#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2212396.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212396_Fobs loop_ _publ_author_name 'Garc\'es-Rodr\'iguez, Alejandra' 'Morales-Morales, David' 'Hern\'andez-Ortega, Sim\'on' _publ_section_title ; [1,1'-Bis(diphenylphosphino)ferrocene-\k^2^P,P']bis(2,3,4,5,6-pentafluorobenzenethiolato)platinum(II) ; _journal_coeditor_code WM2078 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m479 _journal_page_last m481 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.807 _cell_angle_gamma 90.000 _cell_length_a 19.7466 _cell_length_b 22.0846 _cell_length_c 19.7669 _exptl_crystal_F_000 4480.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file wm2078Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 023MMD06 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1029.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 946.17 1171.56 134.22 o 8 0 0 40411.63 42320.08 1527.50 o 10 0 0 14156.80 14361.42 870.84 o 12 0 0 28148.95 27264.30 1462.28 o 14 0 0 4786.60 5617.31 1368.50 o 16 0 0 5361.56 6064.00 782.18 o 18 0 0 15706.07 14930.01 1166.61 o 20 0 0 37981.57 35354.33 2083.75 o 22 0 0 5694.57 6042.13 1060.99 o 1 1 0 1524.92 1598.97 71.15 o 3 1 0 5860.72 5707.07 273.12 o 4 1 0 36593.42 38067.12 1046.08 o 5 1 0 43540.68 47258.07 1295.14 o 6 1 0 49958.31 51364.05 1418.37 o 7 1 0 34828.48 36106.29 1032.07 o 8 1 0 5925.53 5882.71 374.99 o 9 1 0 9618.25 9406.38 371.32 o 10 1 0 15152.19 15521.23 549.75 o 11 1 0 4376.95 4577.30 287.30 o 12 1 0 26232.36 27877.29 900.86 o 13 1 0 14591.03 14470.62 594.15 o 14 1 0 24150.54 23107.80 959.57 o 15 1 0 24725.13 25766.96 1059.47 o 16 1 0 16045.45 14064.70 1250.61 o 17 1 0 1041.02 926.72 356.38 o 18 1 0 4475.60 3759.12 500.30 o 19 1 0 4591.29 4264.42 540.27 o 20 1 0 784.39 769.18 405.52 o 21 1 0 403.30 155.34 347.87 o 22 1 0 343.90 654.25 393.46 o 2 2 0 31473.20 34602.65 844.90 o 3 2 0 27855.55 30204.35 820.17 o 4 2 0 283324.47 314268.44 8127.10 o 5 2 0 14202.52 14674.50 464.92 o 6 2 0 54155.99 58598.43 1606.66 o 7 2 0 38376.73 39099.36 1120.64 o 8 2 0 29.74 46.10 103.91 o 9 2 0 6778.35 6873.10 324.69 o 10 2 0 2680.68 2520.24 318.83 o 11 2 0 1383.83 1631.11 197.43 o 12 2 0 114.56 331.37 243.60 o 13 2 0 45357.32 44061.38 1342.73 o 14 2 0 11629.79 11253.03 626.11 o 15 2 0 544.87 802.23 301.17 o 16 2 0 129.77 117.50 282.33 o 17 2 0 648.12 431.46 338.52 o 18 2 