#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2212388.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212388_Fobs loop_ _publ_author_name 'Huang, Wei-Hao' 'Zavalij, Peter Y.' 'Isaacs, Lyle' _publ_section_title ; Cucurbit[6]uril p-phenylenediammonium diiodide decahydrate inclusion complex ; _journal_coeditor_code TK2125 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1060 _journal_page_last o1062 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.447 _cell_angle_gamma 90.000 _cell_length_a 11.8540 _cell_length_b 15.4605 _cell_length_c 15.2789 _exptl_crystal_F_000 1564.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file tk2125Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' as in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 328.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 26115.41 24131.86 341.48 o 4 0 0 69081.91 69513.75 975.42 o 6 0 0 1220.85 663.13 13.63 o 8 0 0 6151.99 7332.85 106.01 o 10 0 0 1916.38 2116.58 34.75 o 12 0 0 105.09 89.65 5.89 o 14 0 0 710.50 661.61 28.82 o 2 1 0 2631.87 2739.04 24.52 o 3 1 0 24.61 91.59 4.86 o 4 1 0 1253.56 1311.39 14.36 o 5 1 0 15754.31 16475.68 163.45 o 6 1 0 174.83 270.86 5.40 o 7 1 0 1850.94 1443.32 16.72 o 8 1 0 411.93 461.61 8.20 o 9 1 0 2836.27 2658.94 29.53 o 10 1 0 3221.49 3314.25 36.39 o 11 1 0 176.24 156.00 5.01 o 12 1 0 1593.00 1516.15 24.03 o 13 1 0 1119.59 1151.97 28.72 o 14 1 0 10.88 2.55 6.87 o 15 1 0 651.05 654.85 31.37 o 0 2 0 3853.76 2944.43 144.20 o 1 2 0 2090.56 2541.99 30.14 o 2 2 0 36337.16 33555.88 361.52 o 3 2 0 17213.04 18904.83 156.35 o 4 2 0 21699.29 20722.63 185.00 o 5 2 0 2452.86 2951.28 26.63 o 6 2 0 17345.49 17895.90 154.59 o 7 2 0 5.44 0.00 1.37 o 8 2 0 1396.59 1219.28 12.47 o 9 2 0 1070.48 1136.98 12.05 o 10 2 0 230.28 176.54 5.00 o 11 2 0 2494.95 2411.03 25.53 o 12 2 0 2.69 6.12 2.25 o 13 2 0 134.10 100.83 5.49 o 14 2 0 62.63 38.55 4.08 o 15 2 0 41.78 25.36 3.89 o 1 3 0 14.27 0.00 1.91 o 2 3 0 3091.92 3931.92 42.19 o 3 3 0 2214.00 2129.33 18.25 o 4 3 0 2059.35 2041.96 17.65 o 5 3 0 14429.43 17147.48 139.59 o 6 3 0 72.41 48.03 2.06 o 7 3 0 19978.22 20921.91 170.56 o 8 3 0 2083.75 2342.92 22.30 o 9 3 0 6359.37 6262.64 60.05 o 10 3 0 138.99 133.35 3.71 o 11 3 0 1970.21 2040.24 26.32 o 12 3 0 6.28 10.66 2.64 o 13 3 0 2067.35 2090.67 35.39 o 14 3 0 61.00 53.29 9.53 o 15 3 0 108.29 125.79 7.70 o 0 4 0 107938.35 107139.23 1502.87 o 1 4 0 5211.68 6219.66 48.76 o 2 4 0 568.05 91.44 5.59 o 3 4 0 