#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211189.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211189_Fobs loop_ _publ_author_name 'Rubin-Preminger, Janice M.' 'Englert, Ulli' _publ_section_title ; trans-Aquabis(glyoximato-\k^2^N,N')nitrocobalt(III) ; _journal_coeditor_code SG2064 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2972 _journal_page_last m2973 _journal_volume 62 _journal_year 2006 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.4127 _cell_length_b 11.3660 _cell_length_c 9.8590 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high .7497 _[local]_cod_data_source_file sg2064Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' y06_a19 in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 339.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7070.80 8510.23 300.23 o 4 0 0 15599.80 18204.56 584.69 o 6 0 0 3772.12 3793.19 214.25 o 8 0 0 269.95 341.45 35.96 o 10 0 0 3774.99 3441.97 316.45 o 1 1 0 13002.03 13585.55 203.88 o 3 1 0 15119.96 15846.23 293.59 o 5 1 0 2885.36 3072.31 86.65 o 7 1 0 521.35 529.14 28.60 o 9 1 0 359.54 362.80 35.91 o 11 1 0 46.65 62.15 19.15 o 0 2 0 2583.13 2694.98 166.88 o 2 2 0 242.52 251.96 9.00 o 4 2 0 42.73 66.05 7.19 o 6 2 0 3.84 8.67 3.60 o 8 2 0 19.85 26.00 10.35 o 10 2 0 39.18 39.66 13.24 o 1 3 0 5794.21 6083.94 118.81 o 3 3 0 8510.12 8359.59 128.88 o 5 3 0 1583.20 1535.70 43.73 o 7 3 0 64.00 74.54 12.27 o 9 3 0 174.94 181.10 25.52 o 11 3 0 26.99 28.75 19.83 o 0 4 0 115405.87 80628.34 6288.31 o 2 4 0 127.55 125.45 7.13 o 4 4 0 3973.05 4336.35 67.31 o 6 4 0 931.44 897.85 26.82 o 8 4 0 12.20 18.18 9.58 o 10 4 0 2013.49 1880.46 84.88 o 1 5 0 436.84 446.30 17.30 o 3 5 0 2152.13 2090.59 33.83 o 5 5 0 355.78 402.57 17.98 o 7 5 0 229.05 253.00 26.60 o 9 5 0 108.41 111.08 23.03 o 0 6 0 15532.83 15774.39 539.97 o 2 6 0 4354.08 4285.63 121.86 o 4 6 0 1630.97 1680.21 38.21 o 6 6 0 421.92 447.69 26.90 o 8 6 0 344.16 364.12 40.33 o 10 6 0 353.95 374.95 46.17 o 1 7 0 8803.71 8634.87 397.13 o 3 7 0 9305.47 8883.12 231.14 o 5 7 0 3644.98 3502.52 75.90 o 7 7 0 544.10 564.57 44.57 o 9 7 0 567.10 611.04 54.67 o 0 8 0 21904.76 20443.82 2471.71 o 2 8 0 5.77 12.38 5.27 o 4 8 0 1353.82 1372.57 45.39 o 6 8 0 424.48 428.96 28.97 o 8 8 0 43.70 44.65 13.91 o 1 9 0 345.03 303.49 22.87 o 3 9 0 .19 9.87 4.60 o 5 9 0 30.00 41.41 10.94 o 7 9 0 35.42 53.43 16.16 o 9 9 0 .19 14.45 11.55 