#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210533.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210533_Fobs loop_ _publ_author_name 'Cai, Jin-Hua' 'Huang, Ying-Heng' 'Jiang, Yi-Min' _publ_section_title ; Triaqua[N-(5-formysalicylidene)glycinato(2--)-\k^3^O,N,O']zinc(II) monohydrate ; _journal_coeditor_code BX2026 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2432 _journal_page_last m2434 _journal_volume 62 _journal_year 2006 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.2321 _cell_length_b 7.7591 _cell_length_c 30.9730 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.7826 _[local]_cod_data_source_file bx2026Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' f60621b in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 278.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 76915.23 89833.12 653.09 o 4 0 0 40.21 89.84 32.08 o 6 0 0 2071.43 2048.39 109.80 o 8 0 0 11493.06 12990.46 322.27 o 10 0 0 4396.40 4399.08 212.47 o 12 0 0 306.52 283.77 84.84 o 14 0 0 1420.49 1605.63 168.98 o 2 1 0 70070.25 73976.41 764.65 o 4 1 0 1047.32 1087.32 50.12 o 6 1 0 7437.67 7947.75 153.64 o 8 1 0 156.65 171.61 38.07 o 10 1 0 712.55 723.25 72.79 o 12 1 0 916.61 1059.71 90.54 o 14 1 0 677.48 757.29 90.71 o 0 2 0 365.96 213.23 125.84 o 2 2 0 1223.22 1287.99 32.89 o 4 2 0 593.34 748.75 34.40 o 6 2 0 7549.74 7991.81 226.73 o 8 2 0 19963.93 19619.03 286.02 o 10 2 0 934.64 928.11 77.74 o 12 2 0 1.15 22.10 49.03 o 14 2 0 70.53 89.12 89.12 o 2 3 0 22082.06 22058.54 423.05 o 4 3 0 9462.25 8966.12 111.15 o 6 3 0 27697.38 28119.65 1105.83 o 8 3 0 2399.48 2439.62 107.75 o 10 3 0 2876.51 3111.00 134.33 o 12 3 0 1078.56 1060.06 95.52 o 0 4 0 15162.74 15294.10 154.72 o 2 4 0 321.85 336.05 18.54 o 4 4 0 46.84 30.27 14.94 o 6 4 0 25.66 98.73 33.21 o 8 4 0 3475.75 3697.58 136.40 o 10 4 0 774.29 728.09 77.56 o 12 4 0 0.75 -21.39 85.56 o 2 5 0 7815.27 7580.36 178.65 o 4 5 0 2795.63 2846.16 72.26 o 6 5 0 175.97 158.89 58.59 o 8 5 0 305.64 296.65 61.99 o 10 5 0 36.86 54.90 83.42 o 12 5 0 1146.06 1279.08 169.69 o 0 6 0 16817.48 15818.14 327.97 o 2 6 0 5525.71 5290.20 109.57 o 4 6 0 908.27 963.15 57.97 o 6 6 0 2499.96 2359.11 91.10 o 8 6 0 5095.38 4866.79 245.26 o 10 6 0 1304.94 1327.57 160.42 o 2 7 0 1995.14 1968.04 77.41 o 4 7 0 50.27 118.86 43.98 o 6 7 0 77.22 157.07 47.84 o 8 7 0 263.67 297.60 71.06 o 10 7 0 12.40 0.00 99.10 o 0 8 0 5749.63 5785.82 240.99 o 2 8 0 3134.75 2935.13 128.45 o 4 8 0 923.73 851.46 86.67 o 6 8 0 1222.33 1182.38 103.27 o 8 8 0 1045.53 1276.55 89.90 o 2 9 0 857.22 935.81 116.22 o 4 9 0 1845.24 1759.80 119.95 o 6 9 0 1082.67 1268.75 119.28 o 1 1 1 7867.70 8289.16 122.92 o 2 1 1 5866.62 5861.35 122.57 o 3 1 1 734.32 811.28 30.03 o 4 1 1 10194.97 9621.27 95.04 o 5 1 1 1435.60 1467.54 43.67 o 6 1 1 6277.28 6045.42 106.10 o 7 1 1 3567.79 3365.75 77.07 o 