5923.88 7575.53 66.01 o 4 4 0 5067.98 5047.37 42.03 o 5 4 0 4661.94 5451.38 45.45 o 6 4 0 2014.43 1452.16 13.37 o 7 4 0 5840.90 6291.80 54.38 o 8 4 0 14527.00 15920.84 138.29 o 9 4 0 124.04 101.51 3.25 o 10 4 0 661.60 690.81 11.74 o 11 4 0 563.61 546.38 9.96 o 12 4 0 619.29 550.64 9.37 o 13 4 0 41.54 31.77 2.87 o 14 4 0 557.15 510.28 11.69 o 15 4 0 0.02 0.00 3.80 o 1 5 0 8093.95 8928.73 71.33 o 2 5 0 2651.41 2499.30 22.86 o 3 5 0 561.01 182.83 5.24 o 4 5 0 11721.08 13643.39 118.11 o 5 5 0 4933.05 4907.93 41.24 o 6 5 0 1823.23 2188.11 19.48 o 7 5 0 6897.90 7091.88 67.27 o 8 5 0 278.84 314.37 5.34 o 9 5 0 6896.91 6876.16 78.31 o 10 5 0 2158.36 2154.66 30.63 o 11 5 0 5117.53 5078.08 54.23 o 12 5 0 660.67 635.51 10.75 o 13 5 0 2471.20 2557.28 36.17 o 14 5 0 73.00 88.60 4.53 o 1 6 0 1725.41 2184.96 18.24 o 2 6 0 17602.86 16573.14 135.22 o 3 6 0 1163.38 1272.08 13.40 o 4 6 0 8935.92 8744.71 76.50 o 5 6 0 595.16 578.81 6.78 o 6 6 0 6003.64 5771.04 51.47 o 7 6 0 187.90 274.74 6.26 o 8 6 0 1751.59 1675.99 20.84 o 9 6 0 15.47 24.57 2.86 o 10 6 0 126.66 115.76 4.65 o 11 6 0 1300.02 1135.92 16.56 o 12 6 0 198.26 196.38 5.68 o 13 6 0 28.01 19.49 2.92 o 14 6 0 50.50 42.81 3.76 o 1 7 0 6521.47 7243.35 63.81 o 2 7 0 384.21 460.48 7.58 o 3 7 0 2311.99 2018.83 19.34 o 4 7 0 651.41 596.68 7.72 o 5 7 0 6413.56 6173.14 81.16 o 6 7 0 2.23 24.55 2.39 o 7 7 0 6076.07 6109.63 66.11 o 8 7 0 290.25 309.10 6.95 o 9 7 0 5837.32 5601.65 59.30 o 10 7 0 657.01 632.17 9.95 o 11 7 0 3971.39 3954.33 47.93 o 12 7 0 15.98 16.19 2.76 o 13 7 0 4135.22 4180.67 51.26 o 14 7 0 143.21 131.91 5.94 o 0 8 0 21521.09 21419.97 283.56 o 1 8 0 245.80 296.05 3.95 o 2 8 0 12120.48 11643.11 91.06 o 3 8 0 2615.41 3052.74 33.01 o 4 8 0 6649.79 5703.36 54.70 o 5 8 0 2201.26 2150.21 22.43 o 6 8 0 1896.17 1838.01 19.73 o 7 8 0 299.46 257.60 5.59 o 8 8 0 1053.92 950.28 13.10 o 9 8 0 2731.12 2684.11 34.57 o 10 8 0 308.61 275.67 6.30 o 11 8 0 93.96 56.94 4.03 o 12 8 0 129.43 141.09 4.99 o 13 8 0 8.62 10.44 3.04 o 14 8 0 6.96 4.33 3.32 o 1 9 0 1556.86 1538.62 13.88 o 2 9 0 623.91 826.10 8.38 o 3 9 0 2131.94 2288.73 23.73 o 4 9 0 12.79 0.40 1.60 o 5 9 0 5304.97 5246.57 51.01 o 6 9 0 51.97 49.23 3.08 o 7 9 0 1508.85 1447.22 18.20 o 8 9 0 789.35 732.86 11.48 o 9 9 0 2121.16 2139.59 25.66 o 10 9 0 0.89 0.00 2.20 o 11 9 0 2100.47 2165.02 26.83 o 12 9 0 274.92 304.48 7.99 o 13 9 0 422.12 472.84 10.43 o 0 10 0 9975.10 9329.14 104.36 o 1 10 0 168.91 165.52 3.18 o 2 10 0 3911.16 