#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/24/2212403.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212403_Fobs loop_ _publ_author_name 'Yamane, Hisanori' 'Mikawa, Yutaka' 'Yokoyama, Chiaki' _publ_section_title ; Pentaamminechlorogallium(III) dichloride ; _journal_coeditor_code WM2091 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i59 _journal_page_last i61 _journal_volume 63 _journal_year 2007 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.4478 _cell_length_b 10.5181 _cell_length_c 6.7499 _exptl_crystal_F_000 528.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file wm2091Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gax' _shelx_refln_list_code 4 _shelx_f_calc_maximum 308.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, z+1/2' 'x, -y+1/2, z' '-x+1/2, -y, z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, -z-1/2' '-x, y-1/2, -z' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1972.85 1920.59 21.31 o 4 0 0 14733.17 14896.11 175.25 o 6 0 0 41.79 49.46 6.45 o 8 0 0 7168.11 7295.27 70.71 o 10 0 0 1228.02 1169.03 14.92 o 12 0 0 118.53 114.18 8.97 o 14 0 0 407.37 394.35 14.95 o 16 0 0 1832.56 1924.11 73.88 o 2 1 0 18284.81 17854.14 258.48 o 4 1 0 102.65 94.44 2.55 o 6 1 0 5416.74 5358.41 34.62 o 8 1 0 14216.36 13913.90 112.80 o 10 1 0 27.25 21.54 2.97 o 12 1 0 1075.43 1121.65 26.91 o 14 1 0 0.44 0.04 1.94 o 16 1 0 778.98 799.69 29.87 o 0 2 0 9045.02 8560.23 89.67 o 2 2 0 5684.02 6149.00 63.33 o 4 2 0 12118.71 12662.07 112.45 o 6 2 0 5459.31 5340.71 47.74 o 8 2 0 234.01 252.54 7.50 o 10 2 0 10550.46 10549.91 101.97 o 12 2 0 414.42 435.07 13.37 o 14 2 0 3481.27 3578.31 35.77 o 16 2 0 98.32 107.21 12.20 o 2 3 0 4506.05 4490.92 33.12 o 4 3 0 628.25 669.12 12.03 o 6 3 0 2712.54 2517.69 23.30 o 8 3 0 7441.95 7253.80 67.95 o 10 3 0 4.06 10.37 6.21 o 12 3 0 353.86 358.64 9.93 o 14 3 0 3.17 5.78 6.43 o 16 3 0 467.58 468.69 13.66 o 0 4 0 95027.20 89492.63 2010.34 o 2 4 0 892.98 892.43 8.48 o 4 4 0 7308.26 7514.47 148.58 o 6 4 0 168.01 197.02 2.43 o 8 4 0 4402.53 4347.76 42.26 o 10 4 0 421.20 426.61 11.91 o 12 4 0 93.78 119.51 12.88 o 14 4 0 198.50 224.52 11.46 o 16 4 0 1296.13 1323.89 20.94 o 2 5 0 11534.51 11934.38 172.89 o 4 5 0 389.30 360.37 17.54 o 6 5 0 4782.22 4717.37 88.65 o 8 5 0 10323.22 10322.57 96.89 o 10 5 0 32.70 43.23 5.67 o 12 5 0 1210.02 1274.38 17.91 o 14 5 0 1.32 1.46 5.00 o 16 5 0 731.54 741.30 15.31 o 0 6 0 7560.97 7372.25 165.88 o 2 6 0 3770.18 3883.72 56.97 o 4 6 0 482.95 456.30 17.62 o 6 6 0 5242.12 5229.11 199.51 o 8 6 0 410.27 234.74 90.03 o 10 6 0 8076.89 8113.32 107.95 o 12 6 0 207.19 213.31 11.20 o 14 6 0 2914.53 3060.58 46.40 o 2 7 0 3119.36 3092.33 49.24 o 4 7 0 14.40 18.84 5.20 o 6 7 0 2070.29 2125.55 69.16 o 8 7 0 3615.91 3650.07 45.78 o 10 7 0 2.11 4.38 13.03 o 12 7 0 223.75 230.66 21.16 o 14 7 0 0.49 5.43 11.06 o 0 8 0 19977.14 20227.69 416.32 o 2 8 0 246.04 277.53 14.75 o 4 8 0 2214.38 2404.39 49.73 o 6 8 0 208.86 253.03 29.35 o 8 8 0 1575.88 1560.17 38.64 o 10 8 0 41.48 44.64 15.32 o 12 8 0 49.75 69.74 12.60 o 14 8 0 48.09 53.34 18.24 o 2 9 0 2184.23 2415.41 30.35 o 4 9 0 91.21 98.69 9.12 o 6 9 0 1453.17 1509.09 32.15 o 8 9 0 3496.10 3691.94 47.86 o 10 9 0 7.60 10.61 15.28 o 12 9 0 429.34 508.25 22.30 o 0 10 0 2906.63 2902.66 64.13 o 2 10 0 1421.96 1576.03 24.12 o 4 10 0 16.86 8.45 