0 1930.98 2169.90 504.81 o 19 2 0 15836.13 15814.46 865.75 o 20 2 0 28.42 -323.99 341.05 o 21 2 0 30327.55 29643.46 1320.30 o 22 2 0 797.60 833.29 401.43 o 1 3 0 47156.84 51078.00 1352.63 o 2 3 0 495.70 753.40 109.74 o 3 3 0 78560.55 86812.68 2083.22 o 4 3 0 31131.95 33997.80 857.35 o 5 3 0 39012.35 41096.80 1034.88 o 6 3 0 105745.54 115205.77 2789.78 o 7 3 0 13287.27 12998.75 450.77 o 8 3 0 6990.93 7555.53 322.70 o 9 3 0 1845.16 2196.49 219.42 o 10 3 0 1086.96 1262.08 182.28 o 11 3 0 7686.82 7798.52 365.20 o 12 3 0 11520.57 10110.40 445.70 o 13 3 0 37246.96 36254.63 1140.84 o 14 3 0 60642.85 60052.34 1775.23 o 15 3 0 9266.04 9276.34 601.77 o 16 3 0 7844.54 7005.06 586.82 o 17 3 0 233.82 251.52 295.26 o 18 3 0 303.56 63.99 319.09 o 19 3 0 198.27 300.78 352.19 o 20 3 0 421.13 871.47 390.50 o 21 3 0 146.22 -8.10 337.48 o 22 3 0 2081.28 2993.83 537.98 o 0 4 0 37718.04 41217.54 1432.24 o 1 4 0 5336.54 5433.71 198.14 o 2 4 0 14364.58 14388.37 388.59 o 3 4 0 22386.10 23055.39 599.92 o 4 4 0 256.09 177.40 80.38 o 5 4 0 30323.86 32495.90 926.74 o 6 4 0 8912.03 8781.34 292.37 o 7 4 0 4996.78 4965.57 231.01 o 8 4 0 47814.27 45657.34 1308.63 o 9 4 0 1373.24 1396.87 188.88 o 10 4 0 4390.00 4177.82 329.51 o 11 4 0 4868.30 5269.59 336.19 o 12 4 0 38378.18 36376.54 1135.25 o 13 4 0 75.15 159.51 176.12 o 14 4 0 7888.87 7656.48 438.61 o 15 4 0 421.62 499.84 285.18 o 16 4 0 4158.37 4082.78 477.73 o 17 4 0 1030.68 555.45 434.02 o 18 4 0 162.89 -160.76 308.86 o 19 4 0 587.78 889.71 373.10 o 20 4 0 26725.78 26256.63 1377.19 o 21 4 0 34.49 -109.88 407.78 o 22 4 0 13069.94 12830.03 937.44 o 1 5 0 129563.29 141953.88 3691.03 o 2 5 0 184254.00 205099.25 5314.25 o 3 5 0 18674.36 19659.65 576.20 o 4 5 0 1707.70 1984.23 150.27 o 5 5 0 84088.22 92791.03 2260.50 o 6 5 0 15574.44 15106.47 447.37 o 7 5 0 101168.93 107412.42 2629.68 o 8 5 0 28479.11 27208.78 752.56 o 9 5 0 656.76 924.47 121.04 o 10 5 0 56758.65 56420.00 1621.85 o 11 5 0 1089.35 1310.02 212.67 o 12 5 0 45764.25 46035.06 1389.80 o 13 5 0 27638.02 27379.26 922.20 o 14 5 0 32927.96 31765.51 1056.85 o 15 5 0 48061.56 43594.07 2187.11 o 16 5 0 13035.79 13034.31 707.37 o 17 5 0 104.61 -114.40 277.91 o 18 5 0 16.61 -125.63 316.98 o 19 5 0 2355.62 2573.56 456.39 o 20 5 0 913.75 1007.19 394.60 o 21 5 0 1048.72 720.66 385.90 o 22 5 0 1652.08 1267.58 431.13 o 0 6 0 89469.21 97188.25 3323.64 o 1 6 0 167405.02 186493.52 4429.96 