#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213054.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213054_Fobs loop_ _publ_author_name 'Robeyns, Koen' 'Rohand, Taoufik' 'Bouhfid, Rachid' 'Essassi, EL Mokhtar' 'Van Meervelt, Luc' _publ_section_title ; Ethyl 2-(2,3-dioxoindolin-1-yl)acetate ; _journal_coeditor_code WN2122 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1747 _journal_page_last o1748 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.246 _cell_angle_gamma 90.000 _cell_length_a 13.6433 _cell_length_b 4.9505 _cell_length_c 16.2899 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.8186 _[local]_cod_data_source_file wn2122Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wim39 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4161.82 4139.13 135.15 o 2 0 0 1291.45 1285.60 44.38 o 3 0 0 1532.57 1618.36 51.96 o 4 0 0 735.70 845.01 28.80 o 5 0 0 61.05 48.20 4.54 o 6 0 0 320.16 313.85 16.98 o 7 0 0 874.52 982.70 42.62 o 8 0 0 109.54 96.22 11.32 o 9 0 0 1948.08 2153.53 137.20 o 10 0 0 23.71 17.21 4.27 o 11 0 0 1204.07 1310.94 33.61 o 12 0 0 428.19 445.55 13.18 o 13 0 0 4.19 3.39 2.33 o 14 0 0 158.66 154.38 10.12 o 15 0 0 31.90 35.44 3.03 o 16 0 0 376.07 377.99 18.02 o 1 1 0 4448.54 4852.10 115.06 o 2 1 0 35.06 25.12 1.92 o 3 1 0 7583.71 8716.78 188.47 o 4 1 0 0.36 1.47 1.54 o 5 1 0 2158.44 2319.68 54.65 o 6 1 0 336.25 349.60 12.59 o 7 1 0 918.47 999.79 31.23 o 8 1 0 640.60 661.22 23.70 o 9 1 0 1.23 1.82 1.79 o 10 1 0 6.34 4.28 1.89 o 11 1 0 97.82 99.06 3.90 o 12 1 0 76.65 75.61 3.87 o 13 1 0 187.88 188.36 5.22 o 14 1 0 35.17 36.53 2.17 o 15 1 0 26.01 28.59 3.09 o 0 2 0 58.08 61.25 4.06 o 1 2 0 2664.90 2815.36 62.77 o 2 2 0 794.47 913.96 20.17 o 3 2 0 281.82 331.29 11.22 o 4 2 0 71.20 62.04 4.31 o 5 2 0 128.20 132.17 9.99 o 6 2 0 3.95 -4.68 4.68 o 7 2 0 63.16 48.89 7.97 o 8 2 0 2.76 0.71 1.56 o 9 2 0 30.51 25.33 3.31 o 10 2 0 391.36 401.23 9.08 o 11 2 0 157.32 168.60 4.83 o 12 2 0 106.41 110.90 3.74 o 13 2 0 21.74 15.75 2.01 o 14 2 0 205.74 211.91 5.70 o 15 2 0 37.90 35.83 2.67 o 1 3 0 157.57 168.96 6.43 o 2 3 0 181.89 223.10 8.42 o 3 3 0 37.85 26.15 2.56 o 4 3 0 5.51 3.76 1.55 o 5 3 0 17.68 12.61 1.51 o 6 3 0 130.98 117.23 5.31 o 7 3 0 321.16 