6.43 o 6 10 0 2246.94 2310.31 48.41 o 8 10 0 218.17 200.77 14.32 o 10 10 0 3557.59 3726.77 74.90 o 2 11 0 2176.71 2229.45 50.53 o 4 11 0 29.85 23.01 10.82 o 6 11 0 1293.49 1355.00 18.75 o 8 11 0 1818.50 1888.62 47.02 o 10 11 0 4.57 15.32 15.31 o 0 12 0 6200.45 6409.35 140.48 o 2 12 0 109.59 89.19 22.86 o 4 12 0 922.39 922.56 41.65 o 6 12 0 24.24 21.78 7.52 o 8 12 0 557.66 592.98 42.23 o 2 13 0 323.42 323.63 16.58 o 4 13 0 12.49 24.40 10.30 o 1 0 1 2921.86 2922.50 20.37 o 2 0 1 3561.45 3219.52 78.02 o 3 0 1 1625.71 1850.27 31.75 o 4 0 1 14396.25 15225.93 184.41 o 5 0 1 1376.68 1256.42 13.80 o 6 0 1 333.87 345.03 5.97 o 7 0 1 1653.91 1584.58 15.39 o 8 0 1 12464.41 12354.13 101.43 o 9 0 1 1301.16 1224.14 12.72 o 10 0 1 586.10 556.34 8.19 o 11 0 1 507.11 503.76 6.87 o 12 0 1 7281.41 7325.64 108.56 o 13 0 1 2108.14 2049.32 44.96 o 14 0 1 40.50 39.56 3.08 o 15 0 1 779.41 747.31 43.11 o 16 0 1 1540.30 1628.07 40.75 o 17 0 1 3.51 1.84 27.50 o 0 1 1 16728.97 16879.17 164.28 o 1 1 1 824.93 817.12 6.96 o 2 1 1 312.48 276.81 3.97 o 3 1 1 421.08 406.01 3.99 o 4 1 1 6898.85 7171.53 48.44 o 5 1 1 1981.16 2012.27 14.41 o 6 1 1 4254.51 4410.68 44.54 o 7 1 1 3810.55 3812.43 30.31 o 8 1 1 1862.25 1803.47 13.32 o 9 1 1 1790.90 1734.39 14.82 o 10 1 1 3354.82 3245.42 27.71 o 11 1 1 4.57 5.36 1.94 o 12 1 1 11.45 11.35 2.20 o 13 1 1 1.15 4.09 1.62 o 14 1 1 784.70 754.58 21.50 o 15 1 1 181.45 178.45 6.41 o 16 1 1 103.60 130.71 11.67 o 17 1 1 117.16 127.71 19.12 o 1 2 1 6911.04 7684.25 72.29 o 2 2 1 21921.51 23682.76 231.22 o 3 2 1 1954.11 1975.09 20.31 o 4 2 1 37.79 44.23 2.02 o 5 2 1 177.47 186.98 3.23 o 6 2 1 5139.46 5070.74 36.62 o 7 2 1 866.74 878.88 6.74 o 8 2 1 41.05 54.37 2.85 o 9 2 1 5.18 7.78 3.02 o 10 2 1 945.77 928.67 11.49 o 11 2 1 182.17 170.55 5.63 o 12 2 1 85.72 92.95 5.41 o 13 2 1 163.71 133.45 13.11 o 14 2 1 450.88 439.86 8.40 o 15 2 1 296.55 290.72 6.76 o 16 2 1 36.58 41.43 5.32 o 17 2 1 397.28 435.11 16.08 o 0 3 1 3298.79 3333.23 73.15 o 1 3 1 75.10 77.53 5.03 o 2 3 1 8.21 9.55 3.24 o 3 3 1 6.38 9.06 2.04 o 4 3 1 2021.22 1992.12 21.37 o 5 3 1 1236.24 1266.02 14.11 o 6 3 1 1921.18 1884.82 22.64 o 7 3 1 2244.04 2221.58 11.99 o 8 3 1 960.78 921.41 7.95 o 9 3 1 1391.61 1355.55 15.93 o 10 3 1 1926.14 1734.11 63.04 o 11 3 1 4.89 9.06 4.83 o 12 3 1 2.37 3.95 4.12 o 13 3 1 10.37 12.76 4.97 o 14 3 1 452.60 475.31 7.89 o 15 3 1 157.99 164.83 5.74 o 16 3 1 33.64 27.33 5.94 o 1 4 1 1240.39 1258.90 12.34 o 2 4 1 792.10 815.47 8.95 o 3 4 1 1355.49 1375.99 15.85 o 4 4 1 6613.75 6554.95 58.26 o 5 4 1 371.97 336.11 5.94 o 6 4 1 39.42 36.07 2.30 o 7 4 1 984.74 959.46 15.04 o 8 4 1 7205.76 6999.81 42.43 o 9 4 1 761.29 712.90 9.23 o 10 4 1 396.34 400.88 7.80 o 11 4 1 299.21 294.71 7.12 o 12 4 1 4912.93 5012.52 37.55 o 13 4 1 1534.06 1567.88 17.40 o 14 4 1 15.93 14.69 4.88 o 15 4 1 548.88 587.71 9.91 o 16 4 1 1086.07 1133.81 21.42 o 0 5 1 12348.89 12428.26 92.03 o 1 5 1 786.38 747.78 7.25 o 2 5 1 223.45 243.07 4.25 o 3 5 1 594.38 595.50 7.54 o 4 5 1 6555.66 6638.32 64.90 o 5 5 1 1175.55 1202.06 12.46 o 6 5 1 3273.22 3226.94 40.21 o 7 5 1 2963.90 2911.62 27.17 o 8 5 1 1410.87 1365.85 11.18 o 9 5 1 1171.43 1189.50 12.99 o 10 5 1 2730.49 2751.61 23.53 o 11 5 1 6.71 5.61 5.71 o 12 5 1 12.90 20.34 6.22 o 13 5 1 3.04 -3.03 4.91 o 14 5 1 697.85 676.78 12.95 o 15 5 1 128.28 135.36 9.57 o 16 