#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/14/2211411.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211411_Fobs loop_ _publ_author_name 'Ho\/ly\'nska, Ma\/lgorzata' 'Korabik, Maria' 'Lis, Tadeusz' _publ_section_title ; Methyltriphenylphosphonium hexachlororhenate(IV) ; _journal_coeditor_code HB2169 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3178 _journal_page_last m3180 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.130 _cell_angle_gamma 90.000 _cell_length_a 9.1440 _cell_length_b 16.3430 _cell_length_c 12.9760 _exptl_crystal_F_000 942.00 _reflns_d_resolution_high 0.6196 _[local]_cod_data_source_file hb2169Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kmc5 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 248.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 19141.32 20177.04 211.08 o 6 0 0 5594.16 5354.90 155.12 o 8 0 0 6582.90 6504.78 426.28 o 10 0 0 4639.65 5012.83 276.99 o 12 0 0 2248.62 2574.61 577.32 o 14 0 0 934.69 830.95 414.67 o 2 1 0 8988.40 9980.90 118.41 o 3 1 0 16365.06 17366.59 205.90 o 4 1 0 325.98 388.08 42.92 o 5 1 0 3376.80 3222.57 82.55 o 6 1 0 948.40 843.22 68.55 o 7 1 0 1684.85 1600.48 85.95 o 8 1 0 57.18 93.14 61.36 o 9 1 0 5504.67 5590.30 178.98 o 10 1 0 128.77 138.36 81.07 o 11 1 0 949.90 991.11 188.76 o 12 1 0 213.75 546.40 210.61 o 13 1 0 1234.75 1194.33 313.68 o 14 1 0 19.28 188.13 225.12 o 2 2 0 3081.25 3184.85 71.23 o 3 2 0 5810.49 5891.32 91.89 o 4 2 0 14537.18 15120.50 137.79 o 5 2 0 1409.99 1235.45 66.82 o 6 2 0 1952.51 1907.32 96.47 o 7 2 0 35.50 200.17 56.37 o 8 2 0 3347.34 3242.16 141.05 o 9 2 0 89.00 94.40 74.77 o 10 2 0 745.19 396.77 145.29 o 11 2 0 492.15 521.02 139.16 o 12 2 0 921.84 1102.72 362.18 o 13 2 0 11.08 132.83 185.12 o 14 2 0 723.31 1021.27 370.57 o 2 3 0 1673.35 1642.70 63.39 o 3 3 0 34426.89 35690.08 224.64 o 4 3 0 5056.07 5582.48 75.05 o 5 3 0 20305.49 20008.22 256.25 o 6 3 0 348.58 285.42 53.25 o 7 3 0 6054.85 5975.83 139.42 o 8 3 0 16.10 164.45 60.91 o 9 3 0 2247.87 2167.02 196.55 o 10 3 0 1.28 113.69 97.90 o 11 3 0 1315.03 1205.02 193.08 o 12 3 0 619.71 609.32 237.19 o 13 3 0 2476.27 2964.35 372.16 o 14 3 0 29.37 292.98 227.35 o 0 4 0 8542.97 9719.58 122.95 o 1 4 0 4726.00 5153.59 55.98 o 2 4 0 46261.85 50604.82 200.63 o 3 4 0 149.81 218.01 27.83 o 4 4 0 24052.38 24040.99 184.83 o 5 4 0 1057.57 1027.24 47.76 o 6 4 0 7173.12 7186.89 99.47 o 7 4 0 