#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:41:20 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181080 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/60/2216071.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216071_Fobs loop_ _publ_author_name 'Gao, Jin-Sheng' 'Zhang, Yi-Ming' 'Li, Bai-Yan' 'Hou, Guang-Feng' _publ_section_title ; trans-Tetraaquabis(2,6-dimethylpyridinium-3,5-dicarboxylato-\kO)cobalt(II) tetrahydrate ; _journal_coeditor_code NG2335 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2717 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.900 _cell_angle_beta 69.750 _cell_angle_gamma 83.580 _cell_length_a 7.5969 _cell_length_b 8.6506 _cell_length_c 10.7150 _exptl_crystal_F_000 308.95 _reflns_d_resolution_high 0.7691 _cod_data_source_file ng2335Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LBy35 in P-1 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 484.78 470.48 6.32 o 3 0 0 1580.44 1603.25 27.50 o 4 0 0 254.99 224.68 2.35 o 5 0 0 272.24 284.72 4.97 o 6 0 0 3.40 3.49 0.64 o 7 0 0 121.80 128.61 1.55 o 8 0 0 48.70 56.98 1.22 o 9 0 0 4.73 3.22 0.90 o -9 1 0 0.24 0.02 0.73 o -8 1 0 18.20 17.48 1.67 o -7 1 0 112.32 107.56 1.87 o -6 1 0 62.82 71.24 1.02 o -5 1 0 144.60 131.03 2.07 o -4 1 0 306.54 301.48 3.76 o -3 1 0 9.88 15.96 1.52 o -2 1 0 10596.72 10987.16 162.72 o -1 1 0 668.71 633.43 10.63 o 1 1 0 3.10 2.30 0.31 o 2 1 0 1027.72 1166.33 12.93 o 3 1 0 2090.52 2137.85 28.26 o 4 1 0 26.36 21.66 1.43 o 5 1 0 217.00 216.33 4.41 o 6 1 0 38.31 39.73 1.28 o 7 1 0 249.64 237.75 4.92 o 8 1 0 110.84 107.52 3.18 o 9 1 0 31.43 29.57 2.06 o -9 2 0 57.32 55.29 4.77 o -8 2 0 13.53 11.98 2.95 o -7 2 0 65.55 72.41 1.93 o -6 2 0 63.28 62.66 2.09 o -5 2 0 2.36 4.97 0.34 o -4 2 0 1456.69 1502.01 15.10 o -3 2 0 65.84 67.15 0.86 o -2 2 0 499.55 473.10 4.05 o -1 2 0 334.12 323.62 3.62 o 0 2 0 21.39 24.20 0.84 o 1 2 0 696.15 686.80 7.11 o 2 2 0 173.15 188.76 2.18 o 3 2 0 1342.21 1354.74 20.85 o 4 2 0 87.93 80.39 2.60 o 5 2 0 288.19 282.27 3.16 o 6 2 0 343.76 353.61 5.97 o 7 2 0 101.32 100.83 2.45 o 8 2 0 446.39 435.43 5.87 o 9 2 0 20.80 22.37 1.20 o -8 3 0 36.62 35.10 1.35 o -7 3 0 126.45 137.22 3.46 o -6 3 0 426.52 433.43 7.99 o -5 3 0 4.72 4.59 1.40 o -4 3 0 874.29 875.80 12.61 o -3 3 0 256.88 230.78 2.37 o -2 3 0 260.97 267.58 2.87 o -1 3 0 109.37 111.92 1.63 o 0 3 0 299.32 317.19 8.89 o 1 3 0 2684.60 2771.26 45.19 o 2 3 0 1392.58 1560.46 