o 0 10 0 8298.18 8483.63 372.72 o 2 10 0 2221.48 2062.04 134.63 o 4 10 0 969.80 1000.16 44.90 o 6 10 0 215.53 250.40 26.24 o 8 10 0 193.42 268.83 38.81 o 1 11 0 3650.84 3650.62 84.67 o 3 11 0 3663.64 3339.76 231.55 o 5 11 0 2310.00 2179.89 141.61 o 7 11 0 430.28 451.12 47.21 o 0 12 0 4567.91 4307.26 154.59 o 2 12 0 27.50 29.09 11.35 o 4 12 0 603.63 614.70 41.96 o 6 12 0 296.35 309.07 41.08 o 1 13 0 793.69 713.40 43.37 o 3 13 0 296.09 309.99 34.56 o 5 13 0 294.46 301.68 35.30 o 0 14 0 3543.60 3445.60 215.88 o 2 14 0 790.48 741.38 46.48 o 4 14 0 461.84 477.91 44.19 o 1 15 0 376.07 313.00 41.19 o 1 1 1 13825.80 14731.78 189.92 o 2 1 1 445.87 407.53 7.32 o 3 1 1 7843.29 8705.86 128.06 o 4 1 1 1008.05 1113.06 17.91 o 5 1 1 1526.14 1631.45 24.22 o 6 1 1 202.89 211.92 9.43 o 7 1 1 2267.57 2375.08 46.68 o 8 1 1 235.64 228.05 18.38 o 9 1 1 2148.78 2074.71 47.21 o 10 1 1 13.33 24.32 7.66 o 11 1 1 195.82 157.58 20.71 o 0 2 1 23031.71 18541.54 1971.07 o 1 2 1 .75 4.45 1.95 o 2 2 1 811.33 902.86 14.29 o 3 2 1 1360.35 1512.54 22.06 o 4 2 1 13554.39 14429.78 207.11 o 5 2 1 22.04 25.36 3.57 o 6 2 1 3980.72 3913.84 70.55 o 7 2 1 432.42 416.09 16.92 o 8 2 1 258.36 283.11 19.57 o 9 2 1 156.64 152.15 16.40 o 10 2 1 1167.55 1041.52 43.69 o 11 2 1 226.63 224.73 24.92 o 1 3 1 690.92 656.78 9.87 o 2 3 1 417.00 397.50 8.29 o 3 3 1 1023.78 1024.18 15.22 o 4 3 1 381.50 401.04 10.74 o 5 3 1 2.69 8.01 2.50 o 6 3 1 143.85 155.61 9.08 o 7 3 1 319.99 340.84 17.41 o 8 3 1 84.17 80.90 12.18 o 9 3 1 426.14 431.08 26.65 o 10 3 1 1.99 7.06 6.39 o 0 4 1 1026.75 961.55 33.76 o 1 4 1 111.80 109.39 4.47 o 2 4 1 512.72 442.85 9.48 o 3 4 1 180.55 197.56 7.38 o 4 4 1 1639.10 1583.25 22.07 o 5 4 1 5.68 14.06 3.54 o 6 4 1 471.28 465.56 15.95 o 7 4 1 53.62 55.34 7.73 o 8 4 1 140.27 151.64 16.13 o 9 4 1 51.74 51.05 8.83 o 10 4 1 65.57 77.48 13.76 o 1 5 1 14275.78 14010.88 358.41 o 2 5 1 206.43 199.65 6.44 o 3 5 1 7934.44 8184.23 51.95 o 4 5 1 618.22 595.97 13.81 o 5 5 1 2542.00 2553.69 33.55 o 6 5 1 171.64 187.88 11.69 o 7 5 1 2666.24 2612.30 47.80 o 8 5 1 263.94 241.89 23.62 o 9 5 1 2609.15 2577.16 67.87 o 10 5 1 28.35 39.41 9.87 o 0 6 1 16984.46 17122.49 382.99 o 1 6 1 2.00 8.42 3.55 o 2 6 1 876.99 807.69 17.86 o 3 6 1 326.26 314.85 9.27 o 4 6 1 10728.34 11069.04 116.49 o 5 6 1 32.84 32.03 4.87 o 6 6 1 3946.35 3753.37 60.33 o 7 6 1 273.50 301.06 22.89 o 8 6 1 540.75 569.83 33.50 