5 1 122.97 158.58 8.53 o 1 6 1 4890.89 4848.91 30.83 o 2 6 1 16730.70 17121.85 200.67 o 3 6 1 790.19 756.51 7.53 o 4 6 1 202.73 198.26 3.49 o 5 6 1 446.02 429.90 5.04 o 6 6 1 4096.17 4047.44 42.95 o 7 6 1 438.62 433.52 6.71 o 8 6 1 110.35 101.19 6.94 o 9 6 1 42.62 37.91 3.55 o 10 6 1 666.05 687.89 9.32 o 11 6 1 56.40 58.97 6.14 o 12 6 1 255.23 272.05 9.89 o 13 6 1 145.23 171.84 8.74 o 14 6 1 369.23 380.62 14.32 o 15 6 1 272.61 297.11 17.87 o 0 7 1 2017.22 1906.64 17.39 o 1 7 1 56.58 56.21 2.88 o 2 7 1 27.43 30.29 2.40 o 3 7 1 30.39 32.06 2.95 o 4 7 1 1508.43 1487.97 13.50 o 5 7 1 441.43 435.79 9.11 o 6 7 1 1319.50 1289.32 16.28 o 7 7 1 1334.16 1344.78 15.83 o 8 7 1 489.48 484.73 8.08 o 9 7 1 772.49 723.16 25.71 o 10 7 1 1298.67 1343.90 18.46 o 11 7 1 1.31 7.06 4.45 o 12 7 1 0.72 -3.90 7.72 o 13 7 1 2.48 6.49 10.29 o 14 7 1 328.11 383.21 20.24 o 1 8 1 325.52 346.30 7.34 o 2 8 1 62.83 87.40 4.14 o 3 8 1 691.09 680.66 9.85 o 4 8 1 1826.43 1807.53 20.86 o 5 8 1 38.81 39.97 4.08 o 6 8 1 12.05 10.93 3.59 o 7 8 1 331.56 338.03 11.23 o 8 8 1 2450.81 2527.59 28.36 o 9 8 1 247.76 250.83 17.04 o 10 8 1 157.28 164.71 10.57 o 11 8 1 105.48 118.52 10.47 o 12 8 1 1978.36 2082.45 35.23 o 13 8 1 686.49 735.66 19.80 o 14 8 1 2.07 0.36 10.20 o 0 9 1 2838.18 2904.15 64.48 o 1 9 1 171.26 196.28 5.44 o 2 9 1 27.86 38.81 3.98 o 3 9 1 126.08 128.50 6.39 o 4 9 1 1913.95 1996.35 25.36 o 5 9 1 440.89 449.98 7.64 o 6 9 1 818.30 810.32 15.84 o 7 9 1 939.38 940.40 13.17 o 8 9 1 463.56 465.68 9.57 o 9 9 1 389.96 352.39 23.19 o 10 9 1 826.19 842.52 17.24 o 11 9 1 1.43 8.75 9.14 o 12 9 1 3.67 10.90 12.34 o 1 10 1 1837.70 1840.36 24.72 o 2 10 1 6415.38 6483.22 82.62 o 3 10 1 240.66 247.79 6.90 o 4 10 1 137.15 153.03 7.31 o 5 10 1 232.44 237.51 6.86 o 6 10 1 1760.76 1781.37 21.20 o 7 10 1 176.61 183.67 6.39 o 8 10 1 110.00 113.35 7.83 o 9 10 1 38.45 38.02 10.11 o 10 10 1 293.23 302.09 16.63 o 11 10 1 12.21 12.32 11.35 o 0 11 1 1356.46 1341.72 40.59 o 1 11 1 49.21 46.57 6.78 o 2 11 1 53.48 60.24 5.66 o 3 11 1 86.86 85.93 6.27 o 4 11 1 1000.43 1006.31 14.49 o 5 11 1 131.47 148.98 7.07 o 6 11 1 871.23 834.32 70.00 o 7 11 1 676.07 669.37 10.32 o 8 11 1 267.48 280.04 13.82 o 9 11 1 327.18 377.92 15.17 o 10 11 1 871.12 943.80 21.41 o 1 12 1 137.29 141.10 9.59 o 2 12 1 72.43 75.05 8.99 o 3 12 1 197.48 200.71 8.16 o 4 12 1 639.81 646.73 11.95 o 5 12 1 29.56 21.11 7.78 o 6 12 1 6.07 0.52 6.22 o 7 12 1 97.09 84.54 10.52 o 8 12 1 941.27 925.16 35.54 o 0 13 1 565.56 598.42 18.64 o 1 13 1 32.13 26.96 7.86 o 2 13 1 1.87 11.82 9.30 o 3 13 1 20.28 14.45 5.44 o 4 13 1 420.16 419.45 10.99 o 0 0 2 4547.71 4580.85 53.94 o 1 0 2 11938.98 12666.03 114.14 o 2 0 2 280.73 322.65 9.53 o 3 0 2 27804.83 29094.78 327.58 o 4 0 2 21338.70 23083.24 563.01 o 5 0 2 5116.12 5415.87 115.69 o 6 0 2 1717.86 1698.94 39.78 o 7 0 2 1819.52 1686.88 40.06 o 8 0 2 1203.41 1157.15 21.59 o 9 0 2 1373.15 1300.15 26.60 o 10 0 2 328.49 347.41 6.85 o 11 0 2 363.35 371.50 9.15 o 12 0 2 179.90 175.04 16.85 o 13 0 2 717.31 688.92 19.95 o 14 0 2 92.90 80.28 6.68 o 15 0 2 70.34 65.83 5.14 o 16 0 2 54.96 66.65 17.44 o 1 1 2 119.20 124.02 4.55 o 2 1 2 5365.55 5525.25 49.41 o 3 1 2 2850.26 2940.95 45.53 o 4 1 2 4778.66 4842.32 74.41 o 5 1 2 14377.77 14677.27 195.09 o 6 1 2 883.78 909.59 12.59 o 7 1 2 67.39 76.37 2.69 o 8 1 2 163.07 168.34 4.04 o 9 