#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:23:29 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181036 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/16/2211666.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211666_Fobs loop_ _publ_author_name 'Jotani, Mukesh M.' 'Baldaniya, Bharat B.' _publ_section_title ; (2Z)-Ethyl 2-(4-chlorobenzylidene)-7-methyl-3-oxo-5-phenyl-2,3-dihydro-5H-1,3thiazolo[3,2-a]pyrimidine-6-carboxylate ; _journal_coeditor_code WN2094 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5871 _journal_page_last o5873 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.970 _cell_angle_gamma 90.000 _cell_length_a 9.5970 _cell_length_b 10.9070 _cell_length_c 20.6070 _exptl_crystal_F_000 912.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file wn2094Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 14ptm in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 244.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3693.47 3948.56 77.12 o 4 0 0 3447.34 3329.87 77.23 o 6 0 0 1422.11 1327.04 45.17 o 8 0 0 161.26 160.28 32.76 o 10 0 0 390.67 379.15 55.33 o 1 1 0 188.88 167.49 7.41 o 2 1 0 3581.06 3525.51 58.10 o 3 1 0 14.55 15.03 7.97 o 4 1 0 555.95 525.04 17.48 o 5 1 0 241.87 302.62 13.81 o 6 1 0 0.08 5.50 5.52 o 7 1 0 0.25 21.82 10.26 o 8 1 0 540.75 549.86 38.45 o 9 1 0 373.09 387.62 36.41 o 10 1 0 28.96 36.80 24.66 o 11 1 0 466.34 389.45 62.08 o 0 2 0 538.97 469.05 25.12 o 1 2 0 7374.60 7726.11 88.76 o 2 2 0 20509.22 22007.57 272.90 o 3 2 0 1122.75 1143.43 25.22 o 4 2 0 640.28 737.74 20.05 o 5 2 0 28.00 29.27 11.47 o 6 2 0 135.90 155.26 22.47 o 7 2 0 1.86 14.04 9.51 o 8 2 0 2398.51 2218.16 72.40 o 9 2 0 3.72 3.20 14.52 o 10 2 0 111.81 122.34 24.65 o 11 2 0 188.84 213.99 34.59 o 1 3 0 2375.50 2536.71 40.29 o 2 3 0 11628.22 11979.77 137.65 o 3 3 0 1127.77 1055.18 22.92 o 4 3 0 95.21 191.66 30.57 o 5 3 0 459.31 462.22 32.19 o 6 3 0 101.01 103.04 14.76 o 7 3 0 4.45 -0.03 8.19 o 8 3 0 441.33 419.46 43.75 o 9 3 0 195.37 240.36 31.13 o 10 3 0 29.24 41.71 18.63 o 11 3 0 2.76 -5.73 17.80 o 0 4 0 3385.40 3372.26 77.32 o 1 4 0 2148.86 2086.48 45.78 o 2 4 0 31.34 34.84 5.72 o 3 4 0 545.21 469.65 16.06 o 4 4 0 22.30 27.21 5.68 o 5 4 0 421.26 442.15 24.18 o 6 4 0 351.92 361.64 25.63 o 7 4 0 299.55 285.11 26.69 o 8 4 0 991.63 