4.39 88.00 34.42 o 8 4 0 2933.88 2767.15 135.44 o 9 4 0 31.58 201.22 95.26 o 10 4 0 1582.42 1346.28 223.52 o 11 4 0 22.34 251.76 148.50 o 12 4 0 1714.05 1645.18 205.82 o 13 4 0 7.81 88.74 139.22 o 14 4 0 1061.20 871.55 377.93 o 1 5 0 20527.40 21492.56 168.27 o 2 5 0 2587.12 2425.03 48.58 o 3 5 0 4673.25 4343.62 63.74 o 4 5 0 597.87 633.52 42.25 o 5 5 0 10862.67 11399.17 141.66 o 6 5 0 33.71 126.11 32.47 o 7 5 0 2069.68 2084.76 112.63 o 8 5 0 924.50 827.33 115.70 o 9 5 0 808.17 761.08 200.46 o 10 5 0 283.90 393.42 144.33 o 11 5 0 1144.37 1492.54 277.55 o 12 5 0 43.63 191.34 144.59 o 13 5 0 509.44 636.17 308.16 o 14 5 0 0.51 323.44 251.48 o 0 6 0 11260.86 11461.21 157.26 o 1 6 0 9616.71 9895.92 79.02 o 2 6 0 30823.07 32395.30 170.73 o 3 6 0 52.02 141.58 26.89 o 4 6 0 7285.39 7528.83 84.10 o 5 6 0 118.82 125.15 25.12 o 6 6 0 2833.04 2943.42 96.05 o 7 6 0 1959.88 2071.17 106.15 o 8 6 0 2463.00 2607.60 212.55 o 9 6 0 66.45 184.58 101.70 o 10 6 0 2051.07 2234.72 276.35 o 11 6 0 2.05 263.85 172.80 o 12 6 0 1040.80 935.93 269.49 o 13 6 0 123.85 308.56 216.93 o 14 6 0 458.94 498.42 323.26 o 1 7 0 37465.97 37345.20 312.75 o 2 7 0 719.44 740.72 34.97 o 3 7 0 19504.62 20357.75 125.17 o 4 7 0 556.47 560.98 46.29 o 5 7 0 3315.67 3307.35 66.25 o 6 7 0 4.11 134.27 45.57 o 7 7 0 6294.09 6587.31 145.70 o 8 7 0 720.48 710.95 186.99 o 9 7 0 3624.08 3270.98 238.15 o 10 7 0 1.39 140.80 148.20 o 11 7 0 3740.19 3952.02 281.20 o 12 7 0 14.24 224.77 164.73 o 13 7 0 733.95 823.69 267.02 o 0 8 0 25563.09 26214.54 229.36 o 1 8 0 15.95 73.29 19.36 o 2 8 0 29625.36 29703.62 240.90 o 3 8 0 203.71 246.76 38.99 o 4 8 0 904.74 856.11 54.07 o 5 8 0 499.52 448.49 45.29 o 6 8 0 9609.19 9100.78 139.15 o 7 8 0 58.02 118.66 56.39 o 8 8 0 1672.80 1585.64 189.50 o 9 8 0 88.55 166.83 129.44 o 10 8 0 2753.03 3339.89 258.64 o 11 8 0 285.40 377.87 157.77 o 12 8 0 1361.09 1639.95 262.80 o 13 8 0 1.37 316.48 202.92 o 1 9 0 10024.13 9907.09 120.74 o 2 9 0 985.96 896.39 39.01 o 3 9 0 8791.37 9040.47 86.43 o 4 9 0 77.49 167.57 40.37 o 5 9 0 723.62 713.97 85.59 o 6 9 0 359.68 331.87 70.69 o 7 9 0 2155.03 2035.05 137.03 o 8 9 0 167.60 247.94 136.80 o 9 9 0 567.46 636.61 257.73 o 10 9 0 401.12 445.29 159.38 o 11 9 0 1604.70 1659.65 249.82 o 12 9 0 342.68 355.71 256.75 o 13 9 0 54.55 238.55 171.91 o 0 10 0 9923.95 10342.59 187.47 o 1 10 0 2860.93 2906.37 93.96 o 2 10 0 17915.98 18219.45 161.46 o 3 10 0 