o 2 6 0 125.09 202.46 95.04 o 3 6 0 22393.76 23830.42 630.61 o 4 6 0 11185.63 10886.34 337.75 o 5 6 0 12247.94 12613.96 385.22 o 6 6 0 912.31 998.64 131.94 o 7 6 0 108536.34 114713.59 3063.77 o 8 6 0 13346.04 13594.01 582.68 o 9 6 0 15649.22 14665.22 485.24 o 10 6 0 322.88 487.05 119.25 o 11 6 0 31972.52 29974.70 964.89 o 12 6 0 1168.47 1376.24 225.92 o 13 6 0 38044.65 36258.47 1153.76 o 14 6 0 1548.54 2047.81 277.97 o 15 6 0 493.66 812.00 279.50 o 16 6 0 2762.48 2978.76 416.16 o 17 6 0 2403.96 2935.18 424.47 o 18 6 0 3588.41 3598.26 490.24 o 19 6 0 6969.20 6759.33 630.50 o 20 6 0 4.17 59.83 362.43 o 21 6 0 16729.41 16703.71 1180.49 o 1 7 0 2830.52 3042.12 139.13 o 2 7 0 115863.48 124054.81 2982.90 o 3 7 0 3979.27 4270.32 182.30 o 4 7 0 360.26 414.62 97.01 o 5 7 0 1730.02 1967.01 151.11 o 6 7 0 46285.02 48289.65 1235.67 o 7 7 0 32576.87 32356.35 874.96 o 8 7 0 11626.24 11321.50 417.86 o 9 7 0 56784.05 57624.55 1490.41 o 10 7 0 10676.90 11752.31 413.37 o 11 7 0 53002.93 54566.23 1437.94 o 12 7 0 194.97 387.43 188.39 o 13 7 0 36588.20 36898.93 1178.99 o 14 7 0 28764.18 27183.83 945.24 o 15 7 0 16129.24 15933.84 939.27 o 16 7 0 2026.89 1242.18 325.71 o 17 7 0 2019.30 1439.24 356.85 o 18 7 0 3171.55 3007.12 446.01 o 19 7 0 1445.42 1452.48 386.32 o 20 7 0 1163.41 1008.80 379.51 o 21 7 0 828.05 763.11 363.33 o 0 8 0 180778.77 196905.27 6644.50 o 1 8 0 18596.17 18682.11 510.04 o 2 8 0 143037.73 152012.44 3645.67 o 3 8 0 73457.95 74806.94 1843.92 o 4 8 0 46511.46 48041.56 1221.02 o 5 8 0 663.71 986.56 125.29 o 6 8 0 31624.48 29882.49 812.62 o 7 8 0 9532.59 8917.14 327.34 o 8 8 0 112177.02 116622.43 2869.64 o 9 8 0 13514.94 13922.17 466.16 o 10 8 0 68.94 237.88 135.19 o 11 8 0 190.97 58.12 155.67 o 12 8 0 15090.55 14265.27 861.01 o 13 8 0 1381.94 1829.20 344.52 o 14 8 0 2358.52 2312.49 301.51 o 15 8 0 1908.73 1630.12 288.52 o 16 8 0 1782.54 1265.22 389.06 o 17 8 0 11576.25 11314.60 710.27 o 18 8 0 1710.44 1968.01 424.85 o 19 8 0 1430.44 192.54 369.74 o 20 8 0 13990.03 13278.15 832.66 o 21 8 0 683.58 918.46 365.72 o 1 9 0 44113.75 46642.75 1179.55 o 2 9 0 1981.42 2342.75 151.19 o 3 9 0 81771.80 87550.86 2151.61 o 4 9 0 12766.64 11694.50 411.95 o 5 9 0 1016.26 832.91 165.02 o 6 9 0 48568.17 49896.24 1286.31 o 7 9 0 21157.79 20167.37 599.96 o 8 9 0 41517.29 39935.84 1072.94 o 9 9 0 32.24 201.75 128.86 o 10 9 0 19063.72 17686.41 570.58 o 11 9 0 940.36 1340.80 