8 1 1 889.62 881.49 47.12 o 9 1 1 2036.29 2052.44 70.86 o 10 1 1 13.51 23.16 28.49 o 11 1 1 84.31 71.10 31.19 o 12 1 1 1263.75 1328.04 70.36 o 13 1 1 333.60 302.06 45.41 o 14 1 1 1117.43 1250.78 76.64 o 0 2 1 10101.92 9609.46 152.12 o 1 2 1 6723.68 7221.68 81.54 o 2 2 1 25237.93 26489.69 216.53 o 3 2 1 751.14 774.76 94.88 o 4 2 1 79.95 82.30 13.49 o 5 2 1 2715.38 2803.09 87.78 o 6 2 1 5410.73 5975.80 97.41 o 7 2 1 758.20 716.56 41.42 o 8 2 1 8357.60 8052.23 261.90 o 9 2 1 85.17 86.93 31.24 o 10 2 1 396.98 374.28 42.17 o 11 2 1 274.68 375.70 44.18 o 12 2 1 240.82 234.37 40.96 o 13 2 1 197.46 226.25 45.27 o 14 2 1 295.87 354.38 72.60 o 1 3 1 1004.64 956.91 22.38 o 2 3 1 2643.16 2799.34 47.48 o 3 3 1 242.39 271.15 13.47 o 4 3 1 156.51 223.06 23.41 o 5 3 1 202.76 263.77 19.36 o 6 3 1 238.63 422.94 34.51 o 7 3 1 3061.67 3345.38 90.56 o 8 3 1 401.73 419.83 39.48 o 9 3 1 735.58 713.45 50.06 o 10 3 1 148.94 180.47 38.76 o 11 3 1 99.57 83.73 35.86 o 12 3 1 83.63 129.13 42.38 o 13 3 1 53.93 79.92 42.33 o 0 4 1 44875.48 43310.80 410.71 o 1 4 1 445.55 429.06 26.03 o 2 4 1 6457.13 5961.91 42.94 o 3 4 1 1687.01 1505.73 72.78 o 4 4 1 1600.89 1605.03 30.90 o 5 4 1 1690.99 1476.82 98.51 o 6 4 1 4627.02 4047.49 257.24 o 7 4 1 1381.86 1283.98 52.71 o 8 4 1 1902.17 1866.93 70.55 o 9 4 1 506.93 512.22 46.32 o 10 4 1 977.17 969.21 60.25 o 11 4 1 584.03 521.80 61.72 o 12 4 1 2.05 -29.15 41.97 o 1 5 1 448.72 465.19 44.64 o 2 5 1 1009.16 888.36 57.91 o 3 5 1 354.88 318.31 24.83 o 4 5 1 2737.32 2774.93 49.03 o 5 5 1 1273.75 1264.24 32.56 o 6 5 1 3317.59 3161.57 54.65 o 7 5 1 3612.96 3590.35 73.68 o 8 5 1 185.47 163.90 38.58 o 9 5 1 1295.53 1240.36 80.24 o 10 5 1 191.84 259.60 57.20 o 11 5 1 140.94 133.66 55.33 o 12 5 1 495.21 624.40 76.96 o 0 6 1 423.74 609.03 37.35 o 1 6 1 551.10 409.36 65.43 o 2 6 1 151.46 263.20 21.36 o 3 6 1 13.44 33.22 20.23 o 4 6 1 1111.48 1098.18 38.69 o 5 6 1 127.50 161.21 29.53 o 6 6 1 12.03 51.31 28.67 o 7 6 1 324.10 338.60 36.53 o 8 6 1 230.11 390.37 58.22 o 9 6 1 26.66 57.87 61.18 o 10 6 1 153.30 190.26 76.45 o 11 6 1 0.98 65.02 75.27 o 1 7 1 1829.73 1614.65 54.77 o 2 7 1 1440.25 1445.37 54.33 o 3 7 1 31.55 38.31 25.14 o 4 7 1 1830.81 1836.43 55.97 o 5 7 1 4.15 15.94 26.96 o 6 7 1 1806.29 1787.62 61.34 o 7 7 1 678.46 768.30 48.62 o 8 7 1 151.69 152.62 42.04 o 9 7 1 478.84 581.14 68.86 o 10 7 1 187.08 115.78 77.40 o 0 8 1 2646.95 2719.75 120.97 o 1 8 1 209.43 213.05 40.51 o 2 8 1 287.03 340.70 45.51 o 3 8 1 168.62 152.30 41.25 o 4 8 1 1.10 16.43 38.11 o 5 8 1 41.70 60.65 41.31 o 6 8 1 49.63 81.76 38.40 o 7 8 1 61.72 39.20 39.38 o 8 8 1 425.72 535.17 59.02 o 1 9 1 110.57 136.24 41.75 o 2 9 1 52.22 106.56 44.37 o 3 9 1 1.62 -18.60 40.90 o 4 9 1 43.68 122.71 45.75 o 5 9 1 16.55 -10.15 44.59 o 6 9 1 3.31 61.84 58.85 o 0 0 2 33030.26 15948.61 184.66 o 1 0 2 3819.55 4136.99 37.97 