#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/73/2207351.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207351_Fobs loop_ _publ_author_name 'Chang, Hong-Jie' 'Feng, Xiao-Long' 'Zhu, Jia-Rong' 'Ng, Seik Weng' _publ_section_title ; (+)-(Z)-(1S,2S,3S,4R,1'S,2'S,3'S,4'R,5'R)-2,3,4-Trihydroxy-5-(hydroxymethyl)-N-[2',3',4'-trihydroxy-5'-(hydroxymethyl)cyclohex-1'-yl]cyclohex-5-en-1-aminium chloride dihydrate ; _journal_coeditor_code SU6225 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3839 _journal_page_last o3841 _journal_volume 61 _journal_year 2005 _space_group_IT_number 96 _symmetry_space_group_name_Hall 'P 4nw 2abw' _symmetry_space_group_name_H-M 'P 43 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.9421 _cell_length_b 7.9421 _cell_length_c 29.0284 _exptl_crystal_F_000 872.00 _reflns_d_resolution_high 0.7823 _[local]_cod_data_source_file su6225Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 09163m in P4(3)2(1)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 183.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+3/4' 'y+1/2, -x+1/2, z+1/4' '-x+1/2, y+1/2, -z+3/4' 'x+1/2, -y+1/2, -z+1/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 84.69 81.70 2.04 o 0 2 0 33523.95 23478.90 1427.53 o 1 2 0 11243.96 10602.00 148.43 o 2 2 0 420.37 404.02 8.80 o 1 3 0 103.35 147.03 51.53 o 2 3 0 1063.48 1121.38 32.96 o 3 3 0 4553.70 4495.51 89.70 o 0 4 0 7393.80 7393.37 192.50 o 1 4 0 602.01 529.11 55.96 o 2 4 0 44.90 67.34 8.74 o 3 4 0 14.91 17.60 2.28 o 4 4 0 279.53 296.25 8.75 o 1 5 0 419.06 468.86 17.06 o 2 5 0 1.03 14.88 5.03 o 3 5 0 2.94 4.42 1.29 o 4 5 0 42.98 42.58 5.31 o 5 5 0 549.80 543.72 17.52 o 0 6 0 239.54 280.09 20.19 o 1 6 0 1471.90 1452.77 65.45 o 2 6 0 164.77 175.71 15.29 o 3 6 0 363.11 339.34 7.74 o 4 6 0 171.88 171.27 13.31 o 5 6 0 37.72 43.98 3.15 o 6 6 0 20.80 22.50 4.44 o 1 7 0 33.69 43.54 5.50 o 2 7 0 82.04 74.54 7.82 o 3 7 0 877.89 832.20 34.40 o 4 7 0 41.23 41.16 5.12 o 5 7 0 292.34 291.32 8.26 o 6 7 0 0.27 0.98 2.51 o 7 7 0 320.94 336.29 13.63 o 0 8 0 362.27 345.24 12.54 o 1 8 0 10.54 11.50 3.97 o 2 8 0 19.18 21.56 3.29 o 3 8 0 517.67 480.33 12.86 o 4 8 0 148.19 134.28 5.83 o 5 8 0 15.96 20.33 4.28 o 6 8 0 46.75 59.86 12.76 o 1 9 0 0.04 3.47 3.09 o 2 9 0 2.68 1.66 