#------------------------------------------------------------------------------
#$Date: 2016-04-03 01:41:20 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181080 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/60/2216048.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2216048_Fobs
loop_
_publ_author_name
'Song, Wen-Dong'
'Gu, Chang-Sheng'
'Yan, Jian-Bin'
'Ng, Seik Weng'
_publ_section_title
;
 <i>catena</i>-Poly[[silver(I)-\m-pyrazine-\k^2^<i>N</i>:<i>N</i>']
 perchlorate]
;
_journal_coeditor_code           LH2524
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m2701
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   7.4838
_cell_length_b                   7.1954
_cell_length_c                   14.3623
_exptl_crystal_F_000             552.00
_reflns_d_resolution_high        0.7703
_cod_data_source_file            lh2524Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  Cmcm'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            271.40
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x, -y, -z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, -z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z-1/2'
'-x, y, z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'-x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 73657.74 73995.55 3289.50 o
4 0 0 15193.36 15357.55 192.89 o
6 0 0 11069.64 11295.61 165.91 o
8 0 0 3143.41 3198.70 148.23 o
1 1 0 17273.18 18659.63 188.85 o
3 1 0 3711.14 4070.07 43.54 o
5 1 0 925.20 903.27 20.06 o
7 1 0 634.26 664.78 27.18 o
9 1 0 247.05 280.95 38.09 o
0 2 0 48516.38 53619.00 534.88 o
2 2 0 38798.78 39930.41 556.17 o
4 2 0 13521.85 13389.32 138.02 o
6 2 0 3425.12 3333.79 58.29 o
8 2 0 1248.07 1278.55 55.96 o
1 3 0 3743.60 3994.27 41.81 o
3 3 0 266.71 261.11 9.22 o
5 3 0 805.28 746.55 30.81 o
7 3 0 437.70 393.90 26.10 o
0 4 0 63.44 67.21 10.07 o
2 4 0 1005.83 995.44 21.22 o
4 4 0 994.67 989.20 35.57 o
6 4 0 146.62 128.88 18.02 o
8 4 0 7.74 5.37 12.88 o
1 5 0 238.99 212.89 11.24 o
3 5 0 437.13 439.41 19.34 o
5 5 0 110.59 110.16 16.80 o
7 5 0 20.95 24.81 15.85 o
0 6 0 1519.03 1677.79 42.93 o
2 6 0 1480.77 1411.73 40.78 o
4 6 0 501.80 585.80 40.81 o
6 6 0 166.95 260.35 43.76 o
1 7 0 156.83 144.72 17.35 o
3 7 0 12.01 24.14 13.07 o
5 7 0 12.26 10.84 19.02 o
0 8 0 1504.64 1473.00 80.34 o
2 8 0 868.50 829.77 63.54 o
4 8 0 464.83 403.54 56.52 o
1 9 0 19.64 -6.46 16.08 o
1 1 1 742.76 747.26 7.12 o
3 1 1 5016.24 5277.12 38.52 o
5 1 1 316.57 332.72 8.91 o
7 1 1 0.40 4.69 4.78 o
9 1 1 45.32 46.62 20.05 o
0 2 1 23888.13 25460.18 191.23 o
2 2 1 8285.90 8115.29 50.42 o
4 2 1 3264.99 3274.90 28.63 o
6 2 1 2735.03 2762.97 37.63 o
8 2 1 543.56 570.40 40.94 o
1 3 1 9838.74 10228.69 66.99 o
3 3 1 4323.86 4433.79 34.33 o
5 3 1 1449.65 1460.86 27.89 o
7 3 1 359.58 392.12 18.92 o
9 3 1 32.60 55.28 24.84 o