o 2 0 2 24.83 51.04 12.83 o 3 0 2 5209.28 5477.70 118.00 o 4 0 2 5386.27 5880.11 107.30 o 5 0 2 84.34 144.08 27.47 o 6 0 2 2519.90 2681.36 102.67 o 7 0 2 1799.80 1735.69 81.28 o 8 0 2 4595.06 4639.34 197.85 o 9 0 2 137.23 116.68 42.84 o 10 0 2 4725.11 4804.12 156.53 o 11 0 2 756.71 743.68 74.76 o 12 0 2 28.89 13.37 44.95 o 13 0 2 3864.31 4327.81 175.43 o 14 0 2 184.22 214.19 65.29 o 1 1 2 18009.45 19386.30 140.23 o 2 1 2 906.13 1056.78 49.64 o 3 1 2 1348.70 1451.52 40.08 o 4 1 2 97.44 115.05 15.05 o 5 1 2 78.93 98.64 21.71 o 6 1 2 2214.57 2095.31 57.35 o 7 1 2 805.20 760.24 41.78 o 8 1 2 43.91 44.94 25.48 o 9 1 2 288.93 332.62 38.04 o 10 1 2 395.82 368.44 40.49 o 11 1 2 9.73 -12.20 29.45 o 12 1 2 983.59 955.52 61.62 o 13 1 2 15.99 -1.13 35.35 o 14 1 2 88.26 96.47 41.30 o 0 2 2 22389.31 21767.81 199.85 o 1 2 2 8876.15 9313.65 76.55 o 2 2 2 13005.85 14330.80 94.35 o 3 2 2 1420.96 1735.31 55.00 o 4 2 2 3.79 41.70 14.58 o 5 2 2 12494.35 12749.68 132.14 o 6 2 2 525.71 568.69 35.56 o 7 2 2 1170.95 1129.46 49.79 o 8 2 2 5859.98 5758.12 109.76 o 9 2 2 110.65 106.35 30.57 o 10 2 2 124.19 115.84 33.01 o 11 2 2 704.23 702.39 52.96 o 12 2 2 10.86 -8.05 31.75 o 13 2 2 300.96 351.67 49.18 o 14 2 2 179.78 202.96 65.01 o 1 3 2 1348.73 1064.91 50.90 o 2 3 2 15573.33 15894.21 256.13 o 3 3 2 4871.80 4894.42 46.88 o 4 3 2 14515.29 14376.90 94.31 o 5 3 2 2488.13 2462.22 50.83 o 6 3 2 9607.34 9576.21 156.63 o 7 3 2 21208.23 21703.55 240.44 o 8 3 2 173.18 193.02 34.66 o 9 3 2 5637.38 5563.07 117.24 o 10 3 2 1535.95 1564.86 69.90 o 11 3 2 139.54 137.37 38.47 o 12 3 2 1072.61 1105.30 68.55 o 13 3 2 195.32 177.29 44.27 o 0 4 2 1786.78 1818.43 37.46 o 1 4 2 36.75 28.81 9.38 o 2 4 2 1164.50 1115.68 27.68 o 3 4 2 128.55 227.78 18.15 o 4 4 2 34.60 48.56 14.26 o 5 4 2 1624.15 1668.06 35.77 o 6 4 2 43.72 61.26 19.78 o 7 4 2 896.13 957.12 49.38 o 8 4 2 85.97 133.42 33.33 o 9 4 2 400.79 410.14 44.26 o 10 4 2 291.42 281.03 52.17 o 11 4 2 146.78 142.89 48.15 o 12 4 2 21.97 -8.01 45.68 o 1 5 2 7882.93 7351.25 59.58 o 2 5 2 4640.45 4497.05 46.77 o 3 5 2 49.72 48.30 13.10 o 4 5 2 1540.17 1580.59 30.24 o 5 5 2 4710.07 4447.42 61.35 o 6 5 2 2614.18 2657.01 52.23 o 7 5 2 819.06 884.90 46.79 o 8 5 2 134.40 139.99 36.15 o 9 5 2 824.53 928.61 62.00 o 10 5 2 574.09 567.84 67.47 o 11 5 2 756.96 770.23 76.99 o 12 5 2 256.20 324.64 68.32 o 0 6 2 6187.71 5706.87 91.37 o 1 6 2 388.94 365.71 23.18 o 2 6 2 2734.23 2335.08 123.85 o 3 6 2 1956.77 1863.43 50.28 o 4 6 2 95.37 73.51 19.57 o 5 6 2 2913.28 2626.83 129.21 o 6 6 2 336.96 354.46 35.08 o 7 6 2 184.33 244.34 38.69 o 8 6 2 4167.41 4249.92 128.02 o 9 6 2 23.76 35.16 63.09 o 10 6 2 472.28 486.21 84.68 o 11 6 2 480.89 542.27 97.25 o 1 7 2 21.33 136.88 25.94 o 2 7 2 402.51 437.59 37.81 o 3 7 2 527.42 539.20 40.57 o 4 7 2 391.34 444.94 35.53 o 5 7 2 172.16 197.90 32.84 o 6 7 2 