1 2 911.23 967.69 12.59 o 10 1 2 588.89 560.76 7.11 o 11 1 2 772.53 756.97 15.88 o 12 1 2 1788.70 1764.09 36.91 o 13 1 2 395.24 363.64 12.44 o 14 1 2 174.98 160.69 12.21 o 15 1 2 332.90 329.75 11.05 o 16 1 2 291.30 300.64 11.31 o 0 2 2 5246.85 5335.24 52.47 o 1 2 2 4292.13 4559.92 39.32 o 2 2 2 35.24 37.15 3.39 o 3 2 2 2711.50 2845.94 34.27 o 4 2 2 2421.50 2539.62 39.16 o 5 2 2 3855.34 3788.77 56.38 o 6 2 2 4812.72 4788.95 75.31 o 7 2 2 1278.79 1321.10 26.85 o 8 2 2 61.99 55.92 2.83 o 9 2 2 974.78 977.04 17.05 o 10 2 2 2092.20 2034.74 37.43 o 11 2 2 2898.30 2406.92 273.84 o 12 2 2 48.92 53.60 3.96 o 13 2 2 1889.53 1826.28 29.22 o 14 2 2 620.70 564.19 24.84 o 15 2 2 778.83 787.85 21.53 o 16 2 2 63.54 78.92 15.11 o 1 3 2 72.54 99.03 7.29 o 2 3 2 2131.87 2074.26 25.08 o 3 3 2 1749.09 1718.79 16.66 o 4 3 2 2331.67 2320.47 27.39 o 5 3 2 6887.23 7010.42 123.50 o 6 3 2 349.90 348.42 4.85 o 7 3 2 7.15 7.51 2.29 o 8 3 2 12.77 19.44 2.55 o 9 3 2 279.67 266.22 11.04 o 10 3 2 480.46 465.59 8.71 o 11 3 2 372.99 340.42 8.27 o 12 3 2 1129.11 1098.97 28.97 o 13 3 2 191.88 157.64 17.57 o 14 3 2 118.24 122.56 7.22 o 15 3 2 165.92 178.75 9.54 o 16 3 2 189.72 198.48 7.88 o 0 4 2 2245.68 2176.30 22.41 o 1 4 2 6248.47 6289.58 73.00 o 2 4 2 304.33 302.92 5.44 o 3 4 2 12055.52 11837.41 133.43 o 4 4 2 10825.57 9618.74 519.82 o 5 4 2 3225.57 3284.43 54.21 o 6 4 2 810.61 809.89 9.96 o 7 4 2 757.03 726.18 7.78 o 8 4 2 760.44 732.77 7.77 o 9 4 2 1138.28 1080.97 14.70 o 10 4 2 146.67 135.44 4.56 o 11 4 2 170.84 163.98 8.57 o 12 4 2 118.43 99.74 11.22 o 13 4 2 407.65 409.81 8.59 o 14 4 2 41.33 41.26 6.88 o 15 4 2 66.80 68.36 7.87 o 16 4 2 29.09 33.61 7.04 o 1 5 2 800.21 765.52 9.14 o 2 5 2 4334.36 4302.78 37.07 o 3 5 2 1680.20 1652.80 18.07 o 4 5 2 2853.28 2903.41 46.69 o 5 5 2 9061.73 9068.18 125.42 o 6 5 2 645.99 646.91 11.11 o 7 5 2 124.99 124.37 7.53 o 8 5 2 312.49 301.15 8.69 o 9 5 2 1086.75 1054.40 12.25 o 10 5 2 441.08 431.68 11.66 o 11 5 2 723.90 648.53 29.77 o 12 5 2 1513.58 1595.41 19.41 o 13 5 2 405.95 431.07 10.08 o 14 5 2 137.61 155.36 10.29 o 15 5 2 324.07 363.17 10.23 o 0 6 2 117.86 114.36 9.88 o 1 6 2 224.62 212.43 4.90 o 2 6 2 3.03 2.74 3.21 o 3 6 2 2897.14 2728.82 31.03 o 4 6 2 1995.31 1964.85 34.23 o 5 6 2 1657.99 1649.05 18.72 o 6 6 2 3452.42 3443.28 47.37 o 7 6 2 1738.18 1802.71 20.63 o 8 6 2 91.84 91.85 2.88 o 9 6 2 884.78 853.09 15.86 o 10 6 2 1849.53 1809.91 27.35 o 11 6 2 2364.24 2416.46 26.08 o 12 6 2 36.69 50.75 5.96 o 13 6 2 1540.58 1578.48 19.84 o 14 6 2 553.24 577.70 11.91 o 15 6 2 558.04 593.09 27.82 o 1 7 2 114.62 117.67 4.50 o 2 7 2 1526.38 1476.25 11.54 o 3 7 2 1021.08 1002.19 8.87 o 4 7 2 997.37 976.83 9.09 o 5 7 2 3215.75 3232.06 35.96 o 6 7 2 198.79 200.97 5.16 o 7 7 2 2.34 0.60 3.12 o 8 7 2 24.60 26.99 2.69 o 9 7 2 217.01 220.74 8.46 o 10 7 2 272.09 231.91 18.29 o 11 7 2 219.11 214.44 15.42 o 12 7 2 665.66 676.88 16.79 o 13 7 2 102.16 111.22 17.21 o 14 7 2 76.73 97.21 17.76 o 0 8 2 647.29 686.86 11.06 o 1 8 2 2010.02 2046.30 13.13 o 2 8 2 170.17 167.16 3.98 o 3 8 2 3071.61 2980.94 23.65 o 4 8 2 3319.24 3229.14 33.11 o 5 8 2 1192.70 1184.69 13.12 o 6 8 2 194.42 189.19 5.82 o 7 8 2 134.32 145.55 4.80 o 8 8 2 286.57 284.37 6.18 o 9 8 2 629.25 553.82 24.00 o 10 8 2 29.52 12.87 5.61 o 11 8 2 38.49 38.69 8.97 o 12 8 2 46.26 53.95 9.86 o 13 8 2 127.31 141.37 