3.57 o 3 9 0 201.31 164.68 8.89 o 4 9 0 4.01 13.62 4.71 o 0 10 0 46.00 46.80 9.88 o 1 10 0 0.13 -1.01 3.68 o 0 1 1 18.13 31.91 1.48 o 1 1 1 1382.87 1416.09 21.33 o -1 2 1 20936.54 18173.28 373.51 o 0 2 1 130.97 163.61 6.06 o 1 2 1 20921.99 18138.94 347.12 o 2 2 1 15.79 21.60 1.45 o -2 3 1 1352.03 1418.71 37.63 o -1 3 1 291.72 370.91 14.33 o 0 3 1 42.16 62.30 3.07 o 1 3 1 300.14 354.46 7.93 o 2 3 1 1334.70 1375.27 26.38 o 3 3 1 1661.54 1624.83 24.96 o -3 4 1 66.18 75.40 7.52 o -2 4 1 334.35 384.74 26.30 o -1 4 1 426.32 432.05 48.19 o 0 4 1 1610.76 1869.15 37.06 o 1 4 1 430.74 484.30 57.31 o 2 4 1 344.71 390.99 22.28 o 3 4 1 68.82 83.42 6.96 o 4 4 1 579.83 559.95 10.35 o -4 5 1 37.36 36.50 2.59 o -3 5 1 859.26 848.46 14.72 o -2 5 1 163.52 167.17 13.66 o -1 5 1 60.50 81.39 21.43 o 0 5 1 8.51 17.51 1.75 o 1 5 1 64.10 69.74 8.92 o 2 5 1 167.40 167.21 6.75 o 3 5 1 845.44 817.79 14.67 o 4 5 1 40.39 40.22 2.54 o 5 5 1 21.64 22.59 2.51 o -5 6 1 468.73 454.02 11.00 o -4 6 1 202.22 195.04 5.36 o -3 6 1 612.18 604.20 12.14 o -2 6 1 11.23 23.15 2.00 o -1 6 1 453.46 457.88 13.40 o 0 6 1 50.78 42.54 3.04 o 1 6 1 454.97 447.96 10.17 o 2 6 1 13.33 24.68 3.37 o 3 6 1 612.17 597.05 11.78 o 4 6 1 199.96 202.08 9.77 o 5 6 1 464.40 453.90 13.15 o 6 6 1 91.62 79.78 4.01 o -6 7 1 169.71 166.31 9.65 o -5 7 1 1.36 4.44 2.36 o -4 7 1 9.35 8.88 3.08 o -3 7 1 153.96 153.66 5.41 o -2 7 1 393.44 406.11 10.84 o -1 7 1 188.69 174.11 6.27 o 0 7 1 35.37 39.75 3.06 o 1 7 1 190.84 178.72 5.37 o 2 7 1 388.34 400.02 9.63 o 3 7 1 148.40 136.14 6.01 o 4 7 1 8.13 6.04 2.21 o 5 7 1 1.15 3.12 2.37 o 6 7 1 164.37 161.89 11.83 o 7 7 1 28.05 30.02 3.71 o -6 8 1 10.56 22.75 3.86 o -5 8 1 141.75 139.96 12.57 o -4 8 1 111.47 108.13 9.28 o -3 8 1 11.33 21.60 5.38 o -2 8 1 134.66 122.00 4.62 o -1 8 1 12.42 9.05 2.27 o 0 8 1 218.90 220.47 6.51 o 1 8 1 12.40 12.51 2.66 o 2 8 1 131.33 116.06 4.57 o 3 8 1 11.56 15.87 4.79 o 4 8 1 109.81 114.42 9.42 o 5 8 1 141.11 127.21 12.08 o 6 8 1 10.23 15.87 3.42 o -4 9 1 119.04 135.27 21.38 o -3 9 1 68.83 72.30 6.00 o -2 9 1 185.03 183.04 8.28 o -1 9 1 2.92 2.78 3.09 o 0 9 1 18.05 18.93 3.75 o 1 9 1 3.27 2.12 3.06 o 2 9 1 182.69 194.04 11.75 o 3 9 1 66.68 66.53 5.88 o 4 9 1 119.30 138.31 24.96 o -1 10 1 22.94 26.63 4.62 o 0 10 1 