0 4 1 8000.40 7860.02 74.98 o
2 4 1 12368.92 12043.46 85.64 o
4 4 1 7703.84 7590.87 80.09 o
6 4 1 1674.14 1710.48 37.96 o
8 4 1 663.06 706.94 31.66 o
1 5 1 3936.06 3828.59 38.46 o
3 5 1 1400.79 1410.26 26.56 o
5 5 1 832.43 834.15 25.96 o
7 5 1 219.18 209.36 20.81 o
0 6 1 3447.30 3314.51 56.61 o
2 6 1 2422.41 2346.11 43.29 o
4 6 1 1368.17 1275.88 61.25 o
6 6 1 707.24 674.16 61.85 o
1 7 1 230.05 214.98 13.86 o
3 7 1 448.52 419.25 24.95 o
5 7 1 94.24 73.05 19.97 o
0 8 1 98.03 112.58 19.92 o
2 8 1 43.57 64.36 15.37 o
4 8 1 25.14 38.44 17.93 o
1 9 1 16.81 2.29 14.35 o
0 0 2 54047.21 48071.84 2088.10 o
2 0 2 37776.12 39076.92 303.01 o
4 0 2 18758.38 18650.47 175.28 o
6 0 2 7690.97 7513.63 94.68 o
8 0 2 940.63 960.76 44.54 o
1 1 2 66.84 86.27 6.47 o
3 1 2 7309.19 7709.48 53.56 o
5 1 2 1578.21 1572.84 20.53 o
7 1 2 30.51 35.90 6.80 o
9 1 2 13.39 18.62 22.13 o
0 2 2 10569.30 10439.69 97.92 o
2 2 2 17942.28 18205.94 104.62 o
4 2 2 10744.27 10732.51 76.34 o
6 2 2 1565.92 1537.61 23.58 o
8 2 2 435.67 490.58 28.43 o
1 3 2 2230.36 2322.71 20.17 o
3 3 2 23.30 28.17 3.34 o
5 3 2 134.28 122.25 7.65 o
7 3 2 122.63 109.76 11.41 o
9 3 2 0.13 10.61 16.25 o
0 4 2 265.52 261.35 10.59 o
2 4 2 79.66 100.22 5.03 o
4 4 2 8.85 18.62 4.67 o
6 4 2 6.58 7.13 6.53 o
8 4 2 22.97 12.14 9.59 o
1 5 2 34.11 25.39 5.13 o
3 5 2 22.97 17.39 4.74 o
5 5 2 114.39 120.44 12.12 o
7 5 2 6.69 6.61 8.28 o
0 6 2 831.24 837.02 30.31 o
2 6 2 2041.35 2025.24 40.15 o
4 6 2 1808.03 1877.99 48.76 o
6 6 2 253.39 300.86 29.57 o
1 7 2 159.10 145.37 14.83 o
3 7 2 206.75 231.18 20.07 o
5 7 2 77.52 69.10 19.96 o
0 8 2 1563.82 1682.24 49.53 o
2 8 2 1080.35 1186.17 54.43 o
4 8 2 563.66 623.19 38.22 o
1 9 2 63.06 63.53 21.37 o
1 1 3 50.22 48.75 2.35 o
3 1 3 2864.20 2949.75 26.74 o
5 1 3 140.27 139.71 7.47 o
7 1 3 2.02 3.99 5.11 o
9 1 3 27.94 44.50 27.61 o
2 2 3 7276.38 7065.58 53.21 o
4 2 3 2996.06 2857.71 28.04 o
6 2 3 2352.48 2335.08 30.46 o
8 2 3 467.36 505.52 29.12 o
1 3 3 4297.73 4449.25 39.33 o
3 3 3 1462.28 1481.18 19.79 o
5 3 3 601.31 624.69 14.60 o
7 3 3 176.00 191.00 14.94 o
9 3 3 14.57 12.68 20.81 o
0 4 3 8586.26 8131.60 117.10 o
2 4 3 10431.10 9878.18 69.43 o
4 4 3 5870.27 5710.72 55.97 o
6 4 3 1300.09 1276.54 34.75 o
8 4 3 581.35 623.62 44.87 o
1 5 3 1887.77 1874.86 29.40 o
3 5 3 299.64 328.82 11.80 o
5 5 3 219.17 247.64 19.70 o
7 5 3 105.81 88.78 15.82 o
0 6 3 2952.60 2775.18 59.58 o
2 6 3 1823.74 1729.34 31.10 o
4 6 3 725.07 753.59 27.74 o
6 6 3 475.82 495.38 39.08 o
1 7 3 29.81 33.91 7.99 o
3 7 3 93.73 100.14 12.31 o
5 7 3 4.99 -7.61 15.01 o
0 8 3 19.07 5.94 15.74 o
2 8 3 0.63 8.82 9.83 o
4 8 3 0.13 18.99 15.48 o
1 9 3 5.03 5.13 13.39 o
0 0 4 51683.91 47701.55 536.32 o
2 0 4 16394.82 15957.64 137.04 o
4 0 4 4701.77 4325.62 53.26 o
6 0 4 4843.98 4741.36 100.83 o
8 0 4 1225.30 1247.27 55.02 o
