#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211405.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211405_Fobs loop_ _publ_author_name 'Soneta, Yuji' 'Sakamoto, Shigeaki' 'Miyamura, Kazuo' _publ_section_title ; 9-(2-Carboxyphenyl)-3,6-bis(diethylamino)xanthylium bis(2-thioxo-1,3-dithiole-4,5-dithiolato)nickelate(III) ; _journal_coeditor_code GK2032 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3448 _journal_page_last m3450 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 105.729 _cell_angle_beta 96.342 _cell_angle_gamma 91.138 _cell_length_a 10.1874 _cell_length_b 10.7522 _cell_length_c 18.2847 _exptl_crystal_F_000 922.00 _reflns_d_resolution_high 0.7501 _[local]_cod_data_source_file gk2032Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rhodb100 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 311.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4659.51 4493.72 68.30 o 2 0 0 20417.56 22621.15 772.13 o 3 0 0 3332.21 3379.91 202.45 o 4 0 0 3831.46 3680.94 307.44 o 5 0 0 374.77 394.43 38.65 o 6 0 0 149.90 166.69 57.12 o 7 0 0 104.58 94.60 32.73 o 8 0 0 580.25 598.40 112.56 o 9 0 0 261.34 324.96 106.12 o 10 0 0 1.63 -15.15 71.76 o 11 0 0 304.87 339.47 124.15 o 12 0 0 362.11 374.57 132.06 o -12 1 0 344.52 457.95 151.49 o -11 1 0 1082.21 1101.24 177.86 o -10 1 0 1.12 49.81 82.81 o -9 1 0 141.90 76.91 76.99 o -8 1 0 548.18 493.15 103.95 o -7 1 0 550.24 500.96 44.96 o -6 1 0 455.68 422.65 38.67 o -5 1 0 419.96 374.02 33.85 o -4 1 0 2123.21 1615.97 66.38 o -3 1 0 6278.33 5260.86 241.12 o -2 1 0 2308.78 2911.06 957.76 o -1 1 0 15131.97 15669.32 163.52 o 1 1 0 7468.92 7115.79 401.30 o 2 1 0 13600.90 21243.88 2310.44 o 3 1 0 15349.49 18303.96 1016.14 o 4 1 0 3627.13 3118.98 190.93 o 5 1 0 4258.88 4098.53 183.01 o 6 1 0 1684.24 1737.30 142.95 o 7 1 0 4.33 35.67 36.11 o 8 1 0 886.71 906.08 84.02 o 9 1 0 416.96 356.68 113.24 o 10 1 0 873.72 765.11 147.17 o 11 1 0 897.06 843.89 165.07 o 12 1 0 8.87 44.36 96.69 o -12 2 0 256.20 250.31 123.88 o -11 2 0 272.47 239.58 107.74 o -10 2 0 230.37 183.53 101.95 o -9 2 0 13.87 -7.90 59.26 o -8 2 0 25.83 28.67 53.74 o -7 2 0 41.04 41.07 26.67 o -6 2 0 5485.83 5259.65 439.92 o -5 2 0 429.57 438.77 38.26 o -4 2 0 1066.93 1106.35 187.64 o -3 2 0 2461.25 2251.84 207.63 o -2 2 0 668.70 509.42 45.19 o -1 2 0 245.07 250.34 33.77 o 0 2 0 4758.21 5066.62 96.44 o 1 2 0 820.93 642.11 40.01 o 2 2 0 1218.81 1225.68 99.11 o 3 2 0 25.29 44.58 22.24 o 4 2 0 17704.44 16721.97 759.83 o 5 2 0 4826.96 4685.89 192.78 o 6 2 0 3683.75 3246.40 129.26 o 7 2 0 95.57 164.59 40.15 o 8 2 0 6.57 32.58 42.71 o 9 2 0 43.10 14.91 75.50 o 10 2 0 2.91 -1.48 80.72 o 11 2 0 11.49 -34.32 86.12 o 12 2 0 191.69 312.54 132.12 o -12 3 0 204.78 215.07 110.29 o -11 3 0 1706.20 1496.72 