#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/13/2211397.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211397_Fobs loop_ _publ_author_name 'Rademeyer, Melanie' _publ_section_title ; trans-Cyclohexane-1,4-diammonium dibromide ; _journal_coeditor_code FL2078 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5767 _journal_page_last o5769 _journal_volume 62 _journal_year 2006 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.4264 _cell_length_b 8.9074 _cell_length_c 15.8018 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.6732 _[local]_cod_data_source_file fl2078Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TRANS14BRPROFFIT in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 335.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 112495.54 116527.13 1527.29 o 4 0 0 24833.60 25823.96 145.23 o 6 0 0 7507.69 7757.76 48.78 o 8 0 0 3068.07 3141.91 29.00 o 10 0 0 1028.22 1040.45 35.24 o 2 1 0 3799.12 3861.09 16.79 o 4 1 0 765.32 823.37 9.58 o 6 1 0 1.86 -4.55 7.76 o 8 1 0 94.90 85.52 13.77 o 10 1 0 11.53 32.58 23.23 o 0 2 0 63470.47 48066.35 16530.23 o 2 2 0 50074.31 49477.61 1656.63 o 4 2 0 27087.76 26895.74 324.13 o 6 2 0 9950.69 10244.78 78.23 o 8 2 0 2526.87 2579.55 20.60 o 10 2 0 462.77 497.39 29.41 o 2 3 0 161.37 199.42 3.77 o 4 3 0 33.18 58.78 5.89 o 6 3 0 0.21 1.38 8.10 o 8 3 0 23.35 23.77 14.21 o 10 3 0 3.02 14.05 27.87 o 0 4 0 10130.58 10124.89 521.49 o 2 4 0 16884.91 16418.11 139.94 o 4 4 0 14266.36 14406.72 126.09 o 6 4 0 5923.36 6061.86 97.94 o 8 4 0 1132.31 1212.11 27.60 o 2 5 0 826.94 910.24 18.51 o 4 5 0 298.88 294.50 7.11 o 6 5 0 3.89 14.75 12.48 o 8 5 0 66.50 58.87 19.98 o 0 6 0 14636.32 15098.26 1005.90 o 2 6 0 10303.86 10577.90 80.02 o 4 6 0 3875.78 4001.30 53.22 o 6 6 0 1199.11 1239.69 17.72 o 8 6 0 401.40 392.49 21.03 o 2 7 0 1.02 -1.86 9.42 o 4 7 0 1.43 -5.19 9.60 o 6 7 0 0.13 15.96 15.81 o 8 7 0 0.01 7.26 21.06 o 0 8 0 9544.46 10365.22 717.37 o 2 8 0 6315.91 6706.22 33.24 o 4 8 0 2612.71 2712.53 79.76 o 6 8 0 914.21 962.82 20.59 o 8 8 0 336.62 371.36 24.29 o 2 9 0 194.41 217.16 12.85 o 4 9 0 99.22 69.89 20.68 o 6 9 0 0.68 24.19 25.61 o 0 10 0 2906.51 3249.86 227.58 o 2 10 0 3112.05 3282.61 