382.77 409.86 38.99 o 7 7 2 104.87 199.77 36.76 o 8 7 2 115.64 138.95 40.66 o 9 7 2 84.45 181.05 57.52 o 10 7 2 2.27 -30.87 81.99 o 0 8 2 1494.12 1513.18 95.73 o 1 8 2 30.64 15.86 33.83 o 2 8 2 65.32 30.35 35.97 o 3 8 2 266.90 368.75 47.10 o 4 8 2 20.77 50.45 33.57 o 5 8 2 671.76 693.80 50.81 o 6 8 2 230.59 272.01 42.42 o 7 8 2 274.98 309.94 47.10 o 8 8 2 333.62 382.25 55.66 o 1 9 2 819.95 816.90 60.99 o 2 9 2 644.18 578.39 55.69 o 3 9 2 309.16 268.11 48.29 o 4 9 2 191.34 225.72 49.50 o 5 9 2 1.34 2.89 46.72 o 1 1 3 77724.06 79201.45 1702.56 o 2 1 3 1509.37 1318.67 40.25 o 3 1 3 10639.05 11387.13 195.52 o 4 1 3 869.51 1111.53 29.93 o 5 1 3 5217.62 5245.80 104.13 o 6 1 3 2663.33 2697.60 64.54 o 7 1 3 20071.39 21039.62 193.82 o 8 1 3 415.26 457.37 37.43 o 9 1 3 14554.77 14720.31 189.41 o 10 1 3 1039.03 999.78 56.46 o 11 1 3 809.21 788.46 54.44 o 12 1 3 30.83 27.58 34.85 o 13 1 3 192.14 159.56 41.65 o 14 1 3 24.03 11.24 38.21 o 0 2 3 17312.10 17798.57 133.16 o 1 2 3 30276.53 32312.74 443.82 o 2 2 3 19254.91 20807.07 109.40 o 3 2 3 13132.37 13329.56 143.47 o 4 2 3 141.83 198.98 16.64 o 5 2 3 16500.47 17828.98 147.95 o 6 2 3 581.24 672.32 36.80 o 7 2 3 6759.90 7160.27 125.76 o 8 2 3 2862.41 2786.10 100.65 o 9 2 3 1350.55 1394.87 61.44 o 10 2 3 35.25 42.64 31.07 o 11 2 3 3644.64 3708.50 105.80 o 12 2 3 445.90 455.98 49.62 o 13 2 3 981.20 1129.56 71.69 o 14 2 3 53.60 -5.15 56.70 o 1 3 3 198.97 205.24 14.09 o 2 3 3 606.17 659.41 17.52 o 3 3 3 9312.90 10000.80 82.92 o 4 3 3 422.29 502.84 21.78 o 5 3 3 286.94 362.97 22.78 o 6 3 3 94.82 157.55 27.45 o 7 3 3 247.92 469.51 84.18 o 8 3 3 39.01 22.16 28.83 o 9 3 3 86.86 153.64 35.44 o 10 3 3 27.51 31.73 30.63 o 11 3 3 429.77 451.70 47.88 o 12 3 3 132.37 175.83 41.15 o 13 3 3 0.45 14.13 46.33 o 0 4 3 2748.35 2609.07 33.90 o 1 4 3 2891.02 2672.32 39.92 o 2 4 3 19.47 23.98 10.24 o 3 4 3 8350.64 8153.18 87.00 o 4 4 3 5150.91 5288.26 60.19 o 5 4 3 2369.24 2136.03 39.99 o 6 4 3 958.65 1019.80 33.68 o 7 4 3 3177.25 3275.20 73.30 o 8 4 3 200.13 205.39 35.28 o 9 4 3 521.71 580.01 58.95 o 10 4 3 48.09 73.90 41.04 o 11 4 3 1693.44 1613.68 91.68 o 12 4 3 6.79 -1.12 46.01 o 13 4 3 2106.99 2237.33 193.22 o 1 5 3 9220.77 8719.66 104.22 o 2 5 3 269.46 272.69 25.10 o 3 5 3 1106.02 1099.79 26.21 o 4 5 3 13.79 50.13 15.22 o 5 5 3 13.26 50.79 18.03 o 6 5 3 475.49 470.38 28.33 o 7 5 3 1443.38 1486.81 56.31 o 8 5 3 59.55 60.12 33.32 o 9 5 3 2299.53 2325.53 84.84 o 10 5 3 117.80 142.88 43.44 o 11 5 3 66.84 74.03 53.70 o 12 5 3 31.56 57.36 56.57 o 0 6 3 2168.16 1975.75 56.70 o 1 6 3 421.14 418.82 26.37 o 2 6 3 75.52 102.57 19.22 o 3 6 3 591.29 637.84 31.22 o 4 6 3 323.61 340.48 28.13 o 5 6 3 665.90 777.52 37.18 o 6 6 3 16.74 23.22 26.45 o 7 6 3 37.92 60.78 33.35 o 8 6 3 56.89 112.09 48.70 o 9 6 3 27.62 24.13 60.24 o 10 6 3 34.05 1.11 64.77 o 11 6 3 43.73 22.16 70.95 