26.01 101.09 30.99 o 4 10 0 3282.14 3248.31 80.94 o 5 10 0 0.71 179.47 63.04 o 6 10 0 8455.61 8635.86 147.18 o 7 10 0 764.43 701.81 120.33 o 8 10 0 2307.13 2544.26 263.73 o 9 10 0 410.78 414.26 167.57 o 10 10 0 2121.55 2080.59 463.15 o 11 10 0 161.41 712.12 208.51 o 12 10 0 879.87 1253.57 271.76 o 13 10 0 286.75 443.10 211.56 o 1 11 0 12934.28 13201.98 161.46 o 2 11 0 147.78 145.45 27.82 o 3 11 0 16540.27 16421.40 192.27 o 4 11 0 101.29 146.78 40.91 o 5 11 0 8710.12 8406.49 154.04 o 6 11 0 64.31 183.08 77.25 o 7 11 0 7496.28 6937.90 192.36 o 8 11 0 232.52 177.48 209.13 o 9 11 0 1488.35 1530.69 307.25 o 10 11 0 305.60 565.57 203.86 o 11 11 0 1900.52 1732.83 290.12 o 12 11 0 2.83 306.96 176.73 o 13 11 0 1180.60 1276.13 361.16 o 0 12 0 4491.87 4834.44 213.71 o 1 12 0 0.45 115.39 50.69 o 2 12 0 5789.95 5689.29 88.49 o 3 12 0 1750.32 1588.85 58.91 o 4 12 0 7596.28 7628.70 122.93 o 5 12 0 574.78 525.25 88.36 o 6 12 0 1600.52 1363.00 128.26 o 7 12 0 216.69 228.17 120.43 o 8 12 0 182.87 277.31 124.54 o 9 12 0 213.66 781.76 376.76 o 10 12 0 529.49 854.07 245.27 o 11 12 0 2.12 317.90 266.34 o 12 12 0 538.90 684.31 268.83 o 1 13 0 5891.87 5900.13 170.89 o 2 13 0 419.78 504.67 74.76 o 3 13 0 3616.38 3608.87 106.29 o 4 13 0 3162.70 2984.31 146.88 o 5 13 0 3805.03 3709.39 242.91 o 6 13 0 434.84 391.36 157.16 o 7 13 0 1261.48 1286.91 474.91 o 8 13 0 84.61 239.35 146.49 o 9 13 0 385.36 490.64 227.00 o 10 13 0 385.28 472.42 314.05 o 11 13 0 884.64 899.40 312.42 o 12 13 0 30.16 346.35 254.82 o 0 14 0 13676.10 14000.12 325.96 o 1 14 0 37.92 92.93 61.09 o 2 14 0 6308.00 6318.84 178.41 o 3 14 0 2584.19 2440.85 130.93 o 4 14 0 8281.96 8565.05 254.40 o 5 14 0 56.24 181.68 187.94 o 6 14 0 3520.19 3332.34 284.46 o 7 14 0 95.04 165.65 125.38 o 8 14 0 4046.03 3816.03 305.51 o 9 14 0 362.91 521.61 260.10 o 10 14 0 2935.80 2820.01 288.22 o 11 14 0 212.08 357.15 254.85 o 12 14 0 604.86 773.25 283.88 o 1 15 0 9189.51 9082.33 199.52 o 2 15 0 63.93 121.76 65.65 o 3 15 0 3849.76 3660.34 154.36 o 4 15 0 31.08 157.43 89.14 o 5 15 0 1598.48 1051.31 472.27 o 6 15 0 19.55 279.33 131.94 o 7 15 0 1590.74 1612.92 296.92 o 8 15 0 1.98 212.99 220.74 o 9 15 0 3568.49 3870.35 380.11 o 10 15 0 142.15 397.43 286.63 o 11 15 0 388.61 672.79 285.37 o 0 16 0 9391.79 9253.24 302.90 o 1 16 0 22.16 136.52 79.66 o 2 16 0 2267.60 1875.33 147.04 o 3 16 0 247.23 202.52 83.51 o 4 16 0 1479.74 1599.84 164.71 