26.24 34.11 4.95 o 1 10 1 23.26 20.68 4.79 o 0 1 2 616.34 567.16 8.67 o 1 1 2 7891.40 7139.31 105.40 o -1 2 2 5786.96 5765.20 85.54 o 0 2 2 1137.14 1167.68 18.84 o 1 2 2 5797.53 5768.36 85.74 o 2 2 2 631.80 726.09 11.42 o -2 3 2 1354.41 1422.97 25.26 o -1 3 2 1961.07 2042.33 33.04 o 0 3 2 405.79 477.59 9.20 o 1 3 2 2001.58 2068.21 35.09 o 2 3 2 1326.32 1387.56 22.84 o 3 3 2 79.76 81.60 2.14 o -3 4 2 257.60 286.95 43.99 o -2 4 2 138.67 160.16 3.73 o -1 4 2 823.32 868.39 31.77 o 0 4 2 6811.12 6868.22 126.43 o 1 4 2 819.47 847.73 44.60 o 2 4 2 143.23 172.57 12.86 o 3 4 2 251.82 255.53 42.89 o 4 4 2 1013.17 1015.05 16.32 o -4 5 2 80.27 77.18 9.31 o -3 5 2 27.57 31.23 3.63 o -2 5 2 1245.84 1245.77 22.37 o -1 5 2 352.43 347.55 39.97 o 0 5 2 301.09 364.57 8.22 o 1 5 2 349.59 333.86 29.89 o 2 5 2 1244.17 1229.48 22.32 o 3 5 2 29.29 33.44 4.93 o 4 5 2 83.66 88.22 11.53 o 5 5 2 11.64 9.53 1.89 o -5 6 2 137.44 138.15 9.30 o -4 6 2 114.29 123.47 18.20 o -3 6 2 136.42 121.62 4.49 o -2 6 2 196.10 183.89 5.27 o -1 6 2 752.65 766.88 30.09 o 0 6 2 150.41 137.07 6.60 o 1 6 2 751.98 757.23 25.50 o 2 6 2 190.91 183.45 9.33 o 3 6 2 135.65 127.41 4.22 o 4 6 2 110.86 126.20 22.59 o 5 6 2 138.82 145.64 7.58 o 6 6 2 16.67 17.25 2.73 o -6 7 2 4.00 5.59 2.64 o -5 7 2 59.53 56.06 3.53 o -4 7 2 16.80 20.88 2.68 o -3 7 2 400.75 388.31 23.21 o -2 7 2 2.18 1.81 1.93 o -1 7 2 26.62 36.00 7.11 o 0 7 2 2.85 2.67 1.83 o 1 7 2 26.58 30.15 2.56 o 2 7 2 1.98 3.26 1.72 o 3 7 2 400.76 402.43 19.33 o 4 7 2 18.62 29.88 5.58 o 5 7 2 59.73 57.56 3.57 o 6 7 2 4.14 6.19 2.73 o 7 7 2 42.91 46.68 4.24 o -6 8 2 68.56 70.94 5.63 o -5 8 2 42.62 45.64 4.74 o -4 8 2 88.63 94.32 23.51 o -3 8 2 126.58 117.50 5.90 o -2 8 2 4.00 5.96 2.44 o -1 8 2 6.47 6.27 2.43 o 0 8 2 57.43 48.35 3.44 o 1 8 2 6.48 7.46 2.73 o 2 8 2 3.35 4.40 2.48 o 3 8 2 126.73 119.91 10.19 o 4 8 2 85.19 90.48 13.49 o 5 8 2 42.93 43.01 4.16 o 6 8 2 69.98 75.15 6.62 o -4 9 2 28.15 27.66 5.22 o -3 9 2 98.45 94.98 17.43 o -2 9 2 141.15 153.24 6.30 o -1 9 2 12.36 8.88 2.91 o 0 9 2 247.81 249.49 8.24 o 1 9 2 13.21 9.34 2.81 o 2 9 2 143.26 156.86 13.78 o 3 9 2 100.38 99.65 13.82 o 4 9 2 28.78 31.99 4.49 o -1 10 2 10.35 9.42 3.94 o 0 10 2 20.21 23.02 4.43 o 1 10 2 10.23 6.63 4.55 o 0 1 3 752.64 720.87 10.99 o 1 