#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/13/2211395.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211395_Fobs loop_ _publ_author_name 'Li, X.' 'Hu, Y.' 'Gao, Y.' 'Zhang, G. G. Z.' 'Henry, R. F.' _publ_section_title ; A methanol hemisolvate of ciprofloxacin ; _journal_coeditor_code FL2076 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5803 _journal_page_last o5805 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.941 _cell_angle_gamma 90.000 _cell_length_a 26.0361 _cell_length_b 12.6971 _cell_length_c 10.2348 _exptl_crystal_F_000 1464.00 _reflns_d_resolution_high 0.7485 _[local]_cod_data_source_file fl2076Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' x956t in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 299.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 605.49 475.03 7.42 o 4 0 0 28001.52 27808.04 530.10 o 6 0 0 14846.36 16904.55 363.08 o 8 0 0 6911.69 7528.50 149.18 o 10 0 0 6476.86 7000.68 162.62 o 12 0 0 11681.92 13600.08 384.57 o 14 0 0 101.05 117.24 15.15 o 16 0 0 36.11 59.99 14.88 o 18 0 0 864.43 769.47 33.87 o 20 0 0 25626.66 24227.22 1810.09 o 22 0 0 5694.47 5571.48 192.56 o 24 0 0 802.48 782.49 40.29 o 26 0 0 13.34 24.71 29.05 o 28 0 0 117.30 139.69 32.87 o 30 0 0 329.05 451.76 71.54 o 1 1 0 2602.57 2724.50 24.17 o 3 1 0 112.16 123.97 4.18 o 5 1 0 3234.28 3214.32 28.17 o 7 1 0 2906.80 2769.83 37.62 o 9 1 0 283.19 309.90 10.81 o 11 1 0 13.81 20.49 6.63 o 13 1 0 313.46 293.60 13.03 o 15 1 0 209.25 261.34 13.06 o 17 1 0 54.94 53.98 9.55 o 19 1 0 382.66 394.13 23.54 o 21 1 0 7116.84 7039.89 206.66 o 23 1 0 1.60 5.35 10.08 o 25 1 0 291.09 266.66 21.63 o 27 1 0 17.51 19.71 15.06 o 29 1 0 17.85 33.76 24.37 o 31 1 0 348.11 422.28 67.63 o 0 2 0 45200.55 51500.84 892.55 o 2 2 0 9890.49 10453.35 182.72 o 4 2 0 34035.95 36366.21 544.62 o 6 2 0 2122.92 2064.84 40.40 o 8 2 0 510.12 554.08 12.01 o 10 2 0 6937.24 7272.25 82.51 o 12 2 0 45.75 101.70 8.71 o 14 2 0 1758.91 1814.61 26.99 o 16 2 0 1051.75 1018.43 22.25 o 18 2 0 372.54 330.09 16.09 o 20 2 0 6777.84 6640.26 132.39 o 22 2 0 2423.83 2400.18 46.92 o 24 2 0 127.10 133.54 19.13 o 26 2 0 93.89 94.15 19.76 o 28 2 0 347.64 354.18 35.42 o 30 2 0 549.68 659.27 56.72 o 32 2 0 104.80 139.17 49.43 o 1 3 0 7136.78 8277.68 128.16 o 3 3 0 8188.49 9364.45 152.31 o 5 3 0 5114.88 5644.74 81.20 o 7 3 0 5709.85 5840.22 85.85 o 9 3 0 4408.34 4733.05 63.99 o 11 3 0 8238.50 9241.37 104.23 o 13 3 0 247.13 251.52 11.26 o 15 3 0 