o 9 6 1 43.26 39.57 10.24 o 10 6 1 1288.88 1218.31 49.86 o 1 7 1 88.96 80.42 7.47 o 2 7 1 200.02 190.33 10.17 o 3 7 1 367.27 352.74 13.98 o 4 7 1 22.33 25.97 5.78 o 5 7 1 30.67 36.37 7.42 o 6 7 1 54.21 56.36 9.59 o 7 7 1 25.70 40.49 9.66 o 8 7 1 4.02 10.34 7.03 o 9 7 1 22.70 46.32 10.66 o 0 8 1 835.39 823.74 21.48 o 1 8 1 76.32 73.77 7.35 o 2 8 1 438.58 390.80 19.85 o 3 8 1 163.22 170.42 10.67 o 4 8 1 1979.31 1859.41 36.32 o 5 8 1 1.80 6.03 5.19 o 6 8 1 724.33 704.37 26.61 o 7 8 1 119.76 125.70 16.05 o 8 8 1 299.02 314.15 28.19 o 9 8 1 108.19 95.47 15.79 o 1 9 1 2382.12 2179.63 40.60 o 2 9 1 120.12 131.24 9.08 o 3 9 1 1209.33 1184.13 32.56 o 4 9 1 148.76 157.11 14.12 o 5 9 1 391.51 397.30 20.79 o 6 9 1 126.47 134.40 14.19 o 7 9 1 588.92 598.73 30.83 o 8 9 1 169.65 157.10 19.99 o 0 10 1 2178.17 2234.88 78.13 o 1 10 1 60.09 53.72 8.80 o 2 10 1 22.12 28.44 7.81 o 3 10 1 34.33 31.59 7.65 o 4 10 1 1499.43 1490.06 36.59 o 5 10 1 30.98 35.62 7.14 o 6 10 1 537.07 509.83 25.17 o 7 10 1 130.80 150.84 17.88 o 8 10 1 18.02 27.11 8.28 o 1 11 1 424.65 436.69 20.68 o 2 11 1 66.76 67.58 10.65 o 3 11 1 59.03 64.63 12.34 o 4 11 1 .70 10.62 6.42 o 5 11 1 400.21 418.17 26.25 o 6 11 1 9.36 16.64 5.87 o 7 11 1 87.52 101.77 13.31 o 0 12 1 2104.25 2046.06 62.89 o 1 12 1 14.67 23.70 6.82 o 2 12 1 1367.43 1258.17 39.88 o 3 12 1 52.12 68.33 12.12 o 4 12 1 2907.97 2652.24 121.03 o 5 12 1 .75 10.04 6.80 o 6 12 1 1337.44 1348.92 59.28 o 1 13 1 1603.94 1565.67 42.95 o 2 13 1 92.35 87.88 13.27 o 3 13 1 934.75 886.73 35.22 o 4 13 1 19.51 23.67 7.91 o 5 13 1 452.21 461.78 30.96 o 0 14 1 427.45 430.50 40.16 o 1 14 1 88.19 81.12 12.40 o 2 14 1 98.14 108.63 15.57 o 3 14 1 1.96 12.25 6.58 o 4 14 1 173.48 182.62 18.84 o 1 15 1 328.36 347.65 28.16 o 0 0 2 14986.51 15273.55 394.78 o 1 0 2 668.97 678.37 12.67 o 2 0 2 5710.15 6167.15 157.26 o 3 0 2 4076.34 4261.07 87.19 o 4 0 2 10383.61 11521.58 174.82 o 5 0 2 849.70 979.19 29.20 o 6 0 2 5385.00 5494.86 165.71 o 7 0 2 52.86 61.25 10.76 o 8 0 2 8085.44 7855.80 189.74 o 9 0 2 .12 11.58 9.30 o 10 0 2 2253.69 2028.22 100.78 o 11 0 2 44.22 37.66 13.23 o 1 1 2 60.86 54.20 3.44 o 2 1 2 136.92 164.99 5.39 o 3 1 2 5047.71 5435.79 67.82 o 4 1 2 6.26 7.22 3.18 o 5 1 2 4266.95 4356.38 65.66 o 6 1 2 335.35 346.38 14.44 o 7 1 2 1958.00 1992.14 44.67 o 8 1 2 177.29 181.61 16.32 o 9 1 2 1415.06 1303.44 40.53 o 10 1 2 98.09 106.44 15.55 