3728.82 34.78 o 3 10 0 1320.65 1414.43 16.01 o 4 10 0 8752.94 8419.02 80.05 o 5 10 0 1041.77 1038.91 12.82 o 6 10 0 3698.04 3499.05 35.93 o 7 10 0 1006.23 995.89 13.94 o 8 10 0 32.69 36.78 4.64 o 9 10 0 25.69 12.14 2.56 o 10 10 0 146.78 139.28 5.48 o 11 10 0 33.85 19.95 3.60 o 12 10 0 4.39 0.00 2.85 o 13 10 0 163.74 148.07 9.22 o 1 11 0 1904.09 1906.48 19.33 o 2 11 0 2.00 1.60 1.77 o 3 11 0 2538.95 2665.91 27.83 o 4 11 0 53.75 48.28 3.22 o 5 11 0 4629.30 4626.49 50.04 o 6 11 0 52.22 37.77 3.13 o 7 11 0 1525.48 1574.74 20.20 o 8 11 0 5.39 4.18 2.42 o 9 11 0 2617.98 2592.94 31.36 o 10 11 0 96.10 67.60 4.46 o 11 11 0 861.29 938.16 16.07 o 12 11 0 186.27 143.12 6.23 o 0 12 0 6689.14 6620.78 108.56 o 1 12 0 463.22 388.18 6.74 o 2 12 0 10032.13 10237.77 97.03 o 3 12 0 14.53 7.38 2.00 o 4 12 0 5648.33 5314.54 52.48 o 5 12 0 732.39 721.08 15.89 o 6 12 0 2653.35 2636.40 30.90 o 7 12 0 440.64 431.12 8.52 o 8 12 0 71.72 66.72 3.95 o 9 12 0 98.62 73.58 4.25 o 10 12 0 161.09 148.38 6.14 o 11 12 0 24.73 7.72 5.18 o 12 12 0 0.82 0.00 3.08 o 1 13 0 840.55 740.16 13.26 o 2 13 0 777.36 705.15 10.15 o 3 13 0 960.61 992.34 12.96 o 4 13 0 109.57 106.21 4.38 o 5 13 0 1088.43 1065.25 15.23 o 6 13 0 221.04 226.48 6.25 o 7 13 0 1758.49 1877.06 30.29 o 8 13 0 140.20 144.33 5.40 o 9 13 0 1437.11 1389.38 19.47 o 10 13 0 0.42 0.00 2.98 o 11 13 0 1605.04 1730.19 25.93 o 0 14 0 3064.15 2883.61 57.21 o 1 14 0 478.73 469.76 10.77 o 2 14 0 7866.39 7947.83 90.79 o 3 14 0 1705.33 1808.81 25.01 o 4 14 0 3322.48 3282.84 39.19 o 5 14 0 15.67 10.35 2.92 o 6 14 0 1537.62 1516.13 20.39 o 7 14 0 18.68 13.60 3.15 o 8 14 0 875.01 773.25 13.14 o 9 14 0 157.34 127.77 6.24 o 10 14 0 86.77 62.66 4.94 o 11 14 0 4.11 0.00 4.52 o 1 15 0 48.63 30.92 4.09 o 2 15 0 35.49 22.92 3.77 o 3 15 0 752.76 768.86 25.57 o 4 15 0 2.23 0.00 2.95 o 5 15 0 464.71 500.41 9.82 o 6 15 0 6.43 1.01 2.75 o 7 15 0 1714.59 1796.22 23.87 o 8 15 0 9.49 8.05 3.07 o 9 15 0 1010.43 1086.59 18.77 o 10 15 0 4.54 8.07 3.70 o 0 16 0 835.86 791.56 22.25 o 1 16 0 191.77 181.04 7.81 o 2 16 0 1461.36 1511.80 30.45 o 3 16 0 0.74 1.02 3.67 o 4 16 0 2244.78 2141.02 33.43 o 5 16 0 168.71 176.50 7.75 o 6 16 0 672.05 700.72 13.80 o 7 16 0 11.64 7.22 3.25 o 8 16 0 471.54 454.70 10.10 o 9 16 0 4.22 1.63 3.55 o 1 17 0 245.33 222.60 9.88 o 2 17 0 70.47 65.57 7.59 o 3 17 0 129.73 119.18 7.70 o 4 17 0 5.14 0.00 4.09 o 5 17 0 462.67 447.85 12.30 o 6 17 0 83.43 77.26 5.94 o 7 17 0 570.76 633.49 15.13 o 8 17 