1 1 4 6961.35 7394.32 49.71 o
3 1 4 4473.27 4342.16 34.76 o
5 1 4 816.77 799.24 15.49 o
7 1 4 205.66 212.18 13.78 o
9 1 4 59.24 38.26 17.21 o
0 2 4 5917.52 5720.82 148.86 o
2 2 4 7683.53 7352.82 58.78 o
4 2 4 4381.00 4133.49 40.00 o
6 2 4 1030.45 1028.49 19.72 o
8 2 4 418.76 436.62 27.64 o
1 3 4 1796.76 1848.56 17.21 o
3 3 4 13.16 3.65 2.69 o
5 3 4 279.33 255.86 9.71 o
7 3 4 123.78 125.95 14.21 o
0 4 4 310.30 350.03 12.67 o
2 4 4 24.09 29.97 4.24 o
4 4 4 8.97 9.58 4.03 o
6 4 4 5.40 5.42 6.13 o
8 4 4 3.03 -3.81 10.53 o
1 5 4 456.69 433.92 12.03 o
3 5 4 3.58 6.39 3.58 o
5 5 4 10.37 9.53 7.34 o
7 5 4 56.87 55.18 14.00 o
0 6 4 1699.08 1685.18 45.04 o
2 6 4 1915.82 1877.66 30.10 o
4 6 4 1063.61 1024.38 25.93 o
6 6 4 295.93 315.76 29.02 o
1 7 4 324.23 308.68 19.09 o
3 7 4 153.04 170.73 17.14 o
5 7 4 87.45 97.31 17.18 o
0 8 4 1393.67 1363.15 82.46 o
2 8 4 911.92 920.49 39.18 o
4 8 4 525.94 549.41 44.58 o
1 9 4 58.09 63.36 19.69 o
1 1 5 120.09 123.71 3.98 o
3 1 5 1717.92 1707.78 19.28 o
5 1 5 104.85 117.20 7.70 o
7 1 5 0.35 0.91 5.95 o
9 1 5 30.89 14.98 15.36 o
0 2 5 23224.32 23494.95 193.57 o
2 2 5 9873.16 9576.14 67.96 o
4 2 5 3885.08 3725.38 36.58 o
6 2 5 2439.80 2467.37 38.01 o
8 2 5 515.50 554.34 35.08 o
1 3 5 2848.98 2951.57 23.80 o
3 3 5 1435.21 1489.69 21.97 o
5 3 5 609.56 622.91 16.22 o
7 3 5 181.36 162.73 32.62 o
0 4 5 9818.21 9500.11 100.79 o
2 4 5 12766.86 12637.84 105.28 o
4 4 5 7653.59 7427.96 65.07 o
6 4 5 1773.66 1746.13 35.07 o
1 5 5 1215.19 1238.42 22.49 o
3 5 5 602.91 631.38 16.17 o
5 5 5 462.71 478.34 22.88 o
7 5 5 102.87 121.60 19.82 o
0 6 5 3030.43 2800.40 53.19 o
2 6 5 2454.43 2452.36 39.53 o
4 6 5 1537.05 1540.35 38.09 o
6 6 5 646.80 600.47 49.10 o
1 7 5 49.08 55.85 9.92 o
3 7 5 235.18 234.29 22.83 o
5 7 5 49.19 4.99 12.82 o
0 8 5 73.02 126.53 32.68 o
2 8 5 42.04 41.85 14.27 o
4 8 5 24.55 50.74 18.75 o
0 0 6 51317.92 48382.22 600.74 o
2 0 6 19629.17 19213.55 163.44 o
4 0 6 8344.30 8219.89 85.85 o
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8 0 6 1462.99 1445.60 61.12 o
1 1 6 18651.23 19948.32 113.99 o
3 1 6 10603.37 11007.19 72.77 o
5 1 6 2763.08 2640.58 34.28 o
7 1 6 615.97 623.13 22.84 o
9 1 6 177.76 146.20 34.07 o
0 2 6 10620.15 11000.41 91.71 o
2 2 6 11765.44 12036.79 77.28 o
4 2 6 6025.38 5867.89 55.40 o
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8 2 6 659.14 670.69 34.83 o
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3 3 6 945.59 957.14 16.96 o
5 3 6 744.90 718.46 18.71 o
7 3 6 361.57 337.61 27.26 o
0 4 6 117.74 128.52 12.37 o
2 4 6 313.25 345.88 14.40 o
4 4 6 177.94 173.79 10.85 o
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8 4 6 19.73 13.31 19.77 o
1 5 6 35.18 31.92 5.69 o
3 5 6 61.47 55.30 6.65 o
5 5 6 6.83 4.15 6.58 o
7 5 6 2.12 3.37 13.23 o
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2 6 6 930.54 942.68 26.67 o
