#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/60/2216074.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216074_Fobs loop_ _publ_author_name 'Varga, Richard A.' 'Silvestru, Cristian' _publ_section_title ; Tetrakis[2-(dimethylaminomethyl)phenyl]-1\kC,2\kC,3\kC,4\kC-hexa-\m-sulfido-1:2\k^4^S:S;1,4\k^2^S:S;2:3\k^2^S:S;3:4\k^4^S:S-tetratin(IV) chloroform solvate ; _journal_coeditor_code NG2339 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2789 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.957 _cell_angle_gamma 90.000 _cell_length_a 18.3436 _cell_length_b 12.9426 _cell_length_c 20.5064 _exptl_crystal_F_000 2584.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ng2339Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 240rich in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 711.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 110664.88 117217.84 2191.90 o 3 0 0 20510.73 19287.95 431.85 o 4 0 0 67535.53 72184.70 1223.20 o 5 0 0 6240.49 5934.07 168.78 o 6 0 0 6769.47 7345.42 209.90 o 7 0 0 7957.22 8503.40 261.33 o 8 0 0 31219.89 31452.09 649.24 o 9 0 0 2592.60 2775.44 144.81 o 10 0 0 6173.14 5875.53 212.13 o 11 0 0 178930.11 178059.92 3041.80 o 12 0 0 31336.53 27757.41 1441.27 o 13 0 0 20363.01 20228.77 842.57 o 14 0 0 2360.28 2623.25 272.04 o 15 0 0 9219.74 8803.28 432.77 o 16 0 0 18.03 176.69 103.16 o 17 0 0 2453.51 3166.24 320.37 o 18 0 0 300.10 384.98 226.14 o 19 0 0 829.31 1100.53 197.06 o 20 0 0 986.79 1053.58 208.02 o 21 0 0 5554.54 5453.32 589.10 o 1 1 0 115531.03 124540.54 1525.01 o 2 1 0 16667.03 17539.34 230.24 o 3 1 0 10.23 68.06 14.67 o 4 1 0 19293.11 19416.86 274.07 o 5 1 0 8057.67 7730.52 144.00 o 6 1 0 4372.99 4748.69 109.70 o 7 1 0 5595.30 5509.68 128.29 o 8 1 0 50847.45 49504.54 663.32 o 9 1 0 13772.59 13384.38 250.27 o 10 1 0 9938.93 9494.23 204.22 o 11 1 0 4792.35 5017.40 149.74 o 12 1 0 21310.68 20117.07 492.33 o 13 1 0 27697.26 27360.45 580.40 o 14 1 0 1469.49 1474.91 140.80 o 15 1 0 214.22 264.02 73.20 o 16 1 0 3842.91 4227.61 253.94 o 17 1 0 479.16 672.56 105.95 o 18 1 0 1373.69 1662.74 166.35 o 19 1 0 648.46 640.79 123.10 o 20 1 0 3665.94 3589.07 283.86 o 21 1 0 2004.73 2784.02 248.77 o 0 2 0 4237.48 4750.21 149.20 o 1 2 0 5094.10 4876.14 85.62 o 2 2 0 32113.54 34230.46 429.29 o 3 2 0 46117.43 49272.43 640.37 o 4 2 0 56439.59 60437.85 742.87 o 5 2 0 32237.93 33589.42 542.81 o 6 2 0 12336.57 12058.25 212.28 o 7 2 0 358.36 632.01 49.54 o 8 