302.81 11.58 o 8 3 0 52.57 59.52 3.05 o 9 3 0 30.81 29.68 2.41 o 10 3 0 127.03 130.72 4.49 o 11 3 0 27.50 27.51 2.24 o 12 3 0 2.94 3.93 1.60 o 13 3 0 115.33 116.90 4.99 o 0 4 0 202.44 204.88 6.49 o 1 4 0 335.72 357.20 10.23 o 2 4 0 0.69 -0.27 0.99 o 3 4 0 408.60 434.56 9.22 o 4 4 0 57.31 56.98 3.14 o 5 4 0 27.90 26.74 1.94 o 6 4 0 156.09 142.41 6.51 o 7 4 0 0.70 2.18 2.05 o 8 4 0 1.61 -1.95 1.95 o 9 4 0 0.05 -2.30 2.30 o 10 4 0 1.07 3.90 2.15 o 11 4 0 6.84 10.03 2.59 o 1 5 0 6.66 7.59 1.22 o 2 5 0 140.01 162.51 4.09 o 3 5 0 214.98 221.57 5.74 o 4 5 0 1.67 1.99 1.47 o 5 5 0 30.26 33.14 6.95 o 6 5 0 28.99 23.88 2.71 o 7 5 0 192.42 200.49 7.30 o 8 5 0 0.33 -0.76 2.24 o 9 5 0 1.90 5.98 2.15 o 0 6 0 162.94 170.35 15.04 o 1 6 0 107.15 122.63 5.51 o 2 6 0 1.35 3.03 1.57 o -16 1 1 161.00 179.82 8.78 o -15 1 1 0.03 0.28 1.49 o -14 1 1 283.01 293.83 6.93 o -13 1 1 107.73 100.65 3.73 o -12 1 1 39.83 33.74 2.93 o -11 1 1 59.61 49.35 2.72 o -10 1 1 0.00 0.16 1.51 o -9 1 1 211.30 219.77 14.83 o -8 1 1 971.14 1025.24 32.68 o -7 1 1 6.17 -2.50 3.56 o -6 1 1 789.27 814.58 21.94 o -5 1 1 1.61 4.92 2.22 o -4 1 1 1343.97 1340.00 31.29 o -3 1 1 112.25 86.29 6.52 o -2 1 1 1835.72 2043.23 50.10 o -1 1 1 41.71 51.04 2.91 o 0 1 1 955.43 954.58 21.84 o 1 1 1 3.62 2.92 1.34 o 2 1 1 1540.13 1644.98 37.16 o 3 1 1 19221.79 21936.89 469.85 o 4 1 1 6061.60 6793.63 148.45 o 5 1 1 24.08 14.38 3.22 o 6 1 1 35.97 37.30 4.77 o 7 1 1 104.46 109.30 8.48 o 8 1 1 112.08 116.73 10.07 o 9 1 1 45.34 42.74 3.52 o 10 1 1 0.78 -0.73 1.74 o 11 1 1 45.32 41.15 2.71 o 12 1 1 157.87 151.11 5.33 o 13 1 1 190.65 197.64 5.36 o 14 1 1 282.12 320.14 7.31 o 15 1 1 151.90 155.17 5.41 o -15 2 1 47.63 43.05 2.64 o -14 2 1 0.68 -0.41 1.50 o -13 2 1 0.01 0.94 1.42 o -12 2 1 123.64 112.36 3.99 o -11 2 1 680.68 699.61 14.52 o -10 2 1 759.28 788.93 16.14 o -9 2 1 60.83 62.28 3.19 o -8 2 1 105.21 103.64 4.38 o -7 2 1 42.59 16.27 6.33 o -6 2 1 0.73 1.66 4.58 o -5 2 1 462.67 490.33 31.19 o -4 2 1 29.59 23.93 2.52 o -3 2 1 12.11 12.95 1.50 o -2 2 1 25.37 18.37 9.52 o -1 2 1 190.46 190.24 6.61 o 0 2 1 436.75 472.38 14.56 o 1 2 1 1535.39 1584.66 33.22 o 2 2 1 757.70 847.10 21.71 o 3 2 1 1042.85 1102.07 37.53 o 4 2 1 30.26 28.32 5.29 o 5 2 1 1795.39 