2308.78 2650.45 37.17 o 17 3 0 50.82 47.01 8.93 o 19 3 0 803.03 755.57 21.73 o 21 3 0 4693.67 4746.44 100.53 o 23 3 0 16.56 8.85 12.22 o 25 3 0 128.53 159.72 20.93 o 27 3 0 233.20 256.13 26.59 o 29 3 0 19.96 3.76 20.31 o 31 3 0 63.00 118.34 35.29 o 0 4 0 21177.00 24314.51 533.82 o 2 4 0 164.12 213.41 8.42 o 4 4 0 9185.92 9761.90 172.14 o 6 4 0 528.23 537.24 13.44 o 8 4 0 3060.34 3533.97 73.72 o 10 4 0 762.36 684.33 15.97 o 12 4 0 1169.93 1317.43 31.97 o 14 4 0 142.70 119.03 9.58 o 16 4 0 16.18 26.79 7.43 o 18 4 0 70.07 96.25 12.65 o 20 4 0 721.09 737.16 27.74 o 22 4 0 81.21 93.74 17.17 o 24 4 0 108.95 106.58 18.70 o 26 4 0 252.11 224.38 22.74 o 28 4 0 105.04 124.18 27.35 o 30 4 0 3.55 6.56 22.54 o 32 4 0 162.16 275.31 64.17 o 1 5 0 16659.04 19619.02 320.57 o 3 5 0 1705.44 1681.06 34.04 o 5 5 0 203.86 244.55 9.59 o 7 5 0 778.39 876.40 16.11 o 9 5 0 1525.32 1594.94 43.64 o 11 5 0 17386.26 19873.81 439.19 o 13 5 0 566.26 618.96 19.06 o 15 5 0 136.11 125.09 12.31 o 17 5 0 15.13 15.20 10.15 o 19 5 0 631.76 544.27 24.47 o 21 5 0 590.57 576.41 29.77 o 23 5 0 256.67 213.19 21.42 o 25 5 0 1.15 3.00 12.07 o 27 5 0 20.06 19.79 15.73 o 29 5 0 0.82 5.12 22.68 o 31 5 0 1342.49 1672.84 96.41 o 0 6 0 1628.00 1837.06 55.54 o 2 6 0 8599.71 10217.52 174.14 o 4 6 0 545.42 555.30 14.37 o 6 6 0 7.52 16.16 5.88 o 8 6 0 663.21 715.94 19.40 o 10 6 0 643.75 658.25 18.44 o 12 6 0 1218.92 1344.83 26.90 o 14 6 0 1608.72 1626.07 36.50 o 16 6 0 231.04 195.85 17.17 o 18 6 0 194.27 153.54 17.38 o 20 6 0 64.68 38.14 14.39 o 22 6 0 1515.22 1265.62 43.58 o 24 6 0 45.66 45.99 15.61 o 26 6 0 128.29 146.84 29.39 o 28 6 0 17.15 12.31 15.97 o 30 6 0 4.04 4.12 19.21 o 1 7 0 48.60 45.81 7.40 o 3 7 0 34.88 25.42 6.90 o 5 7 0 3405.21 3820.22 63.78 o 7 7 0 4245.00 4737.94 79.80 o 9 7 0 90.60 106.82 13.43 o 11 7 0 4055.51 4179.72 138.28 o 13 7 0 676.03 655.93 28.66 o 15 7 0 50.17 53.58 12.77 o 17 7 0 1087.20 1037.46 33.34 o 19 7 0 571.28 473.05 28.01 o 21 7 0 69.32 52.72 18.16 o 23 7 0 213.17 144.45 24.26 o 25 7 0 64.70 57.08 20.08 o 27 7 0 4.94 6.66 16.88 o 29 7 0 41.05 40.57 19.74 o 31 7 0 282.60 398.00 68.94 o 0 8 0 2401.19 3024.16 79.98 o 2 8 0 839.03 977.98 27.02 o 4 8 0 729.29 774.58 19.08 o 6 8 0 15.07 1.75 7.93 o 8 8 0 4617.03 4708.54 100.07 o 10 8 0 144.25 161.27 15.47 o 12 8 0 41.94 36.57 11.86 o 14 8 0 98.16 110.46 15.91 o 16 8 0 42.66 54.55 13.38 o 18 8 0 52.53 53.42 15.48 o 20 8 0 513.15 412.81 27.98 o 22 8 0 5.07 4.56 12.91 o 24 8 0 118.42 