24.28 o 4 10 0 2849.22 2960.92 65.49 o 6 10 0 1427.07 1493.57 54.59 o 2 11 0 26.33 20.84 16.50 o 4 11 0 10.24 4.26 22.54 o 0 12 0 1909.92 2017.18 34.12 o 2 12 0 1673.56 1754.28 28.84 o 4 12 0 1042.97 931.79 46.36 o 1 1 1 1303.25 1525.77 36.78 o 2 1 1 2284.33 2232.04 12.55 o 3 1 1 5828.15 5528.08 37.90 o 4 1 1 1899.42 1866.28 18.67 o 5 1 1 3461.97 3288.17 41.10 o 6 1 1 1045.46 1049.22 8.54 o 7 1 1 949.34 934.49 9.47 o 8 1 1 467.99 520.96 10.97 o 9 1 1 92.86 100.87 11.93 o 10 1 1 197.03 248.90 16.20 o 0 2 1 2968.05 2905.14 72.51 o 1 2 1 1090.96 1135.51 28.35 o 2 2 1 357.89 332.14 4.86 o 3 2 1 846.32 934.24 9.92 o 4 2 1 6.71 18.24 2.95 o 5 2 1 72.66 91.43 4.45 o 6 2 1 5.23 17.96 6.08 o 7 2 1 66.31 69.70 7.17 o 8 2 1 11.46 10.58 9.85 o 9 2 1 50.37 38.28 11.94 o 10 2 1 17.76 27.55 16.71 o 1 3 1 26588.25 24971.53 233.34 o 2 3 1 4.73 17.20 2.29 o 3 3 1 7223.85 7279.50 66.63 o 4 3 1 547.03 532.71 4.86 o 5 3 1 1901.36 1875.49 7.73 o 6 3 1 1064.44 1040.75 11.46 o 7 3 1 696.07 692.53 12.95 o 8 3 1 673.77 723.39 10.94 o 9 3 1 328.07 330.14 15.43 o 10 3 1 198.00 255.15 21.08 o 0 4 1 54.96 40.14 4.48 o 1 4 1 105.33 114.68 4.50 o 2 4 1 140.25 116.98 2.85 o 3 4 1 229.73 218.01 5.16 o 4 4 1 259.16 238.68 4.72 o 5 4 1 19.04 15.23 5.13 o 6 4 1 123.41 123.17 6.77 o 7 4 1 3.38 0.56 8.54 o 8 4 1 26.85 48.50 13.08 o 9 4 1 2.62 14.90 18.13 o 1 5 1 14920.25 15157.60 71.31 o 2 5 1 180.91 156.80 4.49 o 3 5 1 7808.03 7934.57 83.01 o 4 5 1 585.97 563.91 8.28 o 5 5 1 3564.85 3567.54 15.51 o 6 5 1 608.04 606.69 8.83 o 7 5 1 1286.38 1253.37 15.65 o 8 5 1 372.25 376.50 17.72 o 9 5 1 387.85 414.08 20.99 o 0 6 1 35.91 38.39 7.20 o 1 6 1 98.45 104.64 5.54 o 2 6 1 172.56 138.16 5.87 o 3 6 1 149.22 162.11 5.62 o 4 6 1 291.05 270.59 6.01 o 5 6 1 22.42 23.77 8.93 o 6 6 1 162.39 152.19 10.23 o 7 6 1 10.19 12.55 11.80 o 8 6 1 31.27 24.24 14.22 o 9 6 1 6.61 17.12 20.22 o 1 7 1 3717.69 3832.83 43.51 o 2 7 1 451.19 461.11 7.45 o 3 7 1 4464.75 4549.16 43.87 o 4 7 1 577.17 556.21 9.77 o 5 7 1 3088.11 3047.29 15.64 o 6 7 1 298.71 312.10 12.11 o 7 7 1 1045.20 1055.85 22.14 o 8 7 1 135.96 142.59 15.83 o 9 7 1 161.72 197.25 41.12 o 0 8 1 497.66 497.46 16.72 o 1 8 1 49.65 41.80 7.43 o 2 8 1 295.57 