2001.77 57.21 o 6 2 1 2288.58 2547.62 73.20 o 7 2 1 4.47 6.30 6.87 o 8 2 1 14.41 12.15 1.73 o 9 2 1 5.40 7.27 1.71 o 10 2 1 4.99 4.61 1.56 o 11 2 1 20.19 19.34 2.05 o 12 2 1 12.57 12.08 1.89 o 13 2 1 104.62 88.63 3.55 o 14 2 1 32.12 28.98 2.04 o 15 2 1 0.75 0.95 2.77 o -14 3 1 53.71 36.42 3.54 o -13 3 1 42.84 41.53 2.53 o -12 3 1 2.33 5.73 1.78 o -11 3 1 28.15 23.27 2.50 o -10 3 1 30.63 28.05 2.92 o -9 3 1 8.02 5.39 2.20 o -8 3 1 391.69 374.55 11.12 o -7 3 1 319.83 301.45 26.33 o -6 3 1 286.30 251.14 8.82 o -5 3 1 418.07 433.78 14.93 o -4 3 1 0.16 -0.15 1.32 o -3 3 1 229.63 213.78 7.58 o -2 3 1 10.95 10.84 1.83 o -1 3 1 312.64 342.32 10.59 o 0 3 1 702.52 748.90 19.59 o 1 3 1 1499.43 1736.06 43.01 o 2 3 1 13.57 10.71 1.85 o 3 3 1 118.25 132.84 9.73 o 4 3 1 240.99 246.56 11.78 o 5 3 1 302.78 283.25 7.10 o 6 3 1 97.95 91.29 5.08 o 7 3 1 62.58 54.21 4.32 o 8 3 1 0.22 -0.86 1.52 o 9 3 1 466.97 447.08 10.87 o 10 3 1 64.44 58.37 2.99 o 11 3 1 77.34 71.75 3.17 o 12 3 1 75.24 84.31 4.64 o 13 3 1 12.80 9.45 1.79 o -12 4 1 71.78 73.11 4.71 o -11 4 1 2.69 8.49 3.79 o -10 4 1 198.43 198.70 10.88 o -9 4 1 225.55 231.00 13.14 o -8 4 1 33.18 26.64 7.35 o -7 4 1 50.76 49.30 3.29 o -6 4 1 22.14 19.52 2.83 o -5 4 1 25.36 23.37 1.78 o -4 4 1 486.32 486.76 9.18 o -3 4 1 282.24 300.43 6.19 o -2 4 1 0.06 -0.39 0.94 o -1 4 1 203.73 202.43 4.38 o 0 4 1 0.93 0.36 1.10 o 1 4 1 53.62 39.90 2.07 o 2 4 1 227.20 221.54 5.39 o 3 4 1 61.80 58.16 2.47 o 4 4 1 722.76 695.45 13.75 o 5 4 1 2.91 2.15 1.20 o 6 4 1 329.86 336.93 11.59 o 7 4 1 112.08 116.66 5.99 o 8 4 1 13.42 10.51 2.71 o 9 4 1 0.47 -1.11 3.17 o 10 4 1 220.54 233.57 12.15 o 11 4 1 1.22 -0.90 2.13 o -9 5 1 0.50 3.72 2.17 o -8 5 1 1.61 1.27 2.43 o -7 5 1 5.53 9.07 4.86 o -6 5 1 60.42 57.51 6.16 o -5 5 1 9.52 4.72 2.66 o -4 5 1 6.22 6.69 1.57 o -3 5 1 160.24 160.97 4.51 o -2 5 1 49.19 53.82 5.15 o -1 5 1 0.00 0.36 1.13 o 0 5 1 6.35 6.05 1.25 o 1 5 1 122.20 119.85 3.39 o 2 5 1 149.68 163.69 4.16 o 3 5 1 350.44 343.34 7.36 o 4 5 1 82.61 88.78 4.23 o 5 5 1 99.90 100.41 3.87 o 6 5 1 92.81 89.79 4.56 o 7 5 1 10.19 8.75 2.04 o 8 5 1 6.54 9.13 2.63 o -1 6 1 239.56 267.01 15.42 o 0 6 1 183.43 198.65 7.33 o 1 6 1 71.22 81.78 4.14 o -16 0 2 282.40 297.37 10.05 