o 11 1 2 131.19 130.71 19.07 o 0 2 2 5.14 6.67 3.21 o 1 2 2 18.68 22.81 2.84 o 2 2 2 30.78 31.59 3.82 o 3 2 2 110.55 117.69 5.01 o 4 2 2 61.97 86.28 4.99 o 5 2 2 15.74 18.50 3.90 o 6 2 2 130.94 146.50 9.90 o 7 2 2 .06 8.64 4.86 o 8 2 2 195.37 207.36 17.35 o 9 2 2 .15 9.46 5.14 o 10 2 2 71.57 76.42 12.71 o 1 3 2 2324.36 2541.60 41.30 o 2 3 2 191.22 206.82 7.44 o 3 3 2 1539.87 1436.03 20.59 o 4 3 2 3.05 12.31 3.43 o 5 3 2 3307.04 3205.38 50.81 o 6 3 2 528.02 498.18 18.76 o 7 3 2 1678.79 1623.76 33.43 o 8 3 2 222.93 207.61 17.54 o 9 3 2 1515.21 1372.24 41.88 o 10 3 2 116.05 122.21 16.45 o 0 4 2 1778.36 1538.84 62.33 o 1 4 2 249.91 254.18 7.48 o 2 4 2 215.40 187.14 6.53 o 3 4 2 1986.12 1978.86 24.86 o 4 4 2 2320.35 2327.32 29.01 o 5 4 2 529.20 578.69 15.55 o 6 4 2 1310.96 1188.28 28.35 o 7 4 2 27.55 26.43 5.69 o 8 4 2 3848.93 3756.05 69.78 o 9 4 2 .23 5.60 5.52 o 10 4 2 971.58 878.92 40.99 o 1 5 2 13.07 14.90 3.04 o 2 5 2 14.73 19.91 3.09 o 3 5 2 801.35 799.02 16.68 o 4 5 2 37.15 37.96 5.93 o 5 5 2 385.41 382.43 13.92 o 6 5 2 47.32 62.99 8.32 o 7 5 2 285.59 311.09 16.54 o 8 5 2 96.14 93.19 14.89 o 9 5 2 303.33 316.68 28.09 o 10 5 2 37.72 33.18 9.28 o 0 6 2 1466.90 1382.84 54.26 o 1 6 2 59.91 59.57 4.91 o 2 6 2 721.49 715.56 15.31 o 3 6 2 366.38 345.30 10.05 o 4 6 2 1661.31 1595.12 33.58 o 5 6 2 63.12 73.09 7.84 o 6 6 2 1494.97 1457.13 33.28 o 7 6 2 .06 .39 5.33 o 8 6 2 1633.21 1558.13 51.08 o 9 6 2 .23 4.10 6.64 o 10 6 2 587.75 549.76 38.27 o 1 7 2 259.06 253.71 9.07 o 2 7 2 68.23 71.33 7.34 o 3 7 2 3935.08 3690.83 68.02 o 4 7 2 6.62 11.57 5.02 o 5 7 2 4712.27 4632.53 75.87 o 6 7 2 318.22 330.49 19.92 o 7 7 2 2607.99 2542.98 54.79 o 8 7 2 176.44 183.85 21.50 o 9 7 2 2305.12 2174.45 65.25 o 0 8 2 807.89 723.53 24.74 o 1 8 2 64.98 70.59 7.66 o 2 8 2 164.81 150.95 10.03 o 3 8 2 285.40 281.90 15.40 o 4 8 2 700.20 679.83 21.97 o 5 8 2 151.25 151.43 12.89 o 6 8 2 190.49 196.37 17.06 o 7 8 2 5.27 22.63 6.54 o 8 8 2 1319.19 1286.38 48.59 o 9 8 2 2.44 14.42 7.65 o 1 9 2 2.21 3.79 4.99 o 2 9 2 1.03 6.22 3.67 o 3 9 2 3.21 15.56 4.87 o 4 9 2 36.45 38.94 7.04 o 5 9 2 116.23 120.38 12.78 o 6 9 2 7.13 14.85 5.75 o 7 9 2 24.41 42.80 7.73 o 8 9 2 26.93 36.02 9.20 o 0 10 2 725.85 736.41 34.50 o 1 10 2 44.41 50.52 8.06 o 2 10 2 291.20 291.83 19.45 o 3 10 2 274.39 256.19 18.81 o 4 10 2 924.95 872.32 28.16 o 5 10 2 66.66 76.07 9.48 o 6 10 2 887.91 871.10 