19.52 o 3 3 0 25.44 15.19 1.79 o 4 3 0 353.53 392.53 4.26 o 5 3 0 51.56 55.34 1.36 o 6 3 0 197.31 216.30 2.74 o 7 3 0 61.22 63.12 2.09 o 8 3 0 4.23 3.88 1.19 o -8 4 0 34.64 30.55 3.70 o -7 4 0 55.40 63.84 4.24 o -6 4 0 263.54 287.68 7.70 o -5 4 0 66.04 73.71 0.97 o -4 4 0 154.64 155.78 3.50 o -3 4 0 849.52 852.86 9.29 o -2 4 0 110.52 112.29 2.54 o -1 4 0 735.47 708.46 12.95 o 0 4 0 397.60 441.83 10.41 o 1 4 0 222.60 166.44 4.06 o 2 4 0 211.63 239.55 3.33 o 3 4 0 11.22 10.52 0.67 o 4 4 0 1053.98 1056.91 12.82 o 5 4 0 109.01 113.22 2.00 o 6 4 0 14.66 11.03 2.03 o 7 4 0 8.49 3.94 2.03 o 8 4 0 113.34 113.77 4.36 o -8 5 0 72.10 78.10 3.22 o -7 5 0 156.94 161.92 4.30 o -6 5 0 91.25 97.31 2.12 o -5 5 0 47.80 50.85 0.84 o -4 5 0 171.64 172.26 1.85 o -3 5 0 645.57 650.14 6.26 o -2 5 0 19.15 21.95 0.99 o -1 5 0 106.91 92.79 1.58 o 0 5 0 1869.61 1924.91 34.01 o 1 5 0 891.97 923.47 11.46 o 2 5 0 1005.04 995.10 11.96 o 3 5 0 321.30 325.78 5.25 o 4 5 0 929.84 915.93 12.56 o 5 5 0 167.26 162.19 2.32 o 6 5 0 32.89 35.40 1.17 o 7 5 0 33.13 35.13 1.94 o 8 5 0 29.10 30.61 1.91 o -7 6 0 1.10 1.25 1.55 o -6 6 0 11.16 10.19 0.54 o -5 6 0 52.92 47.56 0.94 o -4 6 0 59.74 63.67 1.06 o -3 6 0 3.92 5.00 0.99 o -2 6 0 78.48 84.92 3.04 o -1 6 0 323.99 345.09 6.95 o 0 6 0 467.67 453.52 6.05 o 1 6 0 118.53 111.87 2.12 o 2 6 0 632.02 617.54 11.13 o 3 6 0 342.89 321.57 4.00 o 4 6 0 58.54 62.46 1.79 o 5 6 0 7.79 9.90 1.19 o 6 6 0 27.66 26.40 2.54 o 7 6 0 22.02 21.58 1.42 o -6 7 0 2.61 4.56 0.54 o -5 7 0 7.73 9.73 0.63 o -4 7 0 8.23 12.35 1.53 o -3 7 0 89.39 92.95 2.11 o -2 7 0 494.42 488.34 7.11 o -1 7 0 23.54 19.86 1.53 o 0 7 0 354.45 335.08 4.51 o 1 7 0 445.05 397.29 5.69 o 2 7 0 142.33 144.47 2.36 o 3 7 0 25.03 15.16 1.35 o 4 7 0 63.68 58.53 1.55 o 5 7 0 72.98 78.46 2.07 o 6 7 0 31.64 28.63 3.43 o -6 8 0 79.73 71.41 4.21 o -5 8 0 0.59 0.63 0.88 o -4 8 0 79.38 63.67 8.93 o -3 8 0 166.92 164.81 3.10 o -2 8 0 101.81 102.66 2.36 o -1 8 0 78.62 71.26 2.31 o 0 8 0 16.62 19.26 2.98 o 1 8 0 1.52 0.54 0.89 o 2 8 0 4.59 5.15 1.01 o 3 8 0 17.48 16.93 1.51 o 4 8 0 6.27 6.63 1.07 o 5 8 0 37.76 38.75 2.52 o -4 9 0 38.14 40.77 1.36 o -3 9 0 98.10 98.71 5.01 o -2 9 0 36.50 36.11 2.71 o -1 9 0 0.86 1.95 1.13 o 0 9 0 9.97 9.55 1.31 o 1 9 0 88.78 84.35 2.17 o 2 9 0 33.28 34.72 1.58 o 3 9 0 8.73 7.71 1.52 o 4 9 0 65.22 67.75 1.98 o -2 10 0 30.93 33.06 2.00 o -1 10 0 95.99 97.49 2.72 o 0 10 0 87.92 86.36 3.02 o 1 10 0 24.32 28.45 