o -15 0 2 588.40 637.16 16.81 o -14 0 2 2.79 5.31 2.10 o -13 0 2 200.63 207.47 7.49 o -12 0 2 133.22 127.48 5.81 o -11 0 2 105.31 101.97 8.04 o -10 0 2 20.09 20.39 4.65 o -9 0 2 144.62 138.53 14.78 o -8 0 2 57.81 91.19 10.79 o -7 0 2 3068.51 3694.91 117.90 o -6 0 2 999.85 1070.04 37.19 o -5 0 2 296.47 289.19 12.45 o -4 0 2 784.77 881.25 29.77 o -3 0 2 976.09 1048.68 34.09 o -2 0 2 6183.84 6327.50 191.69 o -1 0 2 432.81 430.34 14.14 o 0 0 2 4057.14 4071.00 124.21 o 1 0 2 1523.95 1615.13 50.65 o 2 0 2 8465.70 7547.72 269.59 o 3 0 2 5757.31 6212.78 223.69 o 4 0 2 4809.93 5019.96 182.60 o 5 0 2 54.36 52.39 8.88 o 6 0 2 68.45 73.68 8.85 o 7 0 2 582.67 564.11 28.68 o 8 0 2 1421.90 1456.59 62.18 o 9 0 2 336.95 343.55 9.55 o 10 0 2 1.33 4.47 3.36 o 11 0 2 129.81 133.16 5.86 o 12 0 2 142.88 132.95 5.84 o 13 0 2 60.23 57.69 5.27 o 14 0 2 471.97 471.90 23.38 o 15 0 2 0.06 -0.30 1.69 o -16 1 2 146.47 154.36 4.92 o -15 1 2 77.01 79.32 2.85 o -14 1 2 279.74 283.04 6.79 o -13 1 2 365.83 384.89 8.03 o -12 1 2 3.86 1.31 1.49 o -11 1 2 154.03 148.65 4.14 o -10 1 2 234.97 240.66 6.77 o -9 1 2 394.55 398.92 26.57 o -8 1 2 175.94 143.05 8.81 o -7 1 2 268.40 259.30 10.78 o -6 1 2 798.99 842.15 28.40 o -5 1 2 22.56 12.25 2.55 o -4 1 2 954.57 1023.30 24.95 o -3 1 2 214.01 194.37 7.59 o -2 1 2 9.54 5.30 1.19 o -1 1 2 104.83 93.98 4.46 o 0 1 2 855.21 850.44 21.41 o 1 1 2 22294.70 22379.92 477.35 o 2 1 2 1318.38 1406.18 32.04 o 3 1 2 6556.46 7577.52 162.44 o 4 1 2 2031.86 2374.54 58.09 o 5 1 2 303.91 292.60 11.08 o 6 1 2 515.67 514.19 23.23 o 7 1 2 208.18 212.29 13.80 o 8 1 2 339.21 373.88 25.49 o 9 1 2 235.60 226.16 6.63 o 10 1 2 233.81 220.65 5.99 o 11 1 2 464.91 455.16 10.30 o 12 1 2 3.34 3.78 2.01 o 13 1 2 0.33 1.05 1.53 o 14 1 2 28.52 24.95 1.85 o 15 1 2 20.99 22.51 1.87 o -15 2 2 18.30 18.96 2.00 o -14 2 2 2.57 -0.44 1.44 o -13 2 2 7.94 5.53 1.54 o -12 2 2 107.05 103.11 3.90 o -11 2 2 5.28 4.33 1.61 o -10 2 2 213.03 196.72 5.36 o -9 2 2 434.44 443.02 10.42 o -8 2 2 18.72 14.09 2.46 o -7 2 2 6.90 9.68 7.07 o -6 2 2 464.40 491.64 17.52 o -5 2 2 303.98 271.37 13.82 o -4 2 2 17.66 12.82 1.54 o -3 2 2 87.47 75.84 3.80 o -2 2 2 596.95 603.98 14.02 o -1 2 2 356.64 344.28 13.51 o 0 2 2 1089.60 1139.02 24.50 