113.17 24.38 o 26 8 0 386.40 355.18 33.45 o 28 8 0 389.75 429.64 36.74 o 1 9 0 2923.27 3350.32 104.18 o 3 9 0 1065.08 1284.51 28.84 o 5 9 0 506.53 570.67 23.24 o 7 9 0 1331.65 1325.19 49.83 o 9 9 0 6.18 5.36 10.22 o 11 9 0 4.01 1.02 9.84 o 13 9 0 766.76 723.27 28.93 o 15 9 0 696.79 659.96 28.27 o 17 9 0 1204.00 1125.29 41.53 o 19 9 0 93.40 71.14 17.39 o 21 9 0 146.81 129.88 21.37 o 23 9 0 34.76 42.14 19.38 o 25 9 0 98.90 105.23 24.06 o 27 9 0 128.92 139.26 26.65 o 0 10 0 9.38 12.23 11.94 o 2 10 0 176.70 160.51 15.91 o 4 10 0 547.10 486.45 23.07 o 6 10 0 581.17 552.46 24.97 o 8 10 0 206.89 226.34 18.48 o 10 10 0 326.36 297.74 20.62 o 12 10 0 1576.41 1511.92 41.06 o 14 10 0 53.02 56.38 14.42 o 16 10 0 4.24 9.47 12.69 o 18 10 0 31.10 35.09 15.31 o 20 10 0 30.83 23.58 16.62 o 22 10 0 242.45 229.34 28.53 o 24 10 0 190.35 219.24 30.04 o 26 10 0 36.01 74.44 20.40 o 1 11 0 317.50 324.72 22.98 o 3 11 0 31.48 30.29 11.85 o 5 11 0 7.76 4.15 10.71 o 7 11 0 67.60 55.81 13.78 o 9 11 0 635.86 676.93 29.15 o 11 11 0 1489.29 1460.88 45.14 o 13 11 0 3853.68 3998.22 113.07 o 15 11 0 29.94 16.99 13.56 o 17 11 0 39.61 62.69 17.21 o 19 11 0 65.21 45.93 18.39 o 21 11 0 426.23 381.96 33.37 o 23 11 0 11.86 20.02 16.52 o 25 11 0 59.20 124.27 33.40 o 0 12 0 1997.32 1763.13 80.16 o 2 12 0 295.62 295.86 28.66 o 4 12 0 208.32 240.74 19.92 o 6 12 0 410.76 441.20 24.69 o 8 12 0 5029.30 5096.06 152.53 o 10 12 0 12.04 10.13 12.21 o 12 12 0 3554.09 3560.81 94.88 o 14 12 0 287.78 280.70 25.48 o 16 12 0 76.74 64.21 18.22 o 18 12 0 112.12 146.62 25.88 o 20 12 0 0.40 1.62 13.91 o 22 12 0 184.32 226.07 26.88 o 1 13 0 503.87 430.75 32.21 o 3 13 0 586.25 500.28 34.76 o 5 13 0 10.48 4.78 15.14 o 7 13 0 66.48 34.29 16.04 o 9 13 0 1327.05 1362.03 44.56 o 11 13 0 8.07 12.66 13.54 o 13 13 0 699.46 754.50 38.32 o 15 13 0 515.00 485.99 43.83 o 17 13 0 18.06 30.96 16.18 o 19 13 0 0.61 11.28 15.00 o 21 13 0 177.76 290.25 41.85 o 0 14 0 516.03 440.56 57.01 o 2 14 0 213.54 231.66 28.95 o 4 14 0 580.86 547.01 37.99 o 6 14 0 16.47 15.22 17.76 o 8 14 0 281.38 258.51 29.48 o 10 14 0 0.00 -3.29 13.99 o 12 14 0 327.14 332.08 28.40 o 14 14 0 153.33 172.57 28.35 o 16 14 0 210.15 293.18 31.04 o 18 14 0 45.66 77.41 27.53 o 1 15 0 332.30 285.66 31.67 o 3 15 0 51.29 12.83 18.10 o 5 15 0 567.55 610.55 42.13 o 7 15 0 225.53 226.79 32.92 o 9 15 0 395.22 386.13 41.80 o 11 15 0 0.80 13.09 21.34 o 13 15 0 9.75 28.86 19.45 o 15 15 0 95.34 105.77 28.02 o 0 16 0 232.72 168.18 42.65 