o 1 7 3 4196.42 3878.69 72.98 o 2 7 3 53.36 64.26 25.93 o 3 7 3 272.16 232.02 33.54 o 4 7 3 311.37 317.42 37.14 o 5 7 3 1322.06 1320.47 52.15 o 6 7 3 73.46 107.45 31.70 o 7 7 3 4535.93 4622.12 95.79 o 8 7 3 0.33 13.15 37.08 o 9 7 3 2347.00 2409.70 111.35 o 10 7 3 47.00 56.64 56.75 o 0 8 3 79.51 94.30 52.28 o 1 8 3 886.05 784.82 54.66 o 2 8 3 5.06 18.58 34.07 o 3 8 3 1844.37 1797.18 67.06 o 4 8 3 42.90 23.33 32.59 o 5 8 3 406.04 393.21 44.59 o 6 8 3 60.22 68.81 38.07 o 7 8 3 142.57 188.55 43.30 o 8 8 3 48.78 67.72 59.03 o 1 9 3 494.32 620.45 57.06 o 2 9 3 54.17 49.30 40.54 o 3 9 3 145.31 154.48 45.85 o 4 9 3 24.93 31.74 45.09 o 5 9 3 73.15 80.90 49.38 o 0 0 4 6583.84 6255.67 61.32 o 1 0 4 41.82 69.82 6.84 o 2 0 4 3780.56 3919.35 80.92 o 3 0 4 55839.11 61173.71 357.91 o 4 0 4 17167.31 19531.06 461.07 o 5 0 4 6782.89 6654.90 127.63 o 6 0 4 163.44 178.67 33.26 o 7 0 4 292.81 220.40 36.81 o 8 0 4 14.83 51.48 36.53 o 9 0 4 1111.28 1174.00 79.15 o 10 0 4 257.78 307.24 55.69 o 11 0 4 3532.44 3641.61 147.09 o 12 0 4 188.76 174.03 54.15 o 13 0 4 5891.00 6282.89 241.70 o 14 0 4 157.57 136.59 61.24 o 1 1 4 441.59 404.75 20.24 o 2 1 4 485.16 529.85 12.78 o 3 1 4 9263.19 9628.64 128.14 o 4 1 4 63.03 80.05 15.26 o 5 1 4 1727.59 1891.74 42.45 o 6 1 4 438.43 555.93 33.88 o 7 1 4 3406.64 3609.38 80.37 o 8 1 4 943.98 1018.25 49.62 o 9 1 4 1856.68 2015.20 70.62 o 10 1 4 637.86 681.35 49.12 o 11 1 4 471.06 530.39 48.06 o 12 1 4 54.59 57.59 35.04 o 13 1 4 10.15 -35.06 35.06 o 14 1 4 41.30 16.95 39.72 o 0 2 4 7743.31 7900.21 61.92 o 1 2 4 4468.22 4666.74 43.96 o 2 2 4 8642.89 8964.45 61.44 o 3 2 4 4542.31 4519.76 43.07 o 4 2 4 7249.24 8122.23 109.09 o 5 2 4 8096.60 8510.39 116.34 o 6 2 4 1721.95 1764.85 46.33 o 7 2 4 72.87 105.28 26.92 o 8 2 4 858.94 871.39 48.46 o 9 2 4 14.92 41.74 29.01 o 10 2 4 58.36 54.65 31.20 o 11 2 4 175.27 249.94 41.29 o 12 2 4 642.02 651.03 54.92 o 13 2 4 230.11 263.27 46.40 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5 4 1408.62 1421.89 69.23 o 10 5 4 93.66 136.84 43.60 o 11 5 4 207.18 209.18 58.45 o 12 5 4 32.60 50.76 56.56 o 0 6 4 2653.57 2615.63 79.93 o 1 6 4 1495.51 1340.65 42.49 o 2 6 4 1338.68 1312.82 38.41 o 3 6 4 2882.06 2369.54 242.58 o 4 6 4 2.21 35.47 22.63 o 5 6 4 6503.02 6541.00 87.58 o 6 6 4 617.00 613.82 35.43 o 7 6 4 790.65 717.39 41.60 o 8 6 4 7.10 26.07 40.09 o 9 6 4 404.28 448.05 60.76 o 10 6 4 57.94 80.78 53.91 o 11 6 4 471.40 488.46 92.01 o 1 7 4 29.96 127.70 26.23 o 2 7 4 304.68 284.78 30.85 o 3 7 4 16.57 15.26 24.80 o 4 7 4 666.50 689.01 45.94 o 5 7 4 42.35 56.79 32.26 o 6 7 4 92.09 129.06 33.53 o 7 7 4 126.37 344.47 39.58 o 8 7 4 41.64 30.57 41.71 o 9 7 4 1.87 98.88 54.26 o 10 7 4 44.82 42.76 77.89 o 0 8 4 1.82 35.14 49.06 o 1 8 4 373.48 322.91 43.36 o 2 8 4 22.98 20.02 31.09 o 3 8 4 1493.91 1528.89 62.74 o 4 8 4 3.19 -9.83 31.73 o 5 8 4 