#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:11:14 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180977 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/57/2205771.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205771_Fobs loop_ _publ_author_name 'Young, David J.' 'Manuaba, Putra' 'Healy, Peter C.' 'Tiekink, Edward R. T.' _publ_section_title ; Tetrakis[4-(trifluoromethyl)phenyl]stannane ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m956 _journal_page_last m957 _journal_volume 61 _journal_year 2005 _space_group_IT_number 82 _symmetry_space_group_name_Hall 'I -4' _symmetry_space_group_name_H-M 'I -4' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.7480 _cell_length_b 14.7480 _cell_length_c 6.4650 _exptl_crystal_F_000 684.00 _reflns_d_resolution_high 0.7695 _cod_data_source_file ng6134Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NG6134 in space group I-4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 12178.98 14215.18 1072.18 o 2 2 0 1264.36 1072.05 39.44 o -1 3 0 30312.45 30070.73 182.39 o 1 3 0 2101.59 2163.55 55.26 o 3 3 0 74.12 74.51 18.69 o -2 4 0 3778.59 3605.33 80.32 o 0 4 0 50.60 -6.38 36.63 o 2 4 0 8401.47 8105.33 114.01 o 4 4 0 4261.37 3596.08 87.63 o -3 5 0 5209.84 5186.82 105.26 o -1 5 0 7753.69 8627.32 125.70 o 1 5 0 12267.13 12348.17 153.33 o 3 5 0 1402.32 1375.03 64.51 o 5 5 0 7462.58 6838.19 130.89 o -4 6 0 2795.71 2850.19 92.57 o -2 6 0 1259.46 973.17 63.19 o 0 6 0 5187.53 5428.91 114.95 o 2 6 0 5589.80 6549.28 125.95 o 4 6 0 261.22 176.89 23.88 o 6 6 0 739.40 743.14 47.32 o -5 7 0 5952.15 5164.07 129.83 o -3 7 0 7152.23 7025.64 138.39 o -1 7 0 4807.22 6089.04 127.08 o 1 7 0 6221.96 6463.65 138.64 o 3 7 0 511.54 326.22 28.19 o 5 7 0 2322.04 2603.79 97.45 o 7 7 0 1174.12 1337.21 63.38 o -6 8 0 2893.90 2699.48 110.14 o -4 8 0 3030.06 3808.79 118.20 o -2 8 0 1515.97 1455.97 81.45 o 0 8 0 8892.77 8444.55 180.83 o 2 8 0 5605.04 6217.56 146.14 o 4 8 0 3846.32 4180.46 124.33 o 6 8 0 2390.76 2390.89 104.20 o 8 8 0 961.45 962.73 51.88 o -7 9 0 1277.42 1092.74 67.63 o -5 9 0 2712.42 2925.26 118.33 o -3 9 0 2754.38 2221.93 103.26 o -1 9 0 2696.73 2929.01 112.32 o 1 9 0 3224.92 4156.08 131.08 o 3 9 0 1011.50 822.47 43.94 o 5 9 0 1463.67 1489.23 94.26 o 7 9 0 1586.69 1522.04 95.89 o 9 9 0 1607.28 1272.51 73.57 o -8 10 0 171.95 227.34 36.69 o -6 10 0 2425.47 2380.89 120.39 o -4 10 0 2106.01 1949.78 110.70 o -2 10 0 1171.74 1390.15 65.13 o 0 10 0 1304.44 1209.19 64.01 o 2 10 0 1047.31 824.34 50.13 o 4 10 0 2247.69 2344.13 117.14 o 6 10 0 2066.73 2191.55 122.89 o 8 10 0 909.38 1022.42 57.26 o 10 10 0 248.92 284.84 38.69 o -9 11 0 197.64 230.09 40.38 o -7 11 0 5.72 29.25 70.51 o -5 11 0 95.07 53.63 71.82 o -3 11 0 2673.38 2551.97 121.20 o -1 11 0 873.26 788.59 49.26 o 1 11 0 302.71 383.10 40.07 o 3 11 0 432.15 499.62 39.75 o 5 11 0 1220.74 1081.43 58.38 o 7 11 0 485.74 556.00 41.38 o 9 11 0 614.18 621.69 49.19 o 11 11 0 511.33 576.88 49.63 o -10 12 0 345.62 248.15 43.88 o -8 12 0 646.32 656.38 47.13 o -6 12 0 191.59 244.21 39.00 o -4 12 0 189.58 55.44 77.45 o -2 12 0 517.66 511.56 41.19 o 0 12 0 1167.91 1533.92 114.20 o 2 12 0 1204.20 1366.77 75.63 o 4 12 0 1286.92 1129.75 73.76 o 6 12 0 713.14 803.21 48.76 o 8 12 0 527.04 570.81 47.88 o 10 12 0 405.12 377.10 51.07 o 12 12 0 93.92 -55.26 94.20 o -11 13 0 182.32 197.21 44.63 o -9 