o 5 16 0 1.51 187.80 130.78 o 6 16 0 115.83 242.49 211.83 o 7 16 0 83.18 211.81 146.43 o 8 16 0 1688.67 1605.44 267.15 o 9 16 0 93.80 262.29 241.01 o 10 16 0 459.85 574.18 287.03 o 11 16 0 24.22 196.37 260.57 o 1 17 0 4474.52 4389.99 185.48 o 2 17 0 5.09 104.05 77.94 o 3 17 0 2371.64 2347.47 158.80 o 4 17 0 15.35 202.84 137.38 o 5 17 0 3438.55 3332.26 440.15 o 6 17 0 141.98 255.41 172.58 o 7 17 0 597.22 465.19 201.14 o 8 17 0 33.82 227.37 186.29 o 9 17 0 2075.12 2157.19 318.02 o 10 17 0 358.81 436.78 283.95 o 11 17 0 426.39 593.33 358.58 o 0 18 0 6715.29 6386.51 561.64 o 1 18 0 5.63 128.75 91.47 o 2 18 0 1927.62 1893.57 168.83 o 3 18 0 303.16 284.88 89.78 o 4 18 0 6158.70 6746.14 277.62 o 5 18 0 390.42 499.23 193.78 o 6 18 0 2296.72 2622.03 322.45 o 7 18 0 5.07 67.63 147.79 o 8 18 0 2150.68 2123.26 340.48 o 9 18 0 13.98 252.68 211.26 o 10 18 0 454.02 584.93 309.74 o 1 19 0 2071.77 2012.76 163.58 o 2 19 0 64.29 203.42 91.78 o 3 19 0 1810.24 1825.18 215.48 o 4 19 0 0.81 164.90 122.69 o 5 19 0 3135.03 3905.77 355.22 o 6 19 0 150.84 222.01 201.51 o 7 19 0 348.31 327.64 245.37 o 8 19 0 18.15 233.61 206.61 o 9 19 0 914.58 1022.05 364.02 o 10 19 0 13.92 158.02 209.88 o 0 20 0 964.01 797.23 203.14 o 1 20 0 1231.60 1513.42 163.76 o 2 20 0 786.63 849.63 128.79 o 3 20 0 0.62 310.03 190.12 o 4 20 0 1498.74 1404.56 180.72 o 5 20 0 259.69 423.20 201.37 o 6 20 0 733.16 734.92 215.48 o 7 20 0 220.33 241.10 198.86 o 8 20 0 542.06 712.30 323.97 o 9 20 0 157.80 346.78 244.60 o 1 21 0 2087.14 2554.37 269.89 o 2 21 0 419.90 476.79 161.04 o 3 21 0 2102.91 1987.39 292.03 o 4 21 0 87.31 350.44 202.07 o 5 21 0 1793.67 1657.11 291.31 o 6 21 0 35.82 325.41 239.07 o 7 21 0 2073.06 2102.81 380.56 o 8 21 0 495.29 594.65 428.85 o 0 22 0 1572.61 1711.95 456.40 o 1 22 0 297.38 558.80 167.79 o 2 22 0 2855.35 2554.13 225.98 o 3 22 0 35.65 158.89 129.19 o 4 22 0 1146.24 787.05 277.25 o 5 22 0 57.71 183.74 219.05 o 6 22 0 1126.48 1091.84 329.48 o 7 22 0 121.47 292.71 373.65 o 1 23 0 789.43 792.58 202.77 o 2 23 0 62.81 424.97 216.05 o 3 23 0 568.05 621.68 229.67 o 4 23 0 5.09 320.44 259.48 o 5 23 0 50.20 145.61 253.78 o 6 23 0 58.49 492.76 472.62 o 7 23 0 495.57 544.84 474.57 o 0 24 0 863.53 945.83 335.85 o 1 24 0 31.94 209.45 148.93 o 2 24 0 1327.93 1372.95 245.09 o 3 24 0 44.57 347.57 259.51 o 4 24 0 264.54 342.91 406.71 o 5 24 0 31.59 144.81 318.35 o 1 25 0 1364.47 1324.51 369.82 o 2 