907.36 49.66 o 9 4 0 41.35 57.17 28.86 o 10 4 0 125.46 106.77 24.85 o 1 5 0 227.97 246.91 17.63 o 2 5 0 428.79 380.47 14.20 o 3 5 0 788.46 832.98 20.44 o 4 5 0 120.40 135.66 11.21 o 5 5 0 88.54 99.33 14.60 o 6 5 0 1564.49 1503.56 77.40 o 7 5 0 263.20 267.28 25.43 o 8 5 0 2.41 4.02 14.94 o 9 5 0 100.49 108.33 20.35 o 10 5 0 189.08 230.89 48.89 o 0 6 0 18.50 29.12 11.20 o 1 6 0 440.40 510.97 23.93 o 2 6 0 0.53 1.66 6.56 o 3 6 0 459.08 459.79 16.69 o 4 6 0 9.89 23.67 10.25 o 5 6 0 203.89 213.35 20.38 o 6 6 0 431.84 451.13 40.37 o 7 6 0 701.23 681.62 51.18 o 8 6 0 138.20 149.97 26.73 o 9 6 0 208.22 211.50 33.68 o 10 6 0 117.34 156.54 47.11 o 1 7 0 40.97 55.14 17.40 o 2 7 0 2442.19 2373.68 51.13 o 3 7 0 90.06 117.56 15.15 o 4 7 0 18.19 31.29 11.41 o 5 7 0 139.59 143.16 26.65 o 6 7 0 297.01 296.95 88.45 o 7 7 0 42.09 10.83 35.42 o 8 7 0 12.15 19.66 18.24 o 9 7 0 4.76 4.16 34.11 o 0 8 0 204.18 216.76 26.94 o 1 8 0 809.00 742.36 33.81 o 2 8 0 297.39 354.50 23.50 o 3 8 0 47.33 61.49 14.04 o 4 8 0 176.42 166.28 36.96 o 5 8 0 385.07 311.65 44.63 o 6 8 0 58.58 73.82 24.39 o 7 8 0 28.77 58.67 31.04 o 8 8 0 10.30 33.25 20.26 o 2 9 0 1294.36 1176.37 56.13 o 3 9 0 149.09 155.44 45.21 o 4 9 0 11.44 37.52 17.64 o 5 9 0 6.76 16.72 16.63 o 6 9 0 442.83 389.20 47.77 o 7 9 0 83.24 79.66 30.73 o 8 9 0 55.21 84.74 31.88 o 0 10 0 18.70 48.18 17.33 o 1 10 0 5.61 30.04 11.19 o 2 10 0 6.95 35.73 17.44 o 3 10 0 8.62 40.57 29.50 o 4 10 0 29.12 64.80 23.75 o 5 10 0 10.89 30.34 21.66 o 6 10 0 42.60 78.58 28.47 o 7 10 0 11.66 -2.68 22.34 o 1 11 0 255.40 268.12 55.97 o 2 11 0 23.87 62.44 21.74 o 3 11 0 119.73 143.05 29.92 o 4 11 0 36.48 38.73 21.48 o 5 11 0 205.90 152.94 35.12 o 6 11 0 34.36 5.97 30.36 o 0 12 0 6.80 42.57 29.44 o 1 12 0 1.05 38.80 21.26 o 2 12 0 29.84 82.21 26.18 o 3 12 0 42.68 68.76 25.51 o 4 12 0 61.18 37.82 28.80 o -9 0 1 1580.70 1544.07 90.48 o -7 0 1 2.38 2.45 14.05 o -5 0 1 331.78 295.34 19.98 o -3 0 1 4352.98 4710.35 96.68 o -1 0 1 4394.88 4739.91 127.53 o 1 0 1 6198.30 6499.16 288.73 o 3 0 1 1452.61 1457.67 37.14 o 5 0 1 557.88 537.15 24.50 o 7 0 1 768.75 689.10 49.26 o 9 0 1 228.63 229.72 39.44 o 11 0 1 40.43 77.84 32.02 o -11 1 1 14.83 -5.89 23.43 o -10 1 1 59.44 82.69 30.92 o -9 1 1 884.07 858.33 46.89 o -8 1 1 174.99 147.09 23.54 o -7 1 1 157.34 184.23 18.75 o -6 1 1 