13 0 199.61 224.46 45.25 o -7 13 0 496.19 559.00 47.07 o -5 13 0 545.55 587.13 48.51 o -3 13 0 1377.69 1451.47 79.88 o -1 13 0 292.64 168.27 42.07 o 1 13 0 755.84 800.59 50.63 o 3 13 0 477.54 721.45 47.88 o 5 13 0 954.13 1171.07 66.63 o 7 13 0 479.52 483.68 49.51 o 9 13 0 605.50 669.39 53.63 o 11 13 0 195.38 91.32 98.64 o 13 13 0 78.33 35.75 92.89 o -12 14 0 182.59 96.89 111.70 o -10 14 0 188.73 87.82 102.95 o -8 14 0 384.24 352.85 45.50 o -6 14 0 278.08 139.89 89.88 o -4 14 0 1863.55 1706.44 91.20 o -2 14 0 333.14 302.66 45.07 o 0 14 0 338.09 368.92 60.51 o 2 14 0 531.29 552.06 49.82 o 4 14 0 827.27 723.95 53.69 o 6 14 0 33.89 -51.57 84.20 o 8 14 0 180.84 137.20 84.82 o 10 14 0 258.03 251.47 50.76 o 12 14 0 68.24 30.07 91.51 o -11 15 0 198.71 265.84 50.69 o -9 15 0 171.37 222.46 45.38 o -7 15 0 151.56 166.89 45.69 o -5 15 0 417.20 446.99 51.88 o -3 15 0 435.38 397.11 51.51 o -1 15 0 264.84 130.83 91.07 o 1 15 0 425.66 443.86 49.82 o 3 15 0 440.81 421.17 52.07 o 5 15 0 187.79 114.76 99.39 o 7 15 0 45.46 15.94 89.45 o 9 15 0 51.77 104.70 90.07 o 11 15 0 57.44 -14.13 99.76 o -10 16 0 121.22 107.14 104.39 o -8 16 0 140.67 138.14 104.32 o -6 16 0 84.95 115.70 82.38 o -4 16 0 717.71 699.58 56.44 o -2 16 0 102.25 64.19 98.51 o 0 16 0 102.14 118.14 92.07 o 2 16 0 101.08 15.94 99.26 o 4 16 0 340.64 408.23 53.94 o 6 16 0 156.71 156.95 94.45 o 8 16 0 85.83 84.26 96.95 o 10 16 0 26.92 53.44 96.07 o -7 17 0 77.77 149.33 90.45 o -5 17 0 261.34 20.00 115.83 o -3 17 0 126.27 39.44 99.70 o -1 17 0 242.22 184.40 100.95 o 1 17 0 151.99 181.14 50.76 o 3 17 0 268.83 264.34 50.94 o 5 17 0 131.20 137.95 95.32 o 7 17 0 183.46 163.02 53.69 o -6 18 0 74.31 119.64 91.89 o -4 18 0 141.97 44.07 104.14 o -2 18 0 136.06 148.39 94.89 o 0 18 0 120.14 92.89 104.26 o 2 18 0 173.82 245.40 50.88 o 4 18 0 112.67 208.71 111.26 o 6 18 0 147.73 169.21 112.26 o -1 19 0 84.31 156.27 105.39 o 1 19 0 87.66 98.45 101.51 o 1 0 1 4033.74 4136.83 109.14 o 5 0 1 524.74 402.04 44.94 o 7 0 1 3449.39 3941.43 335.60 o 9 0 1 2799.77 3240.67 265.22 o 11 0 1 1136.20 1122.56 123.39 o 15 0 1 251.10 292.16 48.01 o 17 0 1 196.41 92.82 106.95 o 2 1 1 11461.36 10813.12 109.26 o 4 1 1 4921.69 5355.34 97.70 o 6 1 1 11390.46 11730.29 166.02 o 8 1 1 2643.89 2360.51 96.95 o 10 1 1 2841.17 2711.48 123.64 o 12 1 1 1174.07 1100.81 61.13 o 14 1 1 157.13 79.95 85.57 o 16 1 1 305.28 339.29 51.13 o 18 1 1 126.17 14.19 103.20 o 1 2 1 44023.78 44830.04 231.21 o 3 2 1 31327.29 31467.26 214.21 o 5 2 1 7311.31 8103.45 129.64 o 7 2 1 3494.62 3584.46 104.76 o 9 2 1 2478.66 2655.10 108.39 o 11 2 1 2512.59 2219.99 120.58 o 13 2 1 1514.03 1396.59 82.63 o 15 2 1 617.26 651.07 54.88 o 17 2 1 147.92 199.58 104.32 o 0 3 1 7693.93 10079.42 119.70 o 2 3 1 1338.02 1629.74 58.94 o 4 3 1 8733.70 8481.80 127.64 o 6 3 1 6030.72 5896.83 125.76 o 8 3 1 2019.56 2140.48 95.51 o 10 3 1 1107.51 1141.13 64.07 o 12 3 1 995.70 944.10 55.63 o 14 3 1 224.56 236.71 45.82 o 16 3 1 376.66 348.79 53.26 o 18 3 1 101.50 70.01 110.89 o 1 4 1 4570.29 5108.75 97.76 o 3 4 1 6244.93 6105.98 110.45 o 5 4 1 6044.86 5930.52 122.45 o 7 4 1 4081.22 3733.60 111.39 o 9 4 1 2073.48 2063.54 101.26 o 11 4 1 1068.49 1166.82 66.88 o 13 4 1 234.44 61.63 84.26 o 15 4 1 272.55 213.21 47.44 o 17 4 1 121.06 -47.88 111.95 o 2 5 1 2078.72 2306.88 77.70 o 4 5 1 2216.23 2077.04 79.95 o 6 5 1 1168.34 943.98 48.63 o 8 