2 0 2454.78 2551.43 96.02 o 9 2 0 1200.34 1418.68 80.81 o 10 2 0 1761.80 1987.09 96.89 o 11 2 0 468.92 640.78 61.10 o 12 2 0 2016.89 2161.37 133.56 o 13 2 0 11020.92 10818.61 320.43 o 14 2 0 1739.95 2037.74 163.99 o 15 2 0 12945.63 12735.21 376.47 o 16 2 0 3032.67 3295.19 220.70 o 17 2 0 1485.83 1610.28 181.58 o 18 2 0 4.91 162.02 103.66 o 19 2 0 98.26 191.82 93.24 o 20 2 0 857.32 1140.64 176.47 o 21 2 0 318.39 604.67 142.24 o 1 3 0 425981.81 427162.44 4816.51 o 2 3 0 7543.29 7769.30 133.83 o 3 3 0 39361.81 39562.41 541.35 o 4 3 0 19758.73 21220.08 307.97 o 5 3 0 6101.92 6536.41 135.61 o 6 3 0 363.70 502.53 40.57 o 7 3 0 39461.08 40781.13 567.03 o 8 3 0 1597.83 1524.68 90.65 o 9 3 0 6836.59 6399.97 161.44 o 10 3 0 21577.20 22573.73 384.03 o 11 3 0 4906.77 5001.01 156.79 o 12 3 0 41558.99 40255.79 673.75 o 13 3 0 2019.77 2288.57 169.11 o 14 3 0 33439.70 33219.18 681.76 o 15 3 0 2792.73 2629.24 222.57 o 16 3 0 6343.85 6896.11 344.91 o 17 3 0 50.71 325.74 89.72 o 18 3 0 623.69 1114.48 180.42 o 19 3 0 3557.79 3793.09 336.76 o 20 3 0 1906.34 2487.78 263.49 o 21 3 0 870.68 1321.10 202.63 o 0 4 0 89041.42 98375.26 1815.66 o 1 4 0 3689.63 3894.07 92.87 o 2 4 0 45957.09 49055.19 625.06 o 3 4 0 16323.27 16435.88 294.39 o 4 4 0 5649.11 5515.17 119.32 o 5 4 0 3735.16 3519.98 95.13 o 6 4 0 16812.04 17321.93 284.75 o 7 4 0 8449.54 8353.64 180.24 o 8 4 0 6584.92 6492.15 178.38 o 9 4 0 1071.81 1316.75 82.57 o 10 4 0 1213.33 1563.11 91.08 o 11 4 0 7109.95 6519.57 200.49 o 12 4 0 23425.29 23180.20 574.77 o 13 4 0 8199.45 8228.46 276.21 o 14 4 0 4060.55 4203.89 270.39 o 15 4 0 8724.30 8399.99 343.19 o 16 4 0 86.88 227.86 100.10 o 17 4 0 1425.32 1800.25 208.53 o 18 4 0 1406.85 1686.71 206.67 o 19 4 0 757.52 1015.14 236.80 o 20 4 0 819.28 936.14 165.63 o 1 5 0 6110.54 6263.81 159.26 o 2 5 0 9474.02 9393.86 176.63 o 3 5 0 51072.40 52287.28 679.12 o 4 5 0 108576.79 108992.99 1412.27 o 5 5 0 19248.88 18925.96 430.10 o 6 5 0 22494.87 22063.94 408.57 o 7 5 0 80.52 111.13 26.59 o 8 5 0 11298.26 10879.10 224.30 o 9 5 0 3337.43 3476.48 122.83 o 10 5 0 6668.45 6360.88 299.44 o 11 5 0 7236.56 6680.13 221.17 o 12 5 0 3129.23 2903.56 257.28 o 13 5 0 5554.63 5797.89 279.72 o 14 5 0 6742.48 6877.78 395.63 o 15 5 0 3905.45 3661.52 301.05 o 16 5 0 29.53 224.08 97.20 o 17 5 0 4137.75 4172.13 340.42 o 18 5 0 3.31 231.32 106.53 o 19 5 0 49.81 286.88 143.42 o 20 5 0 657.55 1163.87 213.64 o 0 6 0 4534.94 4646.47 234.29 o 1 6 0 5814.66 5642.12 