#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/13/2211399.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211399_Fobs loop_ _publ_author_name 'Bourgeaux, Marie' 'Vomsheid, Sophie' 'Skene, W. G.' _publ_section_title ; Hydrogen-bonded network of diethyl 2,5-diaminothiophene-3,4-dicarboxylate ; _journal_coeditor_code GA2015 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5529 _journal_page_last o5531 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.963 _cell_angle_gamma 90.000 _cell_length_a 9.5306 _cell_length_b 8.8206 _cell_length_c 15.5518 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.8296 _[local]_cod_data_source_file ga2015Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sken17 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 164.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 881.31 906.00 21.66 o 2 0 0 399.95 394.30 13.44 o 3 0 0 1.25 1.07 0.61 o 4 0 0 1786.25 1939.36 22.53 o 5 0 0 17.36 6.44 1.22 o 6 0 0 724.78 722.93 23.64 o 7 0 0 529.20 515.72 13.89 o 8 0 0 150.03 135.04 7.82 o 9 0 0 587.81 595.25 34.32 o 10 0 0 381.56 391.25 11.63 o 1 1 0 4940.10 5089.05 80.73 o 2 1 0 9940.13 9176.82 117.74 o 3 1 0 1159.76 1244.48 20.68 o 4 1 0 11.70 11.83 0.75 o 5 1 0 828.14 831.89 21.93 o 6 1 0 352.47 317.05 5.65 o 7 1 0 81.26 76.36 2.49 o 8 1 0 111.84 95.20 3.34 o 9 1 0 4.36 6.21 1.32 o 10 1 0 95.18 88.39 2.59 o 0 2 0 153.44 148.71 7.65 o 1 2 0 27060.60 20181.71 456.85 o 2 2 0 3617.33 3731.06 42.82 o 3 2 0 1324.92 1469.45 29.11 o 4 2 0 631.28 616.82 14.78 o 5 2 0 332.47 400.28 12.54 o 6 2 0 1.82 2.76 0.97 o 7 2 0 216.06 181.65 3.31 o 8 2 0 917.59 850.50 13.98 o 9 2 0 248.01 265.35 5.20 o 10 2 0 129.40 143.06 8.44 o 1 3 0 122.07 122.59 3.43 o 2 3 0 1772.69 1796.12 24.95 o 3 3 0 2597.04 2510.86 27.92 o 4 3 0 2133.07 2167.63 17.25 o 5 3 0 448.03 416.19 9.89 o 6 3 0 402.17 378.75 8.15 o 7 3 0 210.83 191.60 5.17 o 8 3 0 0.90 1.75 1.19 o 9 3 0 1.32 1.51 1.11 o 10 3 0 61.09 68.74 5.18 o 0 4 0 2251.60 2305.73 155.81 o 1 4 0 130.06 146.45 6.08 o 2 4 0 2925.91 2966.91 34.61 o 3 4 0 1443.12 1509.91 37.19 o 4 4 0 23.49 24.51 1.88 o 5 4 0 32.18 26.19 1.41 o 6 4 0 510.56 443.05 8.47 o 7 4 0 328.21 297.15 10.59 o 8 4 0 64.25 78.60 3.28 o 9 4 0 97.32 111.02 3.64 o 10 4 0 85.30 89.34 5.59 o 1 5 0 583.15 639.74 19.79 o 2 5 0 