5 1 1717.30 1954.84 99.14 o 10 5 1 599.89 530.50 40.00 o 12 5 1 1047.89 1138.25 74.63 o 14 5 1 471.52 511.37 48.76 o 16 5 1 300.39 350.04 49.51 o 18 5 1 71.35 -2.00 105.39 o 1 6 1 7147.66 8923.67 149.58 o 3 6 1 5191.71 5581.92 124.39 o 5 6 1 1595.19 1312.27 76.07 o 7 6 1 2116.43 2029.16 96.39 o 9 6 1 1035.73 1095.93 61.57 o 11 6 1 1388.08 1204.76 72.45 o 13 6 1 278.53 357.54 42.00 o 15 6 1 370.46 258.78 51.51 o 17 6 1 185.49 55.76 103.07 o 2 7 1 2536.30 2692.86 98.39 o 4 7 1 2210.80 2260.00 92.32 o 6 7 1 3687.32 3869.36 120.26 o 8 7 1 3692.59 4060.94 134.89 o 10 7 1 669.53 623.44 44.00 o 12 7 1 428.31 361.10 47.13 o 14 7 1 306.60 308.47 46.88 o 16 7 1 189.78 243.90 49.38 o 1 8 1 1541.17 1524.98 90.01 o 3 8 1 4187.66 4475.43 129.20 o 5 8 1 1353.63 1419.22 88.70 o 7 8 1 992.27 952.54 49.57 o 9 8 1 205.52 240.84 37.25 o 11 8 1 951.31 871.41 57.01 o 13 8 1 328.18 364.54 47.19 o 15 8 1 111.66 62.51 90.82 o 17 8 1 32.11 101.39 102.51 o 2 9 1 2018.38 2147.80 107.76 o 4 9 1 1336.34 1592.42 95.07 o 6 9 1 1969.69 1880.46 107.57 o 8 9 1 1118.89 1150.63 69.57 o 10 9 1 722.55 849.22 54.26 o 12 9 1 364.89 319.91 46.76 o 14 9 1 150.02 54.01 89.01 o 16 9 1 66.95 135.39 90.38 o 1 10 1 925.59 839.40 51.19 o 3 10 1 2090.29 1733.44 109.26 o 5 10 1 1589.82 1693.37 105.57 o 7 10 1 1371.18 1487.54 77.95 o 9 10 1 193.73 194.96 40.94 o 11 10 1 325.47 302.97 46.82 o 13 10 1 306.90 276.22 46.51 o 15 10 1 167.92 134.89 49.26 o 2 11 1 1269.35 1772.88 107.14 o 4 11 1 1808.00 1723.25 114.95 o 6 11 1 1628.72 1794.45 118.64 o 8 11 1 463.04 431.86 44.44 o 10 11 1 480.73 457.18 47.82 o 12 11 1 298.88 293.97 49.76 o 14 11 1 114.38 158.45 107.01 o 1 12 1 434.14 464.80 45.82 o 3 12 1 634.63 612.82 45.57 o 5 12 1 388.96 420.80 42.44 o 7 12 1 843.45 765.21 50.88 o 9 12 1 431.75 548.56 48.13 o 11 12 1 236.52 81.01 101.07 o 13 12 1 140.32 42.44 97.51 o 0 13 1 528.80 541.00 47.69 o 2 13 1 515.47 567.50 47.07 o 4 13 1 289.65 314.66 44.44 o 6 13 1 270.94 277.16 43.63 o 8 13 1 136.07 132.08 76.95 o 10 13 1 170.05 129.01 66.38 o 12 13 1 173.41 206.21 49.76 o 1 14 1 301.08 297.10 45.63 o 3 14 1 726.18 851.78 55.76 o 5 14 1 536.55 412.98 49.07 o 7 14 1 260.65 219.34 45.76 o 9 14 1 132.52 157.58 46.13 o 11 14 1 97.05 83.07 95.57 o 2 15 1 371.57 342.10 47.88 o 4 15 1 172.54 146.45 98.82 o 6 15 1 301.18 261.47 49.01 o 8 15 1 295.11 359.91 50.88 o 10 15 1 96.62 -118.39 118.39 o 1 16 1 316.86 408.48 52.07 o 3 16 1 258.51 333.35 51.38 o 5 16 1 254.07 93.57 110.39 o 7 16 1 173.58 171.46 113.39 o 9 16 1 103.19 147.45 90.70 o 2 17 1 205.72 182.96 100.45 o 4 17 1 130.87 109.51 102.95 o 6 17 1 106.62 105.76 74.26 o 8 17 1 88.01 122.33 93.95 o 1 18 1 145.03 201.27 101.57 o 3 18 1 82.46 119.20 104.26 o 5 18 1 98.51 72.57 117.45 o 0 19 1 104.12 142.70 102.51 o 0 0 2 7502.53 5768.44 97.89 o 4 0 2 7032.41 7598.65 137.45 o 12 0 2 1689.58 1559.86 101.76 o 14 0 2 682.92 690.33 57.63 o 16 0 2 136.91 160.52 99.51 o 1 1 2 1139.69 1651.49 64.94 o 3 1 2 2176.94 2080.23 73.70 o 5 1 2 9734.06 9899.90 157.45 o 7 1 2 4039.78 4160.39 121.39 o 9 1 2 1203.64 1280.33 63.63 o 11 1 2 624.86 679.01 43.88 o 13 1 2 836.95 881.03 55.57 o 15 1 2 392.89 364.91 48.94 o 17 1 2 145.46 72.88 101.07 o 0 2 2 9283.38 8754.27 134.51 o 2 2 2 2839.70 2708.48 75.88 o 4 2 2 7923.50 9612.12 148.14 o 6 2 2 1653.89 1614.61 80.07 o 8 2 2 987.45 1069.05 55.38 o 10 2 2 1249.87 1148.06 