280.89 8.01 o 3 8 1 133.90 128.10 8.09 o 4 8 1 72.91 63.13 11.17 o 5 8 1 8.78 20.30 11.95 o 6 8 1 28.92 45.48 13.85 o 7 8 1 15.06 20.28 15.80 o 8 8 1 23.68 25.54 18.02 o 1 9 1 1788.70 1841.25 21.76 o 2 9 1 55.50 52.65 8.90 o 3 9 1 1060.35 1087.67 20.60 o 4 9 1 164.81 140.43 14.19 o 5 9 1 375.78 416.83 17.43 o 6 9 1 198.04 238.67 19.15 o 7 9 1 120.48 130.05 20.84 o 0 10 1 241.88 251.35 14.94 o 1 10 1 2.69 -0.12 10.05 o 2 10 1 169.70 186.69 10.48 o 3 10 1 4.38 -5.56 12.03 o 4 10 1 75.43 70.00 14.18 o 5 10 1 0.34 14.61 18.91 o 6 10 1 30.44 61.37 20.18 o 1 11 1 432.13 463.06 12.39 o 2 11 1 4.84 10.74 13.04 o 3 11 1 128.77 151.87 15.35 o 4 11 1 41.45 23.27 15.67 o 5 11 1 16.92 13.40 16.71 o 0 12 1 33.87 44.58 18.16 o 1 12 1 13.96 12.87 14.07 o 2 12 1 53.61 77.36 14.66 o 3 12 1 37.57 45.35 17.50 o 4 12 1 78.11 100.42 29.06 o 1 13 1 26.38 35.43 23.75 o 2 13 1 21.57 -2.03 43.45 o 1 0 2 267.73 406.49 4.93 o 2 0 2 1521.89 1722.30 16.19 o 3 0 2 119.15 129.81 2.66 o 4 0 2 1631.32 1498.21 5.93 o 5 0 2 1386.11 1324.69 9.03 o 6 0 2 723.48 661.76 19.65 o 7 0 2 1530.07 1552.30 14.36 o 8 0 2 128.00 123.69 14.27 o 9 0 2 634.03 698.68 20.86 o 10 0 2 4.52 7.51 21.49 o 1 1 2 672.91 771.26 10.95 o 2 1 2 97.65 162.54 4.31 o 3 1 2 109.17 109.28 2.10 o 4 1 2 38.20 47.56 2.65 o 5 1 2 173.52 172.08 4.35 o 6 1 2 0.45 2.31 5.62 o 7 1 2 20.93 23.17 7.45 o 8 1 2 11.92 6.11 10.55 o 9 1 2 2.02 6.38 11.90 o 10 1 2 3.95 8.46 15.84 o 0 2 2 5790.40 6390.12 118.99 o 1 2 2 483.57 528.26 8.73 o 2 2 2 3862.24 4043.73 29.90 o 3 2 2 1862.76 1822.93 13.18 o 4 2 2 1556.39 1511.89 11.62 o 5 2 2 1542.23 1551.09 8.70 o 6 2 2 485.81 465.17 6.50 o 7 2 2 914.11 970.38 9.56 o 8 2 2 126.11 125.09 9.63 o 9 2 2 416.48 477.50 13.20 o 10 2 2 28.05 30.35 16.99 o 1 3 2 58.73 59.12 2.54 o 2 3 2 9.10 17.87 1.87 o 3 3 2 219.89 195.33 3.45 o 4 3 2 3.43 3.14 2.99 o 5 3 2 119.51 125.33 4.27 o 6 3 2 0.70 -2.27 6.12 o 7 3 2 31.41 46.26 7.26 o 8 3 2 3.30 15.64 10.70 o 9 3 2 0.82 4.78 14.12 o 10 3 2 0.68 15.94 20.09 o 0 4 2 7705.42 8146.58 106.83 o 1 4 2 623.06 658.29 15.72 o 2 4 2 4544.15 4706.59 65.77 o 3 4 2 1700.13 1699.50 27.58 o 4 4 2 1973.29 2002.25 19.15 o 5 4 2 1223.50 1219.57 12.13 o 6 4 2 681.26 641.40 7.43 