190.40 o 12 9 0 42563.43 41915.52 1302.39 o 13 9 0 6875.94 7197.81 431.78 o 14 9 0 8422.90 8225.11 487.39 o 15 9 0 14135.04 14872.09 674.88 o 16 9 0 3704.80 3941.52 461.95 o 17 9 0 2498.19 3335.61 460.64 o 18 9 0 3818.31 3761.76 488.39 o 19 9 0 5924.18 5834.96 595.07 o 20 9 0 170.62 183.36 341.99 o 21 9 0 1673.32 1797.31 549.94 o 0 10 0 16759.83 19041.66 993.95 o 1 10 0 267144.63 280271.25 7303.83 o 2 10 0 49114.21 46508.93 1192.83 o 3 10 0 33393.95 36698.92 964.40 o 4 10 0 67322.14 68092.37 1709.97 o 5 10 0 1267.05 1559.71 208.25 o 6 10 0 845.69 1118.14 144.67 o 7 10 0 1420.03 1681.15 177.17 o 8 10 0 7911.45 7786.50 320.36 o 9 10 0 14836.98 15223.33 509.96 o 10 10 0 50.63 -42.93 158.34 o 11 10 0 847.96 1243.21 187.25 o 12 10 0 8662.40 8218.63 444.30 o 13 10 0 3811.84 2933.92 427.44 o 14 10 0 561.15 503.10 255.24 o 15 10 0 1270.54 781.90 248.80 o 16 10 0 9381.50 9853.44 583.85 o 17 10 0 1158.81 1377.02 362.76 o 18 10 0 2456.45 3114.38 486.17 o 19 10 0 9855.13 10328.05 932.17 o 20 10 0 38.65 157.55 381.55 o 1 11 0 380.83 526.91 111.12 o 2 11 0 154833.88 155249.02 4130.86 o 3 11 0 2186.08 1838.56 197.04 o 4 11 0 11252.79 11854.45 388.48 o 5 11 0 61891.57 61744.43 1572.74 o 6 11 0 33763.15 31610.82 874.96 o 7 11 0 22276.25 21441.90 644.03 o 8 11 0 1214.07 1119.87 165.45 o 9 11 0 6751.58 6832.16 340.71 o 10 11 0 13588.19 13819.77 617.38 o 11 11 0 21846.52 22244.81 702.36 o 12 11 0 7.82 -143.98 208.35 o 13 11 0 8250.62 7857.13 487.49 o 14 11 0 15734.86 16272.40 681.33 o 15 11 0 9168.43 9620.40 655.70 o 16 11 0 2184.54 2104.70 322.76 o 17 11 0 2781.67 2755.85 478.94 o 18 11 0 7262.84 7105.96 640.62 o 19 11 0 230.82 6.75 325.09 o 20 11 0 100.69 603.06 397.60 o 0 12 0 291033.28 314024.13 10586.73 o 1 12 0 18612.08 18931.83 595.65 o 2 12 0 27918.79 25781.94 805.25 o 3 12 0 24388.67 23758.13 758.44 o 4 12 0 1972.82 1995.15 159.54 o 5 12 0 20599.30 19929.08 630.27 o 6 12 0 3763.07 3936.24 242.83 o 7 12 0 4226.62 4583.23 274.53 o 8 12 0 4344.07 4658.81 280.24 o 9 12 0 7443.60 7715.08 366.07 o 10 12 0 3508.81 3584.46 274.66 o 11 12 0 679.76 431.42 217.15 o 12 12 0 10266.72 10086.18 500.93 o 13 12 0 2949.10 2603.66 365.36 o 14 12 0 3785.10 3677.24 429.49 o 15 12 0 746.94 953.60 268.97 o 16 12 0 2230.96 2425.25 355.11 o 17 12 0 9256.32 10487.34 704.71 o 18 12 0 668.01 -109.01 487.79 o 19 12 0 167.15 -168.29 331.82 o 1 13 0 25942.92 25740.26 722.50 o 2 13 0 26121.23 