1 3 409.83 388.07 5.80 o -1 2 3 1195.37 1206.32 53.03 o 0 2 3 7405.94 7090.32 104.56 o 1 2 3 1173.77 1217.85 63.22 o 2 2 3 1341.14 1332.89 20.34 o -2 3 3 2934.70 3052.64 54.65 o -1 3 3 1436.44 1370.67 22.22 o 0 3 3 4026.83 4362.51 73.80 o 1 3 3 1424.54 1360.19 23.76 o 2 3 3 2913.82 2976.64 47.97 o 3 3 3 603.60 628.65 10.26 o -3 4 3 233.48 255.83 8.85 o -2 4 3 1255.96 1300.38 63.96 o -1 4 3 6.59 19.54 3.34 o 0 4 3 6585.06 6893.31 116.40 o 1 4 3 6.20 16.95 5.49 o 2 4 3 1268.75 1307.27 43.28 o 3 4 3 240.81 263.87 4.97 o 4 4 3 571.98 576.29 9.86 o -4 5 3 30.55 45.94 7.96 o -3 5 3 68.30 69.89 3.69 o -2 5 3 237.72 221.95 8.90 o -1 5 3 1186.80 1200.40 38.28 o 0 5 3 321.73 356.25 11.41 o 1 5 3 1167.58 1155.19 54.26 o 2 5 3 241.19 224.66 6.38 o 3 5 3 68.02 69.58 3.20 o 4 5 3 30.37 45.58 12.30 o 5 5 3 31.72 39.97 3.12 o -5 6 3 298.85 292.26 8.65 o -4 6 3 17.82 18.17 2.43 o -3 6 3 2.61 21.25 3.85 o -2 6 3 29.66 35.42 3.04 o -1 6 3 1021.50 1077.13 21.51 o 0 6 3 67.21 91.86 4.22 o 1 6 3 1029.08 1066.61 31.08 o 2 6 3 31.47 43.05 3.75 o 3 6 3 3.07 10.92 2.68 o 4 6 3 17.90 17.73 2.18 o 5 6 3 299.29 292.64 8.01 o 6 6 3 1.29 4.97 2.33 o -6 7 3 100.72 108.42 9.34 o -5 7 3 182.19 181.84 6.10 o -4 7 3 98.63 97.49 3.88 o -3 7 3 232.70 233.37 14.77 o -2 7 3 164.53 154.22 21.29 o -1 7 3 1028.68 1008.77 47.25 o 0 7 3 198.55 180.34 7.50 o 1 7 3 1028.40 1016.07 26.96 o 2 7 3 161.39 154.65 17.80 o 3 7 3 236.38 232.75 7.43 o 4 7 3 95.52 94.93 6.35 o 5 7 3 181.54 182.69 6.15 o 6 7 3 97.39 101.90 8.18 o 7 7 3 1.07 0.64 3.26 o -6 8 3 4.90 10.11 4.08 o -5 8 3 37.11 42.63 4.84 o -4 8 3 180.91 216.00 19.04 o -3 8 3 12.67 14.39 4.03 o -2 8 3 168.71 165.35 15.67 o -1 8 3 0.58 0.98 2.30 o 0 8 3 250.26 261.13 8.09 o 1 8 3 0.68 2.05 2.26 o 2 8 3 168.87 148.83 6.58 o 3 8 3 12.25 22.87 5.72 o 4 8 3 180.98 192.14 7.17 o 5 8 3 36.46 36.56 4.12 o 6 8 3 4.87 8.78 3.39 o -4 9 3 97.81 104.13 7.44 o -3 9 3 38.51 37.60 11.50 o -2 9 3 95.68 98.93 10.97 o -1 9 3 47.55 54.92 4.67 o 0 9 3 2.30 5.27 2.75 o 1 9 3 45.39 48.38 5.71 o 2 9 3 95.76 101.98 11.05 o 3 9 3 37.87 38.99 12.30 o 4 9 3 97.33 106.51 5.59 o -1 10 3 60.89 64.54 7.38 o 0 10 3 182.55 198.72 8.61 o 1 10 3 61.55 64.22 6.45 o 0 0 4 11771.65 8660.90 717.29 o 0 1 4 85.83 87.27 1.69 o 1 1 4 5690.38 5468.54 