33.31 24.07 1.55 o 3 5 0 2767.94 2691.49 47.27 o 4 5 0 1535.94 1326.69 12.87 o 5 5 0 700.97 598.47 12.38 o 6 5 0 405.55 390.18 12.10 o 7 5 0 72.12 81.05 2.92 o 8 5 0 142.46 148.90 5.96 o 9 5 0 11.34 10.99 1.41 o 0 6 0 205.71 182.78 6.15 o 1 6 0 165.63 135.52 5.87 o 2 6 0 562.72 554.82 12.24 o 3 6 0 150.42 142.97 3.36 o 4 6 0 378.16 303.12 7.51 o 5 6 0 301.53 287.97 4.76 o 6 6 0 51.12 40.86 2.26 o 7 6 0 42.76 44.47 2.57 o 8 6 0 122.87 121.21 3.67 o 9 6 0 72.05 77.09 3.63 o 1 7 0 515.44 477.47 8.77 o 2 7 0 175.52 168.71 5.96 o 3 7 0 1.66 1.45 1.15 o 4 7 0 530.36 508.06 13.92 o 5 7 0 982.70 974.65 21.62 o 6 7 0 229.67 234.16 5.28 o 7 7 0 172.42 159.23 6.89 o 8 7 0 7.81 8.59 1.54 o 0 8 0 216.94 214.67 6.39 o 1 8 0 405.71 387.83 18.18 o 2 8 0 7.72 7.15 1.48 o 3 8 0 92.86 98.67 3.81 o 4 8 0 28.29 26.97 2.16 o 5 8 0 100.99 116.87 4.28 o 6 8 0 60.88 57.98 2.66 o 1 9 0 50.76 37.65 2.24 o 2 9 0 34.17 34.53 2.30 o 3 9 0 209.96 217.94 13.98 o 4 9 0 82.93 84.69 2.95 o 5 9 0 33.19 33.19 1.97 o 1 10 0 51.99 48.86 2.67 o 2 10 0 177.93 178.88 17.88 o 3 10 0 0.32 0.18 0.97 o -11 1 1 2.69 2.49 1.38 o -10 1 1 53.93 45.51 2.03 o -9 1 1 139.02 132.18 6.11 o -8 1 1 1.23 1.09 1.27 o -7 1 1 23.49 22.77 1.45 o -6 1 1 85.32 90.56 3.30 o -5 1 1 1790.13 1988.02 17.87 o -4 1 1 3090.83 3586.55 77.59 o -3 1 1 108.60 142.24 3.38 o -2 1 1 45.66 64.52 2.31 o -1 1 1 9686.29 8822.86 185.92 o 0 1 1 0.90 2.32 0.60 o 1 1 1 623.78 774.50 17.78 o 2 1 1 5146.30 5274.64 78.20 o 3 1 1 109.77 116.22 4.79 o 4 1 1 920.59 1003.03 19.73 o 5 1 1 1585.67 1621.17 32.17 o 6 1 1 189.19 188.47 5.18 o 7 1 1 82.78 81.22 2.70 o 8 1 1 25.87 23.76 1.91 o 9 1 1 48.39 54.36 3.25 o 10 1 1 12.56 13.86 1.60 o -11 2 1 20.82 16.12 2.80 o -10 2 1 22.82 23.79 1.85 o -9 2 1 2.94 0.34 1.11 o -8 2 1 0.17 0.84 1.12 o -7 2 1 81.68 90.81 2.63 o -6 2 1 448.96 464.28 13.04 o -5 2 1 165.67 174.53 4.70 o -4 2 1 61.85 62.34 1.69 o -3 2 1 7981.83 7922.17 60.13 o -2 2 1 6997.86 7426.19 78.35 o -1 2 1 624.75 737.66 17.37 o 0 2 1 4750.56 4948.48 70.22 o 1 2 1 3307.23 3378.93 76.17 o 2 2 1 92.85 87.03 2.79 o 3 2 1 289.62 300.73 6.47 o 4 2 1 4.16 3.88 0.72 o 5 2 1 158.72 177.88 5.45 o 6 2 1 49.03 49.72 1.87 o 7 2 1 203.84 201.62 4.57 o 8 2 1 10.38 9.19 1.90 o 9 2 1 35.49 33.51 2.31 o 10 2 1 0.01 -0.02 0.97 o -10 3 1 0.20 0.70 1.05 o -9 