o 2 16 0 136.25 161.20 30.07 o 4 16 0 12.18 0.96 17.79 o 6 16 0 189.71 168.90 30.50 o 8 16 0 62.75 64.76 24.49 o 10 16 0 8.06 38.59 35.55 o -33 1 1 91.66 118.87 29.50 o -31 1 1 1139.65 1241.40 77.10 o -29 1 1 513.35 496.88 39.67 o -27 1 1 433.05 455.16 31.36 o -25 1 1 147.72 152.91 22.89 o -23 1 1 1939.69 1921.23 42.18 o -21 1 1 67.62 65.71 11.85 o -19 1 1 160.19 162.29 13.18 o -17 1 1 2229.07 2311.28 51.48 o -15 1 1 768.09 705.71 18.74 o -13 1 1 647.53 607.58 16.23 o -11 1 1 6213.07 6028.23 115.40 o -9 1 1 81.20 88.99 6.87 o -7 1 1 1226.93 1257.44 23.40 o -5 1 1 12099.87 12855.46 126.62 o -3 1 1 330.68 279.87 6.72 o -1 1 1 10709.69 11527.06 153.51 o 1 1 1 10874.50 12204.21 180.84 o 3 1 1 10.59 34.37 3.62 o 5 1 1 1953.62 1950.04 31.70 o 7 1 1 495.16 406.11 11.40 o 9 1 1 4676.92 4660.64 80.96 o 11 1 1 5663.36 6184.67 104.25 o 13 1 1 1586.20 1730.40 32.07 o 15 1 1 585.53 531.89 17.89 o 17 1 1 236.22 205.87 13.64 o 19 1 1 639.21 592.57 23.13 o 21 1 1 4917.72 4673.37 75.43 o 23 1 1 11.98 20.95 10.04 o 25 1 1 367.51 368.69 22.28 o 27 1 1 452.63 464.11 37.20 o -34 2 1 985.57 1318.01 115.33 o -32 2 1 803.61 851.21 76.31 o -30 2 1 725.01 787.03 62.87 o -28 2 1 3.00 -7.95 15.01 o -26 2 1 59.13 34.26 15.96 o -24 2 1 459.69 406.35 24.99 o -22 2 1 6856.01 6356.14 216.28 o -20 2 1 87.04 104.84 13.40 o -18 2 1 11.91 5.25 7.24 o -16 2 1 711.95 684.74 18.32 o -14 2 1 3562.43 3573.49 47.42 o -12 2 1 1700.12 1556.44 26.59 o -10 2 1 18136.42 20478.64 187.47 o -8 2 1 2244.60 2438.11 34.58 o -6 2 1 10126.77 11014.23 125.28 o -4 2 1 14907.61 15872.70 232.20 o -2 2 1 13231.40 13416.75 289.93 o 0 2 1 20894.10 22137.88 412.05 o 2 2 1 8241.20 10073.18 157.99 o 4 2 1 19487.11 21006.14 334.17 o 6 2 1 1588.63 1550.20 31.97 o 8 2 1 7010.42 7397.81 130.04 o 10 2 1 66309.84 74252.29 931.71 o 12 2 1 2389.29 2788.39 38.31 o 14 2 1 3563.82 3769.45 56.45 o 16 2 1 2771.76 2791.39 39.16 o 18 2 1 1618.35 1523.30 36.28 o 20 2 1 671.85 660.47 21.60 o 22 2 1 2790.96 2611.79 42.29 o 24 2 1 30.70 29.59 13.41 o 26 2 1 487.19 395.82 34.74 o 28 2 1 274.19 249.42 31.21 o 30 2 1 1806.64 2220.58 100.39 o -33 3 1 582.83 655.97 84.11 o -31 3 1 1682.87 1828.27 75.48 o -29 3 1 19.80 24.63 18.92 o -27 3 1 85.53 65.46 22.56 o -25 3 1 922.72 899.41 40.77 o -23 3 1 2300.22 2164.41 47.12 o -21 3 1 403.50 382.91 21.36 o -19 3 1 71.18 92.76 13.76 o -17 3 1 9.51 14.49 7.72 o -15 3 1 178.93 169.48 10.69 o -13 3 1 658.93 600.33 15.50 o -11 3 1 25135.67 30353.61 480.34 o -9 3 1 559.41 571.58 12.15 o -7 3 1 1926.94 2134.73 49.56 o -5 3 1 1319.00 1545.25 26.12 o -3 3 1 2744.11 2679.15 48.67 o -1 3 1 17429.36 18442.62 337.53 o 1 3 1 89778.02 92748.31 1333.76 o 3 3 1 13845.27 13917.30 187.96 o 5 3 1 2069.54 2315.01 37.99 o 7 3 1 446.02 289.02 9.19 o 9 3 1 13521.30 15022.22 197.11 o 11 3 1 155.64 94.30 8.49 o 13 3 1 2354.91 2369.44 41.62 o 15 3 1 295.70 329.88 13.92 o 17 3 1 2061.24 1995.95 32.36 o 19 3 1 50.09 60.26 10.47 o 21 3 1 4001.37 3618.21 58.65 o 23 3 1 75.17 100.25 16.11 o 25 3 1 132.47 107.86 25.01 o 27 3 1 19.36 35.92 20.35 o 29 3 1 143.33 162.75 30.68 o 31 3 1 85.18 145.07 40.07 o -32 4 1 54.38 99.76 33.54 o -30 4 1 4.02 11.23 18.59 o -28 4 1 56.81 57.98 22.39 o -26 4 1 47.10 27.77 14.62 o -24 4 1 13.43 18.32 13.57 o -22 4 1 846.19 742.15 32.65 o -20 4 1 184.46 185.87 16.81 o -18 4 1 4761.87 4899.18 66.48 o -16 4 1 10.24 8.44 7.98 o -14 4 1 43.16 56.51 7.94 o -12 4 1 2177.63 2525.81 46.31 o -10 4 1 2996.32 3555.14 66.15 o -8 4 1 710.30 804.62 20.56 o -6 4 1 85.09 95.41 8.17 o -4 4 1 12544.96 13945.11 246.07 o -2 4 1 943.57 753.91 14.83 o 0 4 1 2.42 -2.46 4.43 o 2 4 1 313.00 407.06 10.05 o 4 4 1 1530.30 1571.43 34.00 o 6 4 1 267.42 236.61 10.41 o 8 4 1 419.53 429.16 11.09 o 10 4 1 360.93 331.83 11.45 o 12 4 1 4370.36 4733.85 54.79 o 14 4 1 86.23 90.99 9.51 o 16 4 1 1991.37 1988.40 32.64 o 18 4 1 6.23 10.41 9.94 o 20 4 1 844.81 795.47 28.95 o 22 4 1 1082.29 1068.18 41.07 o 24 4 1 566.87 561.64 35.92 o 26 4 1 392.80 333.62 29.83 o 28 4 1 143.92 144.67 25.64 o 30 4 1 62.39 64.81 31.64 o 32 4 1 205.42 234.78 48.89 o -31 5 1 271.54 334.45 46.41 o -29 5 1 251.65 235.52 29.45 o -27 5 1 247.18 219.48 23.97 o -25 5 1 8.88 3.95 12.70 o -23 5 1 145.89 128.07 19.80 o -21 5 1 144.51 147.23 19.92 o -19 5 1 13.32 32.28 13.77 o -17 5 1 966.21 937.60 25.66 o -15 5 1 1058.44 1105.64 46.45 o -13 5 1 963.11 1033.24 26.95 o -11 5 1 5333.80 5864.29 98.71 o -9 5 1 3.07 -0.25 6.45 o -7 5 1 5.90 10.59 7.00 o -5 5 1 33.08 23.35 5.79 o -3 5 1 6627.03 7248.35 134.45 o -1 5 1 114.80 155.45 9.43 o 1 5 1 44.19 84.70 7.24 o 3 5 1 7160.22 7956.16 157.29 o 5 5 1 834.58 886.54 18.74 o 7 5 1 1242.88 1236.29 22.33 o 9 5 1 6570.95 7189.10 87.73 o 11 5 1 204.54 201.91 9.76 o 13 5 1 37.15 42.03 8.94 o 15 5 1 368.23 362.89 20.36 o 17 5 1 1240.31 1263.72 34.33 o 19 5 1 88.25 67.64 14.11 o 21 5 1 2928.70 2596.50 56.46 o 23 5 1 417.56 400.47 30.53 o 25 5 1 52.90 80.70 20.87 o 27 5 1 14.41 25.47 17.30 o 29 5 1 