85.83 o -1 2 4 271.15 273.56 4.30 o 0 2 4 558.26 660.26 14.33 o 1 2 4 272.82 283.76 6.36 o 2 2 4 19.99 18.35 1.21 o -2 3 4 196.88 183.79 13.49 o -1 3 4 249.33 223.33 16.75 o 0 3 4 1065.69 1180.76 21.89 o 1 3 4 249.97 239.55 24.00 o 2 3 4 203.50 195.63 12.71 o 3 3 4 149.53 158.90 4.33 o -3 4 4 369.08 349.59 15.45 o -2 4 4 778.46 835.84 52.90 o -1 4 4 2213.71 2205.83 46.53 o 0 4 4 1600.47 1514.81 26.52 o 1 4 4 2207.18 2245.34 101.96 o 2 4 4 759.44 811.32 48.85 o 3 4 4 362.97 329.54 12.82 o 4 4 4 1929.77 1888.64 29.20 o -4 5 4 374.19 359.59 10.96 o -3 5 4 355.84 344.67 6.91 o -2 5 4 98.80 96.56 14.85 o -1 5 4 183.53 213.46 15.68 o 0 5 4 38.92 37.06 2.87 o 1 5 4 183.61 200.58 12.44 o 2 5 4 98.58 106.65 37.71 o 3 5 4 349.14 330.26 6.84 o 4 5 4 370.30 363.37 13.32 o 5 5 4 152.35 153.72 4.64 o -5 6 4 67.49 70.07 3.31 o -4 6 4 37.88 40.27 4.64 o -3 6 4 1642.06 1570.55 28.53 o -2 6 4 299.33 303.44 18.27 o -1 6 4 3246.62 3226.07 96.36 o 0 6 4 8.82 15.21 2.39 o 1 6 4 3235.03 3189.88 63.92 o 2 6 4 296.40 298.64 13.23 o 3 6 4 1632.34 1565.85 30.87 o 4 6 4 37.63 36.65 3.07 o 5 6 4 68.09 68.06 3.56 o 6 6 4 4.73 7.53 2.47 o -6 7 4 39.43 44.62 4.07 o -5 7 4 133.65 135.21 5.70 o -4 7 4 58.12 56.93 3.38 o -3 7 4 673.95 677.87 24.36 o -2 7 4 125.09 108.59 9.07 o -1 7 4 541.22 496.39 26.34 o 0 7 4 45.68 39.72 3.44 o 1 7 4 545.35 493.83 27.67 o 2 7 4 125.75 108.19 5.18 o 3 7 4 678.26 643.60 26.68 o 4 7 4 58.63 63.43 5.33 o 5 7 4 138.89 136.86 6.32 o 6 7 4 39.77 39.78 3.71 o 7 7 4 208.27 223.91 9.31 o -6 8 4 32.70 34.64 6.27 o -5 8 4 27.87 33.20 7.44 o -4 8 4 21.22 33.03 12.74 o -3 8 4 407.41 405.76 18.21 o -2 8 4 59.79 72.44 8.23 o -1 8 4 564.32 562.56 14.33 o 0 8 4 217.02 215.38 7.15 o 1 8 4 559.30 555.13 14.10 o 2 8 4 59.85 64.04 7.63 o 3 8 4 404.87 397.11 22.59 o 4 8 4 20.43 21.22 8.68 o 5 8 4 28.84 38.50 4.73 o 6 8 4 32.08 39.66 5.41 o -4 9 4 3.73 4.99 4.47 o -3 9 4 47.34 47.55 6.16 o -2 9 4 14.95 12.37 3.08 o -1 9 4 39.65 48.36 17.37 o 0 9 4 92.48 79.48 4.61 o 1 9 4 39.85 51.12 19.81 o 2 9 4 15.19 16.88 5.58 o 3 9 4 46.02 49.66 7.46 o 4 9 4 3.57 7.20 3.40 o -1 10 4 4.40 6.99 4.16 o 0 10 4 88.04 95.60 6.18 o 1 10 4 3.61 8.73 4.60 o 0 1 5 0.87 -0.56 0.56 o 1 1 5 1270.16 1315.65 20.97 o -1 2 5 483.60 499.31 23.66 o 0 2 5 487.58 518.93 