157.62 o 2 6 0 82976.83 83809.10 1070.95 o 3 6 0 10308.47 10855.62 207.89 o 4 6 0 64272.56 63428.85 893.41 o 5 6 0 20171.97 19826.82 366.07 o 6 6 0 4535.43 4530.59 154.06 o 7 6 0 34899.52 34853.16 575.86 o 8 6 0 272.94 228.20 45.49 o 9 6 0 31527.93 30381.58 538.10 o 10 6 0 2657.37 2780.22 175.13 o 11 6 0 2487.13 2469.80 163.10 o 12 6 0 4992.48 4992.69 283.97 o 13 6 0 21937.81 21092.12 563.95 o 14 6 0 30.09 216.80 100.00 o 15 6 0 13049.75 11737.64 604.31 o 16 6 0 6110.85 5385.92 388.78 o 17 6 0 0.67 215.81 110.33 o 18 6 0 775.00 948.09 168.98 o 19 6 0 105.99 411.86 120.05 o 1 7 0 24.23 145.93 27.45 o 2 7 0 41570.68 42592.66 603.70 o 3 7 0 28241.21 27887.79 449.82 o 4 7 0 263.13 443.02 41.90 o 5 7 0 3159.46 3422.31 141.45 o 6 7 0 82.77 88.95 45.55 o 7 7 0 9516.30 9309.98 276.95 o 8 7 0 18176.13 16892.41 407.86 o 9 7 0 5584.99 5442.05 228.68 o 10 7 0 365.82 548.88 85.77 o 11 7 0 4419.14 4692.77 228.80 o 12 7 0 55.52 232.94 79.29 o 13 7 0 806.21 811.07 130.04 o 14 7 0 17589.48 16909.81 601.45 o 15 7 0 2461.59 2647.47 266.07 o 16 7 0 2847.58 2797.76 280.79 o 17 7 0 825.18 977.55 177.80 o 18 7 0 654.47 1018.32 176.01 o 19 7 0 3516.77 3746.71 347.16 o 0 8 0 13192.44 13173.72 369.69 o 1 8 0 17623.33 17335.75 314.59 o 2 8 0 16.06 26.64 29.78 o 3 8 0 40613.72 39401.31 635.45 o 4 8 0 0.90 53.19 54.18 o 5 8 0 5048.84 4830.88 214.16 o 6 8 0 23846.52 22677.46 494.96 o 7 8 0 1707.82 2132.91 161.00 o 8 8 0 516.80 681.26 92.48 o 9 8 0 4416.08 4566.28 228.87 o 10 8 0 18939.24 18102.69 453.25 o 11 8 0 21519.59 20083.67 493.14 o 12 8 0 2207.04 2348.33 200.13 o 13 8 0 148.54 127.12 86.12 o 14 8 0 364.51 521.35 112.57 o 15 8 0 3922.91 4063.78 342.71 o 16 8 0 506.90 535.25 121.22 o 17 8 0 2426.37 1973.03 227.61 o 18 8 0 5882.56 5476.15 426.95 o 1 9 0 3280.49 3323.12 129.09 o 2 9 0 7448.48 7680.02 254.58 o 3 9 0 6188.30 6136.53 227.02 o 4 9 0 885.40 1250.47 119.98 o 5 9 0 15816.63 14888.93 385.38 o 6 9 0 2057.86 2415.48 173.56 o 7 9 0 16149.22 15938.34 414.61 o 8 9 0 7279.21 7188.05 273.48 o 9 9 0 25.92 171.79 63.30 o 10 9 0 24518.69 24283.79 567.89 o 11 9 0 4563.91 4907.53 266.43 o 12 9 0 14569.64 14315.76 470.29 o 13 9 0 16.72 330.53 95.29 o 14 9 0 77.59 284.29 117.27 o 15 9 0 16.15 358.20 115.73 o 16 9 0 953.44 1457.90 203.92 o 17 9 0 374.98 718.04 159.81 o 0 10 0 270.03 265.21 121.62 o 1 10 0 116.53 212.83 58.09 o 2 10 0 805.89 1042.48 105.80 o 3 10 0 2963.07 3078.52 191.26 o 4 10 0 64.97 130.48 56.71 o 5 10 0 1556.40 