4 6 6 508.31 501.52 26.64 o
6 6 6 114.28 138.28 28.30 o
1 7 6 215.66 230.84 24.38 o
3 7 6 86.61 99.89 16.41 o
5 7 6 32.69 65.37 20.25 o
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2 8 6 614.61 677.29 36.93 o
1 1 7 81.56 84.13 3.94 o
3 1 7 1400.98 1416.55 17.81 o
5 1 7 157.40 165.28 9.79 o
7 1 7 1.73 4.08 5.27 o
0 2 7 15337.88 15671.77 127.39 o
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4 2 7 4117.15 4098.38 41.34 o
6 2 7 2233.10 2197.04 36.44 o
8 2 7 436.31 427.62 32.41 o
1 3 7 2592.95 2588.31 27.04 o
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5 3 7 662.67 687.21 18.75 o
7 3 7 194.86 174.10 23.70 o
0 4 7 10748.82 10879.41 115.21 o
2 4 7 11170.14 11126.84 97.31 o
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6 4 7 1651.42 1740.88 37.67 o
1 5 7 1901.08 1890.67 32.36 o
3 5 7 568.01 587.23 21.62 o
5 5 7 346.81 349.96 17.90 o
7 5 7 157.49 145.07 25.54 o
0 6 7 3753.12 3986.60 131.25 o
2 6 7 2412.03 2370.97 40.16 o
4 6 7 1080.96 1081.95 32.94 o
6 6 7 594.94 574.68 34.59 o
1 7 7 219.74 244.53 23.80 o
3 7 7 205.53 229.94 23.43 o
5 7 7 52.26 36.33 17.21 o
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4 2 8 5121.41 4840.17 60.78 o
6 2 8 1125.90 1154.33 24.35 o
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1 3 8 1739.95 1742.34 24.08 o
3 3 8 242.64 236.25 11.51 o
5 3 8 254.69 241.81 11.96 o
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0 4 8 310.74 354.45 20.06 o
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4 4 8 17.54 25.20 5.94 o
6 4 8 2.78 2.53 6.92 o
1 5 8 39.49 45.96 6.82 o
3 5 8 36.94 29.47 5.72 o
5 5 8 67.22 77.90 10.75 o
7 5 8 3.53 6.22 16.37 o
0 6 8 311.16 293.92 31.70 o
2 6 8 755.33 760.37 22.49 o
4 6 8 761.99 759.81 26.07 o
6 6 8 134.83 200.94 30.16 o
1 7 8 183.00 182.07 26.80 o
3 7 8 214.34 240.41 21.58 o
0 8 8 726.41 922.78 73.21 o
2 8 8 565.97 550.81 44.01 o
1 1 9 274.82 279.86 7.02 o
3 1 9 600.59 591.36 13.56 o
5 1 9 48.40 36.99 5.87 o
7 1 9 3.57 0.19 7.30 o
0 2 9 9620.28 9519.16 86.11 o
2 2 9 4646.33 4551.53 44.09 o
4 2 9 1837.69 1800.74 27.97 o
6 2 9 1197.56 1296.99 32.75 o
8 2 9 346.58 340.51 45.03 o
1 3 9 2158.09 2083.26 30.27 o
3 3 9 800.99 738.45 17.58 o
5 3 9 323.82 337.21 15.55 o
7 3 9 138.83 158.02 21.25 o
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1 5 9 931.92 907.35 23.01 o
3 5 9 418.09 424.57 15.65 o
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2 6 9 1043.73 1006.98 37.41 o
4 6 9 649.76 719.08 29.20 o
1 7 9 40.76 24.33 13.58 o
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0 8 9 1.31 -1.44 20.12 o
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4 0 10 2304.83 2379.80 45.35 o
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1 1 10 3215.70 3285.89 26.78 o
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4 2 10 1840.55 1795.45 33.75 o