151.10 189.44 13.60 o -5 1 1 2291.37 2227.00 48.37 o -4 1 1 423.20 329.02 46.27 o -3 1 1 615.58 662.03 41.28 o -2 1 1 1037.43 1074.26 23.67 o -1 1 1 94.71 98.34 7.61 o 0 1 1 1891.66 1882.00 32.01 o 2 1 1 14487.64 15074.58 216.46 o 3 1 1 9560.17 9964.93 147.28 o 4 1 1 1355.39 1327.31 26.21 o 5 1 1 194.46 192.09 11.22 o 6 1 1 102.98 106.03 13.12 o 7 1 1 920.42 877.04 31.99 o 8 1 1 42.80 65.76 18.80 o 9 1 1 653.11 576.36 60.30 o 10 1 1 48.79 59.42 20.45 o 11 1 1 42.41 54.23 32.14 o -11 2 1 97.31 163.56 37.54 o -10 2 1 127.22 103.43 23.19 o -9 2 1 526.19 523.13 41.36 o -8 2 1 185.12 189.03 20.98 o -7 2 1 156.35 167.60 18.83 o -6 2 1 175.10 115.90 66.62 o -5 2 1 1759.04 1659.75 39.32 o -3 2 1 15.32 13.68 4.94 o -2 2 1 7391.62 7858.20 122.85 o -1 2 1 1397.14 1380.58 20.76 o 1 2 1 353.53 333.36 11.98 o 2 2 1 25869.16 27640.98 341.84 o 3 2 1 445.50 471.62 30.46 o 4 2 1 1189.32 1063.89 32.17 o 5 2 1 737.37 725.89 30.38 o 6 2 1 267.66 260.50 16.86 o 7 2 1 0.03 -1.52 8.60 o 8 2 1 29.83 50.53 12.64 o 9 2 1 0.63 21.05 14.85 o 10 2 1 513.08 455.41 43.94 o 11 2 1 142.30 221.92 67.35 o -11 3 1 86.08 99.23 26.86 o -10 3 1 12.14 11.03 15.83 o -9 3 1 508.83 560.26 45.31 o -8 3 1 409.67 387.17 24.27 o -7 3 1 272.98 300.74 24.83 o -6 3 1 146.48 127.62 20.30 o -5 3 1 1570.66 1536.11 44.51 o -4 3 1 1617.06 1535.29 31.12 o -3 3 1 1592.67 1593.59 30.84 o -1 3 1 9057.38 9467.67 109.99 o 0 3 1 3814.85 3853.18 67.61 o 1 3 1 4403.95 4472.54 56.79 o 2 3 1 3736.25 3794.47 50.06 o 3 3 1 5.91 9.61 5.32 o 4 3 1 664.88 581.34 23.38 o 5 3 1 768.75 738.65 28.44 o 6 3 1 21.69 47.94 11.70 o 7 3 1 240.45 217.51 20.16 o 8 3 1 984.76 890.36 42.54 o 9 3 1 71.24 83.29 20.47 o 10 3 1 94.10 99.59 23.25 o 11 3 1 125.79 151.41 30.09 o -10 4 1 12.16 24.26 17.18 o -9 4 1 24.74 19.52 13.45 o -8 4 1 1228.18 1171.83 47.89 o -7 4 1 0.07 18.81 10.08 o -6 4 1 1020.90 1003.47 37.21 o -5 4 1 34.40 44.93 11.08 o -4 4 1 69.96 100.89 15.37 o -3 4 1 1297.04 1256.59 29.16 o -2 4 1 1681.42 1560.94 39.03 o -1 4 1 564.01 555.31 24.30 o 0 4 1 1023.39 1000.91 28.24 o 1 4 1 4389.19 4590.19 60.93 o 2 4 1 252.97 286.51 11.60 o 3 4 1 2707.90 2839.54 48.97 o 4 4 1 1192.93 1182.09 79.98 o 5 4 1 465.79 516.07 26.53 o 6 4 1 389.58 460.41 51.45 o 7 4 1 170.55 188.20 21.09 o 8 4 1 1563.76 1279.01 68.20 o 9 4 1 60.11 55.26 19.41 o 10 4 1 55.11 