o 7 4 2 564.74 593.12 14.04 o 8 4 2 236.07 233.09 11.60 o 9 4 2 260.97 304.24 18.41 o 1 5 2 1109.14 1090.80 12.71 o 2 5 2 33.79 35.93 3.14 o 3 5 2 176.32 141.24 4.13 o 4 5 2 24.87 28.54 4.89 o 5 5 2 16.50 21.14 6.79 o 6 5 2 0.48 1.90 8.08 o 7 5 2 20.68 23.33 10.54 o 8 5 2 6.81 33.16 14.25 o 9 5 2 28.28 50.99 19.61 o 0 6 2 3069.28 3271.10 28.77 o 1 6 2 21.40 9.01 5.21 o 2 6 2 2719.95 2797.36 54.42 o 3 6 2 243.79 227.87 5.78 o 4 6 2 1876.09 1843.41 24.45 o 5 6 2 648.28 620.50 8.62 o 6 6 2 921.76 892.61 16.53 o 7 6 2 591.28 587.24 14.65 o 8 6 2 271.55 251.08 14.86 o 9 6 2 251.27 309.96 18.31 o 1 7 2 413.23 397.25 6.93 o 2 7 2 7.07 1.60 6.24 o 3 7 2 287.92 276.01 6.92 o 4 7 2 6.71 17.78 9.69 o 5 7 2 174.40 179.03 11.45 o 6 7 2 0.42 14.21 12.63 o 7 7 2 72.51 71.96 13.03 o 8 7 2 0.23 -3.87 16.35 o 9 7 2 27.24 132.26 38.33 o 0 8 2 1130.94 1132.68 16.44 o 1 8 2 6.83 0.90 7.18 o 2 8 2 1088.85 1067.55 12.76 o 3 8 2 116.75 89.93 8.11 o 4 8 2 703.55 677.75 11.92 o 5 8 2 298.64 295.09 13.09 o 6 8 2 295.59 303.32 15.32 o 7 8 2 296.76 292.49 16.81 o 8 8 2 74.18 61.67 18.85 o 1 9 2 119.78 132.76 8.82 o 2 9 2 15.87 14.64 9.01 o 3 9 2 258.31 257.39 10.65 o 4 9 2 11.35 6.08 12.76 o 5 9 2 257.20 276.51 18.26 o 6 9 2 0.06 10.64 15.83 o 7 9 2 97.97 108.41 18.09 o 0 10 2 428.13 429.46 14.73 o 1 10 2 47.46 42.32 9.85 o 2 10 2 281.08 293.42 10.79 o 3 10 2 211.95 196.49 12.00 o 4 10 2 78.24 79.03 14.36 o 5 10 2 157.81 140.05 16.49 o 6 10 2 12.97 41.83 21.25 o 1 11 2 223.50 259.08 12.02 o 2 11 2 7.13 25.02 13.20 o 3 11 2 124.52 151.76 13.33 o 4 11 2 5.46 2.88 15.78 o 5 11 2 57.25 52.50 19.38 o 0 12 2 35.05 41.80 18.76 o 1 12 2 7.96 -7.22 13.67 o 2 12 2 29.18 26.49 14.36 o 3 12 2 47.79 43.65 20.93 o 4 12 2 21.67 13.43 44.82 o 1 13 2 130.97 162.41 29.02 o 1 1 3 49050.61 50739.88 350.65 o 2 1 3 81.89 111.11 2.49 o 3 1 3 29491.86 30026.13 133.92 o 4 1 3 86.94 82.80 3.35 o 5 1 3 12421.99 12592.29 35.08 o 6 1 3 61.64 75.01 5.22 o 7 1 3 3714.02 3709.75 25.84 o 8 1 3 29.98 25.86 9.41 o 9 1 3 853.63 852.42 24.29 o 10 1 3 12.70 6.56 17.47 o 0 2 3 59.29 123.85 3.90 o 1 2 3 58.75 124.65 7.52 o 2 2 3 5.33 50.80 2.70 o 3 2 3 84.56 96.89 2.57 o 4 2 3 0.98 6.62 3.08 o 5 2 3 0.00 6.59 