2.45 o 2 10 0 74.97 80.11 4.00 o -1 -10 1 97.48 98.90 2.74 o 0 -10 1 44.95 46.46 4.47 o 1 -10 1 3.29 4.00 1.43 o 2 -10 1 91.63 91.93 3.04 o -3 -9 1 83.58 95.81 2.82 o -2 -9 1 80.80 84.36 3.91 o -1 -9 1 40.56 39.40 2.18 o 0 -9 1 128.36 122.27 3.20 o 1 -9 1 17.81 14.11 1.80 o 2 -9 1 80.78 85.22 2.38 o 3 -9 1 0.86 0.34 0.76 o 4 -9 1 19.48 20.07 1.72 o -5 -8 1 216.37 247.23 7.28 o -4 -8 1 41.30 43.73 2.86 o -3 -8 1 36.39 36.58 1.83 o -2 -8 1 13.13 14.77 1.52 o -1 -8 1 63.87 58.96 2.16 o 0 -8 1 5.54 3.91 1.08 o 1 -8 1 178.58 152.04 3.28 o 2 -8 1 1.24 1.99 1.33 o 3 -8 1 112.66 111.81 2.51 o 4 -8 1 9.48 13.12 1.94 o 5 -8 1 92.18 92.35 1.62 o -6 -7 1 111.22 120.90 2.51 o -5 -7 1 192.76 199.06 3.80 o -4 -7 1 57.59 57.11 1.68 o -3 -7 1 103.72 98.47 2.17 o -2 -7 1 220.41 208.16 3.53 o -1 -7 1 29.02 23.27 1.67 o 0 -7 1 34.87 33.80 1.70 o 1 -7 1 192.64 183.14 3.35 o 2 -7 1 126.61 121.87 2.76 o 3 -7 1 180.32 163.55 3.35 o 4 -7 1 45.45 41.83 1.72 o 5 -7 1 154.44 162.23 2.36 o 6 -7 1 99.83 101.82 3.36 o -7 -6 1 75.84 81.89 4.77 o -6 -6 1 10.79 9.48 1.89 o -5 -6 1 95.40 95.54 1.98 o -4 -6 1 130.64 123.65 2.50 o -3 -6 1 3.83 3.60 1.09 o -2 -6 1 37.99 40.70 1.58 o -1 -6 1 208.66 186.64 2.74 o 0 -6 1 314.79 312.63 5.97 o 1 -6 1 458.23 420.18 5.29 o 2 -6 1 25.20 21.70 1.25 o 3 -6 1 682.57 630.74 33.37 o 4 -6 1 189.98 189.43 2.33 o 5 -6 1 0.37 0.75 0.52 o 6 -6 1 2.59 3.19 0.52 o 7 -6 1 3.61 1.29 0.68 o -7 -5 1 45.54 52.25 1.92 o -6 -5 1 16.76 18.20 1.37 o -5 -5 1 79.41 79.68 2.56 o -4 -5 1 237.71 247.04 3.28 o -3 -5 1 10.07 9.76 0.88 o -2 -5 1 116.03 114.81 1.83 o -1 -5 1 1043.22 1051.38 12.85 o 0 -5 1 713.23 678.73 11.54 o 1 -5 1 986.70 1018.39 12.46 o 2 -5 1 968.48 950.01 22.25 o 3 -5 1 135.84 125.00 1.65 o 4 -5 1 233.90 222.64 2.57 o 5 -5 1 0.69 0.34 0.47 o 6 -5 1 131.16 130.49 3.38 o 7 -5 1 44.64 40.66 0.92 o 8 -5 1 13.86 20.52 3.34 o -8 -4 1 9.24 9.72 2.68 o -7 -4 1 38.84 41.52 3.28 o -6 -4 1 212.98 212.62 3.39 o -5 -4 1 8.12 9.21 1.09 o -4 -4 1 147.57 142.34 2.38 o -3 -4 1 52.62 53.67 1.40 o -2 -4 1 483.88 454.80 7.01 o -1 -4 1 1299.10 1279.26 16.07 o 0 -4 1 1611.48 1704.81 27.50 o 1 -4 1 21.67 36.78 1.15 o 2 -4 1 128.00 102.97 1.97 o 3 -4 1 311.29 298.43 2.90 o 4 -4 1 149.81 148.15 1.57 o 5 -4 1 54.77 61.45 1.10 o 6 -4 1 75.41 82.58 1.58 o 7 -4 1 184.90 201.00 6.32 o 8 -4 1 13.67 15.81 2.98 o -8 -3 1 188.51 177.19 4.18 o -7 -3 1 26.73 27.74 1.67 o -6 -3 1 55.57 57.26 1.43 o -5 -3 1 12.85 