0 23.46 17.16 4.19 o 0 18 0 1944.56 1975.95 65.17 o 1 18 0 5.20 1.85 4.47 o 2 18 0 2021.76 2085.54 38.66 o 3 18 0 104.54 94.91 7.55 o 4 18 0 1498.90 1523.77 31.01 o 5 18 0 31.95 24.47 5.38 o 6 18 0 608.79 642.36 15.62 o 1 19 0 0.13 0.00 4.41 o 2 19 0 2.27 0.00 4.70 o 3 19 0 305.98 304.92 12.27 o 4 19 0 2.49 0.00 4.86 o 5 19 0 83.86 104.39 8.39 o 0 20 0 1212.49 1380.74 52.65 o 1 20 0 25.28 19.68 7.20 o -13 0 1 3397.59 3637.10 72.05 o -11 0 1 4769.49 4767.78 72.32 o -9 0 1 12778.19 12603.08 179.61 o -7 0 1 2601.88 2761.78 53.57 o -5 0 1 8951.60 8996.55 201.41 o -3 0 1 342.11 327.94 6.35 o 3 0 1 666.22 792.65 20.76 o 5 0 1 19287.08 20479.75 286.74 o 7 0 1 3772.71 3558.61 69.51 o 9 0 1 11171.06 11290.37 161.36 o 11 0 1 8300.77 8477.79 123.83 o 13 0 1 2657.55 2701.18 79.03 o -14 1 1 722.20 725.67 32.03 o -13 1 1 9.00 0.00 5.13 o -12 1 1 19.37 18.63 3.09 o -11 1 1 29.08 17.34 3.43 o -10 1 1 154.23 169.63 4.33 o -9 1 1 134.71 141.00 4.44 o -8 1 1 6914.40 6717.06 68.86 o -7 1 1 90.60 86.48 2.92 o -6 1 1 3671.11 3577.06 40.28 o -5 1 1 775.75 1209.36 13.69 o -4 1 1 16019.25 16062.98 159.18 o -3 1 1 6267.31 7263.23 67.80 o -2 1 1 6821.58 6529.58 57.25 o -1 1 1 4581.06 4518.33 135.19 o 1 1 1 2781.01 2427.59 55.38 o 2 1 1 7525.89 6929.44 103.93 o 3 1 1 7223.84 8281.54 71.98 o 4 1 1 18681.06 17271.46 149.52 o 5 1 1 1708.11 1927.92 24.06 o 6 1 1 5799.42 5499.80 56.54 o 7 1 1 7.33 0.00 1.28 o 8 1 1 3241.25 3183.37 34.25 o 9 1 1 233.59 222.40 5.20 o 10 1 1 388.90 391.65 6.20 o 11 1 1 1179.35 1107.67 13.43 o 12 1 1 93.39 98.24 3.64 o 13 1 1 6.94 4.70 2.36 o 14 1 1 184.63 149.69 14.58 o 15 1 1 3.86 0.00 7.54 o -15 2 1 556.92 564.95 19.34 o -14 2 1 8.43 11.87 3.24 o -13 2 1 1384.01 1442.64 25.84 o -12 2 1 229.60 229.17 5.86 o -11 2 1 1081.88 1071.12 14.18 o -10 2 1 8.72 3.48 1.55 o -9 2 1 7132.43 6946.89 61.82 o -8 2 1 36.56 20.64 2.08 o -7 2 1 17032.96 18018.55 155.81 o -6 2 1 816.75 622.95 6.84 o -5 2 1 556.08 183.33 2.85 o -4 2 1 1270.74 1340.83 11.84 o -3 2 1 4133.77 4043.43 33.80 o -2 2 1 1460.27 1782.22 16.50 o -1 2 1 5051.07 6504.22 65.75 o 0 2 1 45.25 0.00 1.04 o 1 2 1 3772.05 5140.70 45.25 o 2 2 1 353.68 301.58 4.16 o 3 2 1 1884.63 1603.05 16.90 o 4 2 1 134.44 313.50 4.10 o 5 2 1 1444.76 849.89 10.64 o 6 2 1 28.13 14.42 2.11 o 7 2 1 18887.87 20103.36 173.55 o 8 2 1 96.15 107.97 3.14 o 9 2 1 8665.01 8617.69 71.79 o 10 2 1 45.43 37.31 2.23 o 11 2 1 2897.66 2953.59 33.01 o 12 2 1 46.99 51.49 3.47 o 13 2 1 1351.02 1372.36 