3.80 o 6 2 3 4.05 7.78 5.17 o 7 2 3 0.49 0.55 7.78 o 8 2 3 9.91 15.51 9.91 o 9 2 3 0.79 1.07 15.75 o 10 2 3 7.99 8.08 18.45 o 1 3 3 38082.46 35995.25 361.85 o 2 3 3 2.74 21.75 1.99 o 3 3 3 21135.41 21227.84 156.37 o 4 3 3 47.48 63.49 6.73 o 5 3 3 8957.32 8895.43 37.20 o 6 3 3 74.33 79.25 6.26 o 7 3 3 3131.47 3077.44 18.54 o 8 3 3 44.87 54.07 11.34 o 9 3 3 732.16 754.24 16.42 o 10 3 3 12.65 21.06 20.21 o 0 4 3 20.05 35.02 4.11 o 1 4 3 0.00 13.96 2.36 o 2 4 3 32.68 42.65 4.62 o 3 4 3 0.32 5.40 2.50 o 4 4 3 49.84 48.19 2.96 o 5 4 3 4.05 4.38 5.15 o 6 4 3 32.32 24.65 7.65 o 7 4 3 0.07 13.16 8.80 o 8 4 3 13.09 28.24 11.73 o 9 4 3 1.77 13.69 17.94 o 1 5 3 21020.86 20448.23 248.34 o 2 5 3 22.01 27.33 4.08 o 3 5 3 13180.31 12653.60 111.77 o 4 5 3 51.09 52.87 6.10 o 5 5 3 5719.09 5657.87 29.12 o 6 5 3 44.21 39.90 8.29 o 7 5 3 1816.48 1819.01 16.06 o 8 5 3 25.51 46.40 14.18 o 9 5 3 430.08 469.64 18.75 o 0 6 3 58.95 60.10 7.37 o 1 6 3 4.38 1.59 5.45 o 2 6 3 72.66 64.39 10.13 o 3 6 3 11.45 16.83 5.51 o 4 6 3 57.16 54.84 7.76 o 5 6 3 0.46 4.37 8.21 o 6 6 3 24.57 23.43 10.63 o 7 6 3 0.06 8.75 12.96 o 8 6 3 5.23 34.56 15.96 o 9 6 3 0.28 15.25 17.55 o 1 7 3 9824.68 9802.23 88.44 o 2 7 3 29.17 32.21 6.21 o 3 7 3 6920.95 6979.84 74.07 o 4 7 3 39.37 44.15 10.27 o 5 7 3 3237.02 3309.16 20.74 o 6 7 3 22.62 19.71 12.40 o 7 7 3 1001.23 996.71 16.71 o 8 7 3 11.61 3.57 22.39 o 9 7 3 245.63 337.29 40.70 o 0 8 3 104.34 122.19 10.92 o 1 8 3 0.51 -0.77 7.40 o 2 8 3 69.47 76.07 8.71 o 3 8 3 4.15 -5.94 9.37 o 4 8 3 21.72 33.53 11.78 o 5 8 3 5.57 12.00 12.98 o 6 8 3 5.50 10.22 14.70 o 7 8 3 0.22 8.68 16.14 o 8 8 3 1.60 15.88 22.74 o 1 9 3 4177.36 4223.23 16.31 o 2 9 3 3.38 -0.13 8.55 o 3 9 3 3056.03 3069.66 66.15 o 4 9 3 12.21 15.94 13.05 o 5 9 3 1649.58 1690.11 20.41 o 6 9 3 17.00 13.37 15.79 o 7 9 3 621.70 638.23 19.75 o 0 10 3 41.94 54.66 14.28 o 1 10 3 0.89 -1.86 9.75 o 2 10 3 31.49 52.46 11.60 o 3 10 3 4.12 2.76 11.56 o 4 10 3 15.26 20.66 13.92 o 5 10 3 1.00 8.48 18.00 o 6 10 3 5.14 3.12 20.93 o 1 11 3 1840.87 1938.20 44.28 o 2 11 3 0.69 9.24 14.04 o 3 11 3 1259.02 1275.13 30.71 o 4 11 3 4.08 8.65 17.85 o 5 11 3 612.16 553.73 69.33 o 0 12 3 8.01 5.78 18.09 o 1 12 3 0.09 -6.23 