14.60 1.19 o -4 -3 1 326.96 343.04 4.31 o -3 -3 1 56.26 53.70 1.22 o -2 -3 1 244.73 233.21 2.78 o -1 -3 1 99.19 103.82 2.30 o 0 -3 1 62.69 95.19 1.44 o 1 -3 1 59.54 59.26 0.95 o 2 -3 1 34.99 26.72 0.90 o 3 -3 1 274.63 264.62 2.82 o 4 -3 1 47.51 56.54 0.94 o 5 -3 1 25.02 22.01 0.80 o 6 -3 1 7.88 8.53 1.25 o 7 -3 1 119.22 115.38 3.04 o 8 -3 1 56.96 56.98 2.33 o 9 -3 1 15.47 16.28 2.09 o -8 -2 1 5.76 5.43 1.37 o -7 -2 1 29.77 30.25 2.80 o -6 -2 1 550.38 551.92 9.61 o -5 -2 1 95.68 97.93 1.56 o -4 -2 1 1311.11 1306.91 17.15 o -3 -2 1 1298.12 1317.72 15.82 o -2 -2 1 888.43 763.38 8.46 o -1 -2 1 153.02 162.87 1.73 o 0 -2 1 1721.13 1710.43 38.84 o 1 -2 1 274.82 265.58 2.97 o 2 -2 1 294.65 295.11 2.36 o 3 -2 1 94.75 97.09 1.00 o 4 -2 1 220.06 250.95 2.89 o 5 -2 1 268.11 290.87 2.82 o 6 -2 1 269.74 291.61 5.85 o 7 -2 1 49.31 58.32 1.40 o 8 -2 1 96.91 101.30 1.24 o 9 -2 1 3.52 7.94 2.95 o -8 -1 1 340.77 327.20 8.60 o -7 -1 1 158.72 157.43 3.52 o -6 -1 1 245.98 228.32 5.55 o -5 -1 1 284.70 284.28 4.71 o -4 -1 1 965.62 934.76 15.33 o -3 -1 1 1052.99 1040.75 18.08 o -2 -1 1 193.28 210.26 2.07 o -1 -1 1 467.15 451.63 4.43 o 0 -1 1 886.80 830.49 8.42 o 1 -1 1 964.56 976.95 8.43 o 2 -1 1 9502.21 9624.83 136.72 o 3 -1 1 1398.10 1433.42 12.19 o 4 -1 1 2442.95 2874.89 41.15 o 5 -1 1 47.35 56.03 3.73 o 6 -1 1 101.78 112.99 1.46 o 7 -1 1 61.05 56.46 1.08 o 8 -1 1 19.16 17.65 0.61 o 9 -1 1 8.03 5.74 1.08 o -8 0 1 86.73 88.06 2.43 o -7 0 1 108.83 120.07 3.51 o -6 0 1 4.63 5.19 0.97 o -5 0 1 101.49 105.41 2.15 o -4 0 1 269.47 270.50 4.95 o -3 0 1 307.12 302.96 4.30 o -2 0 1 156.49 172.00 2.39 o -1 0 1 3479.54 3682.73 54.64 o 2 0 1 11204.12 11268.10 193.97 o 3 0 1 3994.20 4364.04 69.72 o 4 0 1 2277.07 2581.17 29.97 o 5 0 1 14.80 12.96 0.46 o 6 0 1 235.93 211.92 3.22 o 7 0 1 151.95 150.00 2.22 o 8 0 1 40.61 37.90 1.70 o 9 0 1 8.57 10.09 1.61 o -8 1 1 14.52 18.18 1.48 o -7 1 1 10.72 11.98 0.45 o -6 1 1 56.19 55.66 0.94 o -5 1 1 164.43 167.90 1.52 o -4 1 1 9.38 11.41 0.32 o -3 1 1 574.52 570.90 11.10 o -2 1 1 93.82 93.05 2.65 o -1 1 1 331.51 362.65 4.27 o 1 1 1 2616.65 2533.69 32.78 o 2 1 1 927.45 1006.07 10.50 o 3 1 1 199.33 174.92 2.74 o 4 1 1 549.25 510.57 7.22 o 5 1 1 3.51 2.30 0.40 o 6 1 1 80.90 75.08 1.27 o 7 1 1 216.72 215.42 2.30 o 8 1 1 12.77 11.63 0.72 o 9 1 1 57.18 56.71 3.94 o -8 2 1 16.80 17.03 1.40 o -7 2 1 301.37 300.91 6.92 o -6 2 1 4.57 5.73 0.44 o -5 2 1 13.38 15.44 0.51 o -4 2 1 1.46 1.60 