248.56 288.99 41.03 o 6 8 4 0.56 -4.38 35.77 o 7 8 4 180.95 208.40 44.64 o 8 8 4 307.90 317.40 64.11 o 1 9 4 1241.94 1282.57 73.25 o 2 9 4 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8 7 11 84.21 156.25 65.22 o 9 7 11 776.66 836.72 92.04 o 0 8 11 1040.53 1091.90 72.65 o 1 8 11 1.52 14.79 29.99 o 2 8 11 9.24 34.87 29.81 o 3 8 11 197.42 264.77 35.87 o 4 8 11 75.52 39.05 31.96 o 5 8 11 482.33 608.39 52.54 o 6 8 11 0.54 -12.20 51.06 o 7 8 11 235.14 260.52 75.50 o 1 9 11 79.60 201.93 43.51 o 2 9 11 0.56 47.13 42.94 o 3 9 11 35.52 54.14 39.15 o 4 9 11 255.71 215.69 48.48 o 0 0 12 1720.80 1473.01 49.20 o 1 0 12 2992.60 3010.08 48.48 o 2 0 12 5789.72 5737.23 155.07 o 3 0 12 20053.36 19532.19 280.91 o 4 0 12 3615.49 3844.58 66.04 o 5 0 12 19111.96 19067.02 204.62 o 6 0 12 4117.75 4030.72 106.59 o 7 0 12 218.56 213.05 31.21 o 8 0 12 4328.31 4102.74 93.33 o 9 0 12 222.20 218.44 51.63 o 10 0 12 544.56 507.92 65.29 o 11 0 12 1966.54 1833.21 111.65 o 12 0 12 348.29 283.07 64.16 o 13 0 12 633.44 654.40 84.92 o 1 1 12 14000.92 14393.38 294.84 o 2 1 12 5.77 2.59 10.50 o 3 1 12 2298.26 2312.13 29.02 o 4 1 12 8687.13 8908.88 108.88 o 5 1 12 1171.00 1250.53 31.35 o 6 1 12 1795.70 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10 6 12 337.86 363.25 61.21 o 1 7 12 530.71 575.83 38.93 o 2 7 12 30.97 41.98 27.30 o 3 7 12 501.22 524.69 38.90 o 4 7 12 79.58 185.51 32.46 o 5 7 12 114.92 61.72 35.10 o 6 7 12 13.22 69.27 45.68 o 7 7 12 68.92 46.59 58.65 o 8 7 12 0.10 -1.27 57.37 o 9 7 12 0.88 -12.53 60.57 o 0 8 12 268.68 294.58 52.21 o 1 8 12 311.66 275.36 37.09 o 2 8 12 246.01 257.54 36.14 o 3 8 12 569.82 573.44 42.89 o 4 8 12 40.50 55.68 33.28 o 5 8 12 514.70 591.76 53.29 o 6 8 12 47.06 92.72 47.02 o 7 8 12 73.96 29.38 64.76 o 1 9 12 936.25 959.08 54.82 o 2 9 12 100.68 91.78 41.66 o 3 9 12 464.38 478.32 51.65 o 4 9 12 602.91 655.44 96.10 o 1 1 13 1964.90 1787.57 58.97 o 2 1 13 8447.49 8544.35 112.07 o 3 1 13 2796.75 2667.32 31.64 o 4 1 13 23308.10 23604.40 310.63 o 5 1 13 975.72 1009.69 29.73 o 6 1 13 8276.67 7966.69 106.03 o 7 1 13 133.03 97.98 20.00 o 8 1 13 14.39 14.28 21.44 o 9 1 13 174.28 164.47 28.89 o 10 1 13 2626.61 2426.63 92.31 o 11 1 13 214.99 192.49 35.88 o 12 1 13 3408.31 3412.61 111.82 o 13 1 13 34.30 86.14 44.35 o 0 2 13 18464.33 18913.18 280.91 o 1 2 13 1806.25 1822.08 27.65 o 2 2 13 11624.23 11590.04 146.57 o 3 2 13 5885.14 5179.98 342.34 o 4 2 13 3046.67 3017.33 105.01 o 5 2 13 21.47 18.96 13.77 o 6 2 13 6716.64 6746.22 72.34 o 7 2 13 5.30 -8.77 21.05 o 8 2 13 5637.69 5398.79 101.82 o 9 2 13 202.70 217.18 34.34 o 10 2 13 2357.24 2384.95 89.31 o 11 2 13 207.20 192.43 41.00 o 12 2 13 0.82 -16.66 37.40 o 13 2 13 277.45 284.16 53.82 o 1 3 13 274.28 329.57 15.33 o 2 3 13 1725.75 1843.56 30.73 o 3 3 13 615.31 654.54 20.35 o 4 3 13 2708.56 2423.68 229.81 o 5 3 13 0.21 -13.29 16.66 