15.32 o 2 12 3 9.55 28.68 15.79 o 3 12 3 0.56 28.87 21.03 o 4 12 3 10.22 20.73 44.91 o 0 0 4 43808.09 43317.09 199.44 o 1 0 4 128.77 124.89 5.57 o 2 0 4 30028.00 31271.15 137.92 o 3 0 4 27.54 15.00 2.71 o 4 0 4 12980.52 12867.14 114.78 o 5 0 4 592.86 563.21 5.77 o 6 0 4 5274.76 5334.63 25.00 o 7 0 4 700.81 718.31 10.98 o 8 0 4 1523.70 1600.01 19.08 o 9 0 4 290.75 280.39 19.91 o 10 0 4 277.49 276.20 22.81 o 1 1 4 449.95 450.42 11.14 o 2 1 4 17.00 39.17 4.22 o 3 1 4 26.40 21.87 2.46 o 4 1 4 4.10 5.08 2.98 o 5 1 4 93.96 85.99 3.90 o 6 1 4 0.60 -1.13 5.10 o 7 1 4 21.58 28.41 7.08 o 8 1 4 2.02 8.97 10.25 o 9 1 4 0.35 6.61 16.71 o 10 1 4 1.48 3.45 21.17 o 0 2 4 31524.82 29344.49 208.16 o 1 2 4 188.61 190.29 5.17 o 2 2 4 22803.26 22576.53 145.35 o 3 2 4 794.20 786.42 8.47 o 4 2 4 10678.44 10639.05 52.66 o 5 2 4 704.60 693.52 7.46 o 6 2 4 3774.48 3761.14 29.82 o 7 2 4 422.68 416.08 8.72 o 8 2 4 1046.06 1043.78 11.67 o 9 2 4 189.48 211.51 14.33 o 10 2 4 234.18 234.51 19.13 o 1 3 4 1.71 10.23 2.20 o 2 3 4 0.36 4.29 2.35 o 3 3 4 57.68 64.03 4.58 o 4 3 4 3.61 4.60 3.21 o 5 3 4 73.92 73.01 4.38 o 6 3 4 0.43 12.01 5.97 o 7 3 4 39.99 39.39 9.72 o 8 3 4 0.09 10.20 11.96 o 9 3 4 10.03 24.31 14.73 o 10 3 4 0.00 15.26 20.68 o 0 4 4 12844.45 12453.56 69.21 o 1 4 4 306.27 299.64 4.42 o 2 4 4 10730.69 10334.36 73.01 o 3 4 4 872.59 866.18 7.15 o 4 4 4 6202.33 6176.06 26.24 o 5 4 4 596.39 574.63 7.08 o 6 4 4 2163.20 2187.10 30.37 o 7 4 4 261.24 264.85 10.85 o 8 4 4 578.04 593.05 13.21 o 9 4 4 117.53 142.07 14.38 o 1 5 4 443.89 424.17 7.81 o 2 5 4 2.76 3.06 2.90 o 3 5 4 60.03 60.24 5.40 o 4 5 4 3.09 9.67 6.53 o 5 5 4 4.15 10.54 7.76 o 6 5 4 0.62 5.05 8.83 o 7 5 4 10.43 24.47 9.72 o 8 5 4 1.70 18.45 14.16 o 9 5 4 18.74 37.47 17.47 o 0 6 4 6165.30 6271.74 49.99 o 1 6 4 12.51 12.48 5.39 o 2 6 4 5227.45 5178.82 48.48 o 3 6 4 126.33 123.44 5.62 o 4 6 4 3141.94 3162.41 27.95 o 5 6 4 313.52 288.81 9.17 o 6 6 4 1351.48 1360.92 12.88 o 7 6 4 285.31 268.75 14.12 o 8 6 4 367.17 437.04 21.45 o 9 6 4 124.88 176.73 21.30 o 1 7 4 161.80 147.38 6.35 o 2 7 4 1.19 0.61 6.16 o 3 7 4 97.12 99.15 7.70 o 4 7 4 2.77 4.37 9.74 o 5 7 4 44.95 52.42 11.82 o 6 7 4 0.02 1.99 13.17 o 7 7 4 13.70 