0.36 o -3 2 1 509.42 531.34 8.29 o -2 2 1 88.52 94.24 0.85 o -1 2 1 1.40 2.14 0.50 o 0 2 1 266.63 274.60 3.35 o 1 2 1 102.97 119.68 1.50 o 2 2 1 471.23 497.04 5.17 o 3 2 1 486.81 508.69 7.58 o 4 2 1 671.85 633.71 14.20 o 5 2 1 260.99 263.64 4.00 o 6 2 1 1.08 3.40 0.78 o 7 2 1 198.45 190.24 2.62 o 8 2 1 46.27 45.72 1.20 o 9 2 1 10.64 13.37 1.40 o -8 3 1 15.13 19.09 2.83 o -7 3 1 126.06 122.08 5.25 o -6 3 1 115.40 123.91 3.22 o -5 3 1 105.25 111.80 2.92 o -4 3 1 566.31 605.64 6.54 o -3 3 1 753.95 726.52 8.60 o -2 3 1 1722.18 1671.61 31.59 o -1 3 1 73.69 73.11 1.79 o 0 3 1 4767.28 5239.04 103.54 o 1 3 1 51.66 37.65 0.72 o 2 3 1 698.91 736.43 7.70 o 3 3 1 447.99 464.90 5.10 o 4 3 1 0.69 2.88 1.07 o 5 3 1 326.40 317.30 4.11 o 6 3 1 14.80 13.78 1.01 o 7 3 1 51.07 53.52 1.67 o 8 3 1 137.85 -0.54 0.60 o 9 3 1 17.16 12.61 4.06 o -8 4 1 16.36 13.75 1.46 o -7 4 1 98.85 99.16 5.13 o -6 4 1 53.74 58.94 3.94 o -5 4 1 1.66 12.76 5.73 o -4 4 1 630.11 636.18 7.81 o -3 4 1 629.89 631.95 8.77 o -2 4 1 320.95 292.06 3.70 o -1 4 1 1.55 5.17 2.77 o 0 4 1 2065.58 2099.72 47.52 o 1 4 1 1268.52 1236.56 26.88 o 2 4 1 653.80 737.66 16.20 o 3 4 1 158.80 146.87 1.73 o 4 4 1 45.51 47.10 1.10 o 5 4 1 196.10 204.30 2.73 o 6 4 1 3.10 6.17 1.34 o 7 4 1 48.49 47.07 1.73 o 8 4 1 83.64 77.08 2.27 o -8 5 1 9.82 13.96 2.09 o -7 5 1 1.20 1.37 1.55 o -6 5 1 95.43 97.60 3.22 o -5 5 1 276.10 302.60 3.18 o -4 5 1 267.22 257.27 2.64 o -3 5 1 37.47 34.97 1.42 o -2 5 1 768.90 727.68 8.69 o -1 5 1 556.51 518.78 8.05 o 0 5 1 256.86 242.18 3.76 o 1 5 1 328.47 295.87 4.65 o 2 5 1 86.63 82.09 1.33 o 3 5 1 1395.45 1422.59 18.60 o 4 5 1 225.39 234.77 2.84 o 5 5 1 189.42 183.36 2.38 o 6 5 1 309.23 322.53 7.73 o 7 5 1 139.40 132.93 3.85 o 8 5 1 109.65 108.34 2.86 o -7 6 1 86.85 94.68 3.64 o -6 6 1 133.80 121.72 7.79 o -5 6 1 0.32 -0.18 0.66 o -4 6 1 26.26 23.83 0.88 o -3 6 1 59.15 54.49 1.73 o -2 6 1 54.58 50.22 1.45 o -1 6 1 21.44 24.65 2.30 o 0 6 1 56.88 56.76 2.60 o 1 6 1 1104.12 1148.13 15.01 o 2 6 1 28.24 30.19 2.18 o 3 6 1 166.76 162.39 2.27 o 4 6 1 252.64 272.09 3.80 o 5 6 1 380.13 363.46 7.22 o 6 6 1 126.39 134.83 2.12 o 7 6 1 2.27 2.02 0.95 o -6 7 1 3.59 5.76 1.61 o -5 7 1 0.27 0.80 0.58 o -4 7 1 7.47 7.36 0.79 o -3 7 1 162.00 160.98 2.83 o -2 7 1 2.06 2.42 0.97 o -1 7 1 17.12 20.20 2.10 o 0 7 1 9.18 10.55 2.24 o 1 7 1 304.79 286.25 4.31 o 2 7 1 91.26 95.50 2.54 o 3 7 1 106.48 74.80 1.58 o 4 7 1 289.14 300.92 4.33 o 5 7 1 