3 1 5.09 2.99 1.25 o -8 3 1 28.06 21.01 2.81 o -7 3 1 156.66 122.57 3.82 o -6 3 1 637.07 605.05 10.23 o -5 3 1 1245.11 1190.61 26.02 o -4 3 1 1005.42 1115.61 18.85 o -3 3 1 12.67 32.00 1.16 o -2 3 1 4235.75 4274.06 70.56 o -1 3 1 215.28 266.56 6.87 o 0 3 1 9.55 17.98 0.68 o 1 3 1 2134.17 2241.86 64.14 o 2 3 1 138.18 151.70 2.72 o 3 3 1 268.92 302.32 7.32 o 4 3 1 1685.76 1602.60 41.89 o 5 3 1 105.71 95.06 3.36 o 6 3 1 1.72 2.39 0.95 o 7 3 1 1.61 1.01 1.24 o 8 3 1 133.70 143.60 4.46 o 9 3 1 0.12 0.23 0.99 o 10 3 1 28.98 36.60 2.02 o -10 4 1 1.57 2.33 0.99 o -9 4 1 8.07 11.23 1.65 o -8 4 1 0.97 -0.88 1.01 o -7 4 1 444.17 421.07 14.55 o -6 4 1 0.93 3.95 0.99 o -5 4 1 11.43 9.51 1.05 o -4 4 1 450.25 412.59 6.77 o -3 4 1 468.73 474.51 13.10 o -2 4 1 2138.84 2335.53 43.42 o -1 4 1 183.31 179.23 6.53 o 0 4 1 652.65 662.50 23.05 o 1 4 1 1377.19 1508.74 22.24 o 2 4 1 30.71 35.37 1.46 o 3 4 1 346.05 349.33 7.99 o 4 4 1 4.84 5.30 1.62 o 5 4 1 288.56 237.45 4.36 o 6 4 1 14.57 14.95 1.32 o 7 4 1 45.99 45.02 2.70 o 8 4 1 32.08 30.88 2.09 o 9 4 1 67.75 64.67 2.77 o 10 4 1 10.01 10.44 1.67 o -9 5 1 5.79 4.59 1.21 o -8 5 1 46.77 48.89 3.07 o -7 5 1 2.07 1.30 1.02 o -6 5 1 147.47 147.57 3.65 o -5 5 1 162.29 152.13 3.79 o -4 5 1 96.12 90.59 2.73 o -3 5 1 27.20 30.21 1.92 o -2 5 1 243.57 242.07 4.74 o -1 5 1 8.61 5.58 0.86 o 0 5 1 897.00 888.64 17.19 o 1 5 1 71.61 73.70 2.26 o 2 5 1 723.85 714.42 11.78 o 3 5 1 0.35 0.29 1.12 o 4 5 1 0.40 0.33 0.74 o 5 5 1 84.26 65.19 2.07 o 6 5 1 102.46 87.35 3.41 o 7 5 1 0.40 -0.04 1.14 o 8 5 1 46.04 41.51 2.20 o 9 5 1 34.55 40.37 2.21 o -9 6 1 14.66 15.56 2.11 o -8 6 1 116.78 111.44 3.84 o -7 6 1 37.39 39.73 2.37 o -6 6 1 100.03 92.27 3.58 o -5 6 1 144.15 145.02 6.26 o -4 6 1 192.00 174.84 4.45 o -3 6 1 12.49 9.32 1.10 o -2 6 1 0.79 2.78 0.87 o -1 6 1 179.04 181.94 3.98 o 0 6 1 264.14 238.94 4.62 o 1 6 1 152.35 142.93 3.64 o 2 6 1 493.27 455.76 9.93 o 3 6 1 205.40 189.59 4.28 o 4 6 1 51.37 42.27 2.02 o 5 6 1 47.98 44.90 2.14 o 6 6 1 1.88 0.98 1.00 o 7 6 1 19.37 17.06 1.58 o 8 6 1 2.17 1.71 1.08 o -8 7 1 9.01 9.91 1.57 o -7 7 1 39.15 36.26 2.24 o -6 7 1 84.66 77.74 3.19 o -5 7 1 0.96 1.22 1.22 o -4 7 1 24.52 27.98 2.37 o -3 7 1 143.89 159.62 4.71 o -2 7 1 229.19 209.75 4.41 o -1 7 1 6.83 8.58 1.06 o 0 7 1 80.41 60.15 1.96 o 1 7 1 160.29 