12.08 o 1 9 2 129.24 135.48 4.57 o 2 9 2 1154.54 1165.83 9.05 o 3 9 2 409.05 398.23 9.37 o 4 9 2 839.51 814.55 9.03 o 5 9 2 2502.38 2447.96 31.61 o 6 9 2 146.08 135.30 8.46 o 7 9 2 59.77 55.32 5.06 o 8 9 2 85.03 79.93 7.48 o 9 9 2 376.46 355.17 22.87 o 10 9 2 198.51 227.19 12.36 o 11 9 2 267.82 273.85 15.95 o 12 9 2 606.76 663.40 19.33 o 0 10 2 6.84 9.05 3.70 o 1 10 2 11.60 10.13 3.17 o 2 10 2 4.36 1.90 1.72 o 3 10 2 1248.02 1214.86 18.13 o 4 10 2 831.23 766.43 16.94 o 5 10 2 588.37 565.17 15.39 o 6 10 2 1413.54 1388.11 33.56 o 7 10 2 859.45 863.37 17.02 o 8 10 2 52.47 58.60 7.75 o 9 10 2 391.75 396.85 16.16 o 10 10 2 894.28 940.64 26.88 o 11 10 2 1112.99 1207.17 30.22 o 1 11 2 255.26 240.57 6.43 o 2 11 2 955.26 878.39 16.23 o 3 11 2 534.42 493.93 12.10 o 4 11 2 461.26 456.03 26.90 o 5 11 2 1662.59 1678.76 26.41 o 6 11 2 144.42 152.79 6.52 o 7 11 2 1.47 1.44 4.24 o 8 11 2 59.05 33.12 9.80 o 9 11 2 211.57 242.85 15.46 o 0 12 2 300.91 282.70 12.03 o 1 12 2 734.59 704.30 17.59 o 2 12 2 42.68 35.48 5.00 o 3 12 2 1099.58 1040.93 20.77 o 4 12 2 1122.78 1100.11 18.86 o 5 12 2 354.56 370.17 11.70 o 6 12 2 90.86 89.52 7.98 o 7 12 2 87.08 68.02 8.10 o 1 13 2 9.63 -0.14 7.73 o 2 13 2 230.08 228.36 16.03 o 3 13 2 73.11 54.57 7.56 o 1 0 3 373.19 354.80 8.22 o 2 0 3 739.32 758.09 12.71 o 3 0 3 325.93 293.91 8.54 o 4 0 3 53.07 61.36 6.24 o 5 0 3 11334.42 11275.79 284.68 o 6 0 3 1517.56 1526.41 47.69 o 7 0 3 3392.21 3350.55 104.92 o 8 0 3 1149.05 1166.45 29.36 o 9 0 3 5839.74 5916.28 187.34 o 10 0 3 283.45 284.73 7.31 o 11 0 3 4145.00 4125.14 160.84 o 12 0 3 1.71 4.14 3.47 o 13 0 3 1969.81 1846.46 71.93 o 14 0 3 65.51 60.01 13.01 o 15 0 3 754.03 751.78 28.77 o 16 0 3 67.30 71.14 25.73 o 0 1 3 1955.35 1955.81 20.08 o 1 1 3 2223.72 2120.77 14.63 o 2 1 3 518.61 525.51 7.44 o 3 1 3 11235.57 11708.13 114.73 o 4 1 3 219.22 205.12 4.70 o 5 1 3 7.24 23.43 4.84 o 6 1 3 69.79 84.27 5.40 o 7 1 3 2551.06 2467.24 48.38 o 8 1 3 5.13 7.91 2.91 o 9 1 3 27.05 36.76 3.23 o 10 1 3 100.94 116.76 4.86 o 11 1 3 1883.29 1942.22 38.38 o 12 1 3 107.21 108.08 5.08 o 13 1 3 1355.53 1280.92 47.24 o 14 1 3 434.52 416.49 15.04 o 15 1 3 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874.42 884.98 14.69 o 9 6 3 575.88 571.68 9.74 o 10 6 3 193.99 180.82 9.13 o 11 6 3 91.74 87.52 9.35 o 12 6 3 11.22 10.51 5.68 o 13 6 3 14.86 17.15 7.05 o 14 6 3 45.06 35.11 7.58 o 0 7 3 803.31 808.06 13.42 o 1 7 3 397.19 401.66 8.49 o 2 7 3 254.36 264.51 13.38 o 3 7 3 2813.15 2754.21 29.07 o 4 7 3 41.88 50.32 5.17 o 5 7 3 10.50 10.89 3.51 o 6 7 3 7.04 6.49 3.02 o 7 7 3 804.39 849.24 12.95 o 8 7 3 11.80 4.93 2.50 o 9 7 3 11.66 5.68 3.11 o 10 7 3 26.52 30.87 6.13 o 11 7 3 839.12 828.75 23.63 o 12 7 3 55.23 70.74 7.89 o 13 7 3 548.60 597.30 18.34 o 1 8 3 34.41 38.54 3.64 o 2 8 3 83.68 85.98 4.92 o 3 8 3 215.54 239.91 7.88 o 4 8 3 34.96 21.63 5.21 o 5 8 3 1816.89 1727.70 40.23 o 6 8 3 509.53 524.74 8.38 o 7 8 3 947.62 939.84 14.36 o 8 8 3 348.65 337.19 6.30 o 9 8 3 1320.63 1201.00 32.71 o 10 8 3 99.26 77.90 7.53 o 11 8 3 1140.21 1190.26 19.83 o 12 8 3 1.54 6.31 10.88 o 0 9 3 507.85 498.29 14.19 o 1 9 3 749.34 730.93 9.92 o 2 9 3 198.60 193.77 4.82 o 3 9 3 2494.90 2435.64 21.89 o 4 9 3 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32.62 o 5 0 4 4786.77 4709.38 113.92 o 6 0 4 164.39 179.93 8.07 o 7 0 4 5953.61 6245.47 