31.58 o 7 10 2 1.16 17.21 6.87 o 8 10 2 1415.91 1331.84 51.38 o 1 11 2 432.99 454.28 25.11 o 2 11 2 14.86 20.29 6.99 o 3 11 2 2085.05 1945.18 68.89 o 4 11 2 5.20 12.70 6.33 o 5 11 2 2173.48 2174.18 93.41 o 6 11 2 126.54 144.19 14.78 o 7 11 2 1391.76 1307.77 46.39 o 0 12 2 419.86 407.07 36.12 o 1 12 2 32.62 30.01 7.59 o 2 12 2 181.07 179.59 16.97 o 3 12 2 7.14 12.45 6.89 o 4 12 2 275.17 301.56 24.13 o 5 12 2 28.55 38.77 7.69 o 6 12 2 13.92 32.96 9.75 o 1 13 2 39.00 51.51 9.02 o 2 13 2 6.14 13.86 6.37 o 3 13 2 86.05 99.83 13.76 o 4 13 2 21.10 25.59 7.77 o 5 13 2 510.38 513.39 32.30 o 0 14 2 273.45 344.62 36.05 o 1 14 2 23.71 35.78 8.31 o 2 14 2 80.14 98.36 13.06 o 3 14 2 144.09 171.61 18.53 o 1 1 3 10124.71 10911.92 226.95 o 2 1 3 1085.49 1119.74 19.09 o 3 1 3 606.13 652.13 11.97 o 4 1 3 816.81 818.88 20.23 o 5 1 3 3512.17 3655.25 63.47 o 6 1 3 320.99 333.41 14.50 o 7 1 3 658.20 621.45 21.70 o 8 1 3 32.29 38.88 8.26 o 9 1 3 2122.39 1999.09 50.99 o 10 1 3 115.19 123.68 15.86 o 0 2 3 57.43 67.27 5.01 o 1 2 3 1762.13 1725.07 28.92 o 2 2 3 2733.12 2721.54 40.10 o 3 2 3 32.14 48.84 4.67 o 4 2 3 4396.99 4578.00 58.82 o 5 2 3 388.69 411.04 13.87 o 6 2 3 161.44 166.12 13.60 o 7 2 3 171.50 178.47 14.37 o 8 2 3 2609.64 2462.11 47.31 o 9 2 3 6.23 16.74 6.18 o 10 2 3 372.15 322.32 27.46 o 1 3 3 968.78 870.66 14.93 o 2 3 3 150.02 142.84 7.20 o 3 3 3 185.69 210.92 9.16 o 4 3 3 259.49 265.07 10.76 o 5 3 3 640.39 605.21 16.91 o 6 3 3 213.63 215.90 14.50 o 7 3 3 9.84 14.27 5.83 o 8 3 3 .55 13.89 5.54 o 9 3 3 502.12 524.92 26.04 o 10 3 3 46.65 43.78 9.43 o 0 4 3 803.43 738.30 23.88 o 1 4 3 27.01 29.59 3.91 o 2 4 3 484.40 440.59 11.93 o 3 4 3 30.61 34.80 5.39 o 4 4 3 591.41 579.65 15.29 o 5 4 3 48.01 57.45 6.26 o 6 4 3 100.55 106.07 11.01 o 7 4 3 1.34 5.03 4.52 o 8 4 3 146.54 167.23 14.53 o 9 4 3 16.37 20.57 6.78 o 10 4 3 119.72 133.00 19.54 o 1 5 3 10134.12 9596.30 254.27 o 2 5 3 939.85 878.22 15.50 o 3 5 3 1613.98 1565.03 30.17 o 4 5 3 720.96 712.54 17.62 o 5 5 3 3887.84 3953.30 43.11 o 6 5 3 323.89 322.06 17.20 o 7 5 3 1010.87 974.35 28.49 o 8 5 3 56.82 64.27 11.31 o 9 5 3 2606.52 2507.30 67.40 o 10 5 3 127.96 100.84 15.44 o 0 6 3 1942.35 1841.88 69.33 o 1 6 3 655.25 581.09 17.19 o 2 6 3 4511.02 4488.74 77.72 o 3 6 3 .02 5.83 3.10 o 4 6 3 4911.24 4948.88 83.99 o 5 6 3 126.36 146.02 9.83 o 6 6 3 722.94 750.47 26.47 o 7 6 3 107.13 106.23 12.31 o 8 6 3 