78.29 22.84 o -10 5 1 99.89 42.88 29.50 o -9 5 1 49.52 35.29 22.31 o -8 5 1 5.44 16.31 11.49 o -7 5 1 51.41 80.60 16.08 o -6 5 1 206.82 219.00 21.22 o -5 5 1 228.20 238.83 24.65 o -4 5 1 353.15 344.48 16.27 o -2 5 1 1579.45 1571.45 32.54 o -1 5 1 1.52 -2.21 5.33 o 0 5 1 2159.95 2036.73 47.80 o 1 5 1 139.93 173.57 12.85 o 2 5 1 944.23 978.18 29.39 o 3 5 1 1920.65 1772.02 32.37 o 5 5 1 6.03 -0.60 9.14 o 6 5 1 61.37 101.47 15.54 o 7 5 1 408.70 425.41 30.78 o 8 5 1 501.99 530.42 35.18 o 9 5 1 0.19 15.73 14.06 o 10 5 1 304.12 243.03 52.26 o -10 6 1 15.06 54.59 32.51 o -9 6 1 17.62 18.57 18.52 o -8 6 1 8.49 31.12 24.63 o -7 6 1 1.21 -0.48 14.41 o -6 6 1 2387.03 2107.07 78.41 o -5 6 1 14.22 22.10 15.57 o -4 6 1 1.55 18.44 9.33 o -3 6 1 830.75 852.31 22.15 o -2 6 1 505.13 473.88 36.67 o -1 6 1 58.65 62.74 10.40 o 0 6 1 269.09 296.30 28.06 o 1 6 1 48.51 31.83 8.32 o 2 6 1 39.33 36.51 7.21 o 3 6 1 140.32 181.88 12.00 o 4 6 1 1.48 13.54 10.16 o 5 6 1 780.28 736.22 32.88 o 6 6 1 10.87 18.82 10.87 o 7 6 1 24.28 47.07 18.45 o 8 6 1 9.53 46.90 19.43 o 9 6 1 106.23 156.99 36.31 o 10 6 1 0.35 21.71 34.23 o -9 7 1 4.45 15.76 20.24 o -8 7 1 26.09 49.21 20.75 o -7 7 1 38.90 45.31 20.12 o -6 7 1 50.99 63.93 21.06 o -5 7 1 45.52 66.38 20.69 o -4 7 1 22.91 32.13 12.73 o -3 7 1 419.29 433.04 22.12 o -2 7 1 112.07 103.46 12.90 o -1 7 1 81.17 119.41 14.25 o 0 7 1 2560.81 2403.01 51.07 o 1 7 1 309.09 320.06 26.38 o 2 7 1 62.52 69.02 11.45 o 3 7 1 43.26 41.15 9.38 o 4 7 1 158.29 186.76 34.84 o 5 7 1 8.82 38.15 18.10 o 6 7 1 108.63 106.29 22.84 o 7 7 1 4.38 21.24 18.80 o 8 7 1 71.34 46.22 57.45 o 9 7 1 6.17 24.31 22.31 o -8 8 1 36.47 35.70 42.72 o -7 8 1 298.88 336.99 43.41 o -6 8 1 20.17 55.83 23.14 o -5 8 1 348.31 336.79 39.31 o -4 8 1 92.23 97.74 18.44 o -3 8 1 512.06 543.59 32.89 o -2 8 1 4.81 5.70 8.75 o -1 8 1 22.48 10.34 9.70 o 0 8 1 45.05 47.33 11.27 o 1 8 1 163.82 146.46 15.71 o 2 8 1 1.71 16.89 9.30 o 3 8 1 153.28 137.10 25.17 o 4 8 1 10.87 22.92 16.57 o 5 8 1 1415.54 1187.62 61.21 o 6 8 1 160.45 183.09 56.65 o 7 8 1 42.42 79.59 24.31 o 8 8 1 7.18 21.14 30.42 o -8 9 1 45.11 81.98 32.81 o -7 9 1 172.70 204.72 45.88 o -6 9 1 49.11 36.35 23.60 o -5 9 1 0.41 4.24 15.97 o -4 9 1 101.67 73.75 23.16 o -3 9 1 254.16 273.32 27.05 o -2 9 1 23.83 43.23 12.75 o -1 9 1 264.49 258.11 21.43 o 0 9 1 