1710.31 149.97 o 6 10 0 3690.44 3717.05 225.55 o 7 10 0 4489.57 4542.66 249.49 o 8 10 0 19207.00 17241.19 457.84 o 9 10 0 950.32 1111.71 122.95 o 10 10 0 816.64 880.91 113.22 o 11 10 0 3859.35 3891.44 275.03 o 12 10 0 1.66 202.30 89.17 o 13 10 0 38.69 263.95 92.84 o 14 10 0 35.43 342.59 114.92 o 15 10 0 5.70 150.42 115.80 o 16 10 0 347.10 668.47 168.07 o 1 11 0 2009.44 2327.35 229.62 o 2 11 0 14092.94 13181.54 483.01 o 3 11 0 17.55 106.85 79.08 o 4 11 0 6046.95 6148.10 266.88 o 5 11 0 6278.90 5935.32 280.33 o 6 11 0 277.13 309.42 74.95 o 7 11 0 17.86 69.37 59.83 o 8 11 0 151.12 231.83 77.10 o 9 11 0 5195.43 5295.05 291.57 o 10 11 0 5236.96 5698.07 306.13 o 11 11 0 951.61 1255.30 157.20 o 12 11 0 1962.12 2145.68 254.31 o 13 11 0 160.39 173.23 94.16 o 14 11 0 593.72 607.98 158.36 o 15 11 0 503.56 794.50 162.46 o 0 12 0 162.44 41.13 103.86 o 1 12 0 6878.48 6708.31 402.18 o 2 12 0 243.36 535.15 109.73 o 3 12 0 4475.62 3755.55 308.33 o 4 12 0 2691.44 2464.64 243.19 o 5 12 0 2776.72 3373.49 246.64 o 6 12 0 11214.15 11160.92 359.42 o 7 12 0 3631.76 3709.52 240.55 o 8 12 0 3722.79 3643.01 241.21 o 9 12 0 6707.89 7261.43 333.75 o 10 12 0 1700.87 1674.86 156.17 o 11 12 0 9848.14 10402.49 422.25 o 12 12 0 68.27 234.86 154.03 o 13 12 0 389.99 670.95 176.81 o 1 13 0 1621.34 1734.41 192.39 o 2 13 0 1941.49 2373.81 245.35 o 3 13 0 1051.59 1781.42 216.30 o 4 13 0 4775.11 4673.43 351.79 o 5 13 0 8443.73 8753.02 459.26 o 6 13 0 5737.27 5831.01 449.38 o 7 13 0 22774.55 20928.13 612.05 o 8 13 0 1015.01 1112.97 139.75 o 9 13 0 565.29 504.92 103.50 o 10 13 0 1947.22 2032.67 178.93 o 11 13 0 139.89 347.64 99.26 o 0 14 0 1116.37 1583.46 275.53 o 1 14 0 132.74 323.03 110.77 o 2 14 0 2820.12 2808.95 272.54 o 3 14 0 378.81 551.64 195.71 o 4 14 0 1921.52 2053.96 231.53 o 5 14 0 1644.09 1534.65 195.69 o 6 14 0 4926.60 5034.73 387.19 o 7 14 0 404.24 510.21 144.57 o 8 14 0 2720.05 2867.44 512.41 o 9 14 0 601.88 913.40 155.41 o 1 15 0 178.30 397.67 137.80 o 2 15 0 196.34 167.75 153.13 o 3 15 0 4605.87 4631.11 574.43 o 4 15 0 138.36 463.60 130.67 o -21 1 1 1.36 83.37 142.38 o -20 1 1 4889.47 5082.92 347.69 o -19 1 1 8798.37 8553.87 433.41 o -18 1 1 13358.08 13232.74 416.56 o -17 1 1 484.55 775.97 110.55 o -16 1 1 1590.84 1685.97 156.64 o -15 1 1 376.48 540.82 95.02 o -14 1 1 48.95 132.84 74.83 o -13 1 1 537.54 703.65 112.25 o -12 1 1 5378.34 5433.29 235.84 o -11 1 1 121.37 300.17 36.94 o -10 1 1 15581.78 15353.19 516.24 o -9 1 1 