70.38 o 12 2 2 327.33 262.09 42.88 o 14 2 2 516.84 529.50 50.82 o 16 2 2 109.35 122.45 46.19 o 18 2 2 79.86 33.50 101.70 o 1 3 2 13499.68 13452.66 166.33 o 3 3 2 6719.60 5947.40 115.14 o 5 3 2 1493.37 1214.63 71.51 o 7 3 2 1825.77 2228.68 98.39 o 9 3 2 2782.45 2701.80 119.33 o 11 3 2 997.40 851.28 53.94 o 13 3 2 603.52 603.13 48.51 o 15 3 2 73.54 79.26 91.76 o 17 3 2 133.82 56.51 102.14 o 2 4 2 4225.27 3548.14 98.01 o 4 4 2 11990.62 11553.45 170.21 o 6 4 2 2865.34 2384.82 95.82 o 8 4 2 689.39 556.37 36.69 o 10 4 2 1029.41 955.23 52.63 o 12 4 2 625.60 825.65 54.88 o 14 4 2 313.69 294.72 46.57 o 16 4 2 157.69 87.20 88.01 o 18 4 2 117.64 159.08 107.51 o 1 5 2 4621.60 5229.01 122.20 o 3 5 2 5561.86 5887.96 130.45 o 5 5 2 5299.87 5325.46 130.14 o 7 5 2 2099.60 2195.68 102.07 o 9 5 2 1141.13 1175.32 62.63 o 11 5 2 864.41 767.65 47.51 o 13 5 2 550.39 480.49 48.19 o 15 5 2 78.61 62.63 83.20 o 17 5 2 86.95 88.45 92.57 o 0 6 2 1503.17 1555.05 148.33 o 2 6 2 2972.72 3342.55 106.39 o 4 6 2 2322.87 2295.25 92.07 o 6 6 2 1068.28 1027.80 56.26 o 8 6 2 776.89 953.29 61.13 o 10 6 2 1125.74 1067.30 69.88 o 12 6 2 702.17 660.82 50.69 o 14 6 2 235.65 230.03 46.51 o 16 6 2 76.83 87.13 83.20 o 1 7 2 1478.72 1357.52 88.01 o 3 7 2 1318.17 1622.43 89.20 o 5 7 2 2741.49 2698.61 107.64 o 7 7 2 1498.39 1453.72 95.39 o 9 7 2 1049.06 868.85 54.76 o 11 7 2 507.19 522.56 46.32 o 13 7 2 247.10 89.88 97.07 o 15 7 2 198.38 223.46 48.38 o 17 7 2 111.42 177.83 50.63 o 0 8 2 1155.75 1400.97 75.13 o 2 8 2 3361.32 3285.80 120.39 o 4 8 2 2133.74 2427.83 111.64 o 6 8 2 1560.64 1570.05 100.57 o 8 8 2 578.04 486.87 41.13 o 10 8 2 1236.57 1197.88 73.07 o 12 8 2 634.18 573.00 49.57 o 14 8 2 321.17 314.60 48.51 o 16 8 2 101.14 155.58 93.01 o 1 9 2 2755.88 2714.73 121.33 o 3 9 2 1356.39 1678.62 105.45 o 5 9 2 1469.97 1235.76 68.44 o 7 9 2 453.05 424.05 41.50 o 9 9 2 1156.45 1181.13 75.76 o 11 9 2 403.50 326.85 47.82 o 13 9 2 223.66 199.71 100.95 o 15 9 2 72.13 -88.70 99.32 o 0 10 2 2318.65 2699.61 337.41 o 2 10 2 956.06 987.05 65.38 o 4 10 2 1420.56 1254.70 68.32 o 6 10 2 1339.72 1512.29 74.88 o 8 10 2 718.81 690.45 49.32 o 10 10 2 228.99 243.40 43.75 o 12 10 2 173.42 89.01 86.07 o 14 10 2 132.60 129.83 92.32 o 1 11 2 1757.58 2189.93 120.64 o 3 11 2 413.88 548.81 43.63 o 5 11 2 257.38 378.85 40.57 o 7 11 2 128.46 68.44 45.63 o 9 11 2 543.33 495.18 47.13 o 11 11 2 179.72 150.95 86.82 o 13 11 2 135.76 128.83 46.69 o 15 11 2 34.36 95.39 90.76 o 2 12 2 893.75 987.98 62.38 o 4 12 2 1084.26 952.73 59.13 o 6 12 2 298.48 358.29 41.94 o 8 12 2 368.74 362.23 46.01 o 10 12 2 135.47 60.44 93.39 o 12 12 2 137.53 100.57 47.13 o 14 12 2 48.61 -87.32 102.26 o 1 13 2 403.83 445.11 46.94 o 3 13 2 392.47 413.23 46.19 o 5 13 2 697.32 797.21 54.26 o 7 13 2 611.23 572.75 51.51 o 9 13 2 197.24 249.59 44.75 o 11 13 2 198.02 247.84 48.57 o 13 13 2 89.61 163.14 47.63 o 2 14 2 363.29 391.92 47.51 o 4 14 2 235.18 184.02 96.39 o 6 14 2 288.20 243.40 48.38 o 8 14 2 253.49 255.40 50.01 o 10 14 2 165.09 195.71 49.13 o 12 14 2 84.46 4.56 96.45 o 1 15 2 463.98 456.05 53.88 o 3 15 2 239.49 298.72 46.32 o 5 15 2 180.88 179.89 95.64 o 7 15 2 208.74 328.97 49.32 o 9 15 2 116.86 117.33 112.26 o 11 15 2 111.33 -15.88 104.14 o 2 16 2 158.44 126.95 107.89 o 4 16 2 104.30 107.01 88.32 o 6 16 2 177.77 126.01 99.51 o 8 16 2 91.62 -38.25 101.64 o 1 17 2 212.65 11.31 118.20 