295.29 252.10 20.97 o 1 9 1 93.55 93.05 14.46 o 2 9 1 54.23 63.31 14.40 o 4 9 1 117.59 92.94 25.60 o 5 9 1 0.05 31.42 27.39 o 6 9 1 7.47 17.78 20.03 o 7 9 1 73.70 84.57 26.91 o 8 9 1 62.53 74.08 37.33 o -7 10 1 61.79 68.47 31.07 o -6 10 1 4.34 6.77 30.21 o -5 10 1 30.42 79.55 24.09 o -4 10 1 72.85 88.42 25.73 o -3 10 1 1004.66 930.53 113.30 o -2 10 1 274.06 283.10 23.24 o -1 10 1 11.05 41.86 12.04 o 0 10 1 34.48 36.90 11.75 o 1 10 1 200.73 206.32 20.54 o 2 10 1 259.99 279.69 34.95 o 3 10 1 80.49 124.01 27.62 o 4 10 1 27.02 15.79 20.04 o 5 10 1 34.31 57.06 25.06 o 6 10 1 166.96 196.51 39.24 o 7 10 1 2.26 47.39 28.91 o -6 11 1 50.16 18.70 41.19 o -5 11 1 6.44 8.26 29.23 o -4 11 1 245.05 316.93 44.62 o -3 11 1 112.84 151.41 31.62 o -2 11 1 35.45 29.40 26.04 o -1 11 1 43.06 46.73 13.42 o 0 11 1 202.84 246.12 23.72 o 1 11 1 7.46 43.12 15.38 o 2 11 1 41.76 71.47 22.89 o 3 11 1 33.24 18.18 19.72 o 4 11 1 94.65 124.89 30.05 o 5 11 1 1.00 10.96 23.98 o 6 11 1 142.01 180.79 37.46 o -4 12 1 9.07 5.04 27.28 o -3 12 1 13.49 44.07 39.44 o -2 12 1 89.94 58.49 53.27 o -1 12 1 20.56 33.36 21.31 o 0 12 1 0.01 12.42 14.87 o 1 12 1 140.93 164.81 32.51 o 2 12 1 80.42 148.71 32.75 o 3 12 1 0.04 17.96 21.72 o 4 12 1 7.93 54.46 27.98 o -10 0 2 2.46 38.83 23.19 o -8 0 2 166.20 230.33 40.24 o -6 0 2 2122.54 2243.07 64.42 o -4 0 2 385.49 397.86 27.79 o -2 0 2 68.75 105.69 13.49 o 0 0 2 14185.35 14196.43 209.21 o 2 0 2 29.10 23.72 4.98 o 4 0 2 57.54 51.23 8.80 o 6 0 2 3378.24 3147.39 77.41 o 8 0 2 231.34 217.15 36.07 o 10 0 2 923.58 1042.18 90.23 o -11 1 2 32.33 -12.82 26.44 o -10 1 2 50.28 44.24 18.25 o -9 1 2 158.77 199.15 28.59 o -8 1 2 196.91 206.04 27.25 o -7 1 2 326.49 353.89 24.92 o -6 1 2 6910.95 6859.08 104.89 o -5 1 2 15.64 20.67 7.22 o -3 1 2 501.36 509.34 17.53 o -2 1 2 2842.25 3163.33 55.75 o -1 1 2 2355.80 2482.82 37.20 o 0 1 2 35239.35 35702.18 435.47 o 1 1 2 2505.94 2690.24 38.86 o 2 1 2 1311.47 1365.67 22.21 o 3 1 2 11.37 13.72 4.64 o 4 1 2 71.19 84.64 7.36 o 5 1 2 1.11 10.29 4.74 o 6 1 2 111.86 160.18 15.32 o 7 1 2 28.45 45.62 10.48 o 8 1 2 30.79 37.83 11.40 o 9 1 2 53.42 94.10 32.73 o 10 1 2 12.56 14.98 17.11 o 11 1 2 648.31 541.17 52.29 o -11 2 2 169.47 125.51 27.14 o -10 2 2 0.58 56.13 25.46 o -9 2 2 267.20 252.13 45.45 o -8 2 2 0.57 26.01 11.55 o -7 2 2 24.65 28.91 10.73 