o 1 2 2 1.70 0.85 0.90 o 2 2 2 960.95 1016.18 27.55 o 3 2 2 200.92 186.83 6.20 o 4 2 2 16.00 7.25 1.51 o 5 2 2 57.00 42.72 4.82 o 6 2 2 1618.88 1683.66 58.67 o 7 2 2 1455.02 1468.43 52.31 o 8 2 2 718.19 667.31 15.51 o 9 2 2 76.46 75.24 4.80 o 10 2 2 0.01 -0.85 1.50 o 11 2 2 15.58 10.99 2.19 o 12 2 2 0.01 0.76 1.58 o 13 2 2 17.29 15.81 1.80 o 14 2 2 5.32 7.69 1.53 o -14 3 2 5.53 8.22 2.01 o -13 3 2 0.83 4.06 1.56 o -12 3 2 63.42 58.94 2.97 o -11 3 2 9.27 9.13 1.99 o -10 3 2 17.97 11.64 2.12 o -9 3 2 321.67 287.44 9.12 o -8 3 2 266.33 247.26 9.68 o -7 3 2 1054.94 1081.82 29.06 o -6 3 2 177.10 148.34 7.09 o -5 3 2 162.42 159.73 23.91 o -4 3 2 2.38 2.81 1.82 o -3 3 2 84.50 94.25 5.51 o -2 3 2 6.79 8.96 1.69 o -1 3 2 46.80 37.81 3.57 o 0 3 2 440.03 502.59 14.20 o 1 3 2 71.36 65.32 4.52 o 2 3 2 179.78 176.59 6.73 o 3 3 2 109.43 93.42 4.60 o 4 3 2 1317.34 1341.04 34.74 o 5 3 2 286.78 263.74 8.57 o 6 3 2 40.16 33.10 2.19 o 7 3 2 167.94 149.46 5.67 o 8 3 2 533.71 507.68 10.82 o 9 3 2 51.82 44.75 2.47 o 10 3 2 69.20 63.50 3.10 o 11 3 2 74.25 81.54 3.53 o 12 3 2 6.35 6.48 1.86 o 13 3 2 100.02 102.10 4.63 o -12 4 2 114.05 113.89 7.54 o -11 4 2 1.78 0.39 1.72 o -10 4 2 79.92 76.58 4.20 o -9 4 2 53.12 41.25 3.54 o -8 4 2 13.14 5.83 2.73 o -7 4 2 48.79 43.84 3.65 o -6 4 2 272.82 245.64 14.32 o -5 4 2 238.12 238.21 6.76 o -4 4 2 573.67 588.40 11.88 o -3 4 2 15.13 12.87 1.24 o -2 4 2 87.92 88.93 4.60 o -1 4 2 1.02 2.97 1.06 o 0 4 2 3.58 3.41 1.10 o 1 4 2 36.99 32.68 1.73 o 2 4 2 10.88 8.35 1.36 o 3 4 2 193.10 198.96 4.51 o 4 4 2 9.22 9.82 1.18 o 5 4 2 0.23 1.04 1.03 o 6 4 2 118.26 114.34 4.31 o 7 4 2 2.39 1.21 1.76 o 8 4 2 153.99 136.78 4.93 o 9 4 2 1.50 0.10 1.74 o 10 4 2 0.67 2.17 2.66 o 11 4 2 0.00 2.01 2.22 o -8 5 2 45.82 49.17 4.44 o -7 5 2 96.68 95.61 4.30 o -6 5 2 116.39 137.01 6.89 o -5 5 2 48.26 53.17 8.34 o -4 5 2 151.84 168.60 6.04 o -3 5 2 32.48 32.15 2.45 o -2 5 2 0.63 1.44 1.18 o -1 5 2 92.85 97.86 3.39 o 0 5 2 15.36 16.84 1.46 o 1 5 2 47.35 48.65 3.83 o 2 5 2 444.88 503.00 10.29 o 3 5 2 165.81 187.81 5.37 o 4 5 2 8.30 9.42 1.74 o 5 5 2 19.12 26.45 5.87 o 6 5 2 60.98 67.90 4.14 o 7 5 2 70.64 73.46 4.06 o 8 5 2 42.64 41.76 3.91 o -1 6 2 3.00 6.92 3.61 o 0 6 2 0.28 2.77 1.55 o -16 