177.40 o -10 3 0 1359.48 1269.40 157.87 o -9 3 0 639.49 637.59 119.18 o -8 3 0 1031.48 1115.00 141.00 o -7 3 0 4943.57 5084.18 450.27 o -6 3 0 1964.73 2159.59 460.72 o -5 3 0 148.60 265.92 77.85 o -4 3 0 147.99 163.58 36.21 o -3 3 0 4324.09 4041.73 122.42 o -2 3 0 3381.58 2985.70 105.69 o -1 3 0 6798.72 7270.76 116.13 o 0 3 0 5733.31 6276.76 112.39 o 1 3 0 1120.42 1520.04 94.17 o 2 3 0 7119.66 6886.69 429.21 o 3 3 0 1068.38 960.12 50.44 o 4 3 0 2967.64 2962.78 125.16 o 5 3 0 2553.59 3296.91 245.75 o 6 3 0 503.10 583.02 56.38 o 7 3 0 18.53 38.87 36.01 o 8 3 0 813.09 952.19 95.14 o 9 3 0 675.60 608.42 136.41 o 10 3 0 38.31 55.07 89.74 o 11 3 0 323.64 270.91 113.60 o 12 3 0 51.70 25.52 100.41 o -12 4 0 831.89 853.90 170.73 o -11 4 0 860.87 998.98 168.11 o -10 4 0 435.47 287.87 108.80 o -9 4 0 1610.61 1300.47 149.43 o -8 4 0 1069.51 846.08 126.72 o -7 4 0 1188.69 1182.21 179.00 o -6 4 0 1375.36 1730.74 712.25 o -5 4 0 2310.93 2217.20 86.28 o -4 4 0 8.35 22.18 33.30 o -3 4 0 0.03 0.45 29.71 o -2 4 0 6180.46 5549.06 162.82 o -1 4 0 1466.64 1594.23 70.17 o 0 4 0 12389.20 14046.13 270.82 o 1 4 0 16.47 143.55 46.21 o 2 4 0 15.98 68.80 44.95 o 3 4 0 2986.42 2827.76 150.26 o 4 4 0 22.63 17.75 27.57 o 5 4 0 2191.47 2408.13 199.43 o 6 4 0 150.84 194.18 55.17 o 7 4 0 1891.25 1721.19 108.74 o 8 4 0 798.72 822.30 93.86 o 9 4 0 926.96 1013.40 146.61 o 10 4 0 129.52 140.86 98.01 o 11 4 0 316.54 291.04 119.33 o 12 4 0 27.54 129.08 116.90 o -12 5 0 145.68 240.20 109.78 o -11 5 0 68.67 73.11 77.59 o -10 5 0 0.05 2.59 70.60 o -9 5 0 119.52 125.39 77.22 o -8 5 0 153.28 115.61 73.62 o -7 5 0 2768.23 2607.83 380.56 o -6 5 0 1.97 2.34 30.16 o 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3207.35 3246.74 162.05 o -2 8 0 365.00 338.59 89.85 o -1 8 0 288.22 258.72 88.79 o 0 8 0 410.98 398.30 99.96 o 1 8 0 19.32 33.44 67.52 o 2 8 0 600.70 566.47 116.16 o 3 8 0 89.30 90.92 76.10 o 4 8 0 6352.06 6273.31 296.81 o 5 8 0 394.82 383.63 106.60 o 6 8 0 854.41 831.80 148.67 o 7 8 0 221.22 192.45 104.11 o 8 8 0 335.88 353.74 115.04 o 9 8 0 407.74 361.25 128.48 o 10 8 0 309.79 405.13 142.37 o -10 9 0 193.81 311.87 108.87 o -9 9 0 0.98 4.32 65.14 o -7 9 0 1364.38 1632.96 180.73 o -6 9 0 160.28 198.77 106.39 o -4 9 0 218.69 284.50 88.54 o -3 9 0 1795.39 1801.88 169.67 o -2 9 0 853.51 942.10 136.02 o -1 9 0 371.20 645.40 122.27 o 0 9 0 29.78 53.63 72.08 o 1 9 0 391.58 438.54 116.46 o 2 9 0 20.43 -40.54 74.06 o 3 9 0 1014.42 1017.09 155.60 o 4 9 0 161.45 62.29 88.66 o 5 9 0 371.67 420.27 120.71 o 6 9 0 236.70 240.98 113.83 o 7 9 0 657.58 690.40 153.64 o 8 9 0 148.15 155.52 101.53 o 9 9 0 189.51 329.28 133.43 o -9 10 0 142.23 160.43 90.55 o -7 10 0 5.56 114.67 108.42 o -6 10 0 72.53 87.55 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