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3 3 10 4.08 7.28 4.12 o
5 3 10 71.61 72.93 9.31 o
7 3 10 35.49 31.77 14.64 o
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2 6 10 836.63 844.10 44.41 o
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1 7 10 360.60 361.57 32.43 o
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1 1 11 227.69 245.95 7.37 o
3 1 11 648.08 636.16 16.53 o
5 1 11 160.09 157.19 12.71 o
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1 5 11 1127.89 1103.13 35.98 o
3 5 11 629.35 607.43 25.95 o
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0 6 11 1072.33 1206.64 100.87 o
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3 3 12 259.55 233.82 12.78 o
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0 4 12 325.85 344.89 25.91 o
2 4 12 157.82 175.43 13.73 o
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6 4 12 9.74 7.38 12.40 o
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3 5 12 24.75 28.44 8.46 o
5 5 12 28.57 47.60 16.90 o
0 6 12 243.08 233.05 35.46 o
2 6 12 484.14 479.45 28.99 o
4 6 12 446.12 443.30 32.36 o
1 7 12 92.04 80.00 20.98 o
1 1 13 456.68 460.30 12.35 o
3 1 13 417.78 453.98 14.81 o
5 1 13 95.69 102.29 14.79 o
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2 2 13 2331.50 2307.73 31.22 o
4 2 13 1060.91 1085.14 55.60 o
6 2 13 652.56 672.77 45.97 o
1 3 13 2409.48 2487.64 42.89 o
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5 1 14 664.16 669.22 32.36 o
0 2 14 3538.35 3437.84 68.72 o
2 2 14 2979.56 2911.31 39.69 o
4 2 14 1716.71 1644.67 47.53 o
6 2 14 701.17 809.82 60.03 o
1 3 14 581.87 618.18 27.32 o
3 3 14 329.50 376.81 22.15 o
5 3 14 241.50 218.99 29.75 o
0 4 14 12.26 15.23 11.67 o
2 4 14 54.58 75.11 16.85 o
4 4 14 84.88 39.96 16.54 o
1 5 14 21.56 11.19 9.75 o
3 5 14 6.89 9.90 13.46 o
0 6 14 423.20 454.37 59.28 o
1 1 15 228.36 249.57 11.33 o
3 1 15 249.37 260.57 19.07 o
5 1 15 76.61 63.69 13.35 o
0 2 15 1814.62 1917.40 166.08 o
2 2 15 1366.71 1415.21 33.95 o
4 2 15 812.86 866.84 31.43 o
1 3 15 1074.13 984.31 35.28 o
3 3 15 767.17 716.89 32.53 o
0 4 15 1799.29 1832.56 103.48 o
2 4 15 1834.53 1837.41 58.16 o
4 4 15 1231.55 1229.14 59.07 o
1 5 15 527.81 452.71 83.11 o
0 0 16 3516.75 3366.06 139.01 o
2 0 16 2582.40 2546.01 67.78 o
4 0 16 1382.48 1314.33 51.28 o
1 1 16 1165.50 1233.68 29.69 o
3 1 16 765.01 753.94 28.81 o
0 2 16 1303.73 1329.32 57.33 o
2 2 16 1108.99 1134.33 42.62 o
4 2 16 600.19 601.99 36.16 o
1 3 16 208.75 213.70 20.40 o
3 3 16 60.48 58.73 14.45 o
0 4 16 0.62 8.24 17.46 o
2 4 16 1.86 -1.47 11.42 o
1 1 17 133.32 118.21 20.32 o
3 1 17 159.54 171.22 22.65 o
0 2 17 1096.76 1086.82 171.58 o
2 2 17 914.58 894.67 68.09 o
1 3 17 685.73 698.10 44.42 o
0 0 18 2278.39 2219.30 117.64 o
2 0 18 2192.40 2271.09 108.77 o
1 1 18 1060.99 1064.85 72.84 o
0 2 18 997.53 1036.82 71.56 o