51.46 78.52 21.54 o 31 5 1 129.04 159.57 42.14 o -32 6 1 0.15 7.37 34.68 o -30 6 1 62.05 40.05 20.88 o -28 6 1 0.54 0.99 15.21 o -26 6 1 6.04 16.47 14.21 o -24 6 1 499.03 463.70 29.73 o -22 6 1 1008.99 839.68 36.52 o -20 6 1 2143.37 1996.97 51.66 o -18 6 1 94.56 89.36 16.74 o -16 6 1 576.84 626.71 24.91 o -14 6 1 752.78 695.67 21.60 o -12 6 1 559.52 601.93 19.47 o -10 6 1 502.55 582.68 22.20 o -8 6 1 964.07 976.05 22.03 o -6 6 1 801.82 899.46 26.67 o -4 6 1 473.10 448.52 14.83 o -2 6 1 11997.94 13838.04 227.89 o 0 6 1 8067.12 9150.39 133.84 o 2 6 1 1265.21 1359.78 35.03 o 4 6 1 2146.58 2525.18 59.73 o 6 6 1 1187.67 1319.60 29.20 o 8 6 1 29.84 66.55 8.87 o 10 6 1 61.42 54.10 8.71 o 12 6 1 1.36 -6.18 8.23 o 14 6 1 1253.77 1205.25 32.33 o 16 6 1 4.61 5.14 10.36 o 18 6 1 2338.90 2213.63 50.62 o 20 6 1 18.67 35.81 13.04 o 22 6 1 2122.58 1887.68 60.90 o 24 6 1 159.55 170.82 26.59 o 26 6 1 58.16 65.82 20.68 o 28 6 1 143.41 165.48 28.30 o 30 6 1 285.13 346.18 33.66 o -31 7 1 20.98 26.94 22.89 o -29 7 1 10.01 18.51 19.81 o -27 7 1 407.59 365.61 29.13 o -25 7 1 0.05 -4.53 12.47 o -23 7 1 173.36 170.63 23.28 o -21 7 1 242.79 250.95 23.23 o -19 7 1 1.25 -7.28 11.56 o -17 7 1 218.82 203.43 20.43 o -15 7 1 564.41 469.40 22.99 o -13 7 1 936.74 852.76 27.69 o -11 7 1 361.96 379.06 16.89 o -9 7 1 838.52 886.85 22.80 o -7 7 1 17.23 26.53 8.38 o -5 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o 6 8 1 3534.06 3553.60 102.98 o 8 8 1 686.75 658.97 24.70 o 10 8 1 1438.27 1301.46 34.37 o 12 8 1 536.58 519.50 24.03 o 14 8 1 173.33 170.85 17.91 o 16 8 1 210.66 186.98 17.66 o 18 8 1 776.70 715.30 30.18 o 20 8 1 491.31 412.68 31.64 o 22 8 1 292.54 252.31 28.05 o 24 8 1 5.72 10.23 16.27 o 26 8 1 22.02 36.78 19.14 o 28 8 1 40.31 50.31 19.49 o -29 9 1 91.25 109.69 39.45 o -27 9 1 87.80 84.51 23.09 o -25 9 1 317.14 284.39 30.85 o -23 9 1 1227.97 1102.01 50.94 o -21 9 1 352.21 275.89 28.15 o -19 9 1 2072.35 1800.17 53.58 o -17 9 1 231.26 204.01 21.66 o -15 9 1 61.79 53.28 15.39 o -13 9 1 6.29 4.43 11.94 o -11 9 1 730.56 746.32 28.17 o -9 9 1 0.06 -6.39 9.30 o -7 9 1 0.61 -4.13 9.24 o -5 9 1 229.35 257.11 15.89 o -3 9 1 3401.81 3561.54 101.82 o -1 9 1 2150.50 2362.64 55.49 o 1 9 1 815.19 909.72 26.68 o 3 9 1 131.41 127.11 12.78 o 5 9 1 239.35 266.29 17.80 o 7 9 1 72.73 79.39 14.22 o 9 9 1 215.48 209.28 17.91 o 11 9 1 56.36 56.07 13.55 o 13 9 1 80.25 94.47 15.69 o 15 9 1 609.60 596.12 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