203.27 o 8 0 4 489.11 487.99 12.26 o 9 0 4 312.83 326.08 13.19 o 10 0 4 36.39 39.58 6.41 o 11 0 4 109.77 113.91 6.66 o 12 0 4 30.43 24.98 6.95 o 13 0 4 53.24 37.39 5.60 o 14 0 4 162.24 160.39 12.26 o 15 0 4 1.91 10.49 9.42 o 1 1 4 11160.96 11063.35 76.39 o 2 1 4 230.45 213.91 6.75 o 3 1 4 21.60 36.76 8.01 o 4 1 4 52.13 65.57 7.26 o 5 1 4 1226.90 1277.46 26.86 o 6 1 4 11.52 9.11 4.36 o 7 1 4 3.76 8.07 4.04 o 8 1 4 20.34 22.21 4.18 o 9 1 4 3167.54 3259.01 83.56 o 10 1 4 103.89 103.24 4.69 o 11 1 4 475.06 469.05 14.54 o 12 1 4 26.04 21.26 3.57 o 13 1 4 797.71 729.60 26.66 o 14 1 4 6.98 10.64 4.73 o 15 1 4 820.03 856.28 34.59 o 0 2 4 513.77 528.49 14.15 o 1 2 4 16.70 45.71 7.87 o 2 2 4 12.32 32.91 7.15 o 3 2 4 230.89 260.35 8.06 o 4 2 4 610.89 581.04 8.79 o 5 2 4 231.92 251.21 7.16 o 6 2 4 547.43 571.47 15.21 o 7 2 4 5140.77 5428.34 124.59 o 8 2 4 3.20 7.87 4.59 o 9 2 4 3832.42 3857.28 87.44 o 10 2 4 749.16 722.99 21.46 o 11 2 4 1291.56 1245.51 39.89 o 12 2 4 9.41 9.12 3.03 o 13 2 4 300.30 310.13 8.00 o 14 2 4 51.68 39.22 5.73 o 15 2 4 690.54 608.40 48.11 o 1 3 4 6623.46 6434.38 44.92 o 2 3 4 143.01 129.30 8.93 o 3 3 4 3.03 1.95 4.81 o 4 3 4 18.20 18.35 5.07 o 5 3 4 360.47 376.17 7.71 o 6 3 4 26.17 24.03 4.03 o 7 3 4 7.97 8.80 4.44 o 8 3 4 0.13 -1.91 3.19 o 9 3 4 1862.66 1893.76 49.90 o 10 3 4 74.87 82.78 4.45 o 11 3 4 214.01 197.60 9.33 o 12 3 4 4.13 4.74 2.72 o 13 3 4 529.37 513.98 18.08 o 14 3 4 9.24 5.42 5.42 o 15 3 4 524.99 488.74 31.54 o 0 4 4 1613.63 1569.55 31.75 o 1 4 4 6354.27 6236.14 60.45 o 2 4 4 164.82 169.97 7.71 o 3 4 4 3211.97 3099.62 46.59 o 4 4 4 721.15 715.65 11.78 o 5 4 4 3504.11 3447.24 64.82 o 6 4 4 144.96 146.30 9.25 o 7 4 4 3606.82 3641.10 77.81 o 8 4 4 327.35 315.23 12.14 o 9 4 4 146.19 136.37 5.99 o 10 4 4 47.16 39.42 3.90 o 11 4 4 39.16 32.86 3.10 o 12 4 4 26.44 23.46 5.79 o 13 4 4 15.49 10.13 4.15 o 14 4 4 150.20 176.89 14.10 o 1 5 4 7765.49 7625.39 71.75 o 2 5 4 145.18 154.61 10.45 o 3 5 4 30.60 35.36 5.11 o 4 5 4 73.46 85.35 7.05 o 5 5 4 1515.48 1513.20 18.13 o 6 5 4 6.23 11.23 4.09 o 7 5 4 14.26 14.03 3.86 o 8 5 4 33.52 32.53 5.34 o 9 5 4 2674.11 2686.71 49.71 o 10 5 4 85.50 80.20 7.66 o 11 5 4 474.62 451.53 17.16 o 12 5 4 38.33 25.68 5.15 o 13 5 4 699.49 716.11 14.36 o 14 5 4 3.24 6.22 5.91 o 0 6 4 211.87 213.25 14.12 o 1 6 4 143.82 146.12 6.96 o 2 6 4 7.89 6.58 4.96 o 3 6 4 813.38 834.27 23.96 o 4 6 4 198.82 198.95 7.24 o 5 6 4 119.96 125.01 7.87 o 6 6 4 418.51 424.19 12.74 o 7 6 4 4419.14 4563.97 88.56 o 8 6 4 0.07 0.79 3.79 o 9 6 4 2746.05 2712.35 52.71 o 10 6 4 547.53 471.16 22.62 o 11 6 4 1130.49 1031.88 46.26 o 12 6 4 4.14 4.38 8.00 o 13 6 4 370.35 383.28 12.91 o 1 7 4 3578.46 3592.38 33.67 o 2 7 4 118.86 119.87 7.66 o 3 7 4 12.27 2.71 5.52 o 4 7 4 10.54 11.53 5.90 o 5 7 4 363.31 390.48 10.42 o 6 7 4 5.76 5.29 3.88 o 7 7 4 8.19 8.48 4.37 o 8 7 4 0.78 -0.20 3.33 o 9 7 4 1065.02 1008.44 18.80 o 10 7 4 45.16 46.45 7.09 o 11 7 4 139.41 119.57 12.09 o 12 7 4 1.44 -3.79 10.46 o 0 8 4 558.03 590.56 14.12 o 1 8 4 2187.86 2191.44 20.70 o 2 8 4 82.20 96.44 8.49 o 3 8 4 972.14 958.74 19.91 o 4 8 4 285.39 270.57 8.15 o 5 8 4 1618.56 1679.08 24.36 o 6 8 4 83.59 92.24 6.80 o 7 8 4 1275.47 1249.30 14.10 o 8 8 4 127.64 126.13 6.27 o 9 8 4 31.45 26.78 6.09 o 10 8 4 36.49 29.33 6.06 o 11 8 4 6.31 19.46 9.76 o 1 9 4 2446.90 2435.83 22.34 o 