12007.37 12190.91 228.14 o -8 1 1 370.98 435.07 38.94 o -7 1 1 134265.97 136848.28 1732.42 o -6 1 1 1522.92 1483.47 66.49 o -5 1 1 66304.06 67115.42 820.47 o -4 1 1 328.32 399.26 28.61 o -3 1 1 79280.85 84201.24 988.34 o -2 1 1 1164.03 1164.03 34.31 o -1 1 1 713.74 806.50 24.88 o 0 1 1 7065.86 7974.18 111.70 o 1 1 1 813.99 656.52 31.78 o 2 1 1 7518.71 7391.90 114.69 o 3 1 1 25418.76 25794.18 337.39 o 4 1 1 5265.98 5497.34 133.01 o 5 1 1 3425.83 3559.61 88.95 o 6 1 1 109966.59 113579.45 1449.42 o 7 1 1 14694.58 13968.16 249.40 o 8 1 1 129093.06 129556.57 2017.64 o 9 1 1 2000.30 2289.47 97.06 o 10 1 1 34866.13 32985.84 502.90 o 11 1 1 5477.91 5735.98 163.20 o 12 1 1 8289.73 7868.67 226.66 o 13 1 1 625.02 808.14 101.67 o 14 1 1 9655.10 9315.00 311.76 o 15 1 1 142.93 370.49 82.96 o 16 1 1 2164.67 2721.13 201.40 o 17 1 1 5338.26 5190.49 287.61 o 18 1 1 4725.16 4697.92 281.37 o 19 1 1 1442.02 2053.28 202.45 o 20 1 1 3079.06 3841.57 343.49 o 21 1 1 5763.93 6073.58 482.56 o -21 2 1 3821.25 3860.50 348.84 o -20 2 1 1352.92 1814.78 194.36 o -19 2 1 6913.28 7014.88 396.49 o -18 2 1 11197.56 11178.60 503.04 o -17 2 1 11459.90 11357.77 417.76 o -16 2 1 811.51 1122.87 126.60 o -15 2 1 1596.50 1853.68 156.22 o -14 2 1 1950.28 2268.09 177.23 o -13 2 1 1140.13 1334.67 129.86 o -12 2 1 11234.94 11225.88 363.36 o -11 2 1 53468.53 52866.00 741.60 o -10 2 1 3408.95 3400.87 117.62 o -9 2 1 4017.10 4054.44 120.60 o -8 2 1 47439.81 45993.11 886.87 o -7 2 1 12671.01 11601.80 227.26 o -6 2 1 76837.57 76896.93 1930.26 o -5 2 1 1462.84 1527.26 61.86 o -4 2 1 9625.66 9085.77 157.29 o -3 2 1 15950.97 17635.85 266.75 o -2 2 1 11523.87 11859.60 176.89 o -1 2 1 41588.92 44825.89 544.01 o 0 2 1 594.21 566.70 41.80 o 1 2 1 95562.40 99720.54 1468.64 o 2 2 1 489.51 662.77 37.37 o 3 2 1 46002.16 48776.40 601.16 o 4 2 1 937.41 1178.16 58.93 o 5 2 1 22043.83 20597.71 304.79 o 6 2 1 37259.11 37372.85 548.30 o 7 2 1 186552.23 189144.11 2222.02 o 8 2 1 6278.99 6212.96 150.68 o 9 2 1 56742.67 56062.07 1074.29 o 10 2 1 37363.71 35765.97 539.02 o 11 2 1 23315.15 21740.93 381.19 o 12 2 1 5634.45 5839.22 180.69 o 13 2 1 90.64 284.16 66.11 o 14 2 1 2421.62 2231.86 171.79 o 15 2 1 12345.53 12355.72 368.54 o 16 2 1 192.87 174.77 83.71 o 17 2 1 7.08 188.70 83.02 o 18 2 1 4695.43 5232.84 331.67 o 19 2 1 9475.34 9023.97 397.97 o 20 2 1 1513.19 1683.40 233.06 o 21 2 1 103.40 401.18 140.43 o -21 3 1 8547.34 8942.82 541.17 o -20 3 1 1037.87 1462.96 202.62 o -19 3 1 5643.51 5337.94 491.52 o -18 3 1 1139.60 1360.69 175.63 o -17 3 1 2136.94 2262.52 210.55 o -16 3 1 1614.49 1918.65 188.00 o -15 3 1 4602.57 4769.14 329.42 o -14 3 1 23390.03 21841.29 514.41 o -13 3 1 4288.37 4528.70 225.63 o -12 3 1 8341.47 8892.19 301.29 o -11 3 1 284.52 386.42 62.23 o -10 3 1 53840.77 52370.59 731.78 o -9 3 1 2180.72 2141.08 97.32 o -8 3 1 4.90 46.83 30.81 o -7 3 1 22424.15 22585.79 430.58 o -6 3 1 22699.03 22635.42 343.94 o -5 3 1 3156.74 3404.03 91.67 o -4 3 1 18211.62 18511.57 338.65 o -3 3 1 85573.92 89874.70 1262.08 o -2 3 1 43117.11 42766.31 541.86 o -1 3 1 216.06 453.43 31.94 o 0 3 1 87.18 104.60 14.68 o 1 3 1 26283.64 28544.02 373.61 o 2 3 1 80520.53 82278.06 1056.55 o 3 3 1 50446.17 52561.79 707.79 o 4 3 1 1174.80 1368.25 67.20 o 5 3 1 2433.04 2838.17 82.35 o 6 3 1 15729.14 15679.51 260.51 o 7 3 1 37947.44 37747.47 531.33 o 8 3 1 512.44 623.92 58.33 o 9 3 1 3454.33 3707.67 124.44 o 10 3 1 1955.55 2022.24 107.07 o 11 3 1 63869.98 62314.38 863.44 o 12 3 1 4392.27 3975.16 168.17 o 13 3 1 273.57 325.59 63.21 o 14 3 1 2886.76 3061.31 229.43 o 15 3 1 3800.35 4280.40 280.21 o 16 3 1 5454.40 5569.22 325.65 o 17 3 1 759.97 704.70 133.36 o 18 3 1 9045.49 8958.92 492.63 o 19 3 1 2633.88 3012.24 323.45 o 20 3 1 11.41 19.24 110.10 o 21 3 1 0.01 204.69 131.47 o -21 4 1 2759.29 2774.71 304.02 o -20 4 1 1578.40 1415.08 208.41 o -19 4 1 10073.53 10674.08 544.42 o -18 4 1 2915.22 3294.14 314.16 o -17 4 1 2429.61 2766.62 276.06 o -16 4 1 1830.69 2128.81 233.14 o -15 4 1 24584.47 23261.48 623.62 o -14 4 1 604.72 778.97 121.78 o -13 4 1 11985.60 12120.18 395.35 o -12 4 1 5318.93 5266.26 198.51 o -11 4 1 31742.77 29474.22 521.71 o -10 4 1 10020.64 9931.50 221.79 o -9 4 1 3975.43 3837.41 129.10 o -8 4 1 57856.16 57029.43 770.14 o -7 4 1 11736.43 10586.56 211.67 o -6 4 1 20414.62 20440.06 325.42 o -5 4 1 3135.74 3050.13 93.72 o -4 4 1 89165.13 90924.42 1182.52 o -3 4 1 5557.51 5977.85 127.40 o -2 4 1 24078.87 22714.88 327.69 o -1 4 1 62722.76 66567.38 821.57 o 0 4 1 25650.32 25826.97 359.86 o 1 4 1 3901.93 4174.78 124.94 o 2 4 1 171.62 174.46 21.52 o 3 4 1 59670.37 61585.87 834.16 o 4 4 1 385.71 426.38 39.35 o 5 4 1 25530.50 24979.19 405.09 o 6 4 1 26121.52 26111.60 390.56 o 7 4 1 70372.51 71579.52 921.60 o 8 4 1 1564.86 1660.07 82.37 o 9 4 1 69984.50 67431.37 898.96 o 10 4 1 32008.93 31071.96 492.29 o 11 4 1 200.13 297.06 44.99 o 12 4 1 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