24.72 o 14 2 1 0.69 0.00 4.03 o 15 2 1 1067.18 1185.84 26.81 o -15 3 1 319.49 298.17 10.84 o -14 3 1 44.04 29.43 4.77 o -13 3 1 163.29 145.18 5.78 o -12 3 1 8.85 5.36 2.28 o -11 3 1 1953.17 1895.69 26.70 o -10 3 1 434.42 474.22 7.30 o -9 3 1 819.34 816.28 9.28 o -8 3 1 1886.85 1734.09 17.37 o -7 3 1 254.94 346.51 4.35 o -6 3 1 2792.50 2610.68 22.59 o -5 3 1 8390.06 9424.22 73.41 o -4 3 1 26173.99 24263.95 211.96 o -3 3 1 612.20 751.20 7.11 o -2 3 1 62010.48 62992.73 625.89 o -1 3 1 4915.31 4778.41 44.91 o 0 3 1 39430.29 36125.40 313.42 o 1 3 1 2249.23 2038.88 18.39 o 2 3 1 63404.22 63128.24 544.87 o 3 3 1 494.05 491.25 4.77 o 4 3 1 22741.89 21526.81 174.95 o 5 3 1 830.60 1124.43 12.76 o 6 3 1 2998.31 2783.99 25.57 o 7 3 1 636.73 629.29 7.30 o 8 3 1 2218.53 2122.08 20.42 o 9 3 1 553.69 588.60 8.51 o 10 3 1 774.48 821.14 9.56 o 11 3 1 1049.24 1002.18 12.19 o 12 3 1 99.91 99.41 5.17 o 13 3 1 102.20 89.97 5.38 o 14 3 1 17.99 14.89 3.55 o 15 3 1 356.68 347.09 15.19 o -15 4 1 707.89 790.15 20.75 o -14 4 1 34.19 26.35 4.54 o -13 4 1 1031.83 1000.71 17.71 o -12 4 1 167.99 156.73 4.98 o -11 4 1 3560.08 3632.90 47.19 o -10 4 1 87.44 69.14 3.55 o -9 4 1 2163.73 1925.47 20.41 o -8 4 1 1309.68 1531.78 15.39 o -7 4 1 5961.15 5874.59 58.25 o -6 4 1 125.24 152.46 3.56 o -5 4 1 13507.29 12797.02 104.65 o -4 4 1 104.50 91.65 3.27 o -3 4 1 1920.17 2406.70 21.91 o -2 4 1 1444.52 1551.15 18.33 o -1 4 1 25660.85 26715.13 232.22 o 0 4 1 34.01 55.19 1.74 o 1 4 1 44581.39 45610.70 371.03 o 2 4 1 3180.63 3653.61 33.45 o 3 4 1 13222.77 14669.84 119.52 o 4 4 1 6337.80 7188.17 56.32 o 5 4 1 15063.72 15151.30 130.28 o 6 4 1 3006.16 3500.68 29.95 o 7 4 1 5013.80 5021.26 56.10 o 8 4 1 17.94 32.49 2.01 o 9 4 1 4390.22 4039.01 37.19 o 10 4 1 3.17 0.81 1.51 o 11 4 1 4845.32 4809.45 56.17 o 12 4 1 77.53 63.92 4.16 o 13 4 1 2517.05 2657.18 37.12 o 14 4 1 15.25 14.22 3.07 o 15 4 1 575.73 599.73 14.81 o -14 5 1 14.66 15.12 2.80 o -13 5 1 0.24 0.00 2.81 o -12 5 1 23.94 33.12 3.58 o -11 5 1 478.20 420.61 15.79 o -10 5 1 518.78 488.52 9.69 o -9 5 1 65.15 75.97 3.70 o -8 5 1 1831.70 1788.90 25.47 o -7 5 1 1789.80 1731.94 17.01 o -6 5 1 231.38 83.69 3.69 o -5 5 1 81.51 83.55 2.18 o -4 5 1 7722.21 6155.92 54.21 o -3 5 1 39.33 94.81 3.11 o -2 5 1 7239.78 7638.52 91.39 o -1 5 1 1020.39 860.88 8.35 o 0 5 1 45616.37 41506.73 481.65 o 1 5 1 6470.49 7619.72 59.62 o 2 5 1 15061.71 14576.01 118.89 o 3 5 1 481.99 590.68 9.86 o 4 5 1 16961.22 16444.32 134.15 