2 9 4 22.75 27.83 5.65 o 3 9 4 1.85 8.49 5.26 o 4 9 4 31.23 28.67 4.69 o 5 9 4 454.28 450.95 10.97 o 6 9 4 12.05 11.82 4.51 o 7 9 4 3.47 9.31 5.27 o 8 9 4 13.26 11.53 4.20 o 9 9 4 1014.12 959.02 37.29 o 10 9 4 33.21 49.92 13.29 o 0 10 4 70.02 66.07 7.23 o 1 10 4 96.64 109.71 5.68 o 2 10 4 3.12 5.71 3.25 o 3 10 4 503.84 479.77 7.92 o 4 10 4 57.66 65.30 6.72 o 5 10 4 38.54 33.88 4.61 o 6 10 4 172.77 165.93 8.31 o 7 10 4 2113.79 2087.11 32.63 o 8 10 4 0.33 2.85 6.05 o 1 11 4 1835.45 1775.00 29.54 o 2 11 4 86.80 82.39 6.06 o 3 11 4 33.24 23.51 5.59 o 4 11 4 4.67 4.95 5.84 o 5 11 4 408.89 403.89 10.42 o 6 11 4 0.41 -5.58 5.58 o 0 12 4 195.61 203.26 21.01 o 1 12 4 778.13 733.90 14.88 o 2 12 4 23.31 23.61 7.15 o 1 0 5 2053.14 2058.04 28.96 o 2 0 5 72.50 65.28 9.46 o 3 0 5 6.87 13.88 7.27 o 4 0 5 312.98 327.40 13.06 o 5 0 5 2046.99 2094.04 55.96 o 6 0 5 140.68 148.67 8.19 o 7 0 5 565.22 579.31 26.92 o 8 0 5 5842.46 5857.56 223.58 o 9 0 5 2385.16 2424.64 82.67 o 10 0 5 88.73 98.45 7.36 o 11 0 5 631.20 621.02 35.12 o 12 0 5 759.75 705.59 44.31 o 13 0 5 449.36 410.96 29.13 o 14 0 5 109.49 107.32 20.17 o 0 1 5 4514.37 4573.60 49.33 o 1 1 5 1558.89 1546.73 16.41 o 2 1 5 360.78 363.39 10.05 o 3 1 5 1885.93 1855.64 22.81 o 4 1 5 85.35 82.94 6.25 o 5 1 5 10.67 7.03 5.20 o 6 1 5 179.81 220.52 9.97 o 7 1 5 1859.61 1965.22 48.77 o 8 1 5 166.07 182.59 8.27 o 9 1 5 159.36 151.47 6.91 o 10 1 5 323.21 310.98 10.76 o 11 1 5 787.56 737.05 20.15 o 12 1 5 142.01 137.95 9.50 o 13 1 5 383.68 325.93 21.35 o 14 1 5 400.05 351.14 21.72 o 1 2 5 2610.81 2565.12 21.79 o 2 2 5 3682.18 3574.26 35.53 o 3 2 5 1045.20 1021.75 14.96 o 4 2 5 941.96 890.09 12.34 o 5 2 5 1000.20 1060.15 20.63 o 6 2 5 2548.85 2557.79 53.91 o 7 2 5 73.74 73.21 6.56 o 8 2 5 144.23 163.70 10.29 o 9 2 5 719.74 718.84 16.59 o 10 2 5 8.58 5.79 4.37 o 11 2 5 26.85 22.09 4.52 o 12 2 5 372.52 360.14 16.20 o 13 2 5 14.43 7.82 5.63 o 14 2 5 1.40 -0.06 4.67 o 0 3 5 2650.51 2620.23 37.69 o 1 3 5 915.70 881.62 12.60 o 2 3 5 270.11 284.14 9.18 o 3 3 5 953.76 926.65 14.61 o 4 3 5 3.53 10.41 5.50 o 5 3 5 7.02 9.04 5.24 o 6 3 5 85.86 87.04 6.16 o 7 3 5 1104.11 1148.39 30.25 o 8 3 5 76.19 86.33 6.70 o 9 3 5 74.60 83.00 5.93 o 10 3 5 194.90 181.48 6.57 o 11 3 5 555.45 507.77 21.40 o 12 3 5 133.92 131.47 17.31 o 13 3 5 223.87 224.64 9.44 o 1 4 5 1091.20 1039.17 12.69 o 2 4 5 150.97 161.51 7.43 o 3 4 5 3.06 4.80 5.83 o 4 4 5 164.36 171.69 7.77 o 5 4 5 1200.22 1199.79 22.92 o 6 4 5 57.77 49.19 6.49 o 7 4 5 397.81 387.81 10.45 o 8 4 5 4152.30 4201.98 89.21 o 9 4 5 1614.57 1626.71 44.61 o 10 4 5 83.85 69.94 6.32 o 11 4 5 407.24 382.96 12.61 o 12 4 5 498.48 472.50 26.12 o 13 4 5 330.31 292.91 19.49 o 0 5 5 3757.38 3786.16 45.04 o 1 5 5 1308.97 1300.40 17.72 o 2 5 5 273.21 278.31 10.59 o 3 5 5 1705.25 1698.13 30.85 o 4 5 5 160.98 169.94 12.27 o 5 5 5 8.51 8.27 5.10 o 6 5 5 140.75 125.66 8.13 o 7 5 5 1552.39 1584.06 36.28 o 8 5 5 168.40 166.31 6.73 o 9 5 5 149.67 146.51 7.15 o 10 5 5 264.35 233.38 13.13 o 11 5 5 662.63 630.13 23.65 o 12 5 5 93.95 88.04 10.72 o 1 6 5 2174.68 2176.78 21.07 o 2 6 5 2890.73 2949.41 44.70 o 3 6 5 834.09 837.42 19.10 o 4 6 5 394.29 394.84 11.52 o 5 6 5 1129.48 1134.84 26.40 o 6 6 5 1956.39 1753.71 85.32 o 7 6 5 20.80 25.54 4.40 o 8 6 5 201.46 218.00 9.98 o 9 6 5 688.07 669.42 24.20 o 10 6 5 1.37 -4.88 4.88 o 11 6 5 