151.20 4.47 o 2 7 1 134.88 138.27 4.12 o 3 7 1 34.72 29.81 2.29 o 4 7 1 6.86 5.26 1.30 o 5 7 1 26.63 27.40 1.95 o 6 7 1 53.38 54.63 2.39 o 7 7 1 0.64 0.42 0.99 o 8 7 1 1.84 0.38 1.88 o -7 8 1 36.93 43.78 7.78 o -6 8 1 44.15 42.09 4.03 o -5 8 1 18.78 23.63 2.00 o -4 8 1 159.49 161.77 4.36 o -3 8 1 9.13 7.96 1.58 o -2 8 1 58.46 58.40 2.48 o -1 8 1 70.74 64.87 2.39 o 0 8 1 0.64 1.21 0.99 o 1 8 1 0.79 -0.52 0.94 o 2 8 1 8.69 10.84 1.64 o 3 8 1 15.87 13.13 1.61 o 4 8 1 95.85 99.36 3.63 o 5 8 1 29.24 22.20 1.91 o 6 8 1 27.67 29.35 5.58 o 7 8 1 0.04 0.37 1.79 o -6 9 1 1.29 0.30 2.04 o -5 9 1 2.29 7.98 1.23 o -4 9 1 0.92 0.81 0.94 o -3 9 1 241.95 234.55 11.37 o -2 9 1 25.89 26.68 2.84 o -1 9 1 2.59 2.19 1.02 o 0 9 1 19.87 24.92 1.97 o 1 9 1 5.36 3.41 1.37 o 2 9 1 26.05 26.05 1.90 o 3 9 1 105.92 110.26 3.56 o 4 9 1 11.72 13.93 1.54 o 5 9 1 7.95 7.92 1.20 o -3 10 1 0.04 -0.18 1.10 o -2 10 1 21.59 19.32 6.15 o -1 10 1 5.53 5.60 1.27 o 0 10 1 14.12 11.60 1.78 o 1 10 1 2.83 3.15 1.09 o 2 10 1 0.00 -0.02 0.89 o 3 10 1 24.61 23.45 1.82 o -11 0 2 32.91 35.33 3.84 o -10 0 2 65.09 74.72 7.87 o -9 0 2 453.54 408.55 10.35 o -8 0 2 157.30 185.18 6.01 o -7 0 2 162.89 137.82 4.43 o -6 0 2 982.10 1010.58 21.02 o -5 0 2 6792.41 6524.29 124.01 o -4 0 2 979.57 1153.60 23.00 o -3 0 2 5707.79 5119.99 68.07 o -2 0 2 4440.26 3831.89 95.83 o -1 0 2 29.02 30.00 1.23 o 0 0 2 6823.55 6713.00 178.79 o 1 0 2 4.57 3.55 0.65 o 2 0 2 8341.15 8189.19 105.38 o 3 0 2 2575.90 2577.26 40.14 o 4 0 2 1066.09 1069.83 26.11 o 5 0 2 1669.74 1839.83 33.35 o 6 0 2 200.40 151.17 4.95 o 7 0 2 1346.40 1171.49 31.25 o 8 0 2 325.22 303.36 9.14 o 9 0 2 465.99 479.31 32.71 o 10 0 2 9.37 7.58 1.70 o -11 1 2 8.00 8.09 2.23 o -10 1 2 2.42 1.81 1.09 o -9 1 2 140.70 143.71 6.24 o -8 1 2 236.28 242.06 6.59 o -7 1 2 1411.13 1374.93 21.66 o -6 1 2 1178.66 1331.17 26.86 o -5 1 2 139.30 162.16 4.05 o -4 1 2 1096.84 1286.26 26.65 o -3 1 2 306.39 274.35 4.88 o -2 1 2 55.19 95.73 2.21 o -1 1 2 592.00 539.54 16.81 o 0 1 2 779.94 887.43 29.45 o 1 1 2 682.22 637.95 40.66 o 2 1 2 81.12 100.13 3.64 o 3 1 2 2064.59 1978.72 51.77 o 4 1 2 990.73 974.93 12.23 o 5 1 2 398.93 403.18 7.40 o 6 1 2 11.66 10.65 1.08 o 7 1 2 0.30 0.01 0.91 o 8 1 2 7.39 6.39 1.22 o 9 1 2 46.62 46.43 2.80 o 10 1 2 181.30 197.85 4.15 o -11 2 2 100.80 90.63 