23876.19 768.59 o 3 13 0 7613.86 7313.27 332.74 o 4 13 0 7967.71 8339.31 371.18 o 5 13 0 42300.78 42244.02 1127.66 o 6 13 0 1745.27 2406.39 195.63 o 7 13 0 6991.70 7331.45 357.27 o 8 13 0 20081.40 20799.73 701.54 o 9 13 0 8632.05 9296.08 389.57 o 10 13 0 29190.78 27215.17 822.20 o 11 13 0 11464.32 10788.41 445.80 o 12 13 0 13630.43 13259.42 583.76 o 13 13 0 4647.40 5334.26 412.49 o 14 13 0 4001.56 4557.27 467.09 o 15 13 0 14640.07 13862.59 1329.22 o 16 13 0 4664.38 5429.14 610.44 o 17 13 0 420.88 476.57 560.27 o 18 13 0 2025.02 1894.10 487.70 o 19 13 0 2392.17 3567.42 580.57 o 0 14 0 1009.85 1563.00 276.44 o 1 14 0 75020.89 73907.41 1871.84 o 2 14 0 7642.19 7236.32 343.05 o 3 14 0 3172.99 3456.21 266.45 o 4 14 0 60935.94 60344.24 1733.54 o 5 14 0 2314.14 2634.07 251.88 o 6 14 0 19907.92 19958.58 702.62 o 7 14 0 9698.70 8985.85 422.11 o 8 14 0 250.86 181.51 177.85 o 9 14 0 3008.55 3192.99 306.20 o 10 14 0 439.90 680.03 226.94 o 11 14 0 8672.42 8265.35 478.75 o 12 14 0 3507.38 3084.07 440.04 o 13 14 0 4225.94 4855.23 474.91 o 14 14 0 20.00 -297.17 235.66 o 15 14 0 26.64 265.26 310.36 o 16 14 0 9315.84 10605.69 851.84 o 17 14 0 87.74 428.42 345.64 o 18 14 0 2938.66 3773.19 587.95 o 19 14 0 4263.27 5623.14 701.40 o 1 15 0 1382.22 1835.46 198.62 o 2 15 0 3936.70 4383.72 396.60 o 3 15 0 460.17 336.73 169.64 o 4 15 0 1687.97 1659.60 318.73 o 5 15 0 2404.81 2870.07 271.84 o 6 15 0 7985.61 8016.69 420.34 o 7 15 0 2346.44 2153.57 262.38 o 8 15 0 348.45 399.29 189.70 o 9 15 0 34098.86 32078.59 1342.35 o 10 15 0 16216.70 16437.67 659.88 o 11 15 0 43761.45 40574.51 1296.80 o 12 15 0 4012.60 4042.08 534.63 o 13 15 0 6332.31 6737.69 569.95 o 14 15 0 12185.69 11789.85 705.00 o 15 15 0 2289.19 2029.39 399.51 o 16 15 0 3195.78 3476.83 454.48 o 17 15 0 3662.01 3132.98 505.03 o 18 15 0 3556.67 5571.28 705.57 o 0 16 0 29465.84 28708.98 1529.07 o 1 16 0 205.66 408.11 164.00 o 2 16 0 631.32 579.11 154.86 o 3 16 0 48370.64 47272.19 1417.16 o 4 16 0 149.78 29.46 159.02 o 5 16 0 35760.34 34516.91 1096.49 o 6 16 0 8209.92 7607.65 479.33 o 7 16 0 4925.97 5114.72 374.33 o 8 16 0 4384.25 4750.67 477.84 o 9 16 0 2211.66 3095.87 715.18 o 10 16 0 651.99 654.04 283.49 o 11 16 0 2736.80 2871.76 330.12 o 12 16 0 11452.66 10991.07 652.19 o 13 16 0 903.97 1216.60 331.60 o 14 16 0 2831.22 3819.06 459.26 o 15 16 0 4670.67 3822.21 475.09 o 16 16 0 45.52 0.86 303.82 o 17 16 0 6453.45 6634.94 