2791.30 2708.34 63.80 o 9 6 3 .15 7.62 7.50 o 1 7 3 141.38 131.27 7.83 o 2 7 3 27.16 34.54 4.27 o 3 7 3 40.15 42.67 7.26 o 4 7 3 22.45 30.06 6.72 o 5 7 3 199.48 210.32 13.87 o 6 7 3 101.89 107.02 12.70 o 7 7 3 6.32 11.13 5.96 o 8 7 3 15.34 20.18 6.67 o 9 7 3 61.68 84.52 14.59 o 0 8 3 728.80 641.28 22.01 o 1 8 3 42.14 52.46 7.02 o 2 8 3 428.74 388.33 16.37 o 3 8 3 24.67 19.46 5.62 o 4 8 3 788.37 776.03 23.71 o 5 8 3 58.86 58.98 8.14 o 6 8 3 168.52 180.07 17.82 o 7 8 3 2.52 7.58 5.74 o 8 8 3 357.87 353.35 29.88 o 9 8 3 23.13 32.21 9.59 o 1 9 3 1434.41 1334.25 33.74 o 2 9 3 218.11 201.76 14.18 o 3 9 3 87.92 104.69 11.01 o 4 9 3 345.47 338.97 18.61 o 5 9 3 788.13 794.43 25.47 o 6 9 3 243.31 250.04 21.09 o 7 9 3 163.02 186.80 18.45 o 8 9 3 30.42 34.09 9.97 o 0 10 3 6.51 24.49 9.09 o 1 10 3 174.67 175.52 15.68 o 2 10 3 294.23 339.46 20.62 o 3 10 3 12.87 14.34 6.35 o 4 10 3 564.40 581.88 22.33 o 5 10 3 17.87 24.77 5.54 o 6 10 3 26.01 33.58 7.33 o 7 10 3 43.05 43.59 8.35 o 8 10 3 740.14 731.72 39.56 o 1 11 3 250.68 268.30 19.56 o 2 11 3 102.37 99.18 12.63 o 3 11 3 326.89 325.81 21.62 o 4 11 3 2.05 14.08 6.50 o 5 11 3 23.71 48.54 9.18 o 6 11 3 28.36 37.76 8.06 o 7 11 3 145.56 174.33 16.74 o 0 12 3 1596.84 1532.81 61.93 o 1 12 3 45.05 56.05 8.82 o 2 12 3 1125.53 1132.85 35.82 o 3 12 3 3.33 15.82 5.58 o 4 12 3 1632.14 1589.19 78.98 o 5 12 3 18.01 38.81 8.38 o 6 12 3 618.69 636.14 40.31 o 1 13 3 906.37 922.91 37.07 o 2 13 3 11.30 21.07 5.68 o 3 13 3 243.39 253.18 21.51 o 4 13 3 121.02 110.58 15.72 o 5 13 3 683.08 678.74 37.68 o 0 14 3 39.59 46.86 14.67 o 1 14 3 49.23 76.05 12.05 o 2 14 3 13.05 22.08 8.99 o 3 14 3 22.03 29.51 8.83 o 0 0 4 20733.74 21955.69 712.32 o 1 0 4 14.29 33.34 4.65 o 2 0 4 17021.71 17928.53 487.82 o 3 0 4 310.12 383.15 14.25 o 4 0 4 8930.25 9064.58 119.85 o 5 0 4 1001.22 978.33 31.06 o 6 0 4 1526.01 1573.31 46.74 o 7 0 4 731.05 707.28 34.46 o 8 0 4 3946.22 4158.41 96.14 o 9 0 4 .50 -.93 9.07 o 10 0 4 771.11 771.63 47.45 o 1 1 4 11063.73 11642.35 279.29 o 2 1 4 2819.07 3135.17 54.75 o 3 1 4 178.40 134.93 6.81 o 4 1 4 305.95 339.83 9.42 o 5 1 4 5998.68 6055.58 133.76 o 6 1 4 279.54 271.15 15.81 o 7 1 4 11.29 20.16 5.18 o 8 1 4 25.55 29.41 6.96 o 9 1 4 679.93 661.33 30.01 o 10 1 4 1.09 8.58 6.94 o 0 2 4 469.33 453.44 16.55 o 1 2 4 7.60 8.03 2.81 o 2 2 4 106.81 104.04 6.60 o 3 2 4 24.06 33.65 4.37 o 4 2 4 75.21 84.20 6.29 o 5 