o 3 17 2 111.99 -9.06 93.64 o 5 17 2 120.13 -9.81 106.26 o 7 17 2 70.79 113.45 96.39 o 0 18 2 148.42 68.76 157.77 o 2 18 2 79.40 66.63 106.32 o 4 18 2 57.52 62.19 102.57 o 1 0 3 2284.78 2231.12 83.88 o 13 0 3 613.32 659.13 53.94 o 2 1 3 2409.50 2410.70 96.70 o 4 1 3 1049.15 1201.63 77.45 o 6 1 3 2714.64 2561.34 109.45 o 8 1 3 1677.22 1878.52 110.51 o 10 1 3 389.87 399.42 41.32 o 12 1 3 354.54 390.54 44.94 o 14 1 3 316.35 446.11 49.51 o 16 1 3 174.54 173.58 90.82 o 1 2 3 4323.40 3946.37 114.26 o 3 2 3 4212.53 3682.34 107.20 o 5 2 3 845.74 744.58 41.19 o 7 2 3 1399.15 1397.09 91.39 o 9 2 3 397.24 353.60 41.13 o 11 2 3 422.59 484.24 46.07 o 13 2 3 535.41 473.11 49.69 o 15 2 3 282.89 263.53 51.01 o 17 2 3 84.29 20.25 97.45 o 0 3 3 4045.39 3939.74 120.33 o 2 3 3 3683.45 3714.59 107.01 o 4 3 3 1743.66 1537.98 79.45 o 6 3 3 1935.32 1699.62 92.76 o 8 3 3 1462.15 1517.85 96.89 o 10 3 3 580.96 611.75 44.38 o 12 3 3 394.24 335.47 47.07 o 14 3 3 178.03 66.44 101.51 o 16 3 3 104.84 157.52 91.89 o 1 4 3 5076.78 5370.09 138.95 o 3 4 3 2219.38 1934.15 88.95 o 5 4 3 1358.95 1225.38 58.82 o 7 4 3 2408.48 2696.73 109.89 o 9 4 3 612.78 530.00 41.07 o 11 4 3 651.02 511.24 46.63 o 13 4 3 381.21 427.48 49.94 o 15 4 3 128.87 181.02 96.95 o 17 4 3 42.85 8.69 101.95 o 0 5 3 2020.57 2256.62 102.64 o 2 5 3 5102.29 5022.86 137.45 o 4 5 3 3002.89 2866.38 110.76 o 6 5 3 1562.68 1652.62 96.95 o 8 5 3 787.06 661.01 41.88 o 10 5 3 695.33 829.28 53.44 o 12 5 3 620.14 597.13 50.51 o 14 5 3 227.42 50.51 98.32 o 16 5 3 55.29 114.95 59.26 o 1 6 3 3216.52 3433.38 123.14 o 3 6 3 4099.06 4143.64 130.58 o 5 6 3 3167.73 3077.34 115.95 o 7 6 3 1814.76 1567.11 74.57 o 9 6 3 974.23 855.28 56.26 o 11 6 3 797.46 611.94 51.07 o 13 6 3 323.97 421.98 47.57 o 15 6 3 109.66 131.95 47.63 o 0 7 3 1584.87 2074.60 104.70 o 2 7 3 2554.17 2798.74 115.83 o 4 7 3 1368.02 1211.01 64.13 o 6 7 3 1192.67 1180.38 63.76 o 8 7 3 1147.53 1058.49 58.63 o 10 7 3 596.76 609.88 46.94 o 12 7 3 379.27 445.36 46.19 o 14 7 3 176.46 153.89 47.01 o 16 7 3 113.04 23.69 109.70 o 1 8 3 742.99 689.95 44.75 o 3 8 3 2257.46 2089.48 114.39 o 5 8 3 963.60 1056.24 69.01 o 7 8 3 418.86 509.06 41.25 o 9 8 3 405.60 342.85 44.75 o 11 8 3 277.33 231.90 44.19 o 13 8 3 145.10 117.95 89.01 o 15 8 3 139.62 178.46 98.45 o 0 9 3 647.32 670.51 44.88 o 2 9 3 1245.39 1419.59 74.45 o 4 9 3 378.37 405.92 39.82 o 6 9 3 215.02 176.83 38.57 o 8 9 3 899.92 903.35 53.69 o 10 9 3 527.99 531.50 48.32 o 12 9 3 117.92 158.52 88.45 o 14 9 3 59.92 113.20 89.20 o 1 10 3 1102.82 1216.01 77.82 o 3 10 3 892.86 812.40 48.94 o 5 10 3 250.28 309.53 38.44 o 7 10 3 358.55 447.42 46.88 o 9 10 3 421.70 517.24 46.26 o 11 10 3 199.77 17.94 96.89 o 13 10 3 88.61 98.57 85.13 o 0 11 3 431.35 481.55 57.44 o 2 11 3 1749.41 1868.58 91.51 o 4 11 3 791.83 958.17 58.19 o 6 11 3 233.96 142.33 78.63 o 8 11 3 349.42 100.64 81.57 o 10 11 3 333.97 314.66 50.07 o 12 11 3 161.13 76.01 96.20 o 14 11 3 71.47 -21.50 117.26 o 1 12 3 963.20 1154.31 67.32 o 3 12 3 549.48 626.44 52.26 o 5 12 3 192.14 167.77 86.76 o 7 12 3 441.86 516.87 46.94 o 9 12 3 280.27 308.47 47.63 o 11 12 3 119.08 34.07 97.01 o 13 12 3 51.49 -73.57 95.70 o 2 13 3 639.33 837.40 57.07 o 4 13 3 336.76 365.29 46.88 o 6 13 3 299.64 237.90 47.13 o 8 13 3 189.43 189.96 47.94 o 10 13 3 110.26 120.83 98.57 o 12 13 3 48.43 152.58 99.07 o 1 14 3 380.68 432.17 53.13 o 