o -6 2 2 212.41 279.28 38.71 o -5 2 2 100.76 119.72 11.87 o -4 2 2 294.75 295.69 15.64 o -3 2 2 982.54 1044.54 27.38 o -2 2 2 9815.07 10584.82 162.58 o -1 2 2 3267.69 3419.71 50.86 o 0 2 2 157.24 179.38 9.39 o 1 2 2 155.14 153.06 6.50 o 2 2 2 59957.29 61028.95 741.10 o 3 2 2 1263.12 1385.08 46.95 o 5 2 2 11.36 6.84 5.65 o 6 2 2 155.43 143.95 13.13 o 7 2 2 186.56 188.64 16.53 o 8 2 2 797.17 743.09 50.64 o 9 2 2 12.53 17.76 15.40 o 10 2 2 536.20 510.97 45.60 o 11 2 2 17.80 34.96 27.97 o -11 3 2 111.26 97.42 48.83 o -10 3 2 12.04 9.68 15.05 o -9 3 2 28.06 24.41 25.06 o -7 3 2 1779.57 1711.07 65.53 o -6 3 2 683.13 636.87 39.03 o -5 3 2 1229.80 1154.04 32.83 o -3 3 2 4.97 10.99 6.20 o -2 3 2 951.50 944.40 18.66 o -1 3 2 111.07 114.62 9.04 o 0 3 2 741.98 713.97 29.32 o 1 3 2 1155.43 1213.98 21.59 o 2 3 2 352.96 362.10 10.52 o 3 3 2 490.41 557.50 21.65 o 4 3 2 1566.01 1444.99 49.03 o 5 3 2 443.82 468.68 25.39 o 6 3 2 74.34 82.37 11.32 o 7 3 2 99.06 64.20 31.37 o 8 3 2 235.05 216.83 23.67 o 9 3 2 59.47 64.91 19.93 o 10 3 2 51.83 30.34 17.93 o 11 3 2 1.40 7.23 18.22 o -10 4 2 2.68 4.11 19.41 o -9 4 2 265.34 280.13 33.26 o -8 4 2 32.72 53.06 14.69 o -7 4 2 0.81 -16.59 8.30 o -6 4 2 474.86 510.11 28.05 o -5 4 2 2.94 13.57 8.62 o -4 4 2 576.76 596.44 19.13 o -3 4 2 1265.91 1197.98 27.12 o -2 4 2 1070.90 1099.22 21.76 o -1 4 2 3325.59 3447.41 56.93 o 0 4 2 42.94 44.52 6.89 o 1 4 2 334.82 356.10 12.61 o 2 4 2 272.24 282.33 11.01 o 4 4 2 2046.46 2065.31 51.23 o 5 4 2 11.24 14.53 9.14 o 6 4 2 1.71 6.37 8.82 o 7 4 2 563.06 525.82 31.90 o 8 4 2 447.30 400.28 30.99 o 9 4 2 86.61 94.39 22.12 o 10 4 2 168.91 143.65 28.14 o -10 5 2 6.63 24.90 27.48 o -9 5 2 156.40 152.84 39.23 o -8 5 2 11.48 -5.26 16.08 o -7 5 2 641.67 563.61 34.18 o -5 5 2 46.76 65.57 13.03 o -4 5 2 68.28 94.80 17.32 o -3 5 2 1172.33 1049.12 26.03 o -2 5 2 190.13 222.56 10.70 o -1 5 2 210.39 202.75 14.06 o 0 5 2 3399.96 3338.72 68.72 o 1 5 2 2250.97 2332.08 44.42 o 2 5 2 1074.98 1098.36 23.89 o 3 5 2 2700.76 2682.89 43.11 o 4 5 2 2787.54 2668.66 62.57 o 5 5 2 3.83 7.51 13.18 o 6 5 2 66.88 85.08 15.89 o 7 5 2 16.40 19.05 12.44 o 8 5 2 100.87 158.34 22.40 o 10 5 2 182.73 244.05 73.55 o -10 6 2 52.31 102.29 31.05 o -9 6 2 0.05 32.31 37.85 o -8 6 2 212.97 210.75 74.22 o 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