2 4 53.64 54.35 8.81 o 6 2 4 17.83 24.70 6.69 o 7 2 4 15.08 27.16 6.77 o 8 2 4 38.91 46.81 8.17 o 9 2 4 1.47 1.88 5.60 o 10 2 4 40.23 51.49 9.42 o 1 3 4 6745.93 6842.55 151.40 o 2 3 4 3981.12 4200.48 69.52 o 3 3 4 15.37 49.81 5.89 o 4 3 4 664.53 667.30 16.17 o 5 3 4 4179.61 4189.38 59.69 o 6 3 4 367.06 362.86 18.05 o 7 3 4 57.13 71.12 10.35 o 8 3 4 34.93 38.71 6.75 o 9 3 4 551.31 547.68 29.12 o 10 3 4 .11 3.34 6.28 o 0 4 4 4688.26 4381.19 141.67 o 1 4 4 7.94 14.69 3.77 o 2 4 4 4212.25 4006.19 58.72 o 3 4 4 124.04 141.98 9.02 o 4 4 4 2463.49 2241.10 42.49 o 5 4 4 580.07 531.53 17.19 o 6 4 4 215.64 213.47 15.88 o 7 4 4 510.96 512.06 22.32 o 8 4 4 1730.67 1817.07 40.01 o 9 4 4 .62 5.20 5.61 o 10 4 4 215.21 262.36 28.98 o 1 5 4 1495.48 1459.95 37.52 o 2 5 4 395.12 400.27 11.36 o 3 5 4 135.42 151.28 9.72 o 4 5 4 .04 6.13 3.57 o 5 5 4 1987.03 1977.08 33.59 o 6 5 4 85.68 86.95 10.27 o 7 5 4 21.23 32.51 6.51 o 8 5 4 21.05 33.18 7.55 o 9 5 4 202.84 199.34 22.01 o 10 5 4 .52 11.15 8.14 o 0 6 4 4958.67 4996.15 150.49 o 1 6 4 29.07 28.07 4.58 o 2 6 4 2181.56 2089.72 48.88 o 3 6 4 92.45 96.63 8.50 o 4 6 4 1491.52 1493.66 27.21 o 5 6 4 281.23 278.23 14.11 o 6 6 4 501.62 521.78 23.87 o 7 6 4 115.37 119.47 13.88 o 8 6 4 476.15 538.73 29.91 o 9 6 4 1.69 2.37 7.21 o 1 7 4 8192.32 8060.31 152.92 o 2 7 4 2007.97 1846.90 50.51 o 3 7 4 936.24 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3 0 10 62.44 69.51 19.36 o 4 0 10 4319.94 4010.30 154.12 o 5 0 10 .68 12.64 11.13 o 6 0 10 1286.78 1286.39 71.48 o 7 0 10 36.54 27.08 13.81 o 1 1 10 1674.00 1623.78 39.06 o 2 1 10 178.39 186.15 16.92 o 3 1 10 1052.61 979.68 37.14 o 4 1 10 52.45 45.30 11.24 o 5 1 10 468.87 435.07 32.54 o 6 1 10 5.83 12.16 8.54 o 7 1 10 224.68 281.94 28.94 o 0 2 10 98.44 104.56 17.19 o 1 2 10 .43 5.15 5.59 o 2 2 10 51.13 68.84 10.15 o 3 2 10 10.14 18.93 7.33 o 4 2 10 63.78 66.16 13.15 o 5 2 10 1.69 10.63 7.89 o 6 2 10 19.86 26.36 9.71 o 7 2 10 .09 5.75 8.95 o 1 3 10 1480.38 1454.09 39.56 o 2 3 10 292.46 299.72 20.79 o 3 3 10 743.96 694.08 31.86 o 4 3 10 14.59 14.99 6.35 o 5 3 10 307.54 294.92 27.37 o 6 3 10 11.93 11.88 8.25 o 0 4 10 3470.80 3446.32 104.53 o 1 4 10 .19 11.34 6.41 o 2 4 10 484.13 538.03 25.65 o 3 4 10 41.45 54.09 10.96 o 4 4 10 1909.24 1781.04 57.77 o 5 4 10 .25 17.70 6.97 o 6 4 10 399.62 454.64 34.74 o 1 5 10 239.01 249.36 20.55 o 2 5 10 55.36 71.37 10.00 o 3 5 10 