3 14 3 328.40 270.09 49.76 o 5 14 3 242.99 103.32 105.26 o 7 14 3 193.44 157.02 97.64 o 9 14 3 157.29 52.88 107.70 o 11 14 3 73.26 96.20 112.51 o 0 15 3 281.47 298.60 51.26 o 2 15 3 189.05 186.71 53.07 o 4 15 3 145.29 71.26 97.07 o 6 15 3 93.56 100.57 100.95 o 8 15 3 134.44 86.51 97.45 o 1 16 3 89.59 113.26 103.45 o 3 16 3 193.39 251.09 50.07 o 5 16 3 91.12 169.08 93.32 o 7 16 3 69.46 150.20 84.45 o 0 17 3 44.13 -54.76 99.14 o 2 17 3 83.59 11.56 102.45 o 4 17 3 84.26 107.32 70.45 o 0 0 4 2407.03 2210.43 98.76 o 2 0 4 1236.50 1258.20 109.01 o 4 0 4 1474.80 1427.09 73.38 o 6 0 4 1205.59 1189.44 173.89 o 10 0 4 512.96 492.74 50.82 o 12 0 4 310.96 392.73 168.21 o 16 0 4 143.71 123.95 81.82 o 1 1 4 1085.02 988.92 57.13 o 3 1 4 3106.92 2944.26 123.64 o 5 1 4 1261.04 1246.20 71.07 o 7 1 4 738.73 789.21 47.13 o 9 1 4 1091.58 1211.01 65.32 o 11 1 4 359.59 303.72 46.57 o 13 1 4 240.15 33.50 98.76 o 15 1 4 173.76 124.58 111.76 o 2 2 4 1774.10 1809.01 107.45 o 4 2 4 1721.26 1548.73 102.82 o 6 2 4 1176.31 1156.00 70.38 o 8 2 4 810.92 874.72 57.13 o 10 2 4 386.86 403.86 46.26 o 12 2 4 372.53 450.24 52.88 o 14 2 4 169.99 254.72 48.51 o 16 2 4 130.48 45.50 107.51 o 1 3 4 2438.39 2366.95 117.89 o 3 3 4 1066.64 1063.80 59.94 o 5 3 4 1099.13 1124.69 65.44 o 7 3 4 1017.23 811.96 47.26 o 9 3 4 603.41 650.32 45.94 o 11 3 4 384.40 364.48 50.13 o 13 3 4 178.33 133.45 92.95 o 15 3 4 91.88 120.95 67.69 o 2 4 4 2538.28 2652.04 117.58 o 4 4 4 1415.68 1516.17 93.64 o 6 4 4 1063.67 1005.74 53.88 o 8 4 4 734.65 846.78 54.51 o 10 4 4 439.15 456.05 45.44 o 12 4 4 244.31 190.52 48.13 o 14 4 4 136.07 42.25 103.39 o 16 4 4 66.35 -32.88 105.07 o 1 5 4 2275.92 2022.03 115.51 o 3 5 4 824.12 668.70 43.94 o 5 5 4 1273.74 1221.13 69.32 o 7 5 4 481.83 492.99 42.69 o 9 5 4 446.70 467.93 45.44 o 11 5 4 495.98 499.43 50.44 o 13 5 4 209.77 215.34 46.88 o 15 5 4 64.99 60.13 88.82 o 2 6 4 860.49 1025.11 63.76 o 4 6 4 1690.63 1726.44 78.45 o 6 6 4 494.00 400.29 42.63 o 8 6 4 216.35 195.52 39.88 o 10 6 4 394.31 369.60 46.19 o 12 6 4 240.12 99.64 97.70 o 14 6 4 116.12 -45.76 108.26 o 1 7 4 360.79 517.87 42.50 o 3 7 4 764.83 753.90 46.69 o 5 7 4 1984.60 1606.43 77.70 o 7 7 4 563.54 577.81 45.82 o 9 7 4 307.26 181.96 101.07 o 11 7 4 224.94 258.97 47.32 o 13 7 4 139.52 117.89 71.20 o 15 7 4 74.29 110.07 100.45 o 0 8 4 1124.36 1054.74 67.51 o 2 8 4 360.21 317.16 42.63 o 4 8 4 895.61 948.29 54.76 o 6 8 4 665.19 601.00 46.07 o 8 8 4 481.56 451.92 46.76 o 10 8 4 289.14 287.72 46.38 o 12 8 4 175.85 175.71 47.44 o 14 8 4 89.47 137.64 49.88 o 1 9 4 777.85 922.48 59.57 o 3 9 4 1666.85 1932.77 125.08 o 5 9 4 265.75 366.04 43.32 o 7 9 4 391.97 326.54 44.32 o 9 9 4 440.82 331.72 48.57 o 11 9 4 272.65 333.72 48.38 o 13 9 4 95.65 13.56 98.45 o 2 10 4 641.38 605.82 52.07 o 4 10 4 531.96 644.26 50.07 o 6 10 4 412.44 501.80 46.69 o 8 10 4 241.81 179.33 94.76 o 10 10 4 200.52 55.38 101.89 o 12 10 4 87.31 56.01 89.20 o 1 11 4 296.49 183.33 94.89 o 3 11 4 517.67 515.49 50.01 o 5 11 4 345.93 269.28 47.19 o 7 11 4 165.83 147.20 44.50 o 9 11 4 83.63 41.75 88.01 o 11 11 4 116.80 147.20 47.38 o 2 12 4 323.54 429.73 48.69 o 4 12 4 174.09 334.04 48.69 o 6 12 4 283.01 256.34 49.63 o 8 12 4 99.71 88.07 103.20 o 10 12 4 100.81 128.58 102.14 o 1 13 4 284.98 402.42 49.26 o 3 13 4 71.80 28.19 93.70 o 5 13 4 262.55 229.71 49.38 o 7 13 4 131.91 171.21 93.51 o 9 13 4 