o 5 5 1 1279.17 1223.30 10.92 o 6 5 1 5123.11 4869.20 39.02 o 7 5 1 221.69 274.70 4.01 o 8 5 1 1939.83 1833.17 18.14 o 9 5 1 43.03 38.43 2.78 o 10 5 1 27.00 32.03 2.42 o 11 5 1 130.70 104.05 5.59 o 12 5 1 328.05 291.44 6.65 o 13 5 1 6.49 1.25 2.86 o 14 5 1 5.89 0.00 2.40 o -14 6 1 24.55 15.14 2.99 o -13 6 1 1066.33 1051.17 16.26 o -12 6 1 51.24 55.47 4.30 o -11 6 1 740.54 851.89 12.95 o -10 6 1 2.25 7.35 2.35 o -9 6 1 4496.57 4466.81 52.74 o -8 6 1 1601.20 1608.69 21.90 o -7 6 1 10548.18 11140.22 112.47 o -6 6 1 85.26 139.41 3.30 o -5 6 1 7990.83 7872.81 80.60 o -4 6 1 3762.86 3954.80 38.23 o -3 6 1 362.18 437.45 6.38 o -2 6 1 4516.45 5274.40 50.07 o -1 6 1 71.02 37.05 1.85 o 0 6 1 8945.86 10754.79 83.79 o 1 6 1 2542.65 2828.27 26.45 o 2 6 1 5659.68 6051.64 50.35 o 3 6 1 3064.78 3529.94 31.91 o 4 6 1 458.93 628.89 6.97 o 5 6 1 7149.38 6930.60 57.75 o 6 6 1 785.75 723.37 8.27 o 7 6 1 7164.59 7314.76 64.95 o 8 6 1 34.77 40.68 2.33 o 9 6 1 5547.08 5630.88 73.79 o 10 6 1 4.63 2.76 2.04 o 11 6 1 1370.22 1346.55 18.98 o 12 6 1 3.32 0.00 2.24 o 13 6 1 821.47 855.80 15.36 o 14 6 1 0.01 0.00 2.74 o -14 7 1 452.48 438.14 9.49 o -13 7 1 325.18 322.22 9.14 o -12 7 1 49.60 59.17 3.71 o -11 7 1 177.42 157.99 5.81 o -10 7 1 0.76 4.90 3.78 o -9 7 1 0.76 0.00 2.11 o -8 7 1 305.32 247.19 6.25 o -7 7 1 85.98 50.70 3.15 o -6 7 1 4841.57 4816.60 50.43 o -5 7 1 18.69 57.80 2.38 o -4 7 1 13100.10 12897.45 129.32 o -3 7 1 9.08 2.33 1.19 o -2 7 1 30459.21 32757.41 281.73 o -1 7 1 5612.22 6579.05 54.81 o 0 7 1 16083.42 15191.48 118.03 o 1 7 1 764.79 689.37 8.01 o 2 7 1 29112.88 29440.50 267.20 o 3 7 1 25.97 17.17 1.23 o 4 7 1 14121.38 14182.10 123.16 o 5 7 1 445.56 438.60 6.37 o 6 7 1 4591.42 4219.89 41.29 o 7 7 1 0.16 0.00 1.50 o 8 7 1 742.31 634.02 8.80 o 9 7 1 22.05 8.49 2.98 o 10 7 1 140.70 144.89 4.88 o 11 7 1 1599.79 1489.32 20.90 o 12 7 1 5.62 4.72 2.56 o 13 7 1 71.33 47.33 7.34 o 14 7 1 481.58 509.95 14.97 o -14 8 1 16.88 18.34 4.24 o -13 8 1 664.69 704.14 12.84 o -12 8 1 0.43 0.00 2.42 o -11 8 1 3871.62 3806.56 43.92 o -10 8 1 97.26 80.01 4.40 o -9 8 1 3871.09 3712.83 45.26 o -8 8 1 54.99 54.59 3.55 o -7 8 1 2376.03 2399.31 45.73 o -6 8 1 2.75 12.83 2.30 o -5 8 1 3888.09 3741.10 44.28 o -4 8 1 5038.54 5311.07 65.10 o -3 8 1 487.68 373.56 5.72 o -2 8 1 837.58 850.33 8.76 o -1 8 1 9712.29 10790.70 84.47 o 0 8 1 128.66 159.33 2.89 o 1 8 1 280.89 248.15 4.68 o 2 8 1 1187.95 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