214.86 202.00 20.83 o 4 5 10 64.30 65.86 11.64 o 5 5 10 71.06 63.97 11.98 o 6 5 10 13.88 24.84 8.34 o 0 6 10 1233.50 1267.62 57.20 o 1 6 10 .47 13.44 6.32 o 2 6 10 755.83 800.87 29.91 o 3 6 10 28.91 37.11 9.17 o 4 6 10 796.64 848.73 36.23 o 5 6 10 .01 9.72 8.81 o 1 7 10 2539.18 2506.77 58.28 o 2 7 10 199.28 232.96 19.93 o 3 7 10 1497.78 1456.13 55.39 o 4 7 10 17.25 23.46 8.73 o 5 7 10 847.10 872.32 44.38 o 0 8 10 1443.14 1457.27 62.52 o 1 8 10 .01 6.71 6.93 o 2 8 10 86.32 127.57 18.27 o 3 8 10 1.28 17.57 9.32 o 4 8 10 792.51 873.63 43.70 o 1 9 10 24.24 39.07 11.13 o 2 9 10 2.72 12.02 6.72 o 1 1 11 1985.86 1875.69 44.08 o 2 1 11 4.10 20.66 7.10 o 3 1 11 1430.78 1295.72 48.50 o 4 1 11 19.05 19.57 8.30 o 5 1 11 683.16 635.03 40.06 o 6 1 11 1.15 16.63 9.66 o 0 2 11 2124.14 2076.66 71.43 o 1 2 11 10.38 14.90 5.82 o 2 2 11 1806.93 1658.03 50.17 o 3 2 11 .60 17.80 6.75 o 4 2 11 958.25 849.33 40.36 o 5 2 11 6.66 13.25 8.34 o 1 3 11 290.19 303.78 22.05 o 2 3 11 .05 14.58 6.57 o 3 3 11 228.46 233.56 23.15 o 4 3 11 2.99 9.56 7.53 o 5 3 11 87.99 104.35 16.44 o 0 4 11 472.48 496.78 39.79 o 1 4 11 5.64 9.79 5.83 o 2 4 11 259.68 290.05 23.23 o 3 4 11 .51 6.75 6.66 o 4 4 11 120.88 128.51 16.43 o 5 4 11 4.01 13.87 8.44 o 1 5 11 2636.32 2613.89 63.76 o 2 5 11 8.32 21.64 6.82 o 3 5 11 1952.76 1928.25 56.58 o 4 5 11 27.65 32.27 8.09 o 0 6 11 2067.40 2067.64 77.05 o 1 6 11 2.30 7.85 6.64 o 2 6 11 1891.27 1798.25 53.83 o 3 6 11 .42 20.76 7.36 o 4 6 11 1256.84 1231.57 45.65 o 1 7 11 3.84 22.41 6.97 o 2 7 11 .74 8.40 7.19 o 3 7 11 19.99 28.56 10.10 o 0 8 11 917.60 876.59 48.36 o 1 8 11 8.20 20.34 7.92 o 0 0 12 495.24 482.97 52.65 o 1 0 12 78.96 98.02 17.24 o 2 0 12 1579.46 1486.66 110.60 o 3 0 12 1.40 8.28 10.36 o 4 0 12 1985.88 1802.93 87.40 o 1 1 12 449.93 476.32 26.21 o 2 1 12 47.20 59.41 11.84 o 3 1 12 157.44 157.30 20.97 o 4 1 12 122.03 162.91 20.99 o 0 2 12 7.56 15.21 9.09 o 1 2 12 2.78 2.74 5.67 o 2 2 12 10.78 16.43 7.48 o 3 2 12 .01 5.93 7.26 o 4 2 12 37.09 40.62 11.10 o 1 3 12 197.59 211.98 19.16 o 2 3 12 46.97 57.16 10.71 o 3 3 12 55.91 66.09 12.93 o 4 3 12 156.29 168.13 20.26 o 0 4 12 46.14 52.80 13.71 o 1 4 12 53.81 54.21 9.44 o 2 4 12 506.40 513.05 31.99 o 3 4 12 .26 11.71 7.08 o 1 5 12 120.73 123.24 15.03 o 2 5 12 17.84 41.58 10.89 o 0 6 12 231.95 273.22 32.15 o 1 6 12 22.30 37.05 7.70 o 1 1 13 407.18 416.93 32.54 o 0 2 13 96.33 86.07 15.25 o