80.59 41.25 94.14 o 0 14 4 249.90 277.16 76.76 o 2 14 4 166.52 253.84 47.32 o 4 14 4 176.81 191.77 48.88 o 6 14 4 176.98 224.59 49.57 o 8 14 4 78.77 24.63 100.45 o 1 15 4 119.45 -59.88 111.89 o 3 15 4 56.35 160.14 95.07 o 5 15 4 189.53 258.09 53.63 o 7 15 4 90.80 -81.07 115.58 o 2 16 4 50.56 0.69 107.64 o 4 16 4 85.90 134.45 93.89 o 1 0 5 1212.98 1187.32 91.32 o 3 0 5 1099.23 1069.43 64.69 o 5 0 5 439.98 425.73 47.13 o 7 0 5 700.04 675.32 99.82 o 11 0 5 260.54 360.16 160.71 o 13 0 5 81.43 66.19 100.64 o 15 0 5 116.90 35.13 116.01 o 2 1 5 832.23 802.96 50.26 o 4 1 5 1341.68 1249.45 81.76 o 6 1 5 908.82 1003.30 64.32 o 8 1 5 433.88 347.23 51.88 o 10 1 5 337.79 428.17 50.88 o 12 1 5 146.05 165.64 48.51 o 14 1 5 84.32 -7.19 103.57 o 1 2 5 954.34 1001.55 62.07 o 3 2 5 913.06 952.92 61.32 o 5 2 5 671.74 570.81 49.63 o 7 2 5 1038.84 1052.68 63.38 o 9 2 5 541.09 497.49 52.63 o 11 2 5 215.93 260.84 51.57 o 13 2 5 91.46 40.94 101.95 o 15 2 5 70.14 57.07 108.14 o 2 3 5 636.90 646.76 40.94 o 4 3 5 680.85 675.01 44.75 o 6 3 5 599.05 648.32 47.26 o 8 3 5 492.03 486.49 49.19 o 10 3 5 475.06 545.93 54.44 o 12 3 5 173.47 134.76 104.82 o 14 3 5 114.59 117.95 109.07 o 1 4 5 625.05 682.51 48.88 o 3 4 5 635.29 726.08 44.82 o 5 4 5 398.84 379.10 42.82 o 7 4 5 411.12 367.10 44.57 o 9 4 5 272.48 242.59 47.63 o 11 4 5 139.02 146.45 101.82 o 13 4 5 123.38 48.69 100.51 o 2 5 5 837.98 799.71 48.32 o 4 5 5 516.50 385.54 41.88 o 6 5 5 616.45 599.25 47.82 o 8 5 5 212.52 328.22 44.69 o 10 5 5 122.13 135.58 86.38 o 12 5 5 97.98 68.13 94.45 o 14 5 5 76.70 -80.70 105.26 o 1 6 5 175.27 201.96 45.00 o 3 6 5 159.74 82.51 82.82 o 5 6 5 419.42 392.29 43.82 o 7 6 5 429.19 335.47 46.51 o 9 6 5 202.97 196.33 44.63 o 11 6 5 95.41 -55.94 103.26 o 13 6 5 86.83 111.07 108.64 o 2 7 5 585.49 615.63 50.44 o 4 7 5 202.03 254.34 40.19 o 6 7 5 359.97 332.54 42.94 o 8 7 5 207.90 256.03 45.44 o 10 7 5 125.17 67.76 94.07 o 12 7 5 104.92 -30.19 98.57 o 1 8 5 583.29 659.45 51.76 o 3 8 5 430.74 495.80 48.13 o 5 8 5 664.75 688.64 49.76 o 7 8 5 360.43 319.66 47.94 o 9 8 5 154.60 181.33 100.39 o 11 8 5 67.41 0.94 101.89 o 13 8 5 75.27 22.75 111.64 o 0 9 5 350.58 344.41 52.88 o 2 9 5 272.22 267.03 47.63 o 4 9 5 366.14 393.92 50.94 o 6 9 5 453.73 379.35 49.82 o 8 9 5 211.25 16.19 92.57 o 10 9 5 87.02 196.71 99.26 o 12 9 5 69.83 2.63 106.26 o 1 10 5 317.09 364.98 50.32 o 3 10 5 152.21 35.50 103.64 o 5 10 5 396.52 470.93 52.88 o 7 10 5 224.97 237.84 47.51 o 9 10 5 135.89 75.32 95.26 o 11 10 5 61.76 -104.64 104.64 o 2 11 5 116.50 99.89 66.07 o 4 11 5 248.61 186.52 105.89 o 6 11 5 161.25 164.33 49.88 o 8 11 5 131.81 69.82 97.64 o 10 11 5 41.44 88.26 69.57 o 1 12 5 197.67 170.77 101.20 o 3 12 5 140.00 145.58 105.76 o 5 12 5 132.25 97.20 89.38 o 7 12 5 122.52 184.08 99.70 o 9 12 5 55.28 84.01 93.01 o 2 13 5 67.05 109.14 100.01 o 4 13 5 139.47 -20.44 98.70 o 6 13 5 108.88 -27.32 106.82 o 8 13 5 86.01 29.57 106.76 o 1 14 5 46.55 89.95 107.20 o 3 14 5 63.31 70.38 73.76 o 5 14 5 37.61 -2.06 108.20 o 2 15 5 83.72 142.20 104.26 o 0 0 6 449.48 443.05 43.88 o 4 0 6 209.51 206.71 55.63 o 1 1 6 868.98 856.34 50.57 o 3 1 6 140.50 111.45 99.26 o 5 1 6 379.64 405.29 55.88 o 7 1 6 258.24 216.65 57.01 o 9 1 6 198.74 210.40 54.26 o 11 1 6 95.36 74.26 114.07 o 13 1 6 82.94 25.69 119.01 o 0 2 6 570.00 664.57 68.57 o 2 2 6 467.83 580.50 48.94 o 4 2 6 291.71 327.29 52.82 