61.20 44.81 6.88 o 12 6 5 132.89 110.21 14.04 o 0 7 5 1371.39 1408.32 25.51 o 1 7 5 532.07 554.27 10.66 o 2 7 5 193.95 204.42 13.03 o 3 7 5 623.72 654.55 11.20 o 4 7 5 2.70 -1.38 5.06 o 5 7 5 3.43 6.22 5.38 o 6 7 5 80.34 81.41 5.78 o 7 7 5 681.36 694.27 20.45 o 8 7 5 47.50 44.72 5.88 o 9 7 5 51.81 45.68 7.20 o 10 7 5 158.71 143.84 12.20 o 11 7 5 356.40 263.81 25.53 o 1 8 5 308.44 303.00 9.38 o 2 8 5 165.37 185.62 11.56 o 3 8 5 1.40 6.40 7.00 o 4 8 5 51.42 75.53 10.76 o 5 8 5 399.72 397.92 11.00 o 6 8 5 10.75 7.73 4.63 o 7 8 5 167.45 173.58 13.32 o 8 8 5 1793.79 1708.78 53.23 o 9 8 5 658.30 614.74 29.93 o 10 8 5 52.55 37.76 8.52 o 0 9 5 1409.33 1418.91 26.49 o 1 9 5 458.45 465.28 10.77 o 2 9 5 105.94 125.67 8.81 o 3 9 5 583.14 581.48 12.33 o 4 9 5 50.64 32.36 6.71 o 5 9 5 5.43 6.01 7.19 o 6 9 5 24.18 34.64 7.68 o 7 9 5 570.82 556.43 19.37 o 8 9 5 66.73 41.47 11.11 o 1 10 5 1019.12 976.32 15.44 o 2 10 5 1262.06 1279.31 22.30 o 3 10 5 376.36 388.58 10.89 o 4 10 5 116.96 109.88 9.86 o 5 10 5 619.55 542.37 53.89 o 6 10 5 888.04 770.40 58.25 o 0 11 5 650.97 658.59 15.69 o 1 11 5 299.94 307.42 15.93 o 2 11 5 106.24 99.45 7.61 o 0 0 6 5052.53 5220.08 86.80 o 1 0 6 341.54 338.05 20.70 o 2 0 6 70.32 103.81 13.36 o 3 0 6 1217.65 1229.76 27.24 o 4 0 6 6524.26 6499.35 132.05 o 5 0 6 244.15 248.49 11.65 o 6 0 6 210.65 226.71 10.86 o 7 0 6 168.50 171.32 11.49 o 8 0 6 622.13 615.65 34.11 o 9 0 6 9.86 13.32 6.77 o 10 0 6 5.42 -2.89 6.11 o 11 0 6 512.84 493.19 21.05 o 12 0 6 0.90 -2.75 5.65 o 1 1 6 27.28 31.80 7.39 o 2 1 6 1670.80 1715.19 20.12 o 3 1 6 558.18 527.82 15.51 o 4 1 6 649.34 649.79 12.95 o 5 1 6 1259.05 1257.09 18.06 o 6 1 6 613.40 625.37 13.80 o 7 1 6 41.36 34.51 6.33 o 8 1 6 454.13 450.17 13.17 o 9 1 6 404.89 400.66 11.44 o 10 1 6 136.59 131.22 8.66 o 11 1 6 169.66 168.80 7.01 o 12 1 6 692.18 660.50 32.67 o 0 2 6 333.63 336.14 14.00 o 1 2 6 428.40 436.55 11.20 o 2 2 6 69.89 59.54 7.06 o 3 2 6 929.09 919.83 16.73 o 4 2 6 122.36 128.75 8.80 o 5 2 6 44.13 29.57 6.41 o 6 2 6 2636.37 2603.05 67.46 o 7 2 6 58.37 69.12 7.26 o 8 2 6 8.45 10.08 5.56 o 9 2 6 134.12 144.36 10.45 o 10 2 6 1329.08 1307.85 41.82 o 11 2 6 307.62 310.87 19.49 o 12 2 6 17.41 12.72 4.39 o 1 3 6 2.70 2.76 6.99 o 2 3 6 990.45 983.88 14.95 o 3 3 6 416.06 422.43 10.98 o 4 3 6 340.15 341.65 9.25 o 5 3 6 878.51 883.35 21.75 o 6 3 6 368.93 357.47 12.01 o 7 3 6 31.66 25.01 4.98 o 8 3 6 179.43 175.70 7.78 o 9 3 6 301.85 289.22 9.42 o 10 3 6 96.88 99.49 8.67 o 11 3 6 116.82 124.44 8.44 o 12 3 6 397.05 388.37 19.05 o 0 4 6 3311.43 3392.02 39.86 o 1 4 6 223.90 233.71 11.23 o 2 4 6 72.36 61.86 7.30 o 3 4 6 807.51 808.25 18.02 o 4 4 6 4461.84 4591.08 76.72 o 5 4 6 186.56 197.23 11.83 o 6 4 6 87.83 99.78 8.36 o 7 4 6 97.63 102.49 7.12 o 8 4 6 422.50 433.07 17.20 o 9 4 6 14.68 21.58 5.46 o 10 4 6 12.09 10.43 5.40 o 11 4 6 390.66 350.04 18.07 o 1 5 6 46.71 52.06 7.18 o 2 5 6 1382.90 1398.79 19.35 o 3 5 6 456.47 451.69 14.50 o 4 5 6 586.17 604.74 11.31 o 5 5 6 1017.84 1022.31 20.74 o 6 5 6 526.31 534.69 16.86 o 7 5 6 30.90 30.66 6.01 o 8 5 6 503.91 485.44 16.35 o 9 5 6 330.85 309.37 17.63 o 10 5 6 113.06 88.06 10.17 o 11 5 6 140.31 113.82 9.34 o 0 6 6 30.26 33.61 11.37 o 1 6 6 354.65 361.71 12.53 o 2 6 6 86.64 92.08 9.28 o 3 6 6 771.68 758.26 22.10 o 4 6 6 227.37 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