7.94 5.61 1.13 o 6 7 1 66.97 66.66 1.85 o 7 7 1 8.32 9.94 1.88 o -6 8 1 14.77 16.98 3.16 o -5 8 1 80.06 75.88 1.44 o -4 8 1 230.40 231.50 2.97 o -3 8 1 28.30 29.30 1.65 o -2 8 1 45.15 48.34 2.03 o -1 8 1 182.88 178.65 3.22 o 0 8 1 80.57 81.80 1.92 o 1 8 1 259.83 235.56 3.46 o 2 8 1 126.99 127.95 2.30 o 3 8 1 60.93 50.04 1.47 o 4 8 1 83.18 86.87 2.77 o 5 8 1 17.34 19.03 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29.52 32.57 2.27 o -3 4 10 1.21 2.14 1.55 o -2 4 10 47.86 46.40 1.90 o -1 4 10 59.54 59.14 2.45 o 0 4 10 3.42 1.73 0.79 o 1 4 10 251.13 252.97 2.53 o 2 4 10 110.32 107.47 1.25 o 3 4 10 288.38 272.21 2.60 o 4 4 10 93.23 94.74 3.82 o 5 4 10 204.96 201.47 4.30 o 6 4 10 2.68 3.40 1.37 o 7 4 10 0.99 -0.54 1.31 o 8 4 10 59.27 63.36 2.86 o -3 5 10 131.46 127.98 5.67 o -2 5 10 6.00 7.85 1.24 o -1 5 10 226.14 235.75 3.71 o 0 5 10 84.06 81.69 1.71 o 1 5 10 456.28 434.42 4.04 o 2 5 10 7.98 8.49 0.71 o 3 5 10 65.74 58.38 0.87 o 4 5 10 48.25 51.34 2.03 o 5 5 10 10.51 10.74 1.49 o 6 5 10 13.55 12.77 1.61 o 7 5 10 1.39 2.03 1.43 o 8 5 10 107.63 111.21 3.64 o -3 6 10 104.20 110.54 4.27 o -2 6 10 17.22 22.00 1.27 o -1 6 10 63.06 62.02 1.53 o 0 6 10 152.87 151.00 1.95 o 1 6 10 68.85 64.10 1.21 o 2 6 10 87.90 91.81 1.29 o 3 6 10 2.19 4.53 0.41 o 4 6 10 225.99 222.69 3.38 o 5 6 10 59.41 57.39 2.27 o 6 6 10 84.75 86.15 2.86 o 7 6 10 66.72 66.28 2.80 o 8 6 10 66.96 66.34 3.10 o -2 7 10 67.39 69.10 2.77 o -1 7 10 124.68 121.44 3.55 o 0 7 10 42.53 39.44 0.96 o 1 7 10 21.65 25.91 1.04 o 2 7 10 156.82 151.17 3.55 o 3 7 10 150.49 137.74 1.99 o 4 7 10 41.92 41.91 2.51 o 5 7 10 36.82 41.58 2.09 o 6 7 10 149.78 153.69 4.00 o 7 7 10 34.89 36.75 2.51 o -2 8 10 38.46 31.74 4.12 o -1 8 10 19.25 15.99 1.79 o 0 8 10 10.88 9.30 0.85 o 1 8 10 20.99 16.91 0.77 o 2 8 10 11.70 12.32 0.74 o 3 8 10 42.25 38.78 1.25 o 4 8 10 47.25 43.66 1.07 o 5 8 10 79.67 82.51 2.74 o 6 8 10 40.26 43.55 2.39 o -1 9 10 0.44 -0.72 2.45 o 0 9 10 3.37 1.69 0.79 o 1 9 10 25.80 28.76 1.40 o 2 9 10 1.77 1.01 0.63 o 3 9 10 55.57 53.52 1.22 o 4 9 10 78.56 75.22 1.52 o 5 9 10 10.32 3.76 2.63 o 2 10 10 63.27 63.63 1.43 o 3 10 10 2.69 1.65 0.57 o 1 -3 11 2.37 3.01 0.91 o 2 -3 11 16.71 18.56 1.15 o 3 -3 11 41.12 40.12 1.23 o 4 -3 11 140.66 149.60 2.13 o 0 -2 11 52.32 52.10 2.95 o 1 -2 11 4.29 3.58 0.96 o 2 -2 11 47.89 49.44 1.50 o 3 -2 11 68.88 68.46 1.43 o 4 -2 11 5.76 6.75 0.86 o 5 -2 11 91.34 95.10 1.23 o 6 -2 11 66.63 69.21 3.10 