o 6 3 13 218.31 195.46 24.33 o 7 3 13 176.48 167.18 24.47 o 8 3 13 86.11 56.61 27.50 o 9 3 13 71.70 143.05 33.37 o 10 3 13 159.24 145.12 34.86 o 11 3 13 172.27 166.08 41.82 o 12 3 13 2.02 39.70 40.29 o 0 4 13 5702.66 5293.27 102.69 o 1 4 13 72.46 91.58 18.83 o 2 4 13 8623.05 8131.99 92.31 o 3 4 13 926.32 873.24 30.22 o 4 4 13 1552.06 1444.28 40.40 o 5 4 13 2538.23 2340.12 217.78 o 6 4 13 3270.07 3117.95 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1170.24 69.25 o 4 4 29 263.83 264.54 45.73 o 5 4 29 1712.36 1700.07 81.19 o 6 4 29 131.20 101.95 42.50 o 7 4 29 50.44 33.56 40.07 o 1 5 29 684.11 746.53 62.36 o 2 5 29 1375.97 1452.11 78.63 o 3 5 29 521.95 570.56 58.57 o 4 5 29 288.31 340.61 51.51 o 5 5 29 120.50 113.15 44.30 o 6 5 29 323.47 348.76 53.77 o 0 6 29 813.52 916.35 102.52 o 1 6 29 4.11 -1.33 41.81 o 2 6 29 56.53 110.40 47.26 o 3 6 29 4.51 41.39 43.42 o 4 6 29 9.97 -52.77 58.58 o 0 0 30 12.70 227.44 85.56 o 1 0 30 65.01 112.53 55.67 o 2 0 30 18.61 53.12 54.95 o 3 0 30 3641.78 3781.17 259.17 o 4 0 30 1491.84 1582.05 83.65 o 5 0 30 4472.23 4225.55 258.45 o 6 0 30 480.06 417.87 61.07 o 7 0 30 393.12 406.09 58.79 o 8 0 30 905.03 822.65 74.38 o 9 0 30 347.24 342.88 68.73 o 1 1 30 776.56 979.71 47.74 o 2 1 30 63.33 178.33 36.11 o 3 1 30 729.04 823.70 51.75 o 4 1 30 489.81 535.22 46.09 o 5 1 30 2.25 13.52 33.14 o 6 1 30 752.42 724.38 51.83 o 7 1 30 162.57 184.29 41.04 o 8 1 30 14.08 1.15 35.05 o 9 1 30 261.24 295.78 48.44 o 0 2 30 1327.18 1511.87 100.88 o 1 2 30 696.36 651.16 54.17 o 2 2 30 364.47 398.16 48.20 o 3 2 30 1901.93 2000.48 80.65 o 4 2 30 3.71 -24.50 37.65 o 5 2 30 1007.14 1060.73 65.20 o 6 2 30 208.40 218.10 54.37 o 7 2 30 53.12 71.72 52.87 o 8 2 30 133.87 101.16 54.37 o 1 3 30 2812.13 2945.66 99.79 o 2 3 30 1344.01 1331.35 72.30 o 3 3 30 408.83 467.94 52.77 o 4 3 30 1433.17 1469.62 75.12 o 5 3 30 584.44 583.41 57.09 o 6 3 30 773.52 773.63 60.94 o 7 3 30 922.27 927.05 67.02 o 8 3 30 0.35 -8.12 50.89 o 0 4 30 239.77 286.58 65.78 o 1 4 30 41.47 59.13 38.90 o 2 4 30 269.65 296.23 48.11 o 3 4 30 391.52 500.30 54.41 o 4 4 30 3.18 -6.75 37.58 o 5 4 30 316.90 385.72 51.86 o 6 4 30 86.90 70.26 41.80 o 7 4 30 8.16 0.89 43.79 o 1 5 30 485.41 554.40 58.49 o 2 5 30 316.90 349.21 54.46 o 3 5 30 175.46 208.71 48.55 o 4 5 30 209.21 183.07 47.53 o 5 5 30 87.18 85.18 44.07 o 0 6 30 297.78 437.41 82.01 o 1 6 30 125.33 139.51 47.83 o 2 6 30 458.57 493.53 59.83 o 3 6 30 1358.25 1464.62 124.32 o 1 1 31 2931.46 3158.95 86.46 o 2 1 31 125.73 167.47 37.49 o 3 1 31 601.39 652.79 49.81 o 4 1 31 116.22 119.18 36.49 o 5 1 31 527.52 507.83 47.41 o 6 1 31 78.32 50.47 35.97 o 7 1 31 2314.57 2227.85 80.99 o 8 1 31 14.91 1.40 44.29 o 0 2 31 465.25 445.28 70.75 o 1 2 31 1082.93 1127.54 65.43 o 2 2 31 10.43 16.16 38.29 o 3 2 31 4665.51 4619.24 129.97 o 4 2 31 39.09 37.61 39.88 o 5 2 31 3951.07 