5.55 o -10 2 2 204.39 248.57 9.62 o -9 2 2 53.39 51.14 2.88 o -8 2 2 58.77 55.82 3.15 o -7 2 2 1.76 1.25 0.92 o -6 2 2 1326.90 1247.84 17.36 o -5 2 2 1704.78 1722.84 34.15 o -4 2 2 4826.77 4912.41 36.48 o -3 2 2 49.32 65.79 2.01 o -2 2 2 3860.31 3817.86 63.94 o -1 2 2 8012.72 7780.14 97.03 o 0 2 2 165.86 206.78 5.98 o 1 2 2 3520.65 3349.45 141.77 o 2 2 2 1248.91 1161.92 37.03 o 3 2 2 252.12 240.69 6.95 o 4 2 2 185.01 202.33 3.54 o 5 2 2 1016.10 894.49 13.15 o 6 2 2 2037.60 1855.16 44.52 o 7 2 2 194.67 193.25 4.78 o 8 2 2 428.19 443.20 16.85 o 9 2 2 108.32 127.14 6.03 o 10 2 2 116.55 118.68 7.78 o -10 3 2 221.20 217.71 6.73 o -9 3 2 22.84 28.61 2.33 o -8 3 2 974.50 918.82 10.32 o -7 3 2 348.75 298.71 6.57 o -6 3 2 70.76 55.37 1.99 o -5 3 2 14.25 9.00 1.21 o -4 3 2 2484.71 2655.79 33.94 o -3 3 2 199.30 228.93 5.71 o -2 3 2 1562.21 1727.13 27.64 o -1 3 2 88.98 105.42 3.83 o 0 3 2 517.50 507.76 15.72 o 1 3 2 532.41 540.87 9.77 o 2 3 2 2336.68 2548.49 27.52 o 3 3 2 152.53 190.00 5.78 o 4 3 2 1199.53 1082.69 26.04 o 5 3 2 0.32 3.50 1.73 o 6 3 2 762.20 748.32 21.46 o 7 3 2 1.55 3.89 1.22 o 8 3 2 236.82 214.82 6.65 o 9 3 2 206.11 235.81 5.45 o 10 3 2 24.57 23.10 1.78 o -10 4 2 119.00 129.28 7.68 o -9 4 2 143.68 153.44 4.88 o -8 4 2 49.36 60.10 2.91 o -7 4 2 188.56 172.72 4.11 o -6 4 2 21.32 28.81 1.55 o -5 4 2 135.63 116.50 2.42 o -4 4 2 78.91 56.56 2.00 o -3 4 2 5641.61 5674.93 75.68 o -2 4 2 1119.23 1401.57 38.72 o -1 4 2 52.43 70.67 3.40 o 0 4 2 348.49 373.33 15.19 o 1 4 2 734.72 787.19 22.91 o 2 4 2 20.30 22.53 1.35 o 3 4 2 899.02 844.31 15.60 o 4 4 2 200.28 181.80 4.66 o 5 4 2 13.63 12.79 1.08 o 6 4 2 615.27 546.35 12.88 o 7 4 2 974.67 901.56 11.69 o 8 4 2 175.62 166.38 3.94 o 9 4 2 14.17 14.56 1.53 o -10 5 2 30.35 45.85 3.95 o -9 5 2 507.41 480.18 6.47 o -8 5 2 75.65 80.08 2.81 o -7 5 2 57.76 63.01 2.46 o -6 5 2 166.03 141.25 3.56 o -5 5 2 897.40 781.87 18.93 o -4 5 2 75.82 95.60 3.54 o -3 5 2 14.64 17.61 1.92 o -2 5 2 112.25 134.11 4.88 o -1 5 2 619.68 589.86 11.01 o 0 5 2 867.17 937.78 31.24 o 1 5 2 2244.54 2211.91 42.12 o 2 5 2 217.72 205.99 6.37 o 3 5 2 1093.88 967.80 17.61 o 4 5 2 132.89 129.70 3.22 o 5 5 2 1091.77 996.29 9.70 o 6 5 2 17.11 16.17 1.63 o 7 5 2 4.86 5.23 1.53 o 8 5 2 22.52 25.56 1.74 o 9 5 2 91.86 86.87 2.94 o -9 6 2 31.34 24.60 