o -1 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121.74 128.28 2.80 o 6 2 11 2.16 2.74 1.49 o 7 2 11 69.38 76.60 3.10 o 8 2 11 28.97 29.65 2.39 o -2 3 11 3.51 3.36 1.03 o -1 3 11 33.93 34.63 1.09 o 0 3 11 53.35 52.01 1.22 o 1 3 11 41.41 44.24 1.04 o 2 3 11 84.89 82.56 1.02 o 3 3 11 9.39 10.96 0.60 o 4 3 11 1.97 1.43 0.30 o 5 3 11 19.02 23.45 1.79 o 6 3 11 12.69 11.22 1.73 o 7 3 11 83.40 89.07 3.22 o 8 3 11 97.38 95.81 3.58 o -2 4 11 53.40 55.05 2.11 o -1 4 11 49.67 52.96 4.44 o 0 4 11 177.56 171.33 2.42 o 1 4 11 11.51 11.47 0.82 o 2 4 11 20.79 25.89 0.73 o 3 4 11 3.23 5.78 0.49 o 4 4 11 153.50 157.38 5.07 o 5 4 11 261.98 264.53 5.43 o 6 4 11 4.27 3.76 1.49 o 7 4 11 153.18 145.87 4.12 o 8 4 11 30.47 36.87 2.63 o -2 5 11 87.33 85.29 6.92 o -1 5 11 0.47 0.74 0.91 o 0 5 11 199.19 206.37 4.92 o 1 5 11 165.32 175.68 2.35 o 2 5 11 45.24 46.89 0.79 o 3 5 11 462.35 444.46 4.19 o 4 5 11 60.38 51.29 2.16 o 5 5 11 285.53 273.18 5.61 o 6 5 11 0.88 0.89 1.37 o 7 5 11 0.79 2.74 1.61 o 8 5 11 38.06 46.42 2.80 o -2 6 11 54.19 54.76 2.51 o -1 6 11 41.35 47.85 2.63 o 0 6 11 20.01 23.19 1.16 o 1 6 11 75.68 67.91 4.24 o 2 6 11 41.09 43.76 0.74 o 3 6 11 313.70 287.14 4.78 o 4 6 11 16.06 15.69 0.80 o 5 6 11 3.85 6.68 1.43 o 6 6 11 95.84 97.60 3.16 o 7 6 11 19.23 22.37 2.15 o -1 7 11 2.99 2.48 1.02 o 0 7 11 0.85 1.08 0.43 o 1 7 11 456.19 424.67 4.35 o 2 7 11 31.49 30.63 0.91 o 3 7 11 33.80 36.55 0.62 o 4 7 11 62.53 58.05 2.09 o 5 7 11 137.56 133.22 3.52 o 6 7 11 44.86 48.80 2.45 o 7 7 11 0.66 2.03 1.61 o -1 8 11 99.40 93.96 2.07 o 0 8 11 4.51 1.83 0.87 o 1 8 11 78.19 81.49 2.98 o 2 8 11 14.41 14.81 0.93 o 3 8 11 2.86 4.28 0.82 o 4 8 11 42.17 39.14 3.16 o 5 8 11 8.90 6.56 1.49 o 6 8 11 2.56 1.91 1.49 o 1 9 11 1.95 0.63 0.78 o 2 9 11 5.65 6.44 1.64 o 3 9 11 3.22 1.98 0.98 o 4 9 11 8.25 7.46 1.43 o 1 -1 12 14.88 17.58 0.97 o 2 -1 12 6.73 7.92 0.80 o 3 -1 12 39.76 39.05 1.02 o 4 -1 12 88.12 97.19 1.28 o 5 -1 12 0.37 0.95 1.55 o 0 0 12 90.83 96.43 2.20 o 1 0 12 93.21 93.80 1.77 o 2 0 12 65.57 71.89 1.97 o 3 0 12 94.86 87.45 2.29 o 4 0 12 206.73 208.17 4.41 o 5 0 12 38.32 39.26 2.33 o 6 0 12 122.70 129.46 6.09 o -1 1 12 23.65 28.57 1.71 o 0 1 12 15.73 15.68 1.16 o 1 1 12 13.29 9.94 1.25 o 2 1 12 89.03 95.24 1.63 o 3 1 12 77.16 78.02 2.36 o 4 1 12 170.65 165.72 2.40 o 5 1 12 181.92 20.28 2.03 o 6 1 12 0.57 0.18 1.01 o 7 1 12 5.15 6.59 1.39 o -1 2 12 25.26 30.72 1.29 o 0 2 12 87.03 87.31 1.77 o 1 2 12 