15.80 14.85 o 8 7 4 2.02 29.15 20.23 o 0 8 4 3767.74 3901.09 24.04 o 1 8 4 2.55 -2.20 7.04 o 2 8 4 3084.76 3026.96 54.60 o 3 8 4 52.02 45.10 9.30 o 4 8 4 1686.13 1766.17 15.73 o 5 8 4 151.70 147.13 13.00 o 6 8 4 673.57 695.23 16.70 o 7 8 4 162.76 169.49 16.61 o 8 8 4 182.47 172.51 24.61 o 1 9 4 21.71 26.98 10.77 o 2 9 4 0.46 -0.53 8.48 o 3 9 4 71.31 71.29 10.68 o 4 9 4 0.02 7.34 15.07 o 5 9 4 74.96 82.52 14.88 o 6 9 4 1.46 -0.98 16.25 o 7 9 4 20.74 23.84 18.48 o 0 10 4 2144.06 2047.48 38.91 o 1 10 4 23.75 23.56 9.87 o 2 10 4 1705.97 1742.36 19.06 o 3 10 4 110.05 104.53 11.71 o 4 10 4 879.04 966.38 20.87 o 5 10 4 88.01 75.20 18.26 o 6 10 4 319.76 345.65 22.75 o 1 11 4 47.80 50.94 11.50 o 2 11 4 6.94 9.06 14.44 o 3 11 4 23.74 35.52 14.53 o 4 11 4 10.85 14.69 17.79 o 5 11 4 9.99 1.55 33.14 o 0 12 4 668.58 644.26 25.28 o 1 12 4 4.87 12.36 16.79 o 2 12 4 588.15 654.13 25.45 o 3 12 4 27.38 38.55 23.52 o 4 12 4 405.78 457.73 47.09 o 1 1 5 2167.33 2649.88 27.47 o 2 1 5 1956.85 1920.55 15.07 o 3 1 5 1886.19 2149.99 24.91 o 4 1 5 1995.60 1979.13 17.86 o 5 1 5 1040.00 1015.53 6.62 o 6 1 5 1204.92 1206.04 12.14 o 7 1 5 385.56 342.40 8.05 o 8 1 5 566.94 625.95 13.00 o 9 1 5 57.08 66.60 19.88 o 10 1 5 244.20 284.51 19.28 o 0 2 5 2022.61 1978.94 27.89 o 1 2 5 644.06 767.16 7.26 o 2 2 5 266.67 265.19 8.82 o 3 2 5 505.66 553.64 7.37 o 4 2 5 11.65 19.64 3.68 o 5 2 5 25.64 31.15 4.29 o 6 2 5 14.71 17.16 5.69 o 7 2 5 18.34 14.21 7.61 o 8 2 5 2.96 16.26 13.81 o 9 2 5 11.04 16.48 15.74 o 10 2 5 7.74 15.23 22.12 o 1 3 5 1471.40 1623.82 25.81 o 2 3 5 22.70 30.25 4.33 o 3 3 5 207.35 247.57 6.84 o 4 3 5 692.30 640.51 9.22 o 5 3 5 2.13 9.51 4.26 o 6 3 5 1267.27 1237.41 13.90 o 7 3 5 0.77 6.78 11.26 o 8 3 5 809.73 853.89 13.93 o 9 3 5 11.81 14.46 15.13 o 10 3 5 246.63 286.80 23.68 o 0 4 5 67.58 52.08 3.10 o 1 4 5 18.98 26.74 2.72 o 2 4 5 148.64 129.45 3.16 o 3 4 5 43.25 51.90 6.84 o 4 4 5 248.23 235.16 8.59 o 5 4 5 0.32 4.01 7.62 o 6 4 5 106.01 133.00 10.36 o 7 4 5 14.74 15.53 11.72 o 8 4 5 15.96 26.71 12.28 o 9 4 5 11.94 19.97 14.38 o 1 5 5 19.65 32.34 5.25 o 2 5 5 216.12 200.79 3.50 o 3 5 5 13.56 17.13 4.16 o 4 5 5 699.85 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