2.54 o -8 6 2 6.01 6.45 1.25 o -7 6 2 33.17 29.75 1.86 o -6 6 2 12.90 11.94 1.62 o -5 6 2 1.21 1.42 1.18 o -4 6 2 666.40 611.94 13.65 o -3 6 2 119.89 103.01 2.59 o -2 6 2 686.87 632.85 8.83 o -1 6 2 555.48 534.76 10.39 o 0 6 2 128.57 126.91 2.74 o 1 6 2 147.26 127.34 2.62 o 2 6 2 88.78 83.67 2.57 o 3 6 2 11.66 11.17 1.02 o 4 6 2 28.32 17.68 1.56 o 5 6 2 923.83 887.21 15.85 o 6 6 2 38.66 39.69 2.05 o 7 6 2 59.99 64.74 2.99 o 8 6 2 47.78 43.12 2.27 o -8 7 2 32.35 43.55 8.41 o -7 7 2 103.37 123.86 5.53 o -6 7 2 161.52 149.92 4.92 o -5 7 2 369.19 345.80 8.51 o -4 7 2 79.45 75.57 3.40 o -3 7 2 0.39 0.77 1.06 o -2 7 2 45.33 44.32 2.12 o -1 7 2 335.23 300.79 5.18 o 0 7 2 455.38 384.89 8.62 o 1 7 2 227.35 215.84 4.38 o 2 7 2 1077.60 1095.38 49.93 o 3 7 2 289.20 261.81 5.47 o 4 7 2 639.65 582.90 10.33 o 5 7 2 5.63 4.25 1.09 o 6 7 2 5.97 6.54 1.14 o 7 7 2 1.34 1.83 1.07 o -7 8 2 7.72 6.25 1.15 o -6 8 2 0.34 0.34 0.97 o -5 8 2 98.54 99.47 5.65 o -4 8 2 54.38 59.71 2.79 o -3 8 2 207.98 198.05 5.20 o -2 8 2 103.73 106.60 3.45 o -1 8 2 176.23 162.71 4.69 o 0 8 2 113.73 103.68 5.66 o 1 8 2 94.15 90.31 4.03 o 2 8 2 51.41 47.73 2.69 o 3 8 2 1.58 1.90 1.14 o 4 8 2 305.49 313.67 10.82 o 5 8 2 8.83 9.99 1.44 o 6 8 2 138.91 146.42 4.38 o -5 9 2 0.07 0.89 0.93 o -4 9 2 11.08 9.88 1.53 o -3 9 2 31.57 26.61 2.12 o -2 9 2 4.95 4.41 1.19 o -1 9 2 68.68 53.72 2.48 o 0 9 2 230.11 227.34 9.29 o 1 9 2 291.34 323.30 13.45 o 2 9 2 124.44 134.20 3.63 o 3 9 2 228.85 215.73 5.44 o 4 9 2 17.68 21.96 1.75 o 5 9 2 57.69 61.60 4.40 o -3 10 2 51.06 53.39 4.11 o -2 10 2 88.98 88.10 4.53 o -1 10 2 162.85 209.50 12.05 o 0 10 2 59.15 66.35 3.25 o 1 10 2 0.03 0.16 1.08 o 2 10 2 6.19 5.51 1.10 o 3 10 2 70.04 74.16 2.84 o -11 1 3 2.53 2.08 1.11 o -10 1 3 89.70 88.84 3.67 o -9 1 3 10.56 6.88 1.43 o -8 1 3 1.89 1.51 1.03 o -7 1 3 60.69 69.88 2.03 o -6 1 3 10.68 6.64 1.09 o -5 1 3 97.98 101.68 2.68 o -4 1 3 41.79 44.67 1.44 o -3 1 3 160.46 152.19 3.78 o -2 1 3 691.63 733.11 15.80 o -1 1 3 2264.42 2447.27 30.66 o 0 1 3 981.87 1240.82 21.54 o 1 1 3 8880.56 8997.34 141.14 o 2 1 3 2564.47 2709.97 64.51 o 3 1 3 210.59 219.96 10.92 o 4 1 3 1.46 1.49 0.68 o 5 1 3 26.29 18.85 1.48 o 6 1 3 234.76 214.17 4.27 o 7 1 3 163.26 149.37 4.24 o 8 1 3 37.79 37.41 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