3859.47 132.75 o 6 2 31 159.47 125.22 51.78 o 7 2 31 189.18 128.53 55.68 o 8 2 31 13.45 6.46 50.84 o 1 3 31 335.40 434.61 53.31 o 2 3 31 2.52 14.79 39.40 o 3 3 31 60.49 84.51 41.60 o 4 3 31 37.12 94.44 41.84 o 5 3 31 37.94 41.84 42.06 o 6 3 31 6.26 41.74 40.74 o 7 3 31 189.51 204.63 47.22 o 0 4 31 54.49 52.97 57.05 o 1 4 31 432.73 477.05 53.93 o 2 4 31 237.67 201.24 45.88 o 3 4 31 4094.64 3991.89 118.57 o 4 4 31 109.29 114.62 43.95 o 5 4 31 2060.56 2003.50 89.91 o 6 4 31 57.59 60.36 42.85 o 1 5 31 1980.44 2014.05 92.60 o 2 5 31 0.02 -0.96 40.33 o 3 5 31 646.03 673.36 63.45 o 4 5 31 112.56 106.28 45.01 o 5 5 31 29.50 74.15 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421.44 71.20 o 0 4 32 78.48 78.22 65.24 o 1 4 32 415.56 463.58 55.27 o 2 4 32 145.22 151.48 46.74 o 3 4 32 296.54 427.50 55.06 o 4 4 32 9.61 29.71 41.36 o 5 4 32 9.87 54.29 44.10 o 6 4 32 3.36 20.68 79.14 o 1 5 32 123.58 175.81 48.83 o 2 5 32 3.99 17.57 42.30 o 3 5 32 554.23 587.02 62.03 o 4 5 32 220.21 191.08 91.97 o 1 1 33 756.06 707.86 60.22 o 2 1 33 1020.63 1001.39 57.91 o 3 1 33 425.29 399.14 47.83 o 4 1 33 4003.06 4097.59 103.69 o 5 1 33 78.19 55.72 43.21 o 6 1 33 1440.53 1290.65 75.02 o 7 1 33 948.37 925.38 70.67 o 0 2 33 781.42 778.98 87.64 o 1 2 33 46.56 75.89 41.58 o 2 2 33 621.43 737.05 59.98 o 3 2 33 640.27 670.83 70.17 o 4 2 33 72.71 96.68 53.31 o 5 2 33 1676.55 1593.81 97.99 o 6 2 33 1018.39 1033.24 84.87 o 7 2 33 51.54 67.14 56.27 o 1 3 33 28.96 66.61 41.06 o 2 3 33 190.26 230.97 48.66 o 3 3 33 20.97 21.99 41.68 o 4 3 33 76.66 177.76 48.23 o 5 3 33 75.38 93.79 47.21 o 6 3 33 1.51 19.79 41.73 o 0 4 33 1339.82 1120.82 102.02 o 1 4 33 97.65 95.89 45.98 o 2 4 33 2192.36 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36 205.58 211.62 77.40 o 4 1 36 491.36 588.62 74.53 o 5 1 36 178.97 207.71 65.19 o 0 2 36 346.10 400.69 123.35 o 1 2 36 33.23 18.99 71.04 o 2 2 36 202.05 237.76 62.40 o 3 2 36 840.35 765.31 78.81 o 4 2 36 2.48 -36.43 54.42 o 5 2 36 304.74 362.11 72.10 o 1 3 36 1014.72 1106.37 75.29 o 2 3 36 571.83 660.81 64.67 o 3 3 36 462.88 509.73 74.95 o 4 3 36 1766.96 1735.39 179.67 o 0 4 36 337.30 560.40 121.21 o 1 4 36 9.88 64.01 58.42 o 1 1 37 876.41 974.88 109.13 o 2 1 37 39.18 46.91 72.07 o 3 1 37 152.94 119.43 75.42 o 4 1 37 362.07 486.36 94.08 o 0 2 37 210.02 314.42 121.21 o 1 2 37 31.84 14.58 75.07 o 2 2 37 249.30 275.85 87.71 o 3 2 37 1034.56 1093.35 91.99 o 4 2 37 0.43 47.56 62.02 o 1 3 37 108.63 151.03 51.26 o 2 3 37 205.32 200.63 79.99 o 0 0 38 27.46 129.76 106.23 o 1 0 38 331.80 301.59 83.68 o 2 0 38 61.21 96.26 75.19 o 3 0 38 1719.00 1814.73 132.41 o 4 0 38 204.94 226.01 125.48 o 1 1 38 601.20 713.54 99.64 o 2 1 38 66.92 150.42 84.12 o 3 1 38 258.69 300.36 92.93 o 0 2 38 380.53 375.74 133.33 o 1 2 38 67.62 66.80 83.53 o 2 2 38 37.30 70.44 84.59 o 1 1 39 1010.14 1073.55 116.61 o