o 6 2 6 251.43 262.84 52.07 o 8 2 6 200.73 161.83 97.76 o 10 2 6 139.30 98.95 100.95 o 12 2 6 86.67 147.58 76.45 o 1 3 6 466.44 362.66 42.88 o 3 3 6 230.93 240.40 49.82 o 5 3 6 329.70 327.04 47.82 o 7 3 6 200.63 269.15 50.26 o 9 3 6 182.13 24.94 106.32 o 11 3 6 63.70 72.32 92.51 o 13 3 6 62.31 19.13 123.08 o 2 4 6 103.55 56.07 81.13 o 4 4 6 252.55 233.53 43.88 o 6 4 6 239.40 239.65 47.51 o 8 4 6 373.99 322.10 52.38 o 10 4 6 107.77 150.95 110.76 o 12 4 6 78.08 48.63 119.26 o 1 5 6 251.25 250.46 50.51 o 3 5 6 160.33 164.89 42.32 o 5 5 6 99.17 11.31 84.07 o 7 5 6 302.63 309.03 50.44 o 9 5 6 169.37 137.58 100.01 o 11 5 6 85.96 -3.50 103.32 o 0 6 6 603.43 590.44 57.07 o 2 6 6 410.07 448.36 50.32 o 4 6 6 175.84 276.97 42.69 o 6 6 6 168.74 172.14 46.44 o 8 6 6 256.73 87.76 111.82 o 10 6 6 42.95 -100.64 100.64 o 12 6 6 29.12 -58.88 106.51 o 1 7 6 313.73 300.97 51.26 o 3 7 6 276.25 191.15 50.01 o 5 7 6 104.06 -45.19 98.14 o 7 7 6 233.35 143.02 97.32 o 9 7 6 74.64 141.20 49.26 o 11 7 6 36.08 5.56 103.57 o 0 8 6 235.40 314.28 53.32 o 2 8 6 209.13 280.66 51.88 o 4 8 6 80.33 87.82 99.76 o 6 8 6 101.96 173.14 87.45 o 8 8 6 85.97 20.75 93.64 o 10 8 6 48.14 -59.44 97.26 o 1 9 6 166.59 26.63 104.01 o 3 9 6 165.71 189.40 48.44 o 5 9 6 111.41 71.57 91.07 o 7 9 6 109.34 129.70 47.88 o 9 9 6 27.06 138.14 94.20 o 0 10 6 118.86 208.02 73.57 o 2 10 6 86.47 134.45 90.82 o 4 10 6 115.44 138.64 98.76 o 6 10 6 157.49 157.77 103.57 o 8 10 6 73.52 108.95 96.32 o 1 11 6 83.66 31.82 106.45 o 3 11 6 148.31 174.89 101.01 o 5 11 6 120.37 142.52 105.76 o 7 11 6 104.99 1.00 101.39 o 0 12 6 29.78 24.50 110.89 o 2 12 6 57.09 33.75 95.82 o 4 12 6 74.23 168.27 47.44 o 6 12 6 52.01 20.50 99.70 o 1 13 6 40.57 -30.94 107.95 o 3 13 6 92.02 70.63 110.01 o 1 0 7 220.98 138.89 93.76 o 9 0 7 79.38 126.01 104.76 o 2 1 7 145.14 241.09 49.26 o 4 1 7 216.11 176.58 114.58 o 6 1 7 60.15 56.82 115.76 o 8 1 7 59.19 -75.82 122.58 o 10 1 7 54.03 123.08 128.89 o 1 2 7 49.82 101.95 80.26 o 3 2 7 216.45 177.83 103.76 o 5 2 7 146.14 103.14 111.32 o 7 2 7 66.55 -134.33 134.33 o 9 2 7 60.91 18.13 105.95 o 0 3 7 176.08 -27.94 152.83 o 2 3 7 159.24 163.02 87.76 o 4 3 7 201.56 135.58 124.51 o 6 3 7 95.06 -5.56 107.95 o 8 3 7 57.02 196.21 101.01 o 10 3 7 85.42 118.26 105.57 o 1 4 7 121.29 143.45 43.75 o 3 4 7 186.83 175.64 93.32 o 5 4 7 159.63 139.89 113.07 o 7 4 7 70.18 81.01 61.38 o 9 4 7 47.48 111.45 73.13 o 0 5 7 108.49 224.02 98.45 o 2 5 7 177.61 47.07 115.26 o 4 5 7 127.11 99.51 54.69 o 6 5 7 96.84 76.32 97.32 o 8 5 7 73.39 117.64 96.70 o 1 6 7 83.61 64.26 108.20 o 3 6 7 57.34 80.57 67.94 o 5 6 7 57.09 67.01 97.01 o 7 6 7 46.14 39.32 94.70 o 0 7 7 89.19 54.76 101.82 o 2 7 7 103.24 16.50 106.64 o 4 7 7 62.92 162.96 87.32 o 6 7 7 36.54 24.82 93.51 o 1 8 7 109.76 44.38 94.20 o 3 8 7 84.61 152.39 96.14 o 5 8 7 101.89 205.59 110.82 o 2 9 7 69.10 -122.89 122.89 o 4 9 7 76.29 141.52 90.20 o 1 10 7 51.47 75.32 110.32 o 3 10 7 33.65 18.50 110.64 o 0 0 8 5.59 -73.95 97.82 o 2 0 8 32.11 35.32 94.20 o 4 0 8 43.50 84.26 99.14 o 1 1 8 55.36 -106.57 106.57 o 3 1 8 53.66 190.58 112.26 o 5 1 8 34.79 -62.44 128.58 o 2 2 8 84.74 116.76 92.14 o 4 2 8 84.55 122.70 90.51 o 1 3 8 66.69 29.00 88.20 o 3 3 8 79.44 -100.20 119.33 o 5 3 8 56.42 224.96 135.39 o 2 4 8 58.35 11.44 104.01 o 4 4 8 50.28 -59.13 132.20 o 1 5 8 50.78 65.01 102.32 o 3 5 8 66.78 -39.82 119.89 o