1 3 12.08 7.72 1.70 o -15 1 3 73.00 76.31 2.82 o -14 1 3 160.16 156.21 4.06 o -13 1 3 154.58 162.32 4.34 o -12 1 3 250.30 252.48 5.88 o -11 1 3 0.90 3.46 2.04 o -10 1 3 0.02 0.51 1.74 o -9 1 3 222.68 219.55 39.35 o -8 1 3 2845.41 3029.69 136.44 o -7 1 3 35.23 24.03 4.97 o -6 1 3 1238.87 1235.03 41.93 o -5 1 3 344.12 297.09 10.40 o -4 1 3 2227.66 2360.02 55.17 o -3 1 3 10.88 10.21 1.64 o -2 1 3 41.46 27.42 2.05 o -1 1 3 24.55 3.41 1.47 o 0 1 3 2277.11 2486.28 54.98 o 1 1 3 3566.49 3821.59 83.73 o 2 1 3 72.31 67.94 3.57 o 3 1 3 3410.23 3657.56 154.91 o 4 1 3 374.79 375.40 9.42 o 5 1 3 283.06 300.67 12.51 o 6 1 3 2.76 7.25 4.22 o 7 1 3 473.72 520.20 20.38 o 8 1 3 5.13 8.20 4.64 o 9 1 3 203.04 204.10 5.24 o 10 1 3 2.55 1.92 1.72 o 11 1 3 0.15 -0.47 1.75 o 12 1 3 139.86 141.88 5.10 o 13 1 3 55.02 57.56 2.68 o 14 1 3 2.26 3.43 1.37 o -15 2 3 187.42 206.26 5.39 o -14 2 3 178.37 183.14 5.27 o -13 2 3 647.64 671.13 15.57 o -12 2 3 90.75 83.69 3.74 o -11 2 3 198.53 185.98 5.84 o -10 2 3 384.43 381.03 9.88 o -9 2 3 471.38 445.58 10.47 o -8 2 3 259.63 252.74 8.43 o -7 2 3 184.06 212.19 15.91 o -6 2 3 1474.57 1603.54 51.13 o -5 2 3 86.36 78.98 13.05 o -4 2 3 903.04 931.27 20.87 o -3 2 3 1244.45 1372.87 29.44 o -2 2 3 280.50 269.90 8.00 o -1 2 3 316.78 331.33 9.50 o 0 2 3 21.25 14.90 1.56 o 1 2 3 116.58 104.60 5.78 o 2 2 3 95.15 95.48 7.01 o 3 2 3 481.29 532.92 13.52 o 4 2 3 4088.54 4574.12 103.89 o 5 2 3 109.72 93.93 5.34 o 6 2 3 1046.11 1055.79 39.55 o 7 2 3 1964.78 2029.65 36.39 o 8 2 3 774.52 780.87 13.55 o 9 2 3 3.49 4.04 1.71 o 10 2 3 54.27 49.01 2.75 o 11 2 3 6.93 6.17 1.77 o 12 2 3 5.22 5.14 1.68 o 13 2 3 25.61 19.85 2.03 o 14 2 3 5.42 5.78 1.98 o -14 3 3 15.32 16.69 1.75 o -13 3 3 22.28 20.87 1.87 o -12 3 3 3.80 7.56 1.70 o -11 3 3 53.11 44.53 3.40 o -10 3 3 170.23 178.60 6.47 o -9 3 3 196.75 186.21 5.97 o -8 3 3 50.98 46.01 3.94 o -7 3 3 1.60 1.43 4.20 o -6 3 3 70.37 46.53 3.69 o -5 3 3 313.59 290.56 9.58 o -4 3 3 442.16 451.87 14.53 o -3 3 3 141.13 133.99 9.11 o -2 3 3 25.99 31.62 2.68 o -1 3 3 213.02 237.39 8.42 o 0 3 3 66.09 76.24 5.18 o 1 3 3 0.11 0.40 1.21 o 2 3 3 75.58 82.42 7.75 o 3 3 3 5.80 7.19 3.02 o 4 3 3 95.72 86.64 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