25 0 1.66 214.29 264.70 o 3 25 0 1196.27 1102.60 344.08 o 4 25 0 7.12 333.63 448.82 o 1 26 0 46.04 245.30 412.88 o 2 26 0 779.18 779.52 494.04 o -13 0 1 1533.28 1304.90 499.46 o -11 0 1 1145.03 1104.91 335.72 o -9 0 1 8081.84 8399.88 626.21 o -7 0 1 808.86 826.34 119.77 o -5 0 1 7122.12 7740.44 154.74 o -3 0 1 337.30 412.60 90.97 o 3 0 1 4645.96 4876.14 134.72 o 5 0 1 6777.31 6638.38 244.17 o 7 0 1 4420.73 4233.12 157.22 o 9 0 1 3365.96 3476.47 225.87 o 11 0 1 385.58 435.24 299.59 o 13 0 1 519.08 1023.01 451.61 o -14 1 1 1241.13 1446.52 387.77 o -13 1 1 527.75 555.50 272.77 o -12 1 1 1704.29 1581.38 318.62 o -11 1 1 553.92 528.51 146.81 o -10 1 1 4816.37 4998.69 265.53 o -9 1 1 1086.84 1218.47 145.44 o -8 1 1 7664.47 7409.86 181.11 o -7 1 1 74.33 143.18 44.58 o -6 1 1 2042.25 1900.40 86.51 o -5 1 1 191.33 287.97 56.74 o -4 1 1 11982.85 12353.84 163.20 o -3 1 1 2064.47 1854.54 65.29 o -2 1 1 16169.02 15992.57 583.08 o 2 1 1 58733.25 60509.84 843.81 o 3 1 1 4474.64 4407.16 91.00 o 4 1 1 21154.92 21620.43 211.68 o 5 1 1 888.81 813.50 59.87 o 6 1 1 4615.84 4511.57 105.45 o 7 1 1 897.26 756.14 72.20 o 8 1 1 8908.83 9384.05 488.82 o 9 1 1 375.36 372.03 98.54 o 10 1 1 1508.68 1387.61 153.02 o 11 1 1 15.03 287.18 165.54 o 12 1 1 1737.10 1645.40 308.86 o 13 1 1 0.55 227.45 201.66 o 14 1 1 304.04 552.43 342.94 o -14 2 1 229.39 323.37 268.89 o -13 2 1 1793.77 2393.53 765.72 o -12 2 1 176.17 417.09 184.39 o -11 2 1 2156.10 1830.40 261.73 o -10 2 1 173.75 225.91 94.27 o -9 2 1 6566.08 6472.71 251.19 o -8 2 1 87.43 184.27 69.90 o -7 2 1 6263.13 6339.96 137.28 o -6 2 1 2209.29 2034.73 90.26 o -5 2 1 13322.58 13136.05 179.75 o -4 2 1 2649.15 2545.61 78.15 o -3 2 1 4358.25 4215.89 84.11 o -2 2 1 1426.38 1238.55 51.98 o 2 2 1 9008.31 9263.85 93.81 o 3 2 1 47035.04 48619.53 504.97 o 4 2 1 547.95 556.35 44.76 o 5 2 1 20977.20 21090.61 260.73 o 6 2 1 857.16 695.60 63.91 o 7 2 1 3993.12 4024.79 114.95 o 8 2 1 67.07 105.05 70.04 o 9 2 1 6560.65 6190.05 480.31 o 10 2 1 128.16 315.72 131.63 o 11 2 1 1439.10 1375.62 240.93 o 12 2 1 260.37 620.48 292.47 o 13 2 1 1926.48 2118.35 375.83 o 14 2 1 10.41 425.59 254.29 o -14 3 1 1105.32 1050.08 413.81 o -13 3 1 4.23 301.86 295.33 o -12 3 1 1815.74 1662.50 252.84 o -11 3 1 407.03 427.09 156.32 o -10 3 1 1011.15 925.44 123.50 o -9 3 1 98.44 120.27 82.13 o -8 3 1 1504.57 1383.72 128.60 o -7 3 1 463.00 297.66 64.13 o -6 3 1 4560.64 