8.63 o 1 2 5 503.82 574.27 33.35 o 2 2 5 25.01 35.30 1.67 o -2 3 5 1404.78 1479.89 21.65 o -1 3 5 1252.44 1373.76 29.04 o 0 3 5 508.05 539.32 11.23 o 1 3 5 1235.98 1325.28 27.49 o 2 3 5 1415.08 1494.53 38.75 o 3 3 5 474.86 485.98 9.43 o -3 4 5 100.13 103.91 5.13 o -2 4 5 92.36 120.60 4.69 o -1 4 5 1322.94 1393.48 34.83 o 0 4 5 1.26 9.78 1.29 o 1 4 5 1333.35 1472.84 63.52 o 2 4 5 98.98 127.43 4.46 o 3 4 5 105.15 107.91 8.24 o 4 4 5 18.95 16.48 1.66 o -4 5 5 47.23 45.47 2.97 o -3 5 5 1140.38 1030.50 50.19 o -2 5 5 189.87 170.74 16.87 o -1 5 5 589.41 538.92 15.09 o 0 5 5 217.21 229.84 5.28 o 1 5 5 596.07 562.85 10.79 o 2 5 5 187.87 173.94 13.21 o 3 5 5 1143.56 1079.87 45.65 o 4 5 5 50.68 49.03 4.55 o 5 5 5 720.19 695.09 13.96 o -5 6 5 157.99 180.61 10.11 o -4 6 5 166.12 155.80 9.78 o -3 6 5 681.53 639.50 20.09 o -2 6 5 783.73 738.14 28.40 o -1 6 5 534.13 558.16 19.99 o 0 6 5 923.01 934.63 36.38 o 1 6 5 534.83 561.57 12.11 o 2 6 5 784.22 744.72 43.69 o 3 6 5 691.52 681.58 15.68 o 4 6 5 162.80 170.92 12.38 o 5 6 5 162.09 171.52 6.49 o 6 6 5 338.77 329.68 8.93 o -6 7 5 82.12 75.43 8.28 o -5 7 5 62.94 63.23 6.61 o -4 7 5 0.78 1.73 2.35 o -3 7 5 205.81 207.07 6.97 o -2 7 5 88.45 87.87 23.18 o -1 7 5 355.01 345.76 11.15 o 0 7 5 407.89 418.43 15.17 o 1 7 5 356.18 333.82 18.20 o 2 7 5 87.40 94.18 19.70 o 3 7 5 204.55 230.51 14.52 o 4 7 5 1.13 0.55 2.36 o 5 7 5 62.39 66.25 4.18 o 6 7 5 79.54 75.98 6.49 o 7 7 5 10.08 10.51 4.08 o -6 8 5 20.65 15.12 4.28 o -5 8 5 30.76 35.13 8.08 o -4 8 5 131.24 132.02 7.55 o -3 8 5 8.36 6.14 3.19 o -2 8 5 104.44 103.67 7.93 o -1 8 5 93.03 97.12 4.62 o 0 8 5 18.79 34.51 3.31 o 1 8 5 91.89 90.03 5.34 o 2 8 5 103.82 93.68 6.30 o 3 8 5 7.75 10.62 2.81 o 4 8 5 129.31 140.99 7.16 o 5 8 5 29.91 31.39 3.98 o 6 8 5 20.81 19.96 4.89 o -4 9 5 84.94 88.58 7.01 o -3 9 5 53.37 56.71 5.41 o -2 9 5 150.68 153.39 6.34 o -1 9 5 78.69 78.76 4.48 o 0 9 5 4.84 8.45 2.88 o 1 9 5 81.21 74.93 5.88 o 2 9 5 150.68 157.43 16.34 o 3 9 5 53.93 56.46 4.28 o 4 9 5 85.37 92.17 5.20 o -1 10 5 4.03 6.95 4.61 o 0 10 5 0.80 4.02 3.68 o 1 10 5 3.76 5.60 4.27 o 0 1 6 383.35 345.40 6.76 o 1 1 6 1753.91 1863.89 29.60 o -1 2 6 620.02 659.45 11.44 o 0 2 6 1504.60 1515.25 22.78 o 1 2 6 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