.21 o -15 4 1 16.48 14.98 3.25 o -14 4 1 20.17 23.17 4.21 o -13 4 1 17.02 13.40 1.39 o -12 4 1 22.07 21.92 1.08 o -11 4 1 126.41 120.45 3.50 o -10 4 1 0.27 0.36 1.11 o -9 4 1 176.95 178.68 3.67 o -8 4 1 30.28 30.10 0.56 o -7 4 1 12.24 11.51 0.37 o -6 4 1 869.24 873.44 7.04 o -5 4 1 815.92 855.44 8.90 o -4 4 1 6.01 8.75 0.38 o -3 4 1 151.59 177.08 1.77 o -2 4 1 178.97 171.41 1.50 o -1 4 1 3290.06 3506.72 30.73 o 0 4 1 34.76 35.76 0.56 o 1 4 1 3171.10 3171.06 22.26 o 2 4 1 6205.98 6888.81 30.46 o 3 4 1 2816.98 2887.03 21.96 o 4 4 1 18.82 14.84 0.72 o 5 4 1 135.46 145.57 2.87 o 6 4 1 720.02 730.23 6.72 o 7 4 1 104.95 105.67 2.39 o 8 4 1 35.90 37.81 1.09 o 9 4 1 131.62 133.51 2.24 o 10 4 1 180.04 169.14 4.03 o 11 4 1 41.73 43.34 1.30 o 12 4 1 15.25 13.88 0.94 o 13 4 1 1.58 2.99 0.77 o 14 4 1 0.44 1.76 0.99 o 15 4 1 1.79 -0.08 2.29 o -15 5 1 31.08 37.99 4.79 o -14 5 1 24.24 22.79 1.95 o -13 5 1 348.90 340.90 8.08 o -12 5 1 563.26 597.76 13.02 o -11 5 1 104.92 99.90 3.21 o -10 5 1 2.52 3.06 0.77 o -9 5 1 37.00 41.40 2.42 o -8 5 1 1566.24 1546.69 8.77 o -7 5 1 1572.04 1610.80 10.06 o -6 5 1 984.22 945.61 5.33 o -5 5 1 1869.69 1864.13 16.96 o -4 5 1 2712.22 2723.80 26.17 o -3 5 1 3288.19 3403.33 42.02 o -2 5 1 92.74 71.82 1.02 o -1 5 1 216.33 168.30 0.93 o 0 5 1 3845.29 3868.61 50.26 o 1 5 1 140.92 107.24 1.25 o 2 5 1 64.19 49.87 0.77 o 3 5 1 2315.12 2340.56 7.97 o 4 5 1 1693.06 1630.89 17.60 o 5 5 1 730.04 693.78 5.05 o 6 5 1 358.75 340.72 6.19 o 7 5 1 1307.37 1313.53 9.98 o 8 5 1 271.12 274.05 4.73 o 9 5 1 799.68 757.08 7.81 o 10 5 1 118.21 123.68 2.05 o 11 5 1 671.82 659.41 9.21 o 12 5 1 177.31 168.05 6.74 o 13 5 1 18.57 15.72 2.07 o 14 5 1 23.15 22.49 2.51 o 15 5 1 177.28 205.49 5.09 o -15 6 1 6.50 8.22 5.52 o -14 6 1 5.58 3.67 1.48 o -13 6 1 0.02 1.13 1.57 o -12 6 1 46.84 44.52 1.55 o -11 6 1 700.93 716.86 5.77 o -10 6 1 11.39 9.75 0.73 o -9 6 1 489.51 489.19 10.26 o -8 6 1 274.02 276.84 3.03 o -7 6 1 567.75 606.84 4.73 o -6 6 1 193.14 209.93 1.94 o -5 6 1 16.87 20.69 1.25 o -4 6 1 381.97 381.33 7.39 o -3 6 1 1339.88 1401.61 8.12 o -2 6 1 214.37 199.34 1.64 o -1 6 1 593.02 642.01 3.27 o 0 6 1 4192.84 4547.63 42.68 o 1 6 1 73.96 67.48 1.15 o 2 6 1 295.13 298.86 3.14 o 3 6 1 170.34 167.26 1.63 o 4 6 1 52.22 53.78 1.69 o 5 6 1 225.16 226.16 4.85 o 6 6 1 12.25 10.89 0.69 o 7 6 1 397.73 403.82 6.12 o 8 6 1 810.01 813.05 9.56 o 9 6 1 43.02 48.56 1.00 o 10 6 1 23.31 22.50 0.74 o 11 6 1 56.10 56.59 3.03 o 12 6 1 2.88 3.44 0.83 o 13 6 1 48.08 50.66 1.66 o 14 6 1 7.36 9.68 1.49 o -14 7 1 112.29 115.53 3.82 o -13 7 1 56.86 54.75 1.41 o -12 7 1 283.22 292.33 4.71 o -11 7 1 481.80 487.18 10.78 o -10 7 1 949.83 943.85 18.38 o -9 7 1 455.89 443.00 7.74 o -8 7 1 831.06 835.48 8.97 o -7 7 1 623.73 645.38 5.41 o -6 7 1 2379.19 2495.67 18.16 o -5 7 1 955.07 928.64 2.76 o -4 7 1 502.73 463.88 5.72 o -3 7 1 1353.57 1341.64 13.83 o -2 7 1 1358.99 1352.25 16.32 o -1 7 1 6500.34 6804.53 81.97 o 0 7 1 670.27 642.97 5.77 o 1 7 1 3753.91 3784.48 19.17 o 2 7 1 485.88 472.00 6.90 o 3 7 1 22.67 17.37 0.85 o 4 7 1 62.98 54.88 0.93 o 5 7 1 648.71 642.51 7.41 o 6 7 1 921.22 928.97 5.41 o 7 7 1 5.01 6.99 0.75 o 8 7 1 31.85 31.73 1.32 o 9 7 1 466.31 449.84 5.22 o 10 7 1 396.69 396.44 7.06 o 11 7 1 9.45 8.38 0.90 o 12 7 1 26.63 22.46 1.90 o 13 7 1 30.28 30.26 1.47 o 14 7 1 17.35 17.02 2.28 o -14 8 1 0.67 1.35 1.77 o -13 8 1 12.26 12.38 1.48 o -12 8 1 21.70 19.29 1.50 o -11 8 1 3.44 3.33 0.78 o -10 8 1 12.12 12.79 1.01 o -9 8 1 36.76 32.61 1.29 o -8 8 1 0.00 1.79 0.75 o -7 8 1 44.67 42.58 0.87 o -6 8 1 159.87 138.54 1.83 o -5 8 1 135.71 136.49 1.62 o -4 8 1 9.22 6.18 1.19 o -3 8 1 727.57 708.88 12.10 o -2 8 1 899.07 869.21 4.44 o -1 8 1 1507.67 1480.04 5.65 o 0 8 1 301.59 292.04 4.19 o 1 8 1 100.84 96.65 1.09 o 2 8 1 9.69 7.97 0.91 o 3 8 1 319.45 312.09 4.14 o 4 8 1 632.63 654.15 2.76 o 5 8 1 60.53 68.81 1.26 o 6 8 1 51.77 54.28 1.32 o 7 8 1 3.28 1.42 0.92 o 8 8 1 311.85 315.20 2.38 o 9 8 1 13.12 12.59 0.92 o 10 8 1 33.37 36.92 1.08 o 11 8 1 33.29 27.79 1.70 o 12 8 1 22.21 18.22 1.81 o 13 8 1 0.67 2.23 1.34 o -13 9 1 47.85 49.74 2.69 o -12 9 1 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