4494.43 120.40 o -5 3 1 1103.70 987.38 60.91 o -4 3 1 4518.49 3942.17 83.31 o -3 3 1 1876.90 2012.24 68.21 o -2 3 1 5672.50 5914.10 74.59 o -1 3 1 266.01 344.66 45.20 o 1 3 1 5053.62 5231.69 73.42 o 2 3 1 3500.25 3650.09 90.98 o 3 3 1 6638.12 6535.17 91.67 o 4 3 1 29308.90 29959.90 249.29 o 5 3 1 3214.25 3127.90 101.56 o 6 3 1 4014.12 3818.24 105.02 o 7 3 1 1410.08 1271.44 85.99 o 8 3 1 4163.43 3996.03 164.16 o 9 3 1 305.36 406.54 163.10 o 10 3 1 764.30 634.08 153.45 o 11 3 1 581.63 618.36 163.86 o 12 3 1 986.06 990.02 276.84 o 13 3 1 55.34 241.20 234.48 o 14 3 1 494.73 771.50 368.62 o -14 4 1 12.43 223.71 212.76 o -13 4 1 2417.33 2732.09 423.55 o -12 4 1 970.23 857.98 238.87 o -11 4 1 1517.07 1475.36 199.51 o -10 4 1 0.34 64.93 128.41 o -9 4 1 1733.50 1989.92 158.63 o -8 4 1 2127.00 2321.52 179.01 o -7 4 1 3554.30 3713.46 128.36 o -6 4 1 49.23 108.45 25.42 o -5 4 1 6054.85 5831.11 104.67 o -4 4 1 697.13 732.23 59.18 o -3 4 1 16708.80 17296.96 132.36 o -2 4 1 1605.64 1684.08 55.02 o -1 4 1 10102.95 10998.79 92.12 o 0 4 1 15.70 67.40 19.88 o 1 4 1 24438.03 26899.87 155.94 o 2 4 1 4041.93 4109.33 70.24 o 3 4 1 25587.65 26179.87 232.61 o 4 4 1 77.02 106.10 24.87 o 5 4 1 13150.27 13424.67 162.22 o 6 4 1 4.40 91.90 29.82 o 7 4 1 5342.21 5411.98 102.35 o 8 4 1 206.01 248.60 104.47 o 9 4 1 565.85 612.64 140.05 o 10 4 1 489.80 570.20 140.12 o 11 4 1 612.21 852.58 181.87 o 12 4 1 26.24 215.10 202.92 o 13 4 1 841.54 996.49 436.90 o 14 4 1 91.49 266.60 239.56 o -14 5 1 1010.58 866.79 378.69 o -13 5 1 45.24 296.68 196.68 o -12 5 1 1828.65 1589.77 230.84 o -11 5 1 199.51 259.95 159.02 o -10 5 1 3794.29 3899.67 247.06 o -9 5 1 243.38 401.95 132.04 o -8 5 1 2935.60 3029.59 157.98 o -7 5 1 2824.17 2768.33 121.67 o -6 5 1 9291.11 9328.39 135.49 o -5 5 1 3.67 105.52 38.33 o -4 5 1 12396.75 12796.22 136.42 o -3 5 1 654.14 576.13 45.63 o -2 5 1 8562.58 8505.47 78.01 o -1 5 1 4178.92 4422.59 58.20 o 0 5 1 17214.51 18414.60 100.52 o 1 5 1 10215.16 10278.74 75.74 o 2 5 1 25764.30 26735.64 316.92 o 3 5 1 121.20 161.90 33.42 o 4 5 1 27501.31 28240.11 228.60 o 5 5 1 1039.84 937.28 51.90 o 6 5 1 18672.51 19448.13 194.18 o 7 5 1 741.52 668.45 75.45 o 8 5 1 1380.86 1247.69 153.92 o 9 5 1 200.89 391.75 160.35 o 10 5 1 1637.63 2042.06 234.77 o 11 5 1 94.52 173.01 166.57 o 12 5 1 1565.35 1318.95 480.56 o 13 5 1 108.24 267.04 264.24 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