126.47 127.74 2.20 o 2 2 12 68.35 66.89 1.26 o 3 2 12 142.48 151.53 1.57 o 4 2 12 48.34 46.91 1.58 o 5 2 12 12.58 13.22 1.50 o 6 2 12 67.18 64.12 1.98 o 7 2 12 64.94 62.94 3.04 o -1 3 12 239.01 247.35 4.80 o 0 3 12 87.22 83.32 1.34 o 1 3 12 245.10 241.25 2.47 o 2 3 12 5.67 6.11 0.47 o 3 3 12 13.96 14.22 0.82 o 4 3 12 51.79 47.13 2.09 o 5 3 12 32.76 31.74 2.03 o 6 3 12 15.63 18.61 1.97 o 7 3 12 1.58 3.58 3.04 o -1 4 12 22.52 20.00 1.67 o 0 4 12 70.76 69.96 2.12 o 1 4 12 24.84 24.09 2.15 o 2 4 12 1.22 1.07 0.66 o 3 4 12 0.67 0.53 0.35 o 4 4 12 42.92 46.42 2.03 o 5 4 12 0.96 1.49 1.31 o 6 4 12 17.43 17.60 1.91 o 7 4 12 26.10 23.03 3.88 o -1 5 12 117.30 116.76 6.29 o 0 5 12 58.96 56.73 1.64 o 1 5 12 12.15 12.21 0.65 o 2 5 12 95.87 97.16 1.62 o 3 5 12 123.99 129.87 3.75 o 4 5 12 109.72 105.18 4.30 o 5 5 12 51.57 53.40 2.33 o 6 5 12 78.17 75.47 2.86 o 7 5 12 172.49 166.57 6.86 o -1 6 12 7.49 6.12 0.99 o 0 6 12 8.14 7.49 1.64 o 1 6 12 102.83 114.91 1.97 o 2 6 12 111.40 109.64 1.56 o 3 6 12 4.04 2.99 0.44 o 5 6 12 162.07 158.10 3.94 o 6 6 12 38.95 47.67 2.51 o 0 7 12 66.89 67.22 1.53 o 1 7 12 0.44 1.52 0.56 o 2 7 12 15.19 17.36 0.59 o 3 7 12 21.66 18.49 0.83 o 4 7 12 45.81 46.00 3.28 o 5 7 12 106.19 112.28 3.28 o 6 7 12 11.60 15.15 1.91 o 1 8 12 32.50 29.88 0.89 o 2 8 12 0.65 0.35 0.47 o 3 8 12 94.25 94.32 2.51 o 4 8 12 41.82 38.18 2.03 o 5 8 12 45.09 40.99 3.64 o 3 0 13 156.78 165.97 2.55 o 1 1 13 144.49 155.19 2.79 o 2 1 13 2.65 2.08 0.82 o 3 1 13 23.12 19.84 0.87 o 4 1 13 49.42 50.71 2.51 o 5 1 13 32.94 32.93 2.33 o 1 2 13 12.05 17.18 1.55 o 2 2 13 1.55 1.00 0.63 o 3 2 13 15.80 16.61 1.08 o 4 2 13 88.83 90.21 2.92 o 5 2 13 45.93 48.62 1.85 o 6 2 13 23.27 27.62 1.67 o 0 3 13 70.31 71.68 1.24 o 1 3 13 218.38 225.88 2.46 o 2 3 13 14.39 14.77 1.23 o 3 3 13 94.46 88.29 2.12 o 4 3 13 129.12 132.45 3.52 o 5 3 13 6.42 6.50 1.61 o 6 3 13 21.22 20.58 2.15 o 0 4 13 35.24 39.50 1.91 o 1 4 13 39.45 41.82 2.63 o 2 4 13 41.49 42.42 2.09 o 3 4 13 40.07 40.33 3.04 o 4 4 13 62.05 58.29 2.39 o 5 4 13 7.67 13.42 1.73 o 6 4 13 14.07 14.44 1.97 o 1 5 13 133.64 137.62 2.04 o 2 5 13 114.17 118.45 1.98 o 3 5 13 5.20 5.07 2.09 o 4 5 13 50.24 49.52 3.58 o 5 5 13 176.94 190.67 4.53 o 6 5 13 37.32 39.97 2.45 o 1 6 13 7.32 6.19 0.69 o 2 6 13 13.99 11.22 0.72 o 3 6 13 63.23 65.15 3.28 o 4 6 13 94.07 90.56 2.80 o 5 6 13 89.01 98.80 3.10 o 2 7 13 36.49 36.43 0.83 o 3 7 13 2.76 1.31 1.79 o 4 7 13 14.71 15.45 1.61 o