636.03 o 1 17 0 8935.08 9065.00 552.50 o 2 17 0 230.06 135.86 197.14 o 3 17 0 10445.60 10461.73 680.16 o 4 17 0 521.22 717.30 193.17 o 5 17 0 8105.21 8022.00 470.81 o 6 17 0 1223.86 1064.37 227.89 o 7 17 0 3235.66 3185.59 316.88 o 8 17 0 14276.02 14592.26 942.40 o 9 17 0 7134.53 6345.63 429.74 o 10 17 0 64709.21 63673.73 1907.88 o 11 17 0 12448.02 11108.65 629.24 o 12 17 0 17991.34 18271.68 917.85 o 13 17 0 1761.71 2027.08 586.85 o 14 17 0 1614.22 1537.77 352.25 o 15 17 0 3693.31 3589.28 479.30 o 16 17 0 263.59 359.28 318.95 o 17 17 0 332.54 1056.10 377.74 o 0 18 0 3016.52 2744.14 494.05 o 1 18 0 2314.27 2747.30 355.43 o 2 18 0 11839.31 10518.44 1271.19 o 3 18 0 11825.36 11119.38 600.56 o 4 18 0 45341.64 39905.25 1612.69 o 5 18 0 145.17 225.59 199.79 o 6 18 0 2433.24 2644.86 364.64 o 7 18 0 8640.04 8432.84 474.15 o 8 18 0 11744.21 12223.56 566.75 o 9 18 0 3049.25 3612.79 362.80 o 10 18 0 228.28 341.91 222.81 o 11 18 0 184.27 242.19 257.37 o 12 18 0 3007.30 3087.39 464.60 o 13 18 0 737.53 742.01 313.55 o 14 18 0 79.82 352.09 299.55 o 15 18 0 690.99 588.05 332.39 o 16 18 0 9290.51 10091.19 803.93 o 1 19 0 3887.18 3988.28 488.49 o 2 19 0 43109.81 41025.19 1486.01 o 3 19 0 4614.13 4704.48 461.18 o 4 19 0 7711.15 8514.69 602.65 o 5 19 0 377.90 132.85 316.27 o 6 19 0 6037.92 5452.89 492.53 o 7 19 0 4182.80 4695.89 381.74 o 8 19 0 65.95 201.60 217.23 o 9 19 0 33014.55 31986.84 1101.81 o 10 19 0 8815.38 8916.31 544.28 o 11 19 0 22928.44 23271.26 1037.98 o 12 19 0 1444.01 1847.16 357.54 o 13 19 0 7102.55 7627.53 624.46 o 14 19 0 256.54 629.86 321.24 o 15 19 0 60.01 178.06 322.23 o 0 20 0 7022.98 9585.09 1138.88 o 1 20 0 9374.02 8895.03 1137.60 o 2 20 0 6624.44 6500.57 539.45 o 3 20 0 23187.87 22236.32 1173.00 o 4 20 0 21.57 -15.24 239.70 o 5 20 0 4635.13 5574.63 620.23 o 6 20 0 40.01 3.47 248.89 o 7 20 0 232.29 152.91 270.88 o 8 20 0 3144.49 2682.79 397.66 o 9 20 0 2308.75 2088.88 369.40 o 10 20 0 358.93 243.46 256.16 o 11 20 0 74.81 197.96 517.13 o 12 20 0 19.54 347.90 283.21 o 13 20 0 3300.28 3777.78 473.82 o 14 20 0 97.07 701.36 318.52 o 1 21 0 6904.41 7381.43 600.66 o 2 21 0 30521.71 29846.61 1432.65 o 3 21 0 8702.86 8521.59 668.52 o 4 21 0 3294.09 3349.96 427.27 o 5 21 0 265.66